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Home My WebLink AboutPA2008-040_DEIR MARINA PARK VOL. II OF III111111111111111111111111111111111 Willi 1111 1111111 *NEW FILE* PA2008=040 DEIR Marina Park Vol. 11 of I I I Draft Recirculated Environmental Impact Report Marina Park Newport Beach, Orange County, California Technical Appendices Volume 11 of III State Clearinghouse # 2008051096 Prepared for: CITY COPY DO NOT REMOVE FROM PREMISES City of Newport Beach Planning Department 3300 Newport Boulevard Newport Beach, CA 92658-8915 949.644.3219 Contact: Rosalinh Ung, Associate Planner Prepared by: Sirius Environmental January 2010 PA2008-040 for ER2008-001 1700 W. Balboa Blvd DATE OF MEETING: - Ell ID110 t0 Marina Park 1 t I I I� II II II I I I Appendix G: Hazardous Materials Information 1 1 Marina Park Draft EIR 1 C 1 1 1 1 1 i 1 1 1 1 0 1 1 1 i FirstSearch Technology Corporation Environmental FirstSearch TM Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 Job Number: MARINA PARK PREPARED FOR: I 07-07-08 Eavixunmenta FIRSTS; Tel: (781) 551-0470 Fax: (781) 551-0471 Environmental FirstSearch is a registered trademark of FirstSearch Technology Corporation. All rights reserved. F Environmental FirstSearch Search Summary Report J 1 Target Site: WEST BALBOA BLVD NEWPORT BEACH CA 92663 FirstSearch Summary Database Set Updated Radius Site 1/8 1/4 1/2 1/2> ZIP TOTALS NPL Y 04-07-08 1.25 0 0 0 0 0 0 0 NPL Delisted Y 04-07-08 0.75 0 0 0 0 0 0 0 CERCLIS Y 04-22-08 0.75 0 0 0 0 1 0 1 NFRAP Y 04-22-08 0.75 0 0 0 2 0 0 2 RCRA COR ACT Y 04-01-08 1.25 0 0 0 0 0 0 0 RCRA TSD Y 04-01-08 0.75 0 0 0 0 0 0 0 RCRA GEN Y 04-01-08 0.50 0 0 0 6 - 0 6 RCRA NLR Y 04-01-08 0.50 0 0 0 1 - 0 1 Federal 1C / EC Y 04-01-08 0.50 0 0 0 0 - 0 0 ERNS Y 04-22-08 0.50 0 0 0 0 - 4 4 Tribal Lands Y 12-01-05 1.25 0 0 0 0 0 0 0 Slaterrribal Sites Y 08-08-07 1.25 0 0 0 2 2 0 4 State Spills 90 Y 11-06-07 0.50 0 0 0 3 - 0 3 State/Tribal SWL Y 04-09-08 0.75 0 0 0 0 0 1 1 State/Tribal LUST Y 04-11-08 0.75 0 0 1 0 10 0 11 State/Tribal UST/AST Y 01-03-07 0.50 0 0 0 1 - 0 1 State/Tribal EC Y NA 0.50 0 0 0 0 0 0 state/TribalIC Y 04-27-07 0.50 0 0 0 0 - 0 0 State/Tribal VCP Y 08-15-06 0.75 0 0 0 0 0 0 0 State/Tribal Brownfields Y 08-08-07 0.75 0 0 0 0 0 0 0 State Permits Y 04-16-08 0.50 0 0 0 7 - 2 9 State Other Y 08-08-07 0.50 0 0 1 2 - 0 3 - TOTALS - 0 0 2 24 13 7 46 Notice of Disclaimer Due to the limitations, constraints, inaccuracies and incompleteness of government information and computer mapping data currently available to FirstSearch Technology Corp., certain conventions have been utilized in preparing the locations of all federal, state and local agency sites residing in FirstSearch Technology Corps databases. All EPA NFL and stale landfill sites are depicted by a rectangle approximating their location and size. The boundaries of the rectangles represent the castem and western most longitudes; the northern and southern most latitudes. As such, the mapped areas may exceed the actual areas and do not represent the actual boundaries of these properties. All other sites arc depicted by a point representing their approximate address location and make no attempt to represent the actual areas of the associated property. Actual boundaries and locations of individual properties can be found in the files residing at the agency responsible for such information. Waiver of Liability Although FirstSearch Technology Corp. uses its best efforts to research the actual location of each site, FirstSearch Technology Corp. does not and can not warrant the accuracy of these sites with regard to exact location and size. All authorized users of FirstSearch Technology Corp.'s services proceeding arc signifying an understanding of FirstSearch Technology Corp.'s starching and mapping conventions, and agree to waive any and all liability claims associated with starch and map results showing incomplete and or inaccurate site locations. Environmental Firsdearch Site Information Report Request Date: 07-07-08 Search Type: RequestorName: MBA Job Number: Standard: ASTM-05 Filtered Report Target Site: WEST BALBOA BLVD NEWPORT BEACH CA 92663 Demographics COORD MARINA PARK' SItes: 46 Non-Geocoded: 7 Population: NA Radon: NA Site Location Decrees (Decimal) Decrees (Min/Sec) UTMs Longitude:-117.923035-117;55:23 )tasting: 414366.981 Latitude: 33.608169 33:36:29 Northing: 3718900.557 Zone: 11 Comment Comment: Additional Requests/Services ' Adjacent ZIP Codes: 0 Mile(s) Services: ZIP Code City Name s'r DlauDir Set Requested? Date Sanborns No Aerial photographs No HistoricalTopos No City Directories No Title Search/Env Liens No Municipal Reports No OnlineTopos Yes 07-07-08 II II Environmental FirstSearch Sites Summaq Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 ' TOTAL: 46 GEOCODED: 39 JOB: MARINA PARK NON GEOCODED: 7 SELECTED: 0 ' Map ID__DB Type Site Name/ID/Status Address Dist/Dir Page No. I LUST MOBIL 18-1-107 1500 BALBOA 0.16SE I T0605900496/CASE CLOSED NEWPORT BEACH CA 92663 ' 1 OTHER MOBIL S S 18-1-167 1500 BALBOA BLVD 0.16 SE 2 ORCO_GW_87UTI 66/NOT REPORTED NEWPORT BEACH CA 92659 2 PERMITS SOUTH COAST SHIPYARD 22321 ST ST 0.27 NW 2 ' CAL000300628/ACTIVE NEWPORT BEACH CA 92663 3 RCRAGN SEA SPRAY BOAT YARD 226 21 ST ST 0.27 NW 3 CAD982470718/SGN NEWPORT BEACH CA 92663 ' 4 PERMITS LIDO PENINSULA COMPANY 101 SHIPYARD WAY STE M 0.29 NW 4 CAL000301958/ACTIVE NEWPORT BEACH CA 92663 5 RCRAGN BELLPORT GROUP INC 101 SHIPYARD WAY 0.30NW 5 ' CAR000148882/SGN NEWPORT BEACH CA 92663 6 RCRAGN ERIC KIEVIT MARINE DIESEL 151 SHIPYARD WY BERTH C CBN 0.31 NW 6 CAD983662883/SGN NEWPORT BEACH CA 92663 ' 7 RCRAGN NEWPORT HARBOR SHIPYARD 151 SHIPYARD WAY BERTH C 0.31 NW 7 CAD981653199/SGN NEWPORT BEACH CA 92663 8 RCRANLR LIDO PENINSULA CO 201 SHIPYARD WY CABIN NUMBE 0.31 NW 8 ' CAD983671843/NLR NEWPORT BEACH CA 92663 9 UST LIDO PENINSULA CO 251 SHIPYARD 0.33 NW 9 TISID-STATE33721/ACTIVE NEWPORT BEACH CA 92660 10 PERMITS PETROS MARINE SERVICE, INC. 2270 NEWPORT BLVD 0.34 NW 10 CAL000254471/ACTIVE NEWPORT BEACH CA 92663 10 PERMITS SOUTH COAST BOAT YARD INC 2270 NEWPORT BLVD 0.34 NW I I ' CAL000000944/INACTIVE NEWPORT BEACH CA 92663 II SPILLS ETCO HOMES 2300 NEWPORT BOULEVARD 0.35 NW 12 ' G_SL0605958194/CASE OPEN NEWPORT BEACH CA 92663 7752 MONROE ST 0.36 NW 13 12 RCRAGN W B R TRANSPORTATION LLC CAR00012173 IITRANSPORTER NEWPORT BEACH CA 92663 13 PERMITS BALBOA BOAT YARD INC 2414NEWPORTBLVD 0.39 NW 14 ' CAL000091395/ACTIVE NEWPORT BEACH CA 92663 14 PERMITS TERRY MCKENZIE, INC 1151 W BALBOA BLVD 0.45 SE I5 CAL000141436/ACTIVE NEWPORT BEACH CA 92661 ' 15 NFRAP NEWPORT PLATING CO 2810 VILLA WAY 0.47 NW 16 CAD982360356/NFRAP-N NEWPORT BEACH CA 92663 ' 16 NFRAP NEWPORT PLATING CO 3 CAD982360414/NFRAP-N 2815 VILLA WAY NEWPORT BEACH CA 92663 0.47 NW 16 18 OTHER NEWPORT PLATING COMPANY 3 2815 VILLA WAY 0.47 NW 17 CAL30340151/PROPERTY/SITE REFERR NEWPORT BEACH CA 92661 ' 17 OTHER NEWPORT PLATING CO. 2810 VILLA WAY 0.47 NW 19 CAL30340050/PROPERTY/SITE REFERR NEWPORT BEACH CA 92663 ' 15 RCRAGN NEWPORT PLATING 2810 VILLA WAY NEWPORT BEACH CA 92663 0.47 NW 20 CAD982360356/SGN II Environmental Firsdearch Sites Smnn2al y Report Target Property: WEST,BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 TOTAL: 46 GEOCODEM 39 NON GEOCODED: 7 SELECTED: 0 Map ID_ DB TYPe __ Site Name/ID/Status _ _ _ Address Dist/Dir_ Page No`____i IS SPILLS NEWPORTPLATING 2810VILLA WAY 0.47NW 21 SLC8189/ADDITIONAL CHARACTER NEWPORT BEACH CA 17 SPILLS NEWPORTPLATING 2810VILLA WAY OA7NW 21 , G SL0605980961/NOT REPORTED NEWPORT BEACH CA 92663 16 STATE NEWPORT PLATING COMPANY 3 2815 VILLA WAY OA7 NW 22 CAL303401511PROPERTYISITE REPERR NEWPORT BEACH CA 92661 , IS STATE NEWPORT PLATING CO. 2810VILLA WAY OXNW 25 I. CAL30340050/PROPERTY/SITE REPERR NEWPORT BEACH CA 92663 19 PERMITS SCHOCK MARINE 50429TII ST 0.50 NW 28 CAL000059574/ACTIVE NEWPORT BEACH CA 92663 21 LUST DELANEYS 634 LIDO PARK 0.53 NW 29 T0605901362/CASECLOSED NEWPORT BEACH CA 92663 , 20 LUST UNDESIGNATED PARKING AREA 2809NEWPORT 0.53NW 30 T060590i 199/CASE CLOSED NEWPORT BEACH CA 92660 20 LUST CITY YARD (FORMER) 2809 NEWPORT BLVD 0.53NW 31 083001767T/CASE CLOSED NEWPORT BEACH CA 92663 22 LUST LIDO PARK CONDOMINIUMS 601 LIDO PARK 0.54 NW 32 T0605902220/CASE CLOSED NEWPORT BEACH CA 92663 , 23 LUST UNOCAL 5310 3001 NEWPORT 0.60 NW 33 LUST T0605900346/REMEDIALACTION GERMAN AUTOS NEWPORT BEACH CA 92663 3000 NEWPORT 0.60 NW 34 24 T0605900804/CASE CLOSED NEWPORT BEACH CA 92663 23 LUST UNOCAL 3001NEWPORT 0.60 NW 35 T0605937174/CASECLOSED NEWPORT BEACH CA 92663 ' 25 CERCLIS CAGNEYTRUST SW CORNER OF 32ND ST and NE 0.68NW 36 CAOOOO I 879971NOT PROPOSED NEWPORT BEACH CA 92663 26 LUST BOY SCOUTS OF AMERICA SEA BASE 1931 COAST 0.69 NE 37 T0605901174/CASE CLOSED NEWPORT BEACH CA 92663 27 LUST NEWPORT BEACH CITY HALL 3300 NEWPORT 0.70 NW 38 T0605900150/CASE CLOSED NEWPORT BEACH CA 92658 28 LUST WORLD OIL42 3401NEWPORT 0.73NW 39 T0605901106/CASE CLOSED NEWPORTBEACHCA92660 jl 29 STATE ORANGE COUNTY REPINING CO. WELL 3 213 42ND ST. 1.13 NW 40 , CAL30130028/PROPERTY/SITE REPERR NEWPORT BEACH CA 92660 30 STATE SOUTH BASIN OIL COMPANY 204/20643RD STREET 1.17NW 42 , CAL30130024/PROPERTY/SITE REPERR NEWPORT BEACH CA 92663 I Environmental FirstSearch Sites Summary Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 TOTAL: 46 GEOCODED: 39 JOB: MARINA PARK NON GEOCODED: 7 SELECTED: 0 ' MaP ID DB Type Site Name/ID/Status Address Dist/Dir Page No. ERNS UNKNOWN NEWPORT BEACH HARBOR/3812 R NON GC N/A 297590/MARINE VESSEL (EPA R NEWPORT BEACH CA 92663 ' ERNS UNKNOWN NEWPORT BEACH MARINA NR CORNON GC CA N/A 256292/UNKNOWN(EPA REGIONS NEWPORT BEACH ERNS NEWPORT PLATING CO NEWPORT PLATING CO NONGC N/A ' 13332/UNKNOWN NEWPORT BEACH CA ERNS UNKNOWN PIER 19TH ST NONGC N/A 306819/MARINE VESSEL (EPA R NEWPORT BEACH CA 92663 PERMITS REMOTE/MACHINE SHOP/ HORNBLOWER C815 WEST 17TH ST STE 10 NONGC N/A CAL000326181/ACTIVE NEWPORT BEACH CA 92663 PERMITS CLINICAL FORMULA LLC 888 W 16TH ST NON GC N/A ' CAL000160517/ACTIVE NEWPORT BEACH CA 92663 SWL NEWPORT TERRACE LF WEST I9TH ST. DEAD END NONGC N/A SWIS30-AB-0168/CLOSED NEWPORT BEACH CA ' II II II II II II II II II ' Target Property: SEARCH ID: 34 Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: MOBIL 18-11G7 ADDRESS: 1500 BALBOA NEW PORT BEACH CA 92659 ORANGE DIST/DIR: JOB: MARINA PARK LUST 0.16 SE MAP ID: REV: 04/11/08 lot: T0605900496 ID2: STATUS: CASE CLOSED PHONE: Please now, that some data previously pi ovided by the Slate Water Resources Control Board in the LUSTIS database is not currently being provided by the agency fit the most recent edition. Incidents that occur ed after the year 2000 stay not have much information, Field headers with blank information following a/fersdtou/d be bnteipreted as tun•epm•ted by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 87UT166 RESPONSIBLE PARTY: JOHNNYMEDRANO ADDRESS OF RESPONSIBLE PARTY: 3700 W 190THSTTP77 SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083000618T CASE TYPE: OTHER SUBSTANCE LEAKED: GASOLINE SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOWN LEAK SOURCE: UNKNOWV HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1987-06-18 00:00.00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank if not reported): 9999.09-09 00:00.100 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank If not reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank If not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 2000-10-17 00:00:00 REPORT DATE (blank if not reported): 1987-06-18 00.00:00 MTBE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE MTBE DATE(Date of historical maximum MTBE concentration): 'MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: / 'MTBETESTED: SITE NOT TESTED FOR MTBE. INCLUDES UNKNOWN AND NOTANAL=,D MTBE CLASS: " 1 Site Details Page - I Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 OTITER SEARCH ID: 25 DIST/DIR: 0.16 SE NAME: MOBIL SSI8-H67 ADDRESS: 1500 BALBOA BLVD NEWPORT BEACKCA 92659 ORANGE CONTACT: ORANGE COUNTY GROUNDWATER CLEANUP I,IS7' INFOIZNIA!I'ION Case Type: a Contract Status: 8 Fund: P Substance Code: 8006619 Description: GASOLINE Lead Refferal: N Enforcement: Date Closed: JOB: MARINAPARK MAP ID: 1 REV.. 07/01/99 IDI: ORCO GW 87UTI66 ID2: STATUS: NOTREPORTED PHONE: PERMITS SEARCH 1D: 23 DIST/DIR: 0.27 NW MAP ID: 2 NAME: SOUTH COAST SHIPYARD REV: 04/16/08 ADDRESS: 22321STST IDI: CAL000300628 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: ACTIVE COMPACT: PHONE: Date Record was Created InactivityDale: Facility Mail Nante: Facility Mulling Address: Owner Nome: OnperAddress: Contact Name: Contact Address: Contact Phone: 9:18:49AM 223 21STST, NEIVPORTBEACH, CA 92663 PETESTEIVART 223 21STST, NEIPPORT BEACH, CA 92663 PETE STEWART 22321STST, NEIVPORTBEACH, CA 92663 9496752837 Site Details Page -1 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 SEARCH ID: 8 NAME: SEA SPRAY BOAT YARD ADDRESS: 226 21 ST ST NEWPORT BEACH CA 92663 ORANGE CONTACT: PAULETTE PAPPAS SITE INFORMATION CONTACT INFORMATION: PHONE: UNIVERSE INFORMATION: NAIC INFORMATION 336612 -BOAT BUILDING ENFORCEMENT INFORMATION: VIOLATION INFORMATION: III RCRAGN DIST/DIR: 0.27 NW PAULETTE PAPPAS 1717 E BALBOA BLVD BALBOA CA 92661 7146751155 REV: ID1: ID2: STATUS: PHONE: MAP ID: 3 6/6/06 CAD992470718 SON 7146751155 I Site Details Page - 3 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 PERMITS SEARCH ID: 19 DIST/DIR: 0.29 NW MAP ID: 4 NAME: LIDO PENINSULA COMPANY REV: 04/16/08 ADDRESS: 101 SHIPYARD WAY STE M lot: CAL000301958 NEWPORT BEACH CA 92663 102: ` ORANGE STATUS: ACTIVE i CONTACT: PHONE: ' Date Record Alas Created: 11512006 1:01:45 PAI Inuctivlly Datc: Facility Mail Name: Facility Mailing Address: PO BOX 1549. NEIYPORT BEACIL CA 92659-I549 Owner Name: LIDO PENINSULA CO Onncr Address: POBOX IS49, NEWPORTBEACH, CA 92659.1549 Contact Name: JAMIEDEUTIIIN Contact Address: 151 SHIPYARD IVAYSTE7, NE IPPOR T BEA CH, CA 91663.0000 Contact Phone: 9496739330 Site Details Page - 4 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 SEARCHID: 4 NAME: BELLPORT GROUP INC ADDRESS: 101 SHIPYARD WAY NEWPORT BEACH CA 92663 ORANGE CONTACT: DWAYNE PACE CONTACT INFORMATION: PHONE: UNIVERSE INFORMATION: NAIC INFORMATION 71393 - MARINAS ENFORCEMENT INFORMATION: VIOLATION INFORMATION: HAZARDOUS WASTE INFORMATION: Corrosive waste Ignitable waste III RCRAGN DIST/DIR: 0.30 NW DWAYNE PACE 101 SHIPYARDWAY STEM NEWPORT BEACH CA 92663 949.673-9330 REV: IDI: ID2: STATUS: PHONE: MAP ID: 5 6/6/06 CAR000148882 SGN 949-673-9330 9 II Site Details Page - 5 Environmental FirstSeareh Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 RCRAGN SEARCH ID: 5 DISUDIR: 0.31 NW MAP ID: 6 NAME: ERIC KIEVIT MARINE DIESEL REV: 616106 ADDRESS: 151 SHIPYARD IVY BERTH C CEN 5 IDI: CAD983662883 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: SON CONTACT: ERIC KIEVITS PHONE: 7146730382 SITE, INFORMATION CONTACT INFORMATION; PHONE: NAIL INFORMATION ENFORCHMENTINFORMATION: VIOLATION INFORMATION: ERIC KIEVITS 151 SHIPYARD WY BERTH C CBN 5 NEWPORT BEACH CA 92663 7146730882 Site Details Page - 6 Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 jOB: MARINA PARK Site Details Page - 7 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 RCRANLR SEARCII ID: 10 DISTIDIR: 0.31 NW MAP ID: 8 NAME: LIDO PENINSULA CO REV: 6/6106 ADDRESS: 201 SHIPYARD WY CABIN NUMBER 1 IDI: CAD983671843 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: NLR CONTACT: SEAN M WALSH PHONE: 7146739330 SITF. INFORM1IAT/ON CONTACT INFORMATION: PHONE: UNIVERSE INFORMATION: NAIC INFORMATION ENFORCEMENT INFORMATION: SEAN M WALSH P 0 BOX 1549 NEWPORT BEACH CA 926591549 7146739330 Site Details Page - 8 11 Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 UST JOB: MARINAPARK SEARCH ID: 28 DIST/DIR: 0.33 NW MAP ID: NAME: LIDO PENINSULA CO REV: 01/01/94 ADDRESS: 251 SHIPYARD IDI: TISID-STATE33721 NEWPORT BEACH CA 92660 ID2: Orange STATUS: ACTIVE CONTACT: PHONE: UST HISTORICAL DATA This site was listed in the FIDS Zip Code List as a UST site. The Omce of Hazardous Data Management produced the FIDS list. The FIDS list is an index of names and locations of sites recorded in various California State environmental agency databases. It is sorted by zip code and as an index, details regarding the sites were never included. The UST information included in FIDS as provided by the Once of Hazardous Data Management was originally collected from the SWEEPS database. The SWEEPS database recorded Underground Storage Tanks and was maintained by the State Water Rmourccs Control Board (SWRCB). That agency no longer maintains the SWEEPS database and last updated it in 1994. The last release of that 1994 database was in 1997. Oversight ofUnderground Storage Tanks within California is now conducted by Certified Unified Program Agencies referred to as CUPA s. There are approximately 102 CUPA s and Local Oversight Programs (LOP s) in the State of California. Most arc city or county government agencies. As of 1998, all sites or facilities with underground storage tanks were required by Federal mandate to obtain certification by designated UST oversight agencies (u this case, CUPA s) that the UST/s at their location were upgraded or removed in adherence with the 1999 RCRA standards Information from the FIDS/SWEEPS lists were included in this report search to help identify where underground storage tanks may have existed that were not recorded in CUPA databases or lists collected by Track Into Services. This may occur i f a lank was removed prior to development ofrecent CUPA UST lists or never registered with a CUPA. Site Details Page - 9 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 PERMITS SEARCH ID: 20 DIST/DIR: 0.34 NW MAP ID: 10 NAME: PETROS MARINE SERVICE, INC. REV: 04/16108 ADDRESS: 2270 NEWPORT BLVD IDI: CAL000254471 NEWPORT BEACH CA 92663 1 D2: Orange STATUS: ACTIVE CONTACT: PHONE: Date Record was Created Inuctivity Date: Facility Mall Nnmc: Facility Moiling Address: Onncr Namc: Omer Address: Contact Name: Contact Address: Contact Phone: 2270 NEWPORT BLVD, NEWPORT BEACH, CA 92663 PETROS KOURAKIS 2270 NEWPORT BLVD, NEWPORT BEACH, CA 92663 JILL MCKINNEY 2270 NEWPORT BLVD, NEWPORT BEACH, CA 92663 9496735040 11 11 11 AI 11 Site Details Page -10 it I! ITarget Property: SEARCH ID: 22 Environmental Firsdearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: SOUTH COAST BOAT YARD INC ADDRESS: 2270 NEWPORT BLVD NEWPORT BEACH CA 92663 Orange CONTACT: PERMITS DIST/DIR: 0.34 NW JOB: MARINA PARK MAP ID: 10 REV: 04/16/08 IDI: CAL000000944 ID2: STATUS: INACTIVE PHONE: Date Record was Created: 1111411989 Inactivity Date: 1112112005 Facility Mail Name: Facility Mailing Address: 22311STST, NEWPORTBEACH, CA 92663-4303 Owner Name: SOUTH COAST BOAT YARD INC Owner Address: 2270 NEWPORT BLVD, NEIVPORTBEACIL CA 92663-0000 Contact Name: PETER STEIVART NOTICE- CR, NEWPORT BEACH, CA 92663.4324 Contact Address: , Contact Phone: 9496752837 H WMI WASTE TYPE AND TONNAGE INFORMATION: Waste Type: Unspecified organic liquid mirttue Total Tonnage per Year: 0.22935 H WM I WASTE TYPE AND TONNAGE INFORMATION: Waste Type: Unspec fcd aqueous solution Total Tonnage per Year: 2.06415 HWMI WASTE TYPE AND TONNAGE INFORMATION: Waste Type: Unspecified solvent mixture Total Tonnage per Year: 0.35361 1 J I Site Details Page -11 Environmental FirstSearch r Site Detail Report Target Property: NEST BALBOA BLVD JOB: MARINA PARK r NEWPORT BEACH CA 92663 SPILLS I� i SEARCH -ID: 15 DISTMIR: 0.35 NW MAP ID: 11 i r NAME: ETCO HOMES REV: 01/03/07 II ADDRESS: 2300 NEWPORT BOULEVARD lot: G SL0605958194 NEWPORT BEACH CA 92663 ID2: STATUS: CASE OPEN CONTACT: PHONL•': RELEASE DATA FROM THE CAI IPORNIA STATE. WATER RESOURCES CONTROL BOARD GLOTRACKER SLIC DKI'ABASL I Please nary tharsoinu SWC data previously provided by the State Water Resources Control Board via the Regional Boards Is not currendv provided by the , agony fa the new OCOTRACKER format. To ensure that our date is as complete as posslble a'e have retafned die original Regional Board.v SLIC records as mell as loaded a110EOTRACKCR SLIC Bstfmgs. OCOTRACKCR records are distinguished by an Initial G at the start ofthe 1D. LEADAGENCY: SANTA ANA RIVQCB(REGIONB) r LEAD AGENCYCONTACT: AlANCCKO.CIIICHOAR LEAD AGENCY CASE NUMBER: RESPONSIBLE PARTY: SUBSTANCE RELEASED (please note that not all codes are available and sonic records cony remain encoded): 7439921. 7440473, 7440508 RECENT DT W: STATUS: Case Open �r {r �r .r r �r 1� r r Site Details Page -12 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 SEARCHID: 9 NAME: W B R TRANSPORTATION LLC ADDRESS: 7752 MONROE ST PARAMOUNT CA 90723 ORANGE rnNTArT: CRAIG A BARRETT SITE INFORMATION CONTACT INFORMATION: PHONE: CONTACTINFORMATION: PHONE: UNIVERSE INFORMATIO NAIC INFORMATION 562112 - HAZARDOUS WA; ENFORCEMENT INFORM VIOLATION INFORMATI RCRAGN DISUDIR: 0.36 NW JOHN LINDSEY 2240 NEWPORT BLVD NEWPORT BEACH CA 92663 949-673-1247 JOHN LINDSEY 2240 NEWPORT BLVD NEWPORT BEACH CA 92663 9496731247 REV: IDI: ID2: STATUS: PHONE: MAP ID: 12 411/08 CAR000121731 TRANSPORTER 949-673-1247 Environmental Firsdearch Site Detail Report Target Property: WESTBALBOABLVD JOB: MARINAPARK NEWPORT BEACH CA 92663 PERMITS SEARCH ID: 18 DIST/DIR: 0.39NW MAP ID: 13 NAME: BALBOA BOAT YARD INC REV: 04/16/08 ADDRESS: 2414NEWPORTBLVD 101: CAL000091395 NEWPORT BEACH CA 92663 ID2: Orange STATUS: ACTIVE CONTACT: PHONE: Dale Record %us Created: IUgF]YY4 Inactivity Date: Bucllity Mall Name: raciily Malling Address: 1414 NEIVPORT BLVD, NEWPORTBEACH, CA 92663-0000 Owner Name: BALBOA BOATYARD Owner Address: 2414 NEWPORT BLVD. NEWPORT BEACH, CA 92663.3704 Contact Name: ARTHUR LEIVIS Contact Addresst 2414 NEWPORT BLVD, NEIVPORT BEACH, CA Contact Phone: 7146736834 IIWMI WA51'E TYPI4 AND TONNAGE INFORMATION: Waste Type: Unspealfied aolmou ot&lpre Totarronnage per Year: 0.1251 IIWMI WASTETYPE AND TONNAGE INFORMATION: 1Vn3le'1'ype: 01her mgdnicsoltds Total Tonnage per Year: 0.1 Site Details Page -14 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 PERMITS SEARCH ID: 24 DIST/DIR: 0.45 SE MAP ID: 14 _ NAME: TERRY MCKENZIE, INC REV: 04/16/08 ADDRESS: 1151 W BALBOA BLVD lot: CAL000141436 NEW PORT BEACH CA 92661 ID2: ORANGE STATUS: ACTIVE CONTACT: PHONE'___ Dote Record was Created: Inactivity Date: Vocility Mail Name: 1151 IVBALBOA BLVD, NEWPORT BEACH, CA 92661-1005 Facility Mailing Address: Owner Names TERRY MCKENZIE, INC. Owner Address: 1151 IVBALBOA BLVD, NEWPORT BEACH, CA 92661-1005 Contact Name: LAURIE MC KENZIE-VP. 1151 WEST BALBOA BLVD., NEIVPORT BEACH, CA 92661-1005 Contact Address: Contact Phone 7146732372 HWMI WASTE TYPE AND TONNAGE INFORMATION: Waste Type. Unspecified organic liquid mixture Total Tonnage per Year: 0.13344 Site Details Page -15 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINAPARIG NEWPORT BEACH CA 92663 NFRAP SEARCH ID: 2 DIST/DI-R: 0.47 NW MAP ID: 15 NAME: NEWPORT PLATING CO ADDRESS: 2810 VILLA WAY NEWPORT BEACH CA 92663 ORANGE CONTACT: DESCRIPTION: ACTION/QUALITY ARCHIVE SITE DISCOVERY PRELIMINARY ASSESSMENT NFRAP (No Father Rcmodial Action Planned REV: 4/22/08 lot: CAD982360356 ID2: 0902597 STATUS: NFRAP-N PHONE: AGENCY/RPS EPA In -House Slate, Fund financed Slate, Fund Financed NFRAP STAR77RAA END 04-27-1989 11.01.1987 04.27-1989 SEARCH ID: 3 DISUDIR: 0.47 NW MAP ID: 16 NAME: NEWPORT PLATING CO 3 REV: 4/22108 ADDRESS: 2815 VILLA WAY IDI: CAD982360414 NEWPORT BEACH CA 92661 ID2: 0902599 ORANGE STATUS: NFRAP-N CONTACT: PHONE: DESCRIPTION: ACTION/QUALITY AGENCY/RPS START/RAA END ARCHIVE SITE EPA In -House 10-01-1988 DISCOVERY State, Fund Financed 11-01-1987 PRELIMINARY ASSESSMENT EPA Fund-finnnecd 10.01-1988 NFRAP (No fulhcr Remedial Action Planned Site Details Page -16 J ' Target Property: SEARCH ID: 27 Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: NEWPORT PLATING COMPANY 3 ADDRESS: 2815 VILLA WAY NEWPORT BEACH CA 92661 ORANGE CONTACT: GENERAL. SITE INFORMATION OTHER DIST/DIR: 0.47 NW Site Type: Historical Status: Refer RCRA Status Date: 1988-08-2600:00:00 NPL Site: NO Funding: Regulatory Agencies Involved: NONESPECIFIED Lead Agency: NONE SPECIFIED Project Manager: Supervisor: Rcfen ed - Not Assigned Branch: So Cal- Cypt ess Acres: Assessors Parcel Number: NONE SPECIFIED Past Uses: NONE SPECIFIED Potential Contaminants: NONE SPECIFIED Confirmed Contaminants: NONE SPECIFIED Potential Media Affected: NONE SPECIFIED Restricted Use: NO Site Management Required: NONESPECIMED Special Programs Associated With this Site: +CERC2 OTHER SITE NAMES (blank below= not reported by agency) CAD982360414 30340151 CALDWELL PLATING REV: IDI: ID2: STATUS: PHONE: JOB: MARINA PARK MAP ID: 18 07/18/05 CAL30340151 PROPERTY/SITE REFERRED TO RCRA COMPLETED ACTIVITIES AND DTSC COMMENTS REGARDING THIS SITE (blank below= not reported by aeenc Area Name: PROJECT {VIDE Sub- Area Name: Document Type: Site Screening Completion Date: 1988-08-26 SITE SCREENING DONE NFA UNDER CERCLA; PENDING STATUSFOR DHS BECAUSE RCRA Comments; REGULATED FACILITY. Area Name: PROJECTWIDE Sub- Area Name: Document Type: Preliminary Assessment Report 'Completion Date: 1987-10-19 PRELIMASSESS DONE NO EVIDENCE OFNEWPORT PLATING EVER BEING AT 2815 VILLA Comments: WAY Name: PROJECT IVIDE 'Area Sub- Area Name: Document Type: Site Screening Completion Date: 1987-05-13 SITE SCREENING DONE CERCLA GRANTPA REQ D. Comments: ' Area Name: PROJECT )VIDE - Continued on next page - ' Site Details Page - 17 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 OTHER SEARCH ID: 27 DIST/DII2: 0.47 NW NAME: NEWPORT PLATING COMPANY 3 REV: ADDRESS: 2815 VILLA WAY lot: NEWPORT BEACH CA 92661 I132: ORANGE STATUS: CONTACI': PHONE-. Sub -Area Name: Document Type: Discovery Completion Date: 1981.08.01 Comments: PACILITYIDENTIPIED PRONE CO. SCARCII. MAP ID: 18 07/18105 CAL30340151 PROPERTY/SITE REFERRED TO RCRA Site Details Page -18 ' Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK OTHER SEARCII ID: 26 DISTIDIR: 0.47 NW MAP ID: 17 NAME: NEWPORT PLATING CO. ADDRESS: 2810 VILLA WAY NEWPORT BEACH CA 92663 ORANGE CONTACT: GENERAL SITE INFORMATION REV: lot: ID2: STATUS: PHONE: 07/18/05 CAL30340050 PROPERTY/SITE REFERRED TO ANOT Slte'rype: Historical Status: Rcfer: Other Agency Status Date: 1987-09.30 00:00:00 NPL Sltc: NO Funding: Regulatory Agencies Involved: NONE SPECIFIED Lead Agency: NONE SPECIFIED Project Manager: Supervisor: Referred -Not Assigned Branch: So Cal- Cypress Acres: Assessors Parcel Number: NONE SPECIFIED Past Uses: NONE SPECIFIED Metals- Other lnotganic Solid 1Vaste, AQUEOUS SOLUTION WITH TOTAL ORGANICRESIDUES Potential Contaminants: >=10, CONTAMINATED SOIL, ACID SOLUTION 2>PH WITH METALS, AQUEOUS SOLUTION 2<PH<I2,5, WITH REACTIVE ANIONS, Cadmium and compounds, Chronnum VI Confirmed Contaminants: NONE SPECIFIED Potential Media Affected: NONE SPECIFIED Restricted Use: NO Site Management Required: NONE SPECIFIED Special Programs Associated with this Site: "CERC2 OTHER SITE NAMES (blank below= not renorted by neency) 30340050 COMPLETED ACTIVITIES AND DTSC COMMENTS REGARDING THIS SITE (blank below= not reported by aeenc Area Name: PROJECT {VIDE Sub -Area Name: Document Type: Preliminary Assessment Report Completion Date: 1987-10-16 PRELIMASSESS DONE DHS-PENDING STATUS; RWQCB AND CO HLTH INVOLVED /N AN Comments: ENFORCEMENTACTION. Area Name: PROJECT WIDE Sub- Area Name: Document Type: Site Screening Completion Date: 1987-02-13 SITE SCREENING DONE RATIONALE FOR PA" MORE INFO. NEEDED. Comments: Site Details Page -19 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 RCRAGN SEARCH ID: 7 DIST/DIR: 0.47 NW MAP ID: IS NAME: NEWPORTPLATING REV: 6/6/06 ADDRESS: 2810 VILLA WAY IDI: CAD982360356 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: SGN CONTACT: PHONE: CONTACT INFORMATION: PHONE: UNIVERSE INFORMATION: NAIC INFORMATION ENFORCEMENT INFORMATION: VIOLATION INFORMATION: ENVIRONMENTAL MANAGER 2810 VILLA WAY NEWPORT BEACH CA 92663 7146734440 Site Details Page -10 I ' Target Property: Environmental Firsdearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK SPILLS SEARCH ID: 17 DISTlDIR: 0.47 NW MAP ID: 15 NAME: NEWPORTPLATING REV: 07/01/2003 ADDRESS: 2810 VILLA WAY IDI: SLC8_I89 NEWPORT BEACH CA ID2: STATUS: ADDITIONAL CHARACTERIZATION ORANGE CONTACT: PHONE: Lead Agency: REGIONAL BOARD Program: SLIC Case Type: SOIL AND GROUNDWATER Status: ADDITIONAL CHARACTERIZATION Substance: METALS CONTAMINANTS PRESENT: CYANIDE, CADMINUM, CHROMIUM, NICKEL, Comments: COPPER, AND ZINC. ADDITIONAL ASSESSMENT IYORKNEEDED Thomas Brothers Guide Location: R) SPILLS D: 16 DISUDIR: 0.47 NW MAP ID: 17 rME:NEWPORT PLATING REV: 01/03/07 101: GSLO605980961 2810 VILLA WAY NEWPORT BEACH CA 92663 1D2: STATUS: NOT REPORTED PHONE: CALIFORNIA STATE WATER RESOURCES CONTROL BOARD GEOTRACKER SLIC DATABASE RELEASE DATA FROM THE Please late that some SLIC data in eviously provided by the State IYater Resourem Control Board via the Regional Boards is not currently provided by the in the neiv GEOTRACKER format. To ensure that our data is as complete aspossible ive have retained the original Regional Boards SLIC records 'agency as well as loaded all GEOTRACKER SLIC listings. GEOTRACKER records are distinguished by an initial Gat the start ojthe ID. LEAD AGENCY: SANTA ANA RWQCB(REGION 8) AGENCY CONTACT: MANECKG. CHICHGAR 'LEAD LEAD AGENCY CASE NUMBER: RESPONSIBLE PARTY: SUBSTANCE RELEASED (please note that not all codes are available and some records may remain encoded): 13, 57125, 7440473 'RECENT DTW: STATUS: Site Details Page - 21 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 STATE 9 SEARCH ID: 12 DIST/DIR: 0.47 NW MAP 1D: 16 NAhIE: NEWPORT PLATING COMPANY 3 REV: 07/03/00 ADDRESS: 2815 VILLA WAY IDI: CAL30340151 NEWPORT BEACH CA 92661 ID2: ' Orange STATUS: PROPERTY/SITE REFERRED TO RCRA CONTACT: PHONE: i below- by OTH Fit SITE NAMES (blank not reported neencv) urn Fit SITE NAMES (blank below - not reported by agency). CALDWELL PLATING ' GENERALsiTE INFORMATION File Name (if different than site nuntc)! i Status: PROPERTY/SITEREPERRED TORCRI (REPRO) �I ' ANVP Sile'rvoe: NGI NPL Site: Fund: Status Date: 0826/988 Lead: Staff: SeniorSupervisort DTSC Region and RWQCD : 4/LONGBEACH Branch: SOUTHERN CA. - B RIYQCB: SANTA ANA Site Access: On Corlcse List: Grounduater Contamination: Ham Banking Score: Hat Racking Score: Number or5ources Contributing to Contamination at the Site: 0 01'IIFII AGENCY iD NUMIIRRS (black belov- not reported by acaicv) I D SOURCE NAME, and VALUE: EPA )DENTIFICATIONNUMBERCAD982360414 INFORNIA'11ON QNSPKCIAL PROGRAMS1118,SITE IS ASSOCIATED WITH (blank helosv-not reported by meencv) CERCLIII PROJECTED ACT1 V rrl ES (blank below- tint reported Iw aeene PROJECTED ACTIVITIES (blank below- not reported 4y ame PROJECTED ACTIVITIES (blank below- not revoried.l(v-aee-nc1 PROJECTED ACTIVITIES(blank below -not reported IImmeO ncy Activity: DISCOVERY (DISC) Activity Status: PROPERTY/SITE REFERRED TO RC21 Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: 08011981 Yards of Solids Removed: 0 Yards of Solids Treated: 0 Gallons of Liquid Removed: 0 Gallons of Llquid'rreated; 0 0 1 LJ 11 Captioned on next page - Site Details Page - 22 ' Target Property: SEARCH ID: 12 Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: NEWPORT PLATING COMPANY 3 ADDRESS: 2815 VILLA WAY NEWPORT BEACH CA 92661 Orange CONTACT: Activity: Activity Status: Completion Due Data: Revised Completion Due Date: Date Activity Actually Completed: Yards of Solids Removed: Yards of Solids Treated: Gallons of Liquid Removed: Gallons of Liquid Treated: Activity: Activity Status: Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: Yards of Solids Removed: Yards of Solids Treated: Gallons of Liquid Removed: Gallons of Liquid Treated: Activity: Activity Status: Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: Yards of Solids Removed: Yards of Solids Treated: Gallons of Liquid Removed: Gallons of Liquid Treated: STATE DIST/DIR: 0.47 NW REV: IDI: ID2: STATUS: PHONE: (SS) PROPERTYISITE REFERRED TO RCRA 05131987 0 0 0 0 (PA) PROPERTY/SITE REFERRED TO RCRA 10191987 0 0 0 0 (SS) PROPERTASITE REFERRED TO RCRA 08261988 0 0 0 0 DTSC COMMENTS REGARDING THIS SITE (blank below= not reported by neencv) DATE COMMENT 08011981 FACILITYIDENTIFIEDPIIONE CO. SEARCH. DATE COMMENT 06011982 FINAL STRATEGY SITE REFERRED: TO HWMBIENF DATE COMMENT 06211982 CALDIYELL PLATINGAT SITE 1946 -1947 and DATE COMMENT 06211982 WAS BOAT BUILDER DATE COMMENT 05131987 SITE SCREENING DONE CERCLA GRANT PA REQ D. DATE COMMENT 08101987 ORANGE CO. ENV. HEALTHNO FILES DATE COMMENT 08141987 RIPQCB NO FILES NEWPORTPLA TING 3 DATE COMMENT JOB: MARINA PARK MAP ID: 16 07/03/00 CAL30340151 PROPERTY/SITE REFERRED TO RCRA - Continued on next page - Site Details Page - 23 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 STATE SEARCH ID: 12 DIST/DIR: 0.47 NW MAPID: 16 NAME: NEWPORT PLATING COMPANY 3 ADDRESS: 2815 VILLA WAY NEWPORT BEACH CA 92661 Orangc CONTACT:- 08141987 MAYIIAVE RCLOCATED AFTER FIRE MORE THAN DATE COMMENT 08141987 20 YEARSA00 REV: 07/03/00 IDI: CAL30340151 II 102: ' STATUS: PROPERTY/SITE REFERRED TO RCRA i PHONE: I DATE COMMENT 10161987 FACIL17YDRIPE-BY SITE OCCUPIED BYANOTHERBUSINCSSNO DATE COMMENT 10161987 1NDICATION017ANYPROBLEMSAT SITE DATE COMMENT 10191987 PRELIM ASSESS DONE NO EVIDENCE OFNEIV1`ORTPLI7INGEYER DATE COMMENT 10191987 BEING AT2815VILLA IIIY DATE COMMENT 11161987 SUBAIITTO EPA NFA UNDER CERCLA 2 DATE COMMENT 08261988 SITESCREENING DONE NFA UNDER CERCLA; PENDING STATUS FOR DMS DATE COMMENT 08261988 BECAUSERCRAREGULITEDFACILITY. DATE COMMENT 05191995 RCRA lead, EPA ID CAD962360414 is not an acceplable EPA DATE COMMENT 0519199S ID naniberper EPA 4119195. 11 t I I I Site Details Page - 24 LJ Environmental FirstSearch Site Detail Report ' Target Property: WESTBALBOABLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 STATE ' SEARCH ID: 11 — DIST/DIR: 0.47 NW MAP ID: 15 NAME: NEWPORT PLATING CO. REV: 07/03/00 ADDRESS: 2810 VILLA WAY lot: CAL30340050 NEWPORT BEACH CA 92663 ID2: Orange STATUS: PROPERTY/SITE REFERRED PHONE: OTHER SITE NAMES (blank belmv= not reported by aecncv) NEIVPORT PLATING CO. GENERAL. SITE INFORMATION File Name (if different than site name): Status: PROPERTY/SITE REFERRED TO ANOTHER AGENCY (REFOA) AWP Site Type: N/A NPL Site: Fund: Status Date: 09301987 Lend: Stuff: Senior Supervisor: DTSC Region and RWQCB : 4/LONG BEACH Breach: SOUTHERN CA. - R WQCB: SANTA ANA Site Access: Controlled On Cortese List: Groundwater Contamination: Haz Ranking Score: Haz Ranking Score: Number of Sources Contributing to Contamination at the Site: 0 INFORMATION ON SPECIAL PROGRAMS THE SITE IS ASSOCIATED WITH (blank below= not reported by agency) CERCLA 11 PROJECTED ACTIVITIES (blank below = not reported by agency) PROJECTED ACTIVITIES (blank belmv=not reported by aeenc Activity: Activity Status: (SS) PROPERTY/SITE REFERRED TO ANOTHER AGENCY Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: 02131987 Yards of Solids Removed: 0 Yards of Solids Treated: 0 Gallons of Liquid Removed: 0 Gallons of Liquid Treated: 0 Activity: Activity Status: (PA) PROPERTY/SITE REPERRED TO ANOTHER AGENCY Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: 10161987 Yards of Solids Removed: 0 Yards of Solids Treated: 0 Gallons of Liquid Removed: 0 Gallons of Liquid Treated: 0 - Continued on next page - 5 Site Details -Page - 25 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 STATC SEARCH ID: 11 DISTIDIR: 0.47 NW MAP ID: 15 NAME: NEWPORT PLATING CO. REV: 07/03/00 ADDRESS: 281OVILLANVAY IDI: CAL30340050 NEWPORT BEACH CA 92663 ID2: 1� Omnge STATUS: PROPERTY/SITE REFERRED 1 CONTACT: - - --- PHONE: D'fSC COM DI ENTS REGARDING'fHIS SITE (blank beInw- not renorted by neencv) ' DATE COMMENT 01131982 PHONE F-UJ.LEDIVARDS: CHEM IVERE DISP TO DATE COMMENT' 01131982 SUAW-UNLINED IN USE UNTIL 1980. CLAIMED DATE COMMENT II 01131982 USED HAULER. ' DATE COMMENT 01131982 DATE SUMP EMPTY WHEN CEMENTED. DRUMS HOLDNRIV COMMENT ' 011JI982 SOLUTIONS NOCHEMARERECYCLED. NEVER DATE COMMENT l 01141982 Fi1C1LITYDRIVE-BY LOCOFABAND $AMP UNK STANDING MAI ER ON ' DATE COMMENT 01141982 BACKLOT.B8LSS77LLSTORED HAPHAZIRDLY. , DATE COMMENT 011W1982 MAYBEENFDRCEMENTPRDB. DATE COMMENT ' 06281982 FINALSTRATEGY SITE REFERRED: TOHIVMB-L4ENFORCEMENT. DATE COMMENT 1 02131987 SITESCREENINGDONER4TIONALEFORPi1:MOBEINFO.NEEDED. , It DATE COMMENT 040719,97 INSPECTION(STATE) RIVQCBandN..B.SANITATIONDEPT.PERPORM (� DATE COMMENT ' 04071987 DRYTEST DATE COMMENT 05251987 INSPECTION(SIATE1✓01NT1NSPECTIONBYRIYQCB,01?ANGECO. ' DA'rE COMMENT 05251987 DATE HLTH CAREAGENCY NEIVPORTBEACH POLICE COMMENT t ' i 05251987 and FIRE DEPT.,OBSERVr,thlZIIISTEDISCHARGE DATE COMMENT 051SI987 TO SOILS DATE COMMENT' 100119,77 RIVQCB-FILESONINSPISURFACEWATER { ' UA'fE COMMENT Continued on newipage - Site Details Page - 26 Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK STATE SEARCH ID: 11 DIST/DIR: 0.47 NW MAP ID: 15 NAME: NEWPORT PLATING CO. REV: 07/03/00 ADDRESS: 2810 VILLA WAY IDI: CAL30340050 NEWPORT BEACH CA 92663 ID2: Orangc STATUS: PROPERTY/SITE REFERRED CONTACT: PHONE: 10021987 DNS-SOMEFILES ONFACILITY DATE COMMENT 10161987 PRELIMASSESS DONE DHS-PENDING STATUS; RWQCB AND CO HLTH DATE COMMENT 10161987 INVOLVEDINAN ENFORCEMENTACTION. DATE COMMENT 11161987 SUBMITTOEPA NFA: SITEWILL NOTSCORE BASED ON DATE COMMENT 11161987 AVAILABLEINFO t 1 1 Site Details Page - 27 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 PERMITS SEARCH ID: 21 DIST/D1R: 0.50 NW MAP ID: 19 NAME: SCHOCKMARINE REY: 04/16/08 ADDRESS: 50429THST IDI: CAL000059574 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: ACTIVE CONTACT: PHONE: Date Record was Created: 212411992 I nuclivity Date: Facility Mail Name: Facility Mulling Address: 2900 LAM YEM RD, NEI PPORT BEACH, CA 92663-3718 Owner Nante: SCO77'SCHOCKISCHOCKPAAIILYTRUST Owner Address: 2900 LAM YEME RD, NEIYPORT BEACH, CA 92663.3718 Contact Nume: MARIESCUOCK Contact Address: 2900 LAPAYETTE RD. NEIYPORTBEACH, CA 92663.3718 Contact Phone: 9496732050 H WM I WASTE. TYPE. AND TONNAGE INFORMATION: Waste Type: 14vdrocarbon solvents (benzene, hexane, Stoddard, E(c.) Total Talmage per Year: B/91 Site Details Page - 28 ' Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK LUST SEARCH ID: 31 DIST/DIR: 0.53 NW MAP ID: 21 NAME: DELANEYS REV: 04/11/08 IDI: T0605901362 ADDRESS: 634 LIDO PARK NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: CASE CLOSED CONTACT: PHONE: RELEASE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE Please note that some data previously provided by the State Water Resources Control Board in the LUSTIS database is not cta rendy being provided by the agency in the most recent edition. Incidents that occurred after the year 2000 nhay not have much information. Field headers with blank o formation followbhg after should be intehpreted as uni eported by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 90UT225 RESPONSIBLE PARTY: LEVONGUGASIAN ADDRESS OF RESPONSIBLE PARTY: 17 RIDGELINEDRIVE SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083001822T CASE TYPE: OTHER SUBSTANCE LEAKED: DIESEL SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOWN LEAK SOURCE: UNKNOWN HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1990-09-06 00:00:00 LEAK WAS STOPPED: CLOSE TANK 'HOW STOP DATE (blank if not reported): 9999-09.09 00:00:00 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank If not reported): DATE (blank if not reported): 'REVIEW DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank If not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): 'DATE DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING -BEGAN (blank if not reported): DATE CLOSURELETTER ISSUED (SITE CLOSED) (blank If not reported): 1993-02-18 00:00:00 REPORT DATE (blank if not reported): 1990.09-0600:00:00 MTBE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE MTBE DATE(Date of historical maximum MTBE concentration): GROUNDWATER CONCENTRATION (parts per billion): 'MTBE MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: 0 TESTED: NOTRE•QUIRED TO BE TESTED 'MTBE MTBE CLASS: Site Details Page - 29 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: NEWPORT BEACH CA 92663 SEARCH ID: 36 ` NAME: UNDESIGNATED PARKING AREA ADDRESS: 2809 NEWPORT NEWPORT BEACH CA 92660 ORANGE CONTACT: LUST MARINA PARK DIST/DIR: 0.53 NW _ MAP ID: REV: 04/11/08 IDI: T0605901199 ID2: STATUS: CASE CLOSED PHONE; Please note thatsome data previoua(v provided by the Stale Motor agency in the most recent edition. Incidents that occurred after the following oflershould be interpreted as unreported by the agency. LEAD AGENCY: LOCALACENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 90UT156 RESPONSIBLE PARTY: JOHNNENCOMB ADDRESS OF RESPONSIBLE PARTY: 1800 L4FAYE7TB SITE OPERATOR: WATER SYSTE51: ONTROL BOARD LUSTIS DATABASE �) ' Board bi die LUSTISdambase is not currently being provided by the have much information. Field headers with blank injaroialion CASE NUMBER: 08JO01570T CASETYPE: OTNER SUBSTANCE LEAKED: 8,8008206 SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOIPN LEAKSOURCE: UNKNOMV HOW LEAK WAS DISCOVERED: TANK CLOSURE DATE DISCOVERED (blank if not reported): 1990.05.04 00:00:00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank If not reported): 9999-09.09 00,100.00 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEM ENT (blank If not reported): ENTER DATE (blank if not reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank If not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank If not repbeted)t DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank If not reported): DATE REM EDIATION PLAN WAS SUBM ITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank If not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 1990-11.0700:00:00 REPORT DATE (blank if not reported): 1990.0-04 00:00:00 TILE DATA FROM THE CALIFORNIA STAIR WATER RESOURCFS CONTROL -BOARD LU.STIS DATABASE MTBE DATE(Date of Idstorical maximum MTBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MT11E SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: 0 51TRETESTED: NOTREQUIRED TO BE TESTED MTBE CLASS: C t 1 F LJ I L Site Details Page - 30 LUST SEARCH ID: 30 DIST/D1R: 0.53 NW MAP ID: 20 NAME: CITY YARD (FORMER) REV: 07/11/02 ADDRESS: 2809 NEWPORT BLVD IDI: 083001767T NEW PORT BEACH CA 92663 ID2: ORANGE STATUS: CASECLOSED CONTACT: PHONE: RELEASE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS by the State Water Resources Control Board in the LUSTIS database is DATABASE not currently bemgprovided by the Please note that soon data pr eviously provided agency in the mostrecent edition. Incidents that occurred dating after the year 2000 may not have much information. inforotatimr following after should be itrtetpreled as unt eported by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: SANTA ANA REGION LOCAL CASE NUMBER: 90UTI56 RESPONSIBLE PARTY: UNKNOWN ADDRESS OF RESPONSIBLE PARTY: SITE OPERATOR: WATER SYSTEM: Field headers wah blank CASE NUMBER: 083001767T CASE TYPE: OTHER SUBSTANCE LEAKED: 8008206 SUBSTANCE QUANTITY: 75 LEAK CAUSE: STRUCTURE FAILURE LEAKSOURCE: TANK HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 515190 HOW LEAK WAS STOPPED: REMOVE CONTENTS STOP DATE (blank if not reported): 515190 STATUS: CASECLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): REMOVE FLOATING PRODUCT FROM IVATER TABLE. EXCAVATE AND TREAT. ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): REMOVE FREE PRODUCT - 'DATE ENTER DATE (blank if not reported): 1120191 REVIEW DATE (blank if not reported): 4110198 DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): S15190 DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 1117190 'DATE REPORT DATE (blank if not reported): 6117190 'MTBE MTBE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE DATE(Date of historical maximum MTBE concentration): MTBE GROUNDWATER CONCENTRATION: MTBE SOIL CONCENTRATION: MTBE CNTS: 0 'MTBE FUEL: 0 MTBE TESTED: NOTREQUIRED TO BE TESTED MTBE CLASS: " I Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 LUST JOB: MARINA PARK SEARCH ID: 33 DIST/DIR: 0.54 NW MAP ID: 22_ NAME: LIDO PARK CONDOMINIUMS REV: 04/11/08 ADDRESS: 601 LIDO PARK IDI: T0605902220 NEWPORT BEACH CA 92663 I132: ORANGB STATUS: CASE CLOSED CONTACT: PHONE: Please note thatsonte data previously provided by Ilia Suite Mater Resources Control Board in Ilia LUSTIS dalobase is not currently being provided by ilia agency In the most reeent edition, Incidents that occurred after 1heyear2000 niq not have much injorntadon. Field headers with blank b jorumtion following oftershould be Interpreted os unreported by the agency, LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 98UT090 RESPONSIBLE PARTY: BILL CUNNINGHAM ADDRESS OPRESPONSIBLE PARTY: 601 LIDOPARKDR SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083003306T CASETYPE: OTHER SUBSTANCE LEAKED: DIESEL SUBSTANCE QUANTITY: 0 LEAKCAUSE: UNKNOWN LEAKSOURCE: UNKNONN HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1998-11.09 00.00:00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank if not reported): 9999.09.09 00:00:00 STATUS: CASECLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENpORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank if not reported): REVIEW DATE (blank if not reported): DATE OP LEAK CONFIRMATION (blank If not reported): DATE PRELIMINARY SITE ASSESSM ENT PLAN WAS SUBMITTED (blank If not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank it not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REM EDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank If not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank If not reported): 1999.12.03 00:00:00 REPORT DATE (blank irnot reported): 1998-11-09 00:00:00 MTBE DATE(Date of historical maximum 5ITBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MTDE SOIL CONCENTRATION (parts per million): 11TBE CNTS: 0 MTDE FUEL: 0 MITE TESTED: NOT REQUIRED TO BE TESTED MTBE CLASS: Site Details Page - 32 ' Target Property: BF.ARCH III: 38 Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: UNOCAL 5310 ADDRESS: 3001 NEWPORT NEWPORT BEACH CA 92663 ORANGE CONTACT: DIST/DIR: JOB: MARINA PARK LUST 0.60 NW MAP ID: 23 REV: 04/11/08 IDI: T0605900346 ID2: STATUS: REMEDIALACTION PHONE: RELEASE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE Please note that some data pr eviously provided by lire State {Vater Resources Cann at Board in the LUSTIS database is not cur rendy being provided by die agency 1n the most recent edition. Incidents that occurred after lire year 2000 may not have much information. rield headers with blank information following after should be interpreted as unreported by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 89UT089 RESPONSIBLE PARTY: ROLAND MORA ADDRESS OF RESPONSIBLE PARTY: 145 SOUTH STATE COLLEGE BLVD SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083000431T CASE TYPE: OTHER SUBSTANCE LEAKED: GASOLINE SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOWN LEAKSOURCE: UNKNOWN HOW LEAK WAS DISCOVERED: NO DESCRIPTION DATE DISCOVERED (blank if not reported): 1989-05-12 00:00.00 HOW LEAK WAS STOPPED: OTHER MEANS STOP DATE (blank if not reported): 9999-09.09 00.00:00 STATUS: REMEDIALACTION ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): Letter DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank if nut reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): 1993.08-19 00:00:00 DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): REPORT DATE (blank if not reported): 1989-05-19 00:00:00 Jnforinal Staff Enforcement MTBE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE MTBE DATE(Date of historical maximum MTBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: I MTBETESTED: YES MTBE CLASS: " I Site Details Page - 33 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK LUST SEARCII ID: 32 DIST/DIR: 0.60 NW MAP ID: 24 NAME: GERMAN AUTOS REV: 04/11/08 ADDRESS: 3000 NEWPORT lot; T0605900804 NEWPORT BEACH CA 92663 ID2: ' ORANGE STATUS; CASECLOSED CONTACT: PHONE___-____ RELEASE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE Please note thatsooe datapreviouslyprovided by the State IYater Resources Control Board in the LUSTIS database is not currently beingprovidedby the ' agency in/6e most recent edition. Incidents that occurredafier theyear 2000 may not havenmch hiformation. Fieldheaderswi0ib/ankitjonnation following aJtershould be Interpreted as Unreported by the agency. .LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 88UT124 RBSPONSIBLEPARTY: THBO-YANLINGEN ADDRESS OF RESPONSIBLE PARTY: 3000 NEIYPORT BLYD ' SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083001016T ' CASETYPE: SOIL ONLY SUBSTANCE LEAKED: WASTE OIL SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOIVN ' LEAKSOURCE: UNKNOMN HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1988.06-30 00:00:00 H0W LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank If not reported): 9999.09.09 00.00:00 STATUS: CASECLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEM ENT TYPE (please note Hnot not oil code translations have been provided by the reporting agency): ' DATE OF ENFORCEMENT (blunklf not reported): ENTER DATE (blank If not reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (biankif not reported): DATE PRELIMINARY SITE ASSESSM ENT PLAN WAS SUDM ITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACPERIZA'I'ION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMI'ri'Eb (blank if not reported): ' DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 1988.08.05 00:00:00 REPORT DATE (blank if not reported): 1988.06.30 00:00:00 M'rnP DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE MTDE DATE(Dateofhistorical maximum 51THE concentration): MTDE GROUNDWATER CONCENTRATION (parts per billion): , MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTDE FUEL: 0 111TBETESTED: NOTREQUIRED TO BE TESTED MTDE CLASS: Site Details Page - 34 Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK LUST SEARCH ID: 37 DIST/DIR: 0.60 NW MAP 1D: 23 NAME: UNOCAL REV: 04/11/08 ADDRESS: 3001 NEWPORT IDI: T0605937174 NEWPORT BEACH CA 92663 ID2: ORANGE STATUS: CASE CLOSED CONTACT: PHONE: RELEASE. DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE Please note that some data previously provided by the State Water Resources Control Board ur the LUSTIS database is not can endy being provided by the agency in the most recent edition. hrcidents that occurred after the year 2000 stay not have much information. Field headers ivith blank information (allowing alter should be interpreted as unreported by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 86UTV08 RESPONSIBLE PARTY: RICHGOSSETT ADDRESS OF RESPONSIBLE PARTY: POBOX85176 SITE OPERATOR: WATER SYSTEM: CASE NUMBER: CASE TYPE: UNDEFINED SUBSTANCE LEAKED: GASOLINE SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOWN LEAKSOURCE: UNKNOWN HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1965-01-01 00:00:00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank if not reported): 9999-09.09 00:00:00 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank if not reported): 'REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION(blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank If not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 1986-09-16 00:00:00 'REPORT DATE (blank if not reported): 1965.01-01 00:00:00 MTBE DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL. BOARD LUSTIS DATABASE MTBE DATE(Date of historical maximum MTBE concentration): 'MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: / MTBE TESTED: SITE NOT TESTED FOR MTBE. INCLUDES UNKNOWN AND NOTANALYLED MTBE CLASS: ' Site Details Page - 35 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 CERCLIS SEARCH ID: 1 DIST/DIR: 0.68 NW MAP ID: NAME: CAGNEYTRUST REV: 4/22I08 ADDRESS: SW CORNER OF 32ND STand NEWPORT BLVD. IDI: CA0000187997 NEWPORT BEACH CA 92663 ID2: 0904996 ORANGE STATUS: NOT PROPOSED CONTACT: JEFFINGLIS PHONE: 4159723095 ACPIONIQUALITY AGENCY/RPS START/RAA END discovery EPA Fund -Financed 03-25-1994 preliminary assessment EPA Fund -Financed 02-23-1999 08-30.1999 NFRAP (No Father Remedial Action Planned DESCRIPTION: 25 Site Details Page - 36 ' Target Property: SEARCH ID: 29 Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 NAME: BOY SCOUTS OF AMERICA SEA BASE ADDRESS: 1931 COAST NEWPORT BEACH CA 92659 ORANGE rYINTAr'T- DIST/DIR: JOB: MARINA PARK LUST 0.69 NE MAP ID: 26 REV: 04/11/08 IDI: T0605901174 ID2: STATUS: CASECLOSED PHONE: Please note drat sane data previously provided by the State Water Resources Control Board in the LUSTIS database is not currently being provided by the agency in the most i ecent edition. Incidents that occurred offer dte year 2000 nay not have much information. Field headers with blank information following af)er should be interpreted as unreported by the agency. LEAD AGENCY: LOCALAGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 90UT132 RESPONSIBLE PARTY: MIKE HARRISON ADDRESS OF RESPONSIBLE PARTY: 14321 WCHAMBERSRD SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 083001534T CASE TYPE: SOIL ONLY SUBSTANCE LEAKED: WASTE OIL SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOWN LEAKSOURCE: UNKNOWN HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank if not reported): 1990.05-07 00:00:00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank if not reported): 9999-09-09 00:00:00 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank if not reported): REVIEW DATE (blank If not reported): DATE OF LEAK CONFIRMATION (blank If not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank If not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank if not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank If not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 1990-08-08 00 00:00 REPORT DATE (blank if not reported): 1990-05-07 00:00:00 MTBE DATA FI20M THE CALIFORNIA STATE WATER RESOURCES CONTROL ROARD LUSTIS DATABASE MTBE DATE(Dute of historical maximum MTBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: 0 MTBE TESTED: NOTREQUIRED TO BE TESTED MTBE CLASS: 7 LJ Site Details Page - 37 r Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 LUST SEARCH ID: 35 , DIST/DIR: 0.70 NW MAP ID: -27 NAME: NEWPORT BEACH CITY HALL REV: 04/11/08 ADDRESS: 330ONEWPORT IDI: T0605900150 NEWPORT BEACH CA 92658 ID2: ' ORANGE STATUS: CASE CLOSED PHONE: _CONTACT: RELEASE DATA FROM THE CALIFORNIASTATEWATER RESOURCES CONTROL BOARD LUSTIS DATABASE Pleasenota dtntsmne data pravlousty provided by the State Niter Resources Cuntrul Board in the LUSTIS database is not currently being provided by the agency in the most recent edition. Incidents that occurredaJler iheyear 2000 may not have much information. Field headers aitlt blank lnjorntation following aJlerslmuld ba Interpreted as unreported by the agency. LEAD AGENCY: LOCALAGENCY r REGIONAL BOARD: 08 LOCAL CASE NUMBER: 8807142 RESPONSIBLE PARTY: DONALD SIMPSON ADDRESS OF RESPONSIBLE PARTY: 3300 NENPORTBLVD , SITE OPERATOR: WATER SYSTEM: CASENUMBER: 083000199T (t r CASE TYPE: OTHER SUBSTANCE LEAKED: GASOLINE SUBSTANCE QUANTITY: 0 LEAK CAUSE: UNKNOMN LEAKSOURCE: UNKNOMN r HOW LEAK WAS DISCOVERED: TANKCLOSURE DATE DISCOVERED (blank If not reported): 1988.08-09 00:00:00 HOW LEAK WAS STOPPED: CLOSE TANK STOP DATE (blank if not reported): 9999=09.09 00:00:00 ' STATUS: CASECLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENTTYPE (please note that not all code translations have been provided bythe reporting agency): DATE OF ENFORCEMENT (blank if not reported): r ENTER DATE (blankifnot reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (blank if not reported): ' DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank ifnut reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank If not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): ' DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank If not reported): 1991.06-19 00:00:00 REPORT DATE (blank if not reported): 1988.08.09 00.,00.-00 r MTBF DATA FROM THE CALIFORNIA STATE WATER RESOURCES CONTROL BOARD LUSTIS DATABASE MTBE DATE(Date of historical maximum NI TBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): , MTBE CNTS: 0 MTBE FUEL: 1 MTBETESTED: SITE NOT TESTED FOR MTBE. INCLUDES UNKNOMN AND NOTANALYLED MTBE CLASS: " r i Site Details Page - 38 Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 LUST JOB: MARINA PARK iI SEARCH ID: 39 DIST/D1R: 0.73 NW MAP ID: 28 II NAME: WORLD OIL 42 ADDRESS: 3401 NEWPORT NEWPORT BEACH CA 92660 ORANGE REV: 04/11/08 1Dl: T0605901106 ID2: STATUS: CASE CLOSED PHONE: Please note that some data previously provided by the State Water Resources Conn of Eomd in the LUSTIS database is not currently being provided by die agency in the most recent edition. Incidents that occurred after the year 2000 may not have much information. Field headers with blank information follmving aflershould be interpretedas unreported by the agency. LEAD AGENCY: LOCAL AGENCY REGIONAL BOARD: 08 LOCAL CASE NUMBER: 90UT057 RESPONSIBLE PARTY: JOHNHUNDLEY ADDRESS OF RESPONSIBLE PARTY: 9302 S GARFIELD AVE SITE OPERATOR: WATER SYSTEM: CASE NUMBER: 0830014S6T CASE TYPE: OTHER SUBSTANCE LEAKED: 12035,800661 SUBSTANCE QUANTITY: 0 LEAK CAUSE: CORROSION LEAKSOURCE: TANK HOW LEAK WAS DISCOVERED: NUISANCE CONDITIONS DATE DISCOVERED (blank If not reported): 1999.11-13 00:00:00 HOW LEAK WAS STOPPED: CLOSE TANKAND FILL IN PLACE STOP DATE (blank if not reported): 9999-09-09 00:00:00 STATUS: CASE CLOSED ABATEMENT METHOD (please note that not all code translations have been provided by the reporting agency): ENFORCEMENT TYPE (please note that not all code translations have been provided by the reporting agency): DATE OF ENFORCEMENT (blank if not reported): ENTER DATE (blank if not reported): REVIEW DATE (blank if not reported): DATE OF LEAK CONFIRMATION (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN WAS SUBMITTED (blank if not reported): DATE PRELIMINARY SITE ASSESSMENT PLAN BEGAN (blank if not reported): DATE POLLUTION CHARACTERIZATION PLAN BEGAN (blank If not reported): DATE REMEDIATION PLAN WAS SUBMITTED (blank if not reported): DATE REMEDIAL ACTION UNDERWAY (blank if not reported): DATE POST REMEDIAL ACTION MONITORING BEGAN (blank if not reported): 1999-10.28 00.00:00 DATE CLOSURE LETTER ISSUED (SITE CLOSED) (blank if not reported): 2004-06-15 00:00:00 REPORT DATE (blank if not reported): 1989-11-13 00:00:00 MTBE DATE(Date of historical maximum MTBE concentration): MTBE GROUNDWATER CONCENTRATION (parts per billion): MTBE SOIL CONCENTRATION (parts per million): MTBE CNTS: 0 MTBE FUEL: 0 MTBE TESTED: YES MTBE CLASS: Closure Leiter Site Details Page - 39 Envii•onrnental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 -SEARCHID: NAME: ORANGE COUNTY REFINING CO. WELL 3 ADDRESS: 213 42ND ST. NEWPORT BEACH CA 92660 Orange CONTACT: STATE DIST/DIR: 1.13 NW _ MAP ID_ OTHER SITE NAMES (blank bclaw- not reported by aeencv) ORANGE COUNTYREFININGCO. WELL 3 REV: 07/03/00 ID1: CAL30130028 1D2: STATUS: PROPERTY/SITE REFERRED PIIONE: GENERAL SITE INFORMATION. File Nome (if different than site mmno): Status: PROPERTY/SITE REFERRED TO ANOTHER AGENCYIREFOA) AWII Site Type: N/A NPL Site: Fund: Status Dale: 02021995 Lead: Staff. Senior Supervisor: DTSC Region and RWQCB : 41LONG BEACH Bronchi SOUTHERN CA. - B RIVQCB: SANTAANA SlleAccess: On Cortese List: Listed Groundwater Contamination: Hoz Ranking Score: Haz Ranking Score: Number of Sources Contributing to Contamination at the Site: 0 DTSC COMM ENTS REGARDING THIS SITE (hlnnk helows not reported by aeencv) DATE COMMENT 01011973 VIOLATIONDETECTED OILFLOIVEDINTO HOUSE BUILTOVER IVELL DATE COMMENT 05291974 LETTERFROAfINGRAMINDOGTOCITYOFNB DATE COMDIENT 05291974 RECOMNORTH BEACH TAKE CARE OF WELL DATE COMMENT 0603/974 DOG. LETTER FROMJFAfATTHEI M OUTLINES DATE COMMENT 06031974 ABANDPROCEDURE, DISCUSSPROBB9IVELL DATE COMMENT 11141975 FACILITYDRIVE-BY NOAPPARENTPROB, DATE COMMENT 11141975 INSPECTION(STATE) DOG, CAPPED and C-U IVELL. DATE COMMENT 06261981 DOG. LIST IVELLASIM),APT069.05501 DATE COMMENT 06261981 LEAKING OIL and GAS SINCE 1936. Contintieil on nexlpage - 1 29 Site Details Page - 40 Site Details Page - 40 I ' Target Property: Environmental FirstSearch Site Detail Report WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK ' Site Details Page - 41 Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINA PARK NEWPORT BEACH CA 92663 STATE SCARCH'►D: 14 DISTlDIR: 1.17NW MAP ID: 30 NAME: SOUTH BASIN OIL COMPANY REV: 07/03100 ADDRESS: 204/20643RD STREET IDI: CAL30130024 NEWPORT BEACH CA 92663 ID2: Orange STATUS: PROPERTY/SITE REFERRED CONTACT: PHONE: OTHER SITE NAMES (blank beimv-not reported by neencv) OTHER SITE NAMES (blank below- not reported by aeency) ORANGE CO REFINING COMPANY GENERALSITE INFORMATION File Name (indifferent than site name): Status: FROPERTYISITE REFERRED TO ANOTHER AGENCY (REFOA) AWP Site Type: N/A NPL Site: Farad: Status Date: 0523/988 Lead: Staff: Senior Supervisor: AIMONROY DTSC Region and RWQCB : 4ILONG BEACII Brunei]: SOUTHERN CA. - B RWQCB: SANTAANA Site Access: On Cortese List: Groundwater Contamination: Haz Ranking Score: Hoz Ranking Score: Number of Sources Contributing to Contamination at llte Site: 0 OTHER AGENCY I D NUMBERS (blink below not reported by neencv) ID SOURCE NAME, and VALUE: EPA IDENTIFICATIONNUAIBER CAD982359408 INFORMATION ON SPECIAL PROQRAMS THE SITE IS ASSOCIATED WITH(blankhelow- not renortedhvaeencvl CERCLA 11 PROJECTED ACTIVITIES (Munk below- not reported by neencv) PROJECTED ACTIVITIES (biank_bclmv- not reported by neenc Activity: (PA) Activity Status: PROPERTASITEREFERRED TO ANOTHER AGENCY Completion Due Date: Revised Completion Due Date: Date Activity Actually Completed: 05231988 Yards of Solids Removed: 0 Yards of Solids Treated: 0 Gallons of Liquid Removed: 0 Gallons of Liquid Treated: 0 Activity: (SS) Activity Status: PROPERTY/SITE REFERRED TO ANOTHER AGENCY Completion Due Date: 11 !I LJ I - Condizuetl on Dext page - Site Details Page - 42 II I , Environmental FirstSearch Site Detail Report Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK i STATE ( 1� SEARCH ID: 14 DIST/D1R: 1.17 NW MAP ID: 30 NAME: SOUTH BASIN OIL COMPANY ADDRESS: 204/206 43RD STREET NEW PORT BEACH CA 92663 Orange CONTACT: REV: 07/03/00 ID1: CAL30130024 ID2: STATUS: PROPERTY/SITE REFERRED PHONE: Revised Completion Due Date: Date Activity Actually Completed: 10281994 Yards of Solids Removed: 0 Yards of Solids Treated: 0 Gallons of Liquid Removed: 0 Gallons of Liquid Treated: 0 DTSC COMMENTS REGARDING THIS SITE (blank below- not reported by aeencv) DATE COMMENT 06011981 INSPECTION(STATE) DOG SUPERVISED CAPPING and CLEANUP OF WELL DATE COMMENT 06201981 DOG FILES LIST WELL AS HA&HAS BEENLEAK DATE COMMENT 0610I981 METHANE and HYDROGENSULFIDEGASSINCE 64 DATE COMMENT 06201981 API 059-05474 DATE COMMENT 01141982 FACIL17YDRIVE-BY HOUSESARECOMPLETELYDEMOLISHED-ABAND DATE COMMENT 01141982 APPEARS COMPLETE. STANDING IVATER ONSITE- DATE COMMENT 01141982 BLACKAND ODORONS. DATE 01141982 COMMENT CONTACT DOG and C177OFNEWPORT BEACH DATE COMMENT 01251982 FACILITYDRIVE-BY DETERMINE IF THERE SANYSITE PROB. DATE COMMENT - 12021982 FINAL STRATEGY SITE REFERRED: TO DOG DATE COMMENT 03301988 FACILITYDRIVE-BY LOCATION OF WELL IS INA RESIDENTIAL DATE COMMENT 03301988 NEIGHBORHOOD. DATE COMMENT 05231988 PRELIMASSESS DONE ]VIA; IVELL HAS BEENPROPERLYABANDONED DATE COMMENT 05231988 IN ACCORDANCE WITH DOG POLICIES, DATE COMMENT 06131988 SUBMIT TO EPA NFA FOR EPA: BASED ONA VAILABLEINFO, DATE COMMENT - Combined on next page - ■ Site Details Page - 43 Environmental Firsdearch Site Detail Report Target Property: WEST BALBOA BLVD JOB: MARINAPARK NEWPORT BEACH CA 92663 STATE SEARCH ID: 14 ^4 DIST/DIR: 1.17 NW MAP 1D: 30 NAME: SOUTH BASIN OIL COMPANY REV: 07/03/00 ADDRESS: 204/206 43RD STREET IDI: CAL30130024 NEWPORT BEACH CA 92663 ID2: Omngc STATUS: PROPERTY/SITE REFERRED CONTACT: PHONE: 06131988 THESITEIVILLNOTSCOREPORNPL DATE COMMENT 10281994 SITCSCRCENINO/PILERCVIEWDETERAIINENPArORDTSC. Site Details Page - 44 u Environmental Firsdearch Street Name Report for Streets within 1 Mile(s) of Target Property Target Property: WEST BALBOA BLVD NEWPORT BEACH CA 92663 JOB: MARINA PARK IStreet Name Dist/Dir Street Name Dist/Dir '10th St 0.58 SE Marino Dr 0.79 NE 0.29 NW l llh St 0.50 SE McFadden PI 12th St 0.40 SE Newport Blvd 0.28 NW 13th St 0.32 SE Newport Pier 0.33 SW 141h St 0.24 SE Nomad St 0.29 NW 15th St 0.15 SE Ocean View Ave 0.84 NE 16th St 0.08 SE Old Newport Blvd 0.92 NW 17th St 0.06 SW Park Ln 0.87 NW 0.86 NE 18th St 0.11 SW Park PI 19th St 0.18 NW Piazza Genoa 0.27 NE St 0.22 NW Piazza Lido 0.37 NE '20th 21st P1 0.31 NW Pirate Rd 0.87 NE 21st St 0.27 NW Private St 0.40 NW 22nd St 0.30 NW Rhine PI 0.34 NW 23rd St 0.36 NW River Ave Riverside Ave 0.96 NW 0.83 NW 24th St 0.40 NW 25th St 0.42 NW Saint Andrews Rd 0.79 NE 26th St 0.40 NW Santa Ana Ave 0.96 NW 27th St 0.48 NW Seashore Dr 0.76 NW 281h St 0.41 NW Shipyard Way 0.31 NW 29th St 0.47 NW Short St 0.79 NW 30th St 0.50 NW Signal Rd 0.92 NE 31st St 0.55 NW Snug Harbor Rd 0.90 NE 32nd St 0.55 NW Strada Ctr 0.37 NE 33rd St 0.73 NW Strada Palermo 0.47 NE '34th St 0.77 NW The Arc 0.28 NW 0.35 NW 35th St 0.81 NW The Rhine 36th St 0.86 NW The Rialto 0.90 NW 37th St 0.91 NW Tustin Ave 0.78 NE 38th St 0.93 NW Via Antibes 0.52 NW 39th St 0.98 NW Via Barcelona 0.48 NW 61h St 0.96 SE Via Cordova 0.43 NE 7th St 0.87 SE Via Dijon Eboli 0.39 NE 0.37 NE 8th St 0.77 SE Via 9th St 0.65 SE Via Fermo 0.33 NE Ave 0.85 NE Via Firenze 0.30 NE 'Aliso Anchorage Way 0.21 NW Via Florence 0.35 NE Anza St 0.31 NW Via Genoa 0.28 NE Arbor Dr 0.84 NE" Via Graziana 0.29 NE Avon Aly 0.75 NE Via Havre 0.27 NE Avon St 0.84 NE Via Ithaca 0.28 NE Balboa Coves 0.91 NW Via Jucar 0.30 NE Bayshore Dr 0.73 NE Via Koron 0.31 NE 'Beach Dr 0.19 NW Via Lido 0.52 NW Beacon St 0.88 NE Via Lido Nord 0.46 NE Bolivar St 0.24 NW Via Lido Soud 0.27 NE Vista Blvd 0.93 SE Via Lorca 0.33 NE 'Buena Cabrillo St 0.20 NW Via Malaga 0.60 NW I Environmental FirstSearch Street Nante Report for Streets within 1 Mile(s) of Target Property Target Property: _Street Name____ Central Ave Channel PI Channel Rd Circle Dr Clay St Cliff Dr Clubhouse Ave Coral PI Court St Crestview Dr Drake St Edgewater Ave EI Modena Ave El Pasco St Finley Ave Fremont St Fullerton Ave Irvine Ave Kings Rd La Jolla Dr La Jolla Ln Lafayette Rd Lake Ave Lido Park Dr Linda Ave Marcus Ave WEST BALBOA BLVD NEWPORT BEACH CA 92663 Dist/Dir 0.78 NW 0.92 NW 0.19 NW 0.83 NE 0.98 NE 0.79 NE 0.69 NW 0.93 NE 0.19 SW 0.74 NE 0.19 NW 1.00 SE 0.88 NE 0.19 NW 0.72 NW 0.19 NW 0.82'NE 0.80 NE 0,73 NE 0.98 NW 0.98 NW 0.42 NW 0.67 NW 0.34 NW 0.97 SE 0.69NW JOB: MARINA PARK 1 F Street Name Dist/Dir I Via Mentone Via Nice Via Oporto Via Orvieto Via Palermo Via Quito Via Ravenna Via San Remo Via Trieste Via Undine Via Venezia Via Waziers Via Xanthe Via Yella Via Zurich Vilelle PI Villa Way Vista Dr W Balboa Blvd W Bay Ave W Coast Hwy W Oceanfront Waverly Dr Zurich Cir 0.35 NE 0.37 NE 0.61 NW 0.39 NE 0.41 NE 0.44 NE 0.47 NE 0.49 NE 0.52 NE 0.54 NE 0.57 NE 0.60 NE 0.64 NE 0.67 NE 0.69 NE 0.11 SW 0,43 NW 0.81 NE 0.05 SW 0.11 NW 0.72 NE 0.12 SW 0.95 NE 0.70 NE I I I I I I I Environmental FirstSearch n 1 Mile Radius ASTM Map: NPL, RCRACOR, STATE Sites 6' WEST BALBOA BLVD, NEWPORT BEACH CA 92663 Source: 2005 U.S. Census TIGER Files Target Site (Latitude: 33.608169 Longitude:-117.923035) ............................. Identified Site, Multiple Sites, Receptor.......................................................... NPL, DELNPL, Brownfield, Solid Waste Landfill (SWL), Hazardous Waste Tnballand.............. ............................ .......... ........................................................ Railroads........................................................................................................... Black Rings Represent 114 Mile Radius; Red Ring Represents 500 ft. Radius FIRST4--q'.d�H _t Environmental FirstSearch .5 Mile Radius ASTM Map: CERCLIS, RCRATSD, LUST, SWL 3 WEST BALBOA BLVD. NEWPORT BEACH CA 92663 Source: 1005 U.S. Census TIGER Fifes Target Site (Latitude: 33.608169 Longitude:-117.923035)............................. Identified Site, Multiple Sites, Receptor.......................................................... NPL, DELNPL, Brownfield Solid Waste landfill (SWL), Hazardous Waste Tribelland........................................... ............................................................ ..... Railroads.........--............................................................................................. Black Rings Represent 1/4 Mile Radius; Red Ring Represents 500 R. Radius FIRSTS Environmental FirstSearch .25 Mile Radius h, ASTM Map: RCRAGEN, ERNS, UST WEST BALBOA BLVD NEWPORT BEACH CA 92663 Source: 1005 U.S. Census TIGER Files Target Siw(Latitude: 33.608169 Longitude:-117.923035)............................. Identified Site, Multiple Sites, Receptor- ........................................................ NPL, DELNPL, Brownfield Solid Waste Landfill (SWL), Hazardous Waste Trl6alland.... ............................................................... --..................................... Railroads............................................................................ Black Rings Represent 1/4 Mile Radius: Red Ring Represents 500 ft. Radius Enviconsimemou FI im Environmental FirstSearch ` .5 Mile Radius h':r > ` Non-ASTM Map: RCRANLR, Spills 90, Permits, Other WEST BALBOA BLVD, NEWPORT BEACH CA 92663 Source: 2005 U.S. Census TIGER Files Target Site (latitude: 33.608169 Longitude:-117.923035). r Identified Site, Multiple Sites, Receptor ............ ............................. -.-............ ® ■ NPL. DELNPL, Brotfield. Solid Waste landfill (SWL), Hazardous Waste Tribelland............................................................................................................ Nations] Historic Sites and Landmark Sites ...................................................... m O Rellmads........................................................................................................... — Black Rings Represent 114 Mile Radius; Red Ring Represents 500 1L Radius FIRST Site Location Map Topo : 1.25 Mile Radius WEST BALBOA BLVD, NEWPORT BEACH CA 92663 t r Newport lleighLv 'i ��p $ II N«+pnrt fie Y �lYwpo rltM' ti y'[ Erj� t�a.un p,.✓'� Al .cn K ti s T.rluro '.•. � Uuvm -. bSI Lind Lidolge 3 y r ignt Harbor 1, Lpgnl L ighl Pa, kmµ A,,, Las Arenas tY �r )��r•,,/ „_ "' Light !pY CoHir Park +� 9fk r, rr ry A 3'I Bay 1- ., 4ry4' NEWPORT BEACH New 8each ` •Sla 9aJbOa SOURCE: SCANNED USG TOPOGRAPHIC QUADRANGLES SCANNED BY MAP'I HCH AND USGS DISTRIBUTED AUGUST, 2005. Black Rings Represent L4 Mile Radii; Red Ring R,,,vent500fr. Radius �~ `�•, 0 825 1,650 3.300 4,950 6.600 Feet Dana Supplied by: JOB NO. Prepared by FirstSearch Technology Corporation 07-07-08 MARINAPAF ap Name: NEWPORT BEACH Data Created: 1965 Dam Revised: 1981 FIGURE NO. MAP � L-CI+ [Map Reference Code: 33117-ES-TF-024 Contour Interval: 5 feet 1 1 Marina Park nrarr Fin 1 1 1 u 1 1 11 1 i 1 1 1 1 1 1 1 G.2 - HAZARDOUS RECORDS SEARCH 1 ' 6.0 REGULATORY RECORDS REVIEW MBA reviewed available Standard Environmental Record Sources from federal and state regulatory agency databases to identify use, generation, storage, treatment and/or disposal of hazardous materials and chemicals or release incidents of such materials, which may have ' impacted the Property/Site. The regulatory databases were provided to MBA from FirstSearch (see Environmental FirstSearch Report dated July 7, 2008 in Appendices). The Standard Environmental Record Sources that were included in this review follow the ASTM standard E1527-05 guidelines. ' TABLE 1 Summary of Regulatory Database Search Database Min. Search Distance (miles) map Finding Summary National Priorities List (NPL) 1.25 0 DelistedNPL 0.75 0 Comprehensive Environmental Response, Compensation, and Liability Information Systems List (CERCLIS) 0.75 1 CERCLIS — No Further Remedial Action Planned (CERCLIS — NFRAP) 0.75 2 Resource and Recovery Information System — Permitted Treatment and Disposal Facilities (RCRA— TSD) 0.75 0 Corrective Action Report (RCRA COR) 1.25 0 RCRA Generators (LQG, SQG) 0.50 6 RCRA-NLR 0.50 1 , Federal, State, Tribal IC/EC 0.50 0 Emergency Response Notification System (ERNS) 0.50 0 Tribal Lands 1.25 0 State Sites Database (CalSites) 1.25 4 State/Tribal VCP 0.75 0 State/Tribal Brownfields 0.75 0 Spills-1990 0.50 3 Solid Waste Facilities/Landfill Sites (SWL) 0.50 1 Other 0.50 3 Permits 0.50 9 Active Underground Storage Tank Facilities/ Aboveground Storage Tank (UST/AST) 0.50 1 Leaking Underground Storage Tank (LUST) 0.75 11 MBA Marina Park July 7, 2008 Page 2 Due to the Property's length covering roughly three city blocks, the approximate minimum search distance for each Standard Environmental Record Source listed above was increased by at least 0.25 mile. Leakine Underground Storaee Tanks (LUST) Each California Regional Water Quality Control Board (RWQCB) compiles an underground storage tank (UST) case list that identifies sites of soil and groundwater contamination caused by unauthorized releases from leaking USTs (LUSTS). A review of the LUST case list identified LUST sites within the search radius as listed in Table 1 and summarized below: According to the database report, the closest LUST site is Mobil 18-HG7 at 1500 Balboa in Newport Beach. According to the database, this facility reported a gasoline release in June 1986 that affected other groundwater and the case was closed in October 2000, Based on the regulatory status, the above identified LUST activities at this facility are not considered a concern to the Property. Based on information obtained during the site visit and review of the database report, all remaining LUST sites are located at least 0.40 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. Other This database contains information concerning Orange County groundwater cleanup facilities. A review of the database identified sites within the search radius as listed in Table 1 and summarized below: According to the database report, the closest Orange County groundwater cleanup site is Mobil 18-HG7 at 1500 Balboa in Newport Beach. According to the database, a release of gasoline affected the groundwater and no additional violations were listed in the database. This facility is also identified in die LUST database and is discussed in detail above. Based on the distance, topographic location, and/or regulatory status, this facility is not considered a concern to the Property. Based on information obtained during the site visit and review of the database report, all remaining Orange County groundwater cleanup sites are located at least 0.3 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. I 1 F MBA Marina Park July 7, 2008 Page 3 Registered Underground Storage Tanks (UST) The County EHD compiles a registered underground storage tank (UST) list that identifies facilities with on -site USTs. A review of the UST list identified sites within the search radius as listed in Table 1 and summarized below: Based on information obtained during the site visit and review of the database report, the identified UST site is located approximately 0.2 mile from the Property. Based on the distance, topographic location, and/or regulatory status, this facility is not considered a concern to the Property. State Sites Database This California EPA database identifies known and potential hazardous substance sites targeted for cleanup). A review of the State Sites case list identified facilities within the search radius as listed in Table 1 and summarized below: Based on information obtained during the site visit and review of the database report, all identified State Sites facilities are located at least 0.3 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. RCRIS Generator ' The EPA's Resource Conservation and Recovery Act facilities database identifies properties which report generation, storage, transportation, treatment, or disposal of hazardous waste. RCRIS small and very small quantity generators are facilities which generate less than 1000 kg/month of non -acutely hazardous waste. RCRIS large quantity generators are facilities which generate more than 1000 kg/month of non -acutely hazardous waste. A review of the Generator list identified Generator sites within the search radius as listed in Table 1 and summarized below: ' Based on information obtained during the site visit and review of the database report, all identified Generator sites are located at least 0.15 mile from the Property. Based on the distance, ' topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. Solid Waste Facilities/Landfill Sites (SWF/LF) The California Integrated Waste Management Board maintains the Solid Waste Information ' System which is an inventory of the solid waste facilities in the state of California. A review of the SWF/LF list identified SWF/LF sites within the search radius as listed in Table 1 and summarized below: ' One solid waste landfill was listed as an unmapped site in the FirstSearch report. This facility cannot be plotted due to errors or missing information in the regulatory records. MBA reviewed 1 L_J i MBA Marina Park July 7, 2008 Page 4 the unmapped solid waste landfill site in the database report and determined the facility is not considered,a concern to the Property. Permits This database contains information concerning Orange County permitted facilities. A review of the database identified sites within the search radius as listed in Table I and summarized below: Based on information obtained during the site visit and review of the database report, all identified Permits sites are located at least 0.15 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. RCRA-NLR The EPA's list of all registered hazardous waste generators includes sites that are classified as NLR (no longer regulated) generator facilities. A review of the NLR list identified NLR sites within the search radius as listed in Table 1 and summarized below: Based on information obtained during the site visit and review of the database report, the identified NLR site is located approximately 0.2 mile from the Property. Based on the distance, topographic location, and/or regulatory status, this facility is not considered a concern to the Property. CERCLIS/NFRAP The Comprehensive Environmental Response, Compensation and Liability Information Sys (CERCLIS) database contains data on potentially hazardous waste sites that have been reported to the US EPA by states, municipalities, private companies and private persons. CERCLIS contains sites which are either proposed to or on the National Priorities List (NPL) and sites which are in the screening and assessment phase for possible inclusion on the NPL. The No Further Action Planned Report (NFRAP) database contains information pertaining to sites which have been removed from the U.S. EPA's CERCLIS database, NFRAP sites may be sites where, following an initial investigation, no contamination was found, contamination was removed quickly without need for the site to be placed on the NPL, or the contamination was not serious enough to require federal Superfund action NPL consideration. The database identified sites within the search radius as fisted in Table 1 and summarizedbelow: Based on information obtained during the site visit and review of the database report, all identified CERCLIS/NFRAP sites are located at least 0.3 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. I �I F I MBA Marina Park July 7, 2008 Page 5 CERCLIS ' CERCLIS contains data on potentially hazardous waste sites that have been reported to the US EPA by states, municipalities, private companies and private persons. CERCLIS contains sites which are either proposed to or on the National Priorities List (NPL) and sites which are in the ' screening and assessment phase for possible inclusion on the NPL. The database identified sites within the search radius as listed in Table 1 and summarized below: ' Based on information obtained during the site visit and review of the database report, the identified CERCLIS site is located approximately 0.55 mile from the Property. Based on the distance, topographic location, and/or regulatory status, this facility is not considered a concern to ' the Property. Emergency Response Notification System (ERNS) Emergency Response Notification System (ERNS) records and stores information on reported releases of oil and hazardous substances. The database identified sites within the search radius as listed in Table 1 and summarized below: Seven ERNS facilities were listed as unmapped sites in the FirstSearch report. These facilities cannot be plotted due to errors or missing information in the regulatory records. MBA reviewed ' the unmapped ERNS sites in the database report and determined the facilities are not considered a concern to the Property. ' SPILLS This database is provided by the California Regional Water Quality Control Board. The database identified sites within the search radius as listed in Table 1 and summarized below: Based on information obtained during the site visit and review of the database report, all identified Spills sites are located at least 0.25 mile from the Property. Based on the distance, topographic location, and/or regulatory status, these facilities are not considered a concern to the Property. Orphan Sites Seven additional facilities were listed as unmapped sites in the FirstSearch report. These ' facilities cannot be plotted due to errors or missing information in the regulatory records. MBA reviewed the unmapped sites in the database report and determined the facilities are not considered a concern to the Property. L 1 Marina Park Draft REIR ' G.3 - DREDGED MATERIAL EVALUATION Dredged Material Evaluation for the Marina Park Master Plan Newport Beach, California Final Report PREPARED FOR: City of Newport Beach Planning Department 3300 Newport Boulevard Newport Beach, California 92663 PREPARED BY: NewFields PO Box 216 4729 View Drive Port Gamble, Washington 98364 June 2009 NEwFIELDS ' June 2009 Dredged Material Evaluation Marina Park Executive Summary The City of Newport Beach is in the process of preparing the Environmental Impact Report (EIR) and submitting permit applications in support of the Marina Park project, located on the Balboa Peninsula. The Marina Park project includes the expansion of existing beach areas and marina ' facilities, including the conversion of approximately 1.13 acres of uplands to a 28-slip marina. Sediment and soils throughout the proposed marina complex will be excavated to accommodate the project depth of -12 ft. MLLW plus a 2 ft. overdredge. Approximately 63,700 cubic yards (CY) of ' soil/sediment is proposed for removal. Approximately 5,000 CY representing the top five feet of soil in the upland area will be excavated and used for project fill and is not considered as part of the proposed dredge volume. Approximately 58,700 CY is proposed for aquatic disposal. The primary ' disposal options under consideration for the dredged materials are 1) beach nourishment under Regional General Permit Number 67 or individual permit for unconfined aquatic disposal as governed by the U.S. Army Corps of Engineers (USACE)/U.S. Environmental Protection Agency (USEPA) guidelines set forth in the Inland Testing Manual (ITM; USACE/USEPA 1998), and 2) ' ocean disposal at disposal site LA-3 based on guidance provided by the Ocean Testing Manual (OTM; USACE/USEPA 1991). NewFields LLC conducted a dredged -material evaluation of the proposed dredged material from the Marina Park marina. The objective of this sampling and analysis program was to characterize the dredged materials from three dredged material management areas (Areas A, B, and C) within the Marina Park project area. Area A included that portion of the site currently occupied by the mobile home park and represented an estimated dredge volume of 21,328 cy with 2,370 cy of overdredge. Area B included that area currently occupied by the exposed beach above 0 ft MLLW, with an ' estimated volume of 13,869 cy with 2,849 cy of overdredge. Area C included that portion of the site that is below 0 ft. MLLW, with an estimated volume of 13,713 cy with 4,571 cy of overdredge. Sediment was also collected from the LA-3 Reference site. The reference sediment provided a point ' of comparison for material proposed for placement at the LA-3 ocean disposal site. Sampling and Analysis Sediment samples were collected from five stations in Area A and four stations in Area B using a direct -push corer on November 26, 2008. Samples from Area A were sampled from 5 ft. below the ground surface to a depth of-14.5 ft. MLLW (project depth plus a 241 overdredge and 0.5 ft. z-layer ' sample). The surface material (upper 5 ft.) was not included in the dredged material evaluation. Sediment samples from Area B included the surface sediment (beach sands) to a -14.5 ft MLLW. Sediment samples from Area C were collected from seven stations using a vibracorer ' sampler, sampling from the sediment surface (from -4 to -8 ft MLLW to -14.5 ft MLLW). Each of the cores was divided into an upper and lower section. For Areas A and B, that division was ' based on the transition from recent sands to ancient Bay sand deposits. That layer generally occurred between 10 and 12 ft. below ground surface. For Area C, the upper composite represented more recently deposited fine sediments and the lower composite represented the coarser ancient Bay sand deposits. The upper section of each core within an area was combined into an upper area composite ' and each of the lower sections within an area was combined into a lower area composite. NEWFIELDS E1 June 2009 Dredged Material Evaluation , Marina Park Sediment chemistry was evaluated for all upper and lower composites. Analytical chemistry included sediment conventionals (grain size, organic carbon, ammonia, sulfides, Atterberg limits, total recoverable petroleum (TRPH), oil and grease, metals (arsenic, cadmium, chromium, copper, lead, mercury, nickel, selenium, silver, and zinc), organochlorine pesticides, polychlorinated biphenyls (PCBs), organotins, petroleum aromatic hydrocarbons (14 PAHs), and phthalates. For the Area C upper and lower composites, Tier III biological tests were conducted, including benthic toxicity tests, water -column toxicity tests, and bioaccumulation tests. Benthic tests provided an estimate of toxicity to benthic organisms at the placement site and included 10-day acute tests with the amphipod, Ampelisca abdita and the polychaete, Neanthes arenaceodentara. Water -column tests were conducted with the suspended -particulate phase (SPP) to provide an estimate of toxicity to water column organisms exposed to sediment as it falls through the water column at the disposal site. It also provided an indication of water -column toxicity that might be encountered during the dredging process. SPP is the liquid portion of a 1:4 sediment/seawater slurry that is designed to simulate the dredging process. Water -column tests were conducted with a dilution series of 1% (larval test only), 10%, 50%, and 100% SPP for each of the test composites using fish, Menidia beryllina, the mysid, Americamysis bahia, and larval mussels (Mytilus sp.). Sediment from -the LA-3 disposal site reference site (LA-3 Reference) was included in the benthic tests, but is not required for the SPP tests. Bioaecumulation potential (BP) testing was conducted with both Area C composites, as well as LA-3 Reference. The bioaccumulation test evaluates the potential for uptake of chemical constituents in the sediment to tissues of benthic organisms at the placement site. The bioaccumulation tests were conducted as 28-d exposures with 4he clamp Maconia nasuta, and the polychaete worm, Nephtys caecoides. Following the 28-d test, tissues were analyzed for tissue residues. The chemistry analyte list for tissues exposed to the Area C composites included mercury and lipids. Evaluation Criteria Evaluation criteria were based on the 1TM/RGP-67 guidance for nearshore placement and OTM guidance for open ocean placement at the LA-3 disposal site. Under the RGP-67 and ITM, sediment is suitable for beach nourishment projects or nearshore placement if the sediment is >80% sand and gravel, is free from chemical contamination, is not plastic (a measure of cohesiveness), and is not likely cause adverse aesthetic effects to the receiving beach. According to the RGP-67, sediments with slightly higher percentages of fines (15% to 45% fines) may be considered for placement in the surf zone. n order to determine whether test sediments were free of chemical contamination, chemical concentrations in test sediments were compared to National Oceanographic and Atmospheric Administration (NOAA) effects -based guidance values called Effects -Range Low (ERL) and Effects -Range Median (ERM). The ERL represents the 10"' percentile in NOAA effects data base and the ERM represents the 50"' percentile. While not criteria, these guidance values provide an indication of whether chemical concentrations are sufficient to predict benthic community effects. If the ERL/ERM values are exceeded, further biological testing might be required as directed by the ITM. Under the OTM, sediment is suitable for placement in an open -ocean disposal site if it does not exceed the limiting permissible concentration (LPC) for the disposal site. The LPC is based on comparisons of the results of the sediment chemistry, toxicity tests, and bioaccumulation test in the test treatments with those of the LA-3 Reference site. Chemical concentrations were also screened using the NOAA ERL and ERM values. For benthic toxicity tests, the LPC was defined as no significant toxicity, relative to the LA-3 Reference and survival within 10% of the reference for die polychaete test and 20% for the amphipod test. For the SPP tests, the LPC was based on a NEwFiFLDS E2 11 I I I [1 I I June 2009 Dredged Material Evaluation Marina Park I L rI u n L Ll 1 I P I comparison of survival or normal development (larval test only) in the 100% SPP of the test treatments with that of the control seawater. If there is a significant difference, then the median lethal concentration (LCso) for the test treatments is compared with a modeled concentration of SPP at the boundary of the disposal site. Concentrations of targeted chemical analytes in the tissues exposed to test sediments are first compared to the tissues exposed to the LA-3 Reference sediment and second compared to guidance values from the Food and Drug Administration (FDA) and USEPA. USEPA Region IX and the USACE-LA District will make the final determination of suitability. Sediment Evaluation The following section discusses each of the Area composites in context of the requirements for each of the disposal options. Sediment in the upper composite from Area A (Comp A-U) was characterized by 96% sand and gravel and 0.15% TOC. Sediment from the upper Area B composite (Comp B-U) was also characterized by 96% sand and gravel, with 0.02% TOC. Sediment in the lower composites from Areas A and B (Comp A-L and Comp B-L) were very similar to each other and likely represented the same ancient Bay -sand layer. Sediments in the lower composites were >98% sand and gravel with <0.1% TOC. None of the Comp A or B sediments were plastic, indicating that they would not hold their form. All of the metals were either undetected or detected very near the detection limits. Pesticides, PCBs, tributyltin, TRPH, oil and grease, and phthalates were not detected in any of the four Area A and B composites. PAHs were either undetected or detected at very low concentrations (:532 µg/kg total PAHs). Sediment from Areas A and B met the requirements for beach nourishment, as defined by the ITM and RGP-67. Both the upper and lower composites from Areas A and B were >95% sand and gravel, were free of contamination, and were not plastic. Additionally, sediment had low or no ammonia, sulfides and oil and grease, indicating that it would not have adverse aesthetic effects on the receiving beaches. This material would also meet the requirements for open -ocean disposal at LA-3, as defined by the OTM/ITM. Sediment in Area C was comprised of either a thick layer of sand, overlying a silt layer, overlying the ancient Bay sands (in the nearshore portions of Area C) or by silts and clays overlying the ancient Bay sands (in the channel portion of Area Q. Sediment in the upper composite from Area C (Comp C-U) was 77.9% sand, with 0.68% TOC. Silver and selenium were not detected in Comp C-U. All other metals were detected in Comp C-U sediments. With the exception of mercury, all metals were detected at concentrations below those of the LA-3 Reference sediment and below the ERL. Mercury was detected in Comp C-U at a concentration of 0.36 mg/kg, which is slightly above that of the LA-3 Reference site (0.10 mg/kg) and the ERL of 0.24 mg/kg, but below the ERM of 0.76 mg/kg. Pesticides, PCBs, tributyltin, TRPH, oil and grease, and phthalates were not detected in the upper Area C composite. PAHs were either undetected or were detected at very low concentrations, with total, detected PAHs of 108 µg/kg, well below the ERL of 4,022 µg/kg. Upper and lower segments of individual cores from Area C were also analyzed for mercury and sediment grain size. The upper segment from the cores in the nearshore portion of Area C was characterized as a mixture of sand and silt. Mercury concentrations ranged from undetected to 0.85 mg/kg. The upper segment of cores from the offshore portion of Area C was dominated by fine- grained silts and clays and mercury concentrations were higher, ranging from 1.11 to 3.35 mg/kg. The lower segments for both the nearshore and offshore stations were similar, dominated by sand NEwRELDS E3 June 2009 Dredged Material Evaluation Marina Park with concentrations of mercury that were either undetected or detected at concentrations very near the detection limit. The upper silt layer that occurred in each of the cores was 2 to 3 ft thick and comprised relatively small portion of the material in the Area C-U composite. Sediment from the lower Area C composite was very similar to the dower composites from Areas A and B, with 99% sand and 0.05% TOC. Metals were either undetected or detected very near the detection limits. Pesticides, PCBs, tributyltin, TRPH, oil and grease, plithalates, and PAHs were not detected in the Comp C-L. Both Area C composites were evaluated for potential biological effects related to the dredging and placement of the proposed dredged material at the LA-3 disposal site. No toxicity was observed in either of the benthie tests. Amphipod survival ranged from 87% to 92% and polychaete survival ranged from 840% to 92%. No significant differences were observed between the test treatments and the LA-3 Reference for either test. No toxicity was observed in any of the SPP exposures, with >88% survival or normal development in all test treatments for each SPP test. There were no significant differences between the 0% and 100% treatments and no calculable LCso for any of the SPP test treatments. Mercury was not detected in any of the tissues exposed to Comp C-L or LA-3 Reference. Mercury was either undetected or detected at the detection limit (0.01 to 0.013 mg/kg) in tissues exposed to Comp C-U. The mean tissue concentrations in clams and worms exposed to Comp C-U were within 20% of the detection limit, the standard margin of error for this analytical method. The tissues concentrations of mercury were also well below the FDA limit of 1.0 mg/kg and the risk -based guidance value of 0.3 mg/kg (USEPA 2000). Sediment from the Area C upper composite would not meet the requirement for beach nourishment, with <80% sand and gravel. The nearshore portion of Area C represented by Stations 10, 12 and 16 would meet the requirements for placement in the surf zone or for open -ocean disposal. With the exception of mercury, concentrations for chemicals of potential concern were either not detected or detected at concentrations below those of the LA-3 Reference site. Mercury was detected above the ERL, but below the ERM. No significant toxicity was observed in any of the biological tests.and no significant bioaccumulation of mercury was observed in the bioaccumulation tests. Sediment from the offshore portion of the Area C upper composite represented by Stations 11, 13, 14, and 15 would not meet the requirements for beach replenishment or open -ocean disposal due to mercury concentrations in the sediments. Alternative disposal options including upland disposal or placement in a confined aquatic disposal facility will need to be evaluated prior to dredging this material. Sediment from the lower Area C composite met the requirements for beach nourishment and ocean disposal. If the lower portions of Area C represented by Stations 11, 13, 14, and 15 are disposed of separately from the upper portion, the dredged material will be monitored for grain size during removal to ensure that surface sediment are not placed on beaches or in the open ocean. Because the demarcation from the overlying silt/clay layer and the underlying clean sands is distinct, dredging for upland disposal will be considered complete when field monitoring indicates that the remaining sediment face is>80% sand. NEWFIELDS E4 I 11 I I I 11 CI I I I 1 I I I I F �l I� I L LJ I June 2009 TABLE OF CONTENTS Dredged Material Evaluation Marina Park ACRONYMS AND ABBREVIATIONS iii 1.0 INTRODUCTION........................................................................................................................1 1.1 Background and History ............................................................................................. I 1.1.1 Existing Soil and Sediment Characteristics...................................................3 1.1.2 Chemical Evaluations of Existing Soils and Sediments................................4 2 METHODS................................................................................................................................5 2.1 Definition of Areas and Sample Locations.................................................................6 2.2 Overview of Analyses...............................................................................................10 2.3 Field Collection Program for Soil/Sediment Core Samples......................................11 2.3.1 Sampling Locations and Depths..................................................................11 2.4 Sediment Sampling...................................................................................................12 2.4.1 Core Collection...........................................................................................12 2.4.2 Navigation...........................................................................................13 2.4.3 Core Handling...........................................................................................13 2.4.4 Sample Processing and Storage...................................................................13 2.4.5 Shipping...........................................................................................13' 2.4.6 Decontamination of Field and Laboratory Equipment.................................14 2.5 Bioassay Testing.......................................................................................................14 2.5.1 Benthic Toxicity Tests................................................................................ 14 2.5.2 Water -Column Tests....................................................................................15 2.5.3 Bioaccumulation Potential Tests..................................................................15 2.5.4 Seawater for Bioassay Testing.....................................................................16 2.6 Quality Assurance/Quality Control...........................................................................16 2.7 Physical and Chemical Analysis...............................................................................17 2.7.1 Physical Analyses........................................................................................17 2.7.2 Sediment Chemistry.....................................................................................17 2.7.3 Bioaccumulation Tissue Chemistry .............................................................19 2.7.4 Quality Assurance/Quality Control..............................................................19 2.8 Data Review, Management, and Analysis................................................................20 2.8.1 Data Review...........................................................................................20 2.8.2 Data Analysis...........................................................................................20 3 RESULTS................................................................................................................................21 3.1 Sampling Results.......................................................................................................21 3.2 Physical and Chemical Analysis of Sediment...........................................................24 3.2.1 Physical Characteristics and Conventional Chemical Analysis...................24 3.2.2 Metals...........................................................................................25 3.2.3 Organotins...........................................................................................26 3.2.4 Polycyclic Aromatic Hydrocarbons.............................................................26 3.2.5 Chlorinated Pesticides..................................................................................27 3.2.6 PCB Arocolors...........................................................................................28 3.17 Phthalates...........................................................................................28 3.3 Results of Benthic and Water -column Bioassays.....................................................29 3.3.1 10-Day Benthic Amphipod Test..................................................................29 3.3.2 10-Day Solid -Phase Polychaete Worm Test................................................31 3.3.3 Results of the Water -Column Test with Menidia beryllina .........................33 3.3.4 Results of the Water -Column Test with Americamysis bahia.....................35 NEWFIELDS Dredged Material Evaluation 1 June 2009 Marine Park 3.3.5 Results of the SPP Test with Mytilus sp......................................................37 , 3.3.6 Bioaccumulation Test Results......................................................................39 3.4 Tissue Chemical Analysis......................................................................................41 4 DISCUSSION...........................................................................................................................42 REFERENCES..................................................................................................................................47 FIGURES Figure 1. Location of Marina Park Master Plan area (dashed line) and proposed marina within Figure 2. NewportBay......................................................................................................................2 Locations of recent samples collected near the proposed marina....................................4 ' Figure3. Figure 4. Areas and Station Locations..............................................................................................7 Project Areas and Station Locations with Proposed Project Plan and Current Bathymetry ......................................................................................................8 Figure 5. Direct -push CPT (a,b) and Vibracore (c, d) samplers, Marina Park 2008.........................12 Figure 6. General Characterization of Sediment in Cores from Marina Park...................................23 Figure 7. Portion of Area C that is not considered to be suitable for beach replenishment or open - oceandisposal...................................................................................................................46 TABLES ' Table 1-1. Data for soil/sediment samples at Marina Park, May 2008............................ ................. 5 Table 1-2. Nearshore sediment data, September 2007......................................................................5 Table 2-1. Estimated Volumes for Project Areas..............................................................................9 , Table 2-2 Station Designations within Each Area, Marina Park 2008.............................................. I I Table 2-3 Sample Designations for Chemical and Biological Analyses ........................................... I I Table 2-4. Analytical Laboratories, Points of Contact, and Shipping Information ............................14 Table 2-5. Bioassay Testing Proposed for Suitability Evaluations of Dredged Material..................14 Table 2-6. Chemical and Physical Parameters, Analytical Methods, and Target Detection Limits ..18 Table 3-1. Sample Log Data, Marina Park 2008..............................................................................22 Table 3-2. Summary of Conventionals, Marina Park 2008................................................................24 Table 3-3. Inorganic Metals in Sediment, Marina Park 2008......................................... ................25 Table 3-4.Organotins in Sediment, Marina Park 2008 ......................................................................26 Table 3-5. PAHs in Sediment, Marina Park 2008...................... :.......................... I ............................ 26 , Table 3-6. Chlorinated Pesticides in Sediment, City of Newport 2008.............................................27 Table 3-7. PCB Aroclors in Sediment, City of Newport 2008...........................................................28 , Table 3-8. Phthalates in Sediment, City of Newport 2008.................................................................28 Table 3-9 Survival Summary for the 10-day Benthic Test with A. abdita.........................................29 Table 3-10. Summary of Water Quality for the 10-day Benthic Test with A. abdila ........................29 Table 3-11 Test Condition Summary forAmpelisca abdita...............................................................30 , Table 3-12. Survival Summary for the 10-day Bnethic Test with N. arenaceodentata ..................... 31 Table 3-13. Summary of Water Quality, 10-Day Benthic Test with N. arenaceodentata .................31 Table 3-14. Test Condition Summary for Neanthes areanaceodentala 32 Table 3-15. Summary of Results for the Water -column Test with M. beiyllina............... 4................ 33 Table 3-16. Summary of Water Quality for the Water -column Test with M. beryllina.....................33 , NEWFtE.Ds I� IDredged Material Evaluation June 2009 Marina Park Table 3-17. Test Condition Summary for Menidia beryllina.............................................................. 34 Table 3-18. Summary of Results for the Water -column Test with A. bahia...................................... 35 Table 3-19. Summary of Water Quality Observations; Water -column Test with A. bahia...............35 Table 3-20. Test Condition Summary for Americamysis bahia......................................................... 36 Table 3-21. Summary of Results for the Water -column Test with Mytilus sp................................... 37 ' Table 3.22 Summary of Water Quality Observations, Water -column Test with Mytilus sp.............. 37 Table 3-23. Test Condition Summary for Mytilus sp......................................................................... 38 Table 3-24. Summary of M. nasuta and N. caecoides Survival 28-d Bioaccumulation Test ............39 Table 3-25. Summary of Water Quality for the 28- day Bioaccumulation Test................................39 Table 3-26. Test Condition Summary for Macoma nasuta and Nephtys caecoides .......................... 40 Table 3-26. Summary of Mercury Concentrations in Tissues............................................................41 1 I 17 F LJ Ll I Lr ,J lJ APPENDICES A Field Logs and Photographs of Cores B Chemistry Laboratory Reports C Benthic Test Data Sheets and Supporting Information D Water -Column Test Data Sheets and Supporting Information E Bioaccumulation Test Data Sheets and Supporting Information NEWFIELDS Dredged Material Evaluation June 2009 Marina Park ACRONYMS AND ABBREVIATIONS ARI ASTM Analytical Resources Incorporated American Society for Testing and Materials BP bioaccumulation potential CPT cone penetration test COC chain of custody DGPS differential global positioning system ERL effects range -low ERM effects range -medium GC/MS gas chromatograph-mass spectrometry with selected ion monitoring ICP-MS inductively coupled plasma, emissions spectrometer equipped with a mass detector ID identification ITM Inland Testing Manual , LPC limiting permissible concentration MLLW mean lower low water OTM Ocean Testing Manual PAH polynuclear aromatic hydrocarbon PCB PEL polychlorinated biphenyl Probable effects level POC point of contact QA/QC quality assurance/quality control QAP quality assurance plan ' RGP regional general permit SAP sampling and analysis plan SIM selective ion method SM Standard Methods SOP standard operating procedure SP solid phase SPP suspended particulate phase STFATE Short Term Fate model SVOC semivolatile organic compound TBT tributyltin TOC total organic carbon TPH USACE total petroleum hydrocarbon United States Army Corps of Engineers USEPA United States Environmental Protection Agency NewFields NewFields Northwest LLC. I II 1 NEWFIELDS iV I June 2009 UNITS OF MEASUREMENT °C degree(s) Celsius $ feet µg/kg microgram(s) per kilogram µg/L microgram(s) per liter µm micrometer(s) ng/kg nanogram(s) per kilogram cm centimeter(s) L liter m meter(s) mg/kg milligram(s) per kilogram mL milliliter(s) mm millimeter(s) ppb parts per billion ppm parts per million ppt parts per thousand v/v volume per volume CY cubic yards Dredged Material Evaluation Marina Park PI June 2009 Dredged Material Evaluation Manna Park IJ L I Cl I I l� 1.0 INTRODUCTION The City of Newport Beach is in the process of preparing the Environmental Impact Report (EIR) for the CEQA process and submitting permit applications in support of the Marina Park project, located on the Balboa Peninsula. The Marina Park project includes the expansion of existing beach areas and marina facilities, including the conversion of approximately 1.13 acres of uplands to a 28-slip marina. Sediment and soils throughout the proposed marina complex will be excavated to accommodate the project depth of 12 ft. MLLW plus a 2 ft. overdredge. Approximately 63,700 cubic yards (CY) of soil/sediment is proposed for removal. Approximately 5,000 CY representing the top five feet of soil in the upland area will be excavated and used for project fill and is not considered as part of the proposed dredge volume. Approximately 58,700 CY is proposed for aquatic disposal. The primary disposal options under consideration for the dredged materials are 1) beach nourishment under Regional General Permit Number 67 or individual permit for unconfined aquatic disposal as governed by the U.S. Army Corps of Engineers (USACE)/U.S. Environmental Protection Agency (USEPA) guidelines set forth in the Inland Testing Manual (ITM; USACE/USEPA 1998), and 2) ocean disposal at disposal site LA-3 based on guidance provided by the Ocean Testing Manual (OTM; USACE/USEPA 1991). Based on previous soil and sediment data collected by NewFields and Terra Costa from the site, the majority of the excavated material is expected to be available for on -site beach replenishment and expansion. It is also anticipated that a portion of the material will need to be disposed of either at the LA-3 ocean disposal site or upland, either as clean fill or as contaminated material. The objective of this sampling and analysis program (SAP) is to characterize the dredged materials and upland excavation material from study units within the proposed marina area in the Marina Park Master Plan to determine environmental suitability for beach replenishment or ocean disposal. The material under consideration for ocean disposal will be tested based upon criteria outlined in the OTM (USEPA/USACE 1991) and the ITM (USACE/USEPA 1998). 1.1 BACKGROUND AND HISTORY Newport Bay is a coastal embayment located adjacent to the City of Newport Beach, California. The Newport Bay area supports a variety of land uses including navigation, marine industry, private and public marinas, recreational activities, and residential uses. Upper and lower Newport Bay are estuarine and nearshore marine environments, supporting both resident and migratory fish and bird species as well as a variety of native plant species. In addition, San Diego Creek, which supports agricultural land use and provides habitat for aquatic and terrestrial ecosystems, flows into the upper reaches of Newport Bay. The proposed Marina Park is located in Lower Newport Bay, on the bay side of the Balboa Peninsula between 15`h and 18`h Streets immediately north of West Balboa Boulevard (Figure 1). The site currently includes some recreational areas and mobile homes. The Marina Park Master Plan includes ' a 28-slip marina, a small -boat basin, and moorage for visiting vessels in the northeast corner of the site. I I NEwRELDS 1 a ��'/•'}�v'r-y.�-c �^� �•'1ate. Proposed MaPina ;_ ' Dredged Material Evaluation June 2009 Manna Park 1.1.1 EXISTING SOIL AND SEDIMENT CHARACTERISTICS The Balboa Peninsula was primarily formed from sand deposits overlying Bay sediments following a series of extreme storms in the 1860's. Subsequent dredging and construction has increased the size of the peninsula. In May 2008, the City conducted a geotechnical investigation of soils at the proposed Marina Park site (Terra Costa 2008). Terra Costa conducted soil borings (B-1 and B-2) and cone penetration tests (CPT-7 and CPT-12) at two locations within the footprint of the proposed marina. The cone penetration test (CPT) evaluated sediment type, as well as other physical features. The borings included a visual description at 5 ft intervals, as well as subsampling for grain size analysis. 1 The geotechnical survey characterized the project soils (upland mobile -home park and beach face) as follows: "The site is underlain by hydraulic fill, bay deposits, and older alluvial deposits beyond the depths of our deepest exploratory drilling at 50 feet. These soil and geologic units are described below in order of Iincreasing age. Hydraulic Fill Soils: Our test borings indicate that the project site -area is generally underlain by from 5 to 6 feet of loose to medium dense, gray -brown, damp to wet, hydraulically placed sands and silty sands (SP/SM), with occasional shell fragments. It is likely that these relatively "clean" granular soils were placed as the result of dredging during one or more phases of the development of Newport. Harbor. SPT blow counts within these artificially placed dry to saturated sands ranged from 7 to 25 blows per foot. Bay Deposits: The hydraulic fill sands are typically underlain by a 2- to 2 '/2 - foot -think soft to firm compressible sandy silt to silt clay bay mud, which is un cum underlain by relatively clean, medium dense, gray sands (SP/SM), with shells and shell fragments, characteristic of Holocene - age bay deposits below an elevation of approximately -2 to -3 feet. SPT blow counts within these 1 clean, saturated, natural bay deposit sands range from 13 to 24 blows per foot." The Bay Deposits extend to approximately project depth at -14 ft. MLLW. Groundwater elevations appeared to match tidal elevations in the Bay. A subsample of porewater from the borings indicated that the groundwater was at least 20%o. Samples may have been compromised by freshwater added to the sample hole used to facilitate the boring. Grain size analysis of the soil borings resulted in a similar characterization, with sand dominating throughout the area (Table 1-1). IBased on the results of the geotechnical investigation, the soils underlying the mobile -home park and neighboring beach are comprised of sand to silty sand, with shell fragments. Soils were either hydraulically -placed from dredging events, the result of deposition following historic storm events, or are Holocene-cra sediments, representative of soils underlying much of Lower Newport Bay. The sediments occupying the intertidal and subtidal portion of the proposed marina were characterized during a recent evaluation of West Lido Channel (Figure 2; Table 1-2). Marine sediments in the area appeared to be comprised of either all sand at the shallower stations (-6 to -8 & MLLW) or more recent deposits of fine-grained sediment overlying sand in the deeper stations (-10 to -15 ft. MLLW). While the surface material was determined to be too fine-grained to qualify for beach nourishment, the underlying sand appeared to be a distinctly different stratigraphic layer and would likely qualify for beach nourishment. NEwFIELDS 3 Dredged Material Evaluation ' June 2009 Manna Park Figure 2. Locations of recent samples collected near the proposed marina. Existing stormwater outfalls denoted by blue circles. 1.1.2 CHEMICAL EVALUATIONS OF EXISTING SOILS AND SEDIMENTS Concentrations of contaminants of concern were evaluated for the soils collected in borings B-1 and B-2, as well as the sediments in the neighboring channel areas (NewFields 2007). The soil borings were evaluated for metals and DDT and associated breakdown products (Table 1), contaminants of concern that have been found in other portions of Newport Bay. Metals were present very near or below the detection limits and DDT, DDE, and DDD were undetected in both soil borings. Marine sediments sampled in the subtidal portion of the proposed marina were evaluated for EPA priority pollutants (metals, petroleum aromatic hydrocarbons (PAHs), polychlorinated biphenyls (PCBs), chlorinated pesticides, and organotins) and did not show detected contaminants of concern, with the exception of mercury. Mercury was detected in some of the stations at concentrations exceeding the ERM (Long et.al. 1995). These concentrations appeared to be associated with the more recent, finer -grained material at the surface. Samples that were predominantly sand had lower mercury concentrations. The differences between the physical and chemical profiles of the surface and subsurface materials suggests evaluating the marine portion of this site as two separate upper and lower composites. Locations of current stormwater outfalls are indicated in Figure 2. Land use of the site has been limited to residential activities and to the City's knowledge there are no reported major spills on the site. NEwRELDs I I I I I I I i i I I I June 2009 Dredged Material Evaluation Marina Park 'r ki., e_a n.*. fnr enn/cartimant eamnlPs at Marina Park. Mav 2008. I awl.. .-I. vuaM .v, Anal to w...w-.....�.. Units -. B-1 - B-2 Depth below surface ft 5 10 15 20 25 5 10 20 30 Gravel % TO 0.0 1.0 0.0 5.0 11.0 1.0 2.0 0.0 Sand % 92.7 97.2 98.2 96.0 93.0 84.1 98.5 96.6 97.8 Silt & Clay % 6.3 2.8 0.8 4.0 2.0 4.9 0.5 1.4 2.2 Anal to Units Composite Surface ,'Subsurface 4,4'-DDE k <2.0 U <2.0 U <1.9 U 4,4'-DDD µg/kga U <2.0 U <t .9 U 4,4'-DDT µg/kg U <2.0 U <1.9 U 2,4'-DDT µg/kS U <2.0 U <1.9 U 2,4'-DDE µg/kg U <2.0 U <1.9 U 2,4'-DDD µg/kg U <2.0 U <1.9 U Arsenic mg/kg <6 U <6 U Cadmium mg/kg U <0.2 U <02 UChromium mg/kg 1.6 3.0 Copper mg/kg 2.8 1.2 Lead mg/kg <2 U <2 U Mercury m8lkg<l U <0.04 U <0.06 U Nickel mg/kgSilver U<I U mg/kg U <0.3 U <03 U Zinc mg/kg3 4 T bl 1 2 M rshore sediment data Se tember 2007. a e - Sample ea Water Depth (ft below MLLW) 1 Core Depth (ft below MLLW) Gravel&Sand (%) Silt&Clay (%) Mercury (µg/kg) C6 5.4 7.7 97.0 3.0 0.11 C8 7,7 9.5 96.8 3.2 0.23 C10 9.9 11.7 67.3 32.7 2.60 CIS 13.1 15.6 25.9 74.1 3.33 B6 6.1 8.7 86.8 13.2 0.37 B8 8,0 11.2 75.4 24.6 3.09 B10 11.6 14.1 70.9 29.1 2.22 B15 13.1 16.4 27.2 72.8 2.30 2 METHODS ' The objective of this sampling and analysis program (SAP) was to characterize the proposed excavated and dredged materials in the proposed Marina Park marina to evaluate environmental suitability for beach nourishment and/or ocean disposal. Material under consideration for beach ' nourishment was tested based on criteria in the ITM (USACE/USEPA 1998) and requirements under Regional General Permit Number 67 for physical appearance, composition, and chemical concentrations. The material under consideration for ocean disposal was tested based upon criteria outlined in the OTM (USEPA/USACE 1991). Dredged material for ocean disposal from this project is proposed for disposal at the USEPA-designated LA-3 disposal site. Chemical and biological analysis were conducted with reference sediment concurrent to the test sediment evaluations. I NEWFIELDS 5 Dredged Material Evaluation June 2009 Marina Park 2.1 DEFINITION OF AREAS AND SAMPLE LOCATIONS ' Core samples were collected from the upland and aquatic areas of the site to a depth of -12 ft MLLW (+2 R overdredge) as shown in Figure 3. The project footprint was divided into three dredged ' material management areas, A, B, and C (Figures 2 and 3). Area A included that portion of the site currently occupied by the mobile home park. Area B included that area currently occupied by the exposed beach above 0 ft MLLW. Area C included that portion of the site that is below 0 fl. MLLW. Five stations were sampled in Area A. The upper 5 fl. of soil from each Area A station was not included in this investigation, as the upper 5 11. of soil within the mobile home park will be used as fill material during park construction. Each of the five cores was approximately 20 ft. in length, extending from approximately +5 ft. MLLW to -15 t. MLLW. The estimated volume of proposed dredged material from Area A is 21,328 cy with 2,370 cy of overdredge (Table 1-3). ' Four stations were sampled for Area B. The entire core from each Area B stations was evaluated for aquatic disposal. Cores ranged from 15 to 21 ft in length, extending from the beach face (between +1 ft. MLLW and +6 11. MLLW) to project depth. The estimated volume of proposed dredged material from Area B is 13,869 cy with 2,849 cy of overdredge. Seven stations were sampled for Area C. Cores ranged from 5 to 14 ft in length, extending from the sediment surface (between -1 ft. MLLW and — 10 ft. MLLW) to project depth. The estimated volume of proposed dredged material from Area C is 13,713 cy with 4,571 cy of overdredge. As noted above, each of the cores was divided into an upper and lower section, For Areas A and B, that division was based on the transition from hydraulic fill material to historic Bay deposits. That layer generally occurred between 10 to 12 ft. below ground surface. For Area C, cores were based on apparent grain size with the upper composite representing the more recently deposited fine sediments and the lower composite representing coarser ancient Bay deposits. Each of the upper cores within an area was combined into an upper composite and each of the lower cores within an area will be combined into a lower Area composite. A more complete description of each core is provided in Section 3.1. A sample of the "z-layer" was collected for each. core. Z-layer samples include sediment from the 6" segment immediately underlying the proposed dredged material and are intended to represent the exposed sediment face once the dredging is completed. For this project, the Z-layer is comprised of material from -14 ft. MLLW to -14.5 ft. MLLW. Z-layer samples from each of the Area A and Area B cores were combined into one composite sample. Where possible, z-layer samples were collected from each core collected in Area C. Z-layer samples were archived for possible future analysis and were not analyzed with the project samples. , Sediment was also collected from the LA-3 Reference site. The reference sediment provides a point of comparison for material proposed for disposal at the LA-3 ocean disposal site. The coordinates for the LA-3 Reference collection site were as follows: Latitude: 31" 31.70" N Longitude: 117 ° 51.30" W i NEWFIELDS 6 June 2009 Dredged Material Evaluation Manna Park I I I I I I I I I I i Figure 3. Area and Station Locations. Proposed locations denoted by green, blue and orange symbols. Actual locations denoted by red symbols. NEWFIELDS 7 June 2009 Dredged Material Evaluation Marina Park IqRp I 07 P. P P, a 1 .I ! P-6a MP-6b r • M 5- i MP-11 �lE I � � MP-3 L 4 limb vm SCHEMATIC PLAN C..h a Az$OCW.. MARINA PARK �... Figure 4. Project Areas and Station Locations with Proposed Project Plan and Current Bathymetry NEWFIELDS e m mr June 2009 Table 2-1. Estimated Volumes for Project Areas Dredged Material Evaluation Marina Park Area Composite Approximate Volume cubicyards) Overdepth (2 ft) Cubic Yards Area A 21,328 2,370 Area B 13,869 2,849 Area C 13,713 4,571 Total 48,910 9,790 Grand Total 58,700 NEWFIELDS 9 Dredged Material Evaluation June 2009 Marina Park 2.2 OVERVIEW OF ANALYSES Upper and lower composite samples from Areas A and B were analyzed for sediment grain size, total organic carbon, sediment conventionals, and sediment chemistry. The upper and lower composite samples from Area C were analyzed for sediment chemistry, as well as biological testing for toxicity and bioaccumulation. In addition, subsamples from the upper and lower segment of each individual core within Area C were analyzed for sediment grain size and mercury. Z-layer samples were archived for possible future analysis depending upon the dredged material evaluation. Sediment grain size is critical to beach nourishment suitability determinations. Each composite and the reference sediment were processed for sediment conventionals (total solids, sediment grain size and total organic carbon), aesthetics (oil and grease, total recoverable petroleum hydrocarbons (TRPH) sulfides, and ammonia), and for plasticity (Atterberg test). Chemical analysis was performed on each of the six test composites, as well as the LA-3 reference sediment. Chemical analysis of the test and reference material for each study unit included metals, , organotins, chlorinated pesticides, PCBs, PAHs, and phthalates. Upper and lower portions of each individual core from the Area C composites were analyzed for sediment grain size and mercury. All analyses were performed following USEPA and USACE guidelines for beach nourishment and for ocean ' disposal (USEPA/USACE 1991, 1998). Subsamples of sediment from each station were also frozen for archive in case future chemical analysis is required on individual stations. The two marine composites (C-upper and C-lower) were evaluated for potential. biological effects related to the dredging and placement of the proposed dredged material at LA-3. Solid -phase tests provided an estimate of toxicity to benthic organisms at the disposal site. Benthic tests included 10-day acute tests with the amphipod, Anipelisca abdila and the polychaete, Neanthes arenaceodentata. Water -column 1 tests were conducted with the suspended -particulate phase (SPP) to provide an estimate of toxicity to water column organisms exposed to sediment as it falls through the water column at the disposal site. It also provided an indication of water -column toxicity that might be encountered during the dredging process. SPP is the liquid portion of a 1:4 sediment/seawater slurry that is designed to simulate the dredging process. Water -column tests were conducted with a dilution series of 10%, 50%, and 100% SPP for each of the test composites. A 1% dilution was also tested during de larval exposures. Reference sediments are not included in the SPP test. SPP tests were conducted with the fish, Manidia beryllina, the mysid, A. bahia, and larval mussels (Mytilus sp.). Bioaccumulation potential testing was performed on materials proposed for open ocean disposal. The bioaccumulation potential test was performed with a clam, Maconia nasuta, and a polychaete worm, Nephtys caecoides. The chemistry analyte list for these tissues was determined by sediment chemistry results. i i 1 MwFIELDS 10 I June 2009 Dredged Material Evaluation Manna Park I t r 1 1 1 1 1 I 2.3 FIELD COLLECTION PROGRAM FOR SOIUSEDIMENT CORE SAMPLES The sampling design designated 15 stations for the collection of soil or sediment core samples within the three proposed study units. Marine sediment cores were collected with a vibracorcr; upland soil/sediment coring was conducted by Gregg Drilling using continuous direct push coring. All core samples targeted a project depth of -12 fit MLLW (+2 ft overdredge). 2.3.1 SAMPLING LOCATIONS AND DEPTHS Each station was given a unique identification code (MP-1 through 16). For the purposes of sample identification, stations were numbered sequentially. All study unit composites were denoted with the identifier "Comp" combined with the abbreviation for that study unit and a U or L denoting upper and lower composites. Composite titles were as follows: Table 2-2. Sample Designations for Chemical and Biological Analysis Study Unit Sample Desi nation Upper Composite Lower Composite Upland Comp A-U Comp A-L Upland Beach Comp B-U Comp B-L Marine Aquatic Comp C-U Comp C-L The area and station identification numbers, approximate depths, and proposed compositing strategy are provided in Table 2-3. Table 2-3. Station Designations within Each Area, Marina Park 2008 Area A Stations Elevation / Water Depth ft. MLL Elevation / Area B Water Depth Stations ft. MLL Area C Stations Elevation / Water Depth ft. MLL MP-1 +9-10 MP-6a +7-8 MP-10 -4 MP-2 +9-10 MP-6b +7-8 MP-11 -9 MP-3 +9-10 MP-7 +3 MP-12 -5 MP-4 +9-10 MP-8 +3 MP-13 -8 MP-5 +9-10 MP-9 +3 MP-14 -7 MP-15 -8 MP-16 -5 NEwFiEt Ds 11 1 Dredged Matenal Evaluation June 2009 Manna Park 2.4 SEDIMENT SAMPLING Samples collected above 0 ft. MLLW were obtained by Gregg Drilling & Testing, Inc using a direct push coring technique. Marine sediment below 0 ft. MLLW was collected by NewFields and Weston staff using a vibracore sampler to obtain samples to project depth. In addition to the project sediment, a reference sediment sample was collected from the USACE-USEPA approved reference sediment sampling location for LA-3. Reference sediment was collected using a stainless -steel dredge bucket. Control sediment was provided with the bioassay test organisms where appropriate (i.e., SPP tests do not use a control sediment). A sample of site water (approximately 100 L) was also collected from the Marina Park area for use in the 100% SPP concentrations for the SPP tests. 2.4.1 CORE COLLECTION Upland cores were collected using a Warthog M1.5T track mounted drill rig in direct push mode (Figure 5). Cores were collected to project depth (+2 ft overdredge and 6" z-layer). Separate acetate liners were used for each core sample. Samples were collected in 4 ft. sections and the cut into 2 ft. sections and placed into a cooler. Samples were processed in the laboratory. Marine sediment cores were collected using a 4—inch diameter vibracore deployed from a 25 ft. barge that allowed for sample collection in shallow nearshore waters. The vibracore is an aluminum tube attached to a vibrating head. A liner is inserted into the core barrel in order to keep the sample from coming in contact with the aluminum barrel. Once aboard the vessel, the core liner was removed from the corer and the core was characterized for length and geotechnical characteristics. Figure 5. Direct -push CPT (a,b) and Vibracore (c, d) samplers, Marina Park 2008 NEwFIELDS 12 Dredged Material Evaluation June 2009 Marina Park ' 2.4.2 NAVIGATION Locations were determined using a combination of Global Positioning System (dGPS) and triangulation using visual landmarks and water depth. Actual sampling locations were recorded in the field logs. 2.4.3 CORE HANDLING 1 A representative core from each sample location was photographed and characterized for sediment characteristics. The core stratigraphy and other pertinent data and observations were logged. Each core was split into separate upper and.lower samples for analysis based on sediment composition as described previously. The geologic description of each core included the apparent grain size, odor, color, length, ' and any evident stratification of the sediment. Sediment from each station was placed into clean, food -grade —quality plastic bags, labeled (project ' name, date, sampler ID, analysis, and preservative where applicable), logged into a field chain -of - custody (COC) form, and placed into a cooler. Cores remained on ice and in the dark until shipped via overnight delivery service to the NewFields' laboratory in Port Gamble, Washington for processing. 2.4.4 SAMPLE PROCESSING AND STORAGE Sample processing and composting was performed at NewFields' Port Gamble laboratory. Station ' samples were stored in the dark at 4 degrees Celsius (°C) until processed. Each station sample was homogenized to a uniform consistency at the laboratory using stainless steel spoons. Composites were generated by homogenizing all station samples from a given area as described in Section 2.1. Samples ' for physical and chemical analysis were placed into certified clean glass jars with Teflon -lined lids and shipped to the analytical laboratories. Sub -samples for archive were placed in certified clean glass jars with Teflon -lined lids and frozen at -20°C for possible future chemical analysis in the event that further ' delineation of chemical contamination is required. The remainder of the composite sample was analyzed for toxicity or, in the case of Composites A and B, stored at 4°C in case biological testing is determined to be needed. ' 2.4.5 SHIPPING Prior to shipping, sample containers were placed in sealable plastic bags and securely packed inside ' coolers with ice packs or crushed ice. COC forms were filled out, and the original signed COC forms was placed in a sealable plastic bag and placed inside the cooler. The cooler lids were securely taped shut. Samples were delivered to the analytical laboratories. Table 2-4 lists the laboratories, the particular analyses performed by each, and the point of contact and pertinent shipping information for each ' laboratory. T_u_ n I n-...6A:...,� I �L...r ft Aac Pnintc of Contart. and Shinning Information 1 1 I CUIC 4' . MJ 101Y L14P1 1_4L/vl Laboratory uwuvvl �•••-� Analyses Performed �- o - Point of Contact Shipping1tiformation NewFields Northwest LLC. SPP, SP testing and Mr. William Gardiner NewFields Northwest Bioaccumulation testing Mr. Brian Hester 4729 NE View Drive 360 297-6040 Port Gamble, WA 98364 Analytical Resources Inc Sediment and Ms. Sue Dunnihoo Analytical Resources bioaccumulation tissue (206) 695-6200 4611 S.134°i Pl, Suite 100 chemistry Tukwila, WA 98168 NEWFIELDS 1 d Dredged Material Evaluation Marina Park All coring equipment was cleaned prior to sampling. Between marine stations, core barrels and the deck of the vessel was rinsed with site water. Core tubes were cleaned between cores using biodegradable soap, a site water rinse and a deionized water rinse. Before creating each composite, all stainless steel Utensils (stainless steel bowls, spoons, spatulas, mixers, and other utensils) were cleaned with soapy water, rinsed with tap water, and,then rinsed three times with deionized water. Samples were evaluated in accordance with procedures outlined in the OTM (USEPA/USACE 1991) to establish suitability for ocean disposal and the more recent procedures described in the Inland Testing Manual (ITM; USEPA and USACE 1998) and by the ASTM (2003a). This program included bioassay analysis of three project samples: two Area C composite samples and the LA-3 Reference sediment. In addition, appropriate laboratory control samples were run with each of the selected test species. Bioassdy testing for this project consisted of two benthic toxicity tests, three water -column toxicity tests, and two bioaccumulation potential tests. The bioassays performed for this project are summarized in Table 2-5. Bioassay testing of materials began as soon as possible after the time of collection. Control Type of Project Sediment/ Reference) Rcrerence' Test T a Organism Taxon Sediments Seawater Sediment Toxicant Bivalve larvae Mylllus edulis X2 X X Water column Fish Menidia beryllina X2 X X Mysid shrimp Anrerlcamysis babla X2 X X mphipod Ampelisca abdira X X X X Henthic Polychactc N. aenaceodentara X X X X Bivalve Maconta nasula X X X Bioaccumulation polychaete Nepbrys caecoides X X X Shaded areas indicate tests or treatments that are not applicable to the selected tests. 2 Sediment elutriates of project material Benthic bioassays were performed to estimate the potential impact of ocean disposal of dredged material on benthic organisms that attempt to re -colonize the area. Dredge material was tested in 10-day benthic tests using two species: an amphipod species Arnjoelisca abdita and a polycbaete, Neanthes arenaceodentala. Amphipod tests were conducted in accordance with procedures described in Appendix E of the ITM (USEPA/USACE 1998) and ASTM Standard E1367-99 (ASTM 2003c). Tests with the polycbaete were conducted in accordance with procedures outlined in the ITM (USEPA/USACE 1998). Each sediment type (test, references, and control) was run with five replicates. Control sediment was sediment from the area where the organisms were collected (i.e., native sediment). Since N. arenaceodentata are cultured in the absence of sediment, clean sand from Newport, Oregon was used as control sediment for the 10-day polychaete test. This sediment has been used successfully in previous tests with Neandtes. Test organists were exposed to the sediment for ten days in 1-liter glass test chambers. Two centimeters of sediment (approximately 150 mL) was placed into each chamber with 800 mL of overlying water, Tests were conducted as static tests with no feeding. Initial stocking densities in each replicate were 20 organisms per test chamber for the amphipod test, and 5 organisms per test chamber for the polychaete ' Dredged Material Evaluation June 2009 Marina Park test. Trickle -flow aeration was provided through glass pipettes, in such a way as to avoid disturbing the sediment surface. Water quality measurements were taken in one chamber from each test treatment daily ' and included pH, salinity, temperature, and dissolved oxygen. Ammonia was measured in both interstitial (pore water) and overlying water at the start and finish of the test from one replicate for each test sample. Sediment pore water was extracted via centrifugation. All instruments used were calibrated ' and logged daily. Using methods described in the OTM (USEPA/USACE 1991) the sediments were carefully sieved to remove the test organisms and then survivorship was assessed. To evaluate the relative sensitivity of the organisms, reference toxicity tests were performed using standard reference toxicants (Lee 1980). 2.5.2 WATER -COLUMN TESTS ' Water column bioassay tests were performed to estimate the potential impact of ocean disposal of dredged material to organisms that live in the water column. The water -column test was performed using a 4:1 seawater to test dredged material suspended -particulate phase preparation (SPP). To make the ' SPP, dredged material from each composite was combined with dredging -area site seawater in a 4:1 ratio by volume, vigorously agitated for 30 minutes, and then centrifuged for approximately 10 min. at room temperature (16-18°C). Following centrifugation, the supernatant was gently decanted. This supernatant ' represented the 100% SPP test concentration and was used to create serial dilutions with clean seawater (0.45-gin-filtered Hood Canal seawater) to create subsequent test concentrations for the SPP tests. Three species were tested with the SPP: Menidia beryllina (inland silverside fish), Americamysis (formerly ' Mysidopsis) bahia (mysid shrimp), and Mytilus sp. (bivalve larvae). For the shrimp and the fish, the SPP was tested at 100%, 50%, and 10% percent concentrations against a seawater control under static conditions. Each of these tests was conducted in accordance with ' procedures outlined in the ITM (USEPA/USACE 1998). Ten animals were used per replicate with five replicates per elutriate concentration. The test ran for 96 hours. ' The bivalve larvae test was run on the test dredged material elutriates at 100%, 50%, 10%, and 1% dilutions, and a seawater control. The test was run for 48 hours, until development of the bivalve larvae to the D-binge stage in the control. At the termination of the study, survival and normal development were compared between the control and test groups to determine if significant mortality or abnormal development existed. 1 Daily water quality monitoring of test chambers was carried out for pH, dissolved oxygen, salinity, and temperature. Ammonia was analyzed at the start of the test in the 100% concentration. Measurements in other concentrations were not performed as the readings in the 100% concentration were not greater than 4 mg/L total ammonia. To evaluate the relative sensitivity of the organisms, reference toxicity tests were performed using standard reference toxicants (Lee 1980). 2.5.3 BIOACCUMULATION POTENTIAL TESTS Assessment of bioaccumulation potential was carried out using the polychaete worm N. caecoides and the bivalve M. nasuta over a 28-day test period on the marine composite samples and the LA-3 Reference sediment only. Bioaccumulation potential tests were conducted in accordance with those procedures outlined in Guidance Manual: Bedded Sediment Bioaccumulation Tests (USEPA 1993) and Appendix E of the ITM (USEPA/USACE 1998). Each of these tests was initiated using test and control sediment in the same manner as the 10-day benthic test. N. caecoides exposures were conducted using 60 animals in each of five replicate test chambers. For M. nasuta exposures, 25 animals were placed in each of five replicate test chambers. The test chambers were maintained under flow -through conditions, and daily water quality measurements were taken on each chamber. On Day 28, the sediment was sieved to remove the worms and clams. The surviving animals were placed in clean flow -through aquaria to 1VEWFIELDS 15 Dredged Material Evaluation June 2009 Marina Park purge their gut contents for 24 hours, and then tissues were placed into certified -clean glass sample jars, frozen and then sent to the chemistry laboratory for tissue analysis The analysis of bioaccumulation was made by statistically comparing tissue levels from the reference group to those of the test group for each species. The analysis will be conducted using Analysis of Variance, T-test, or non -parametric tests, depending on the assumptions of the individual tests (i.e., homogeneity of variance) as specified in the OTM (USEPA/USACE 1991). Contaminant concentrations found to be significantly elevated above reference were interpreted by comparing to FDA limits and USEPA risk -based guidance values. 2.5.4 SEAWATER FOR BIOASSAY TESTING Seawater used in -this study, including the flow -through tests, came from the Hood Canal at Port Gamble, Washington, Hood Canal, seawater is continuously pumped through the NewFields facility. Seawater is filtered using a 25 µm sand filter, with subsequent polishing with a 0.45-µm filter for the toxicity tests. This seawater source has been used successfully on similar bioassay testing programs. Extensive testing on a variety of test species has shown that there is no significant potential for toxicity or bioaccumulation from this source, 2.6 QUALITY ASSURANCEIQUALITY CONTROL The quality assurance objectives for toxicity testing are detailed in the OTM (USEPA/USACE 1991), ITM (USEPAIUSACE 1998), and NewFields' laboratory quality assurance plans (QAPs). These objectives for accuracy and precision involve all aspects of the testing process, including the following: • Water and sediment sampling and handling • Source and condition of test organisms • Condition of equipment, test conditions • Instrument calibration • Use of reference toxicants • Record keeping & data evaluation Each test organism was evaluated in reference toxicant tests during the test period to establish the sensitivity of the test organisms. The reference toxicant LC50 or ECSO should fall within two standard deviations of the historical laboratory mean. Water quality measurements were monitored to ensure that they fall within target limits. All limits established for this program meet or exceed those recommended by USEPA. The methods employed in every phase of the toxicity testing program are detailed in NewFields' Standard Operating Practices (SOP). All NewFields staff members receive regular, documented training in all SOPS and test methods. Finally, all data collected and produced as a result of these analyses were recorded on approved data sheets, which are part of the permanent data record of the program. If any aspect of a test deviated from protocol, the test was evaluated to determine whether it was valid according to the regulatory agencies responsible for approval of the proposed permitting action. H I 1 C I L NEWFIELDS 16 ' Dredged Material Evaluation June 2009 Manna Park 2.7 PHYSICAL AND CHEMICAL ANALYSIS ' Physical and chemical parameters measured in this testing program were selected to provide data on potential chemicals of concern in the dredged material from the Marina Park site, in accordance with the OTM (USEPA/USACE 1991), ITM (USEPA/USACE 1998), and regional guidance. Test composites and reference sediment were analyzed for all of the analytes listed in Table 2-6. The target detection ' limits (sediment — dry weight) are also presented in Table 2-6. All analytical methods used to obtain contaminant concentrations follow EPA or Standard Methods (SM; APHA/AWWA 1998). 1 1 `_J 1 1 2.7.1 PHYSICAL ANALYSES To characterize the physical properties of the sediment, tests were performed to determine the physical characteristics of the sediment for potential beach nourishment, to predict the behavior of sediment after disposal, and to compare reference and test sediment. Physical -chemical analyses of the sediment included grain size, specific gravity, total organic carbon (TOC), total solids, and plasticity (Atterberg Limits). Grain size was analyzed to determine the general size classes that make up the sediment (e.g., gravel, sand, silt, and clay) and the frequency distribution of the size ranges (reported in millimeters [nun]). Grain size measurements were conducted using the gravimetric procedure described in Plumb (1981). The TOC, made up of volatile and nonvolatile organic compounds, was determined as recommended in the OTM (USEPA/USACE 1991) or equivalent (modified SW846). This procedure involves dissolving inorganic carbon (carbonates and bicarbonates) with hydrochloric acid or sulfuric acid prior to TOC analysis (Plumb 1981). Total solids were also measured to convert concentrations of the chemical parameters from a wet -weight to a dry -weight basis. Percent solids was determined by USEPA Method 160.3 (USEPA 2001). Total petroleum hydrocarbons and total residual petroleum hydrocarbons (TRPH) were analyzed using EPA Method 1664. Atterberg limits were determined using ASTM D-4318. 2.7.2 SEDIMENT CHEMISTRY The following analyses were performed as recommended by the ITM/OTM (USEPA/USACE 1998; 1991). The analysis for priority pollutant metals was conducted using an inductively coupled plasma emissions spectrometer equipped with a mass detector (ICP-MS), in accordance with USEPA 6010. Mercury analysis was conducted using cold vapor atomic absorption (CVAA) using EPA 7471A (USEPA 1994). The ammonia and dissolved sulfides analysis were conducted in conjunction with toxicity testing and followed SM4500-NH3F and N (APHA/AW WA 1998). Total sulfides were analyzed following PSEP (1986). Semivolatile organics (SVOC; PAHs only) were analyzed using gas chromatography -mass spectrometry with selected ion monitoring (GC/MS SIM), using USEPA Method 8270 SIM (USEPA 2001). This followed serial extraction with methylene chloride and alumina cleanup procedures. Organochlorine pesticides and PCBs were analyzed using dual column GC/ECD following USEPA Method 8081 and 8082 respectively (USEPA 2001), with extraction modifications to reach lower detection limits. The PCBs were identified to the Aroclor level. The analytical method used to determine TBT involves methylene chloride extraction, followed by Grignard derivatization and analyzed by GC/MS (Krone et al., 1989). NEWFIELDS 17 I June 2009 Dredged Material Evaluation Marina Park Table 2-6. Chemical and Physical Parameters, Analytical Methods, and Target Detection ' Limits Parameter Method Procedure SedimentTarget Reporting Limit d wei ht(wet Tissue Target Reporting Limit wei ht Physical / Conventional Tests Grain Size Plumb 1981 Sieve/Pipette 1.0% n/a Atterberg Limits ASTM D-4318 n/a TOC ASTM D2579 Combustion IR 0.1% n/a Percent Solids EPA 160.3 Grvimetrc 0.1% n/a Sulfides PSEP 1986 Coiorimetric 1.0 rir n/a Oil and Grease EPA 1664*- Gmvimetric n/a TRPH EPA 1664' Gmvimetric n1a Ammonia SM 4500N H317 ICP-MS 0.001 m k n/a Lipids Bli h Dyer Gmvimetric nla 0.1 0 Metals Arsenic As USEPA 6010 ICP-MS 0.5 mg/kgmg/kg n/a Cadmium Cd USEPA 6010 ICP-MS 0.2 m n/a Chromium Cr USEPA 6010 ICP-MS 0.5 mgIkg n/a Copper Cu USEPA 6010 ICP-MS 0.5 m n/a Lead(Pb)USEPA 6010 ICP-MS 1.0 mg/kgmg/kg n/a Mercury H USEPA7471A CVAA 0.05m 0.01 mg/kg Nickel(Ni)USEPA 6010 ICP-MS 0.5 mglkg We Selenium Se USEPA 6010 ICP-MS 0.5 m n/a Silver A USEPA 6010 ICP-MS 0.5 m n/a Zinc Zn USEPA 6010 I ICP-MS 4 mgIkg We Pesticides 4.4' DDD USEPA 8081 GC/ECD 2 VgIkg on 4-4'-DDE USEPA 8081 GC/ECD 2 n/a 44'-DDT USEPA 8081 GCBCD 2 pgtkg n/a 2-4' DDD USEPA 8081 GC/ECD 2 P&S n/a 24'-DDE USEPA 8081 GC/ECD 2 µ n/a 24'-DDT USEPA 8081 GCBCD 2 n/a Aldrin USEPA 8081 GCBCD 1 pgtkg n/a a-BHC USEPA 8081 GCBCD l pglkg n/a BHC USEPA 8081 GC/ECD l pgtkg n/a Chlordane USEPA 8081 GCBCD 2 upJkR n/a 8-BHC USEPA 8081 GC/ECD 1 Agtkg n/a Dieldrin USEPA 8081 GC/ECD 2 pgtkg n/a Endosulfan I USEPA 8081 GC/ECD 1 jiglkg n/a Endosulfan 11 USEPA 8081 GCBCD 2 n/a Endosulfan Sulfate USEPA 8081 CC/ECD 1 pglkg n/a Endrin USEPA 8081 GC/ECD 1 n/a Endrin Aldehyde USEPA 8081 GCBCD 1 n/a Heptachlor USEPA 8081 GCBCD I pgtkg do Heptachlor Eoxide USEPA 8081 GCBCD I 11wkg nta -BHC USEPA 8081 GC/ECD t n/a Methox chlor USEPA 8081 GC/ECD 10 pglkg n/a Lindane USEPA 8081 GC/ECD 1 We Toxa hone USEPA 8081 GC/ECD 100 pgtkg n/a PCBs Aroclor 1016 USEPA 8082 GCBCD 4 pgtkg n/a Aroclor 1221 USEPA 8082 GCBCD 4 pg/kg n/a Aroclor 1232 USEPA 8082 GC/ECD 4 pgtkg n/a Aroclor 1242 USEPA 8082 GC/ECD 4-pglkg n/a Aroclor 1248 USEPA 8082 GC/ECD 4 n/a Aroclor 1254 USEPA 8082 GCBCD 4 pg/kg nta Aroclor 1260 USEPA 8082 GCBCD 4 n/a L LI L7 L� �I L' L NEWFIELDS 18 ' Dredged Material Evaluation June 2009 Marina Park C' I Parameter 'Method Procedure Sediment Target Reporting Limit . dr -wei' ht Tissue Target Reporting Limit wetwei hl SemNolatile Or anics Acena hthene USEPA 8270 GC/MS SIM 7 k n/a Flumene USEPA 8270 GC/MS SIM 7 n/a Phenanthrene USEPA 8270 GC/MS SIM 7 k n/a Anthracene USEPA 8270 GC/MS SIM 7 pg1kg n/a Fluoranthene USEPA 8270 GC/MS SIM 7 /k n/a P rene USEPA 8270 GC/MS SIM 7 k n/a Chrysene USEPA 8270 GC/MS SIM 7 gglkg n/a Benzo a antltracene Benzo b fluoranthene Benzo a rene USEPA 8270 USEPA 8270 I USEPA 8270 GC/MS SIM GC/MS SIM GC/MS SIM 7 k 7 pgtkg 7 ggtkg n/a n/a n/a indeno 1 2,3-cd rene Dibenzo a,h anthracene I3enzo(g,hJ)perylenc USEPA 8270 USEPA 8270 USEPA 8270 GC/MS SIM GC/MS SIM GC/MS SIM 7 7 /k 7 pgtkg n/a n/a n/a Phthalates Dieth I hthalate Dimeth I hthalate Butylbenzylphthalate bis 2-Eth Ihex Iphthalate Di-n-octylpbthalate USEPA 8270 USEPA 8270 USEPA 8270 USEPA 8270 USEPA 8270 GC/MS GC/MS GC/MS GC/MS GC/MS 20 pgtkg 20 ggtkg 20 pglkg 20 pg/kg 20 pgtkg n/a n/a n/a n/a n/a Or anotins Monobutyltin Krone et al. 1989 GC/MS SIM 1 10 ggtkg n/a Dibu Itin Krone et al. 1989 GC/MS SIM 10 n/a Tributyltin Krone et al. (1989) J GC/MS SiM 1 10 k n/a %: percent ng/kg: nanogram per kilogram µg/kg: microgram per kilogram g/cc: gram per cubic centimeter n/a: not applicable GC/MS: gas chromatography/mass spectrometry SIM: selected ion monitoring * EPA Method 1664 is substituted for EPA 413.2 2.7.3 BIOACCUMULATION TISSUE CHEMISTRY Tissue analysis was performed to determine the availability of sediment contaminants taken up by the test organisms. The chemical constituents for tissue analysis (including pre -exposure samples) were determined following a review of the sediment chemistry results, in consultation with USACE and USEPA. Based on sediment chemistry results, mercury and lipids were analyzed in test tissues. Tissue composites from each replicate were analyzed separately. 2.7.4 QUALITYASSURANCEIQUALITY CONTROL The QA objectives for chemical analysis conducted by the participating analytical laboratories are detailed in their Laboratory QA Manual(s), These objectives for accuracy and precision involve all aspects of the testing process, including the following: • Methods and SOPS • Calibration methods and frequency • Data analysis, validation, and reporting • Internal QC • Preventive maintenance I • Procedures to ensure data accuracy and completeness NEwRELDS 19 Dredged Material Evaluation June 2009 Manna Park Results of all laboratory QC analyses are reported with the final data. Any QC samples that failed to meet the specified QC criteria in the methodology or QAP were identified, and the corresponding data was appropriately qualified in the final report. All QA/QC records for the various testing programs will be kept on file for review by regulatory agency personnel. 2.8 DATA REVIEW, MANAGEMENT, AND ANALYSIS 2.8.1 DATA REVIEW All data were reviewed and verified by participating team laboratories to determine whether all data quality objectives had been met, and that appropriate corrective actions bad been taken, when necessary. NewFields' QA Officer or her delegate was responsible for the final review of all data generated. 2.8.2 DATA ANALYSIS Data analysis consisted of tabulation and comparison with reference sites. Sandy sediments were also evaluated for suitability for use in beach nourishment under Regional General Permit 67 or under an individual permit. Marine sediments that did not qualify for beach nourishment, either due to grain size or the presence of contaminants were reviewed for open ocean disposal at LA-3. Biological results were compared to appropriate laboratory controls and reference results where applicable as designated in the OTM (USEPA/USACE 1991). Additional interpretation criteria are discussed in Section 4. 1 11 u I d NEWFIELDS 20 ' Dredged Material Evaluation June 2009 Marina Park 3 RESULTS 3.1 SAMPLING RESULTS Sediment cores were collected from a total of 15 stations. Five stations were located in Area A, four stations were sampled in Area B, and six stations were sampled in Area C. With the exception of MP-9, samples were collected from each of the proposed stations. Station MP-3 was moved south from the proposed location due to a lack of access. Station MP-9 was replaced with Station MP-6b to provide a better indication of sediment in the upper beach area. In Area C, an additional station was sampled, Station MP-16, to provide a better indication of the deeper sediment in the nearshore portion of that area. Information on sample location, depth (MLLW), targeted core length; penetration depth and length of core recovered are included in Table 3.1. Reference samples were collected from LA-3 Reference on December 1, 2008. Field logs are presented in Appendix A. The approximate location of each sediment core is provided in Figure 1.2. Samples from Areas A and B were collected using a direct -push CPT on November 26, 2008. Sediment was collected to the proposed sampling depth (14.5 fl. MLLW) for each of the Area A and B stations. In some cases, a void appeared in the core, generally one foot in length. This was caused by compaction of loose sands by the head of the CPT. Subtidal samples in Area C were collected using a vibracorer on December 12, 2008. Penetration depths at each station were sufficient to reach the ancient Bay sand layer; however, refusal was observed at this layer for nearshore stations MP-10, MP-12, and MP-14. An additional station, Station MP-16, was sampled to determine the precise location of the ancient Bay sand layer and to retrieve sufficient material to characterize this layer for the nearshore portion of Area C. With the exception of Station MP-14, project depth (42 ft. MLLW) was sampled for all stations within Area C. Stations located further offshore, Stations MP-11, MP-13, and MP-15, were sampled to the project depth plus the 2 ft. overdredge and the z-layer sample. Z-layer samples were archived for possible future analysis. Sediment cores in Area A were generally characterized by sand overlying coarse sand (Figure 3.1). The boundary layer between the finer, more recent sands and the ancient -Bay sands was at approximately -4 to -5 ft. MLLW. Area B included lighter beach sands overlying the upper layer, gray sands, overlaying the coarser deep sands. As with Area A, the boundary between the finer sands and coarser sands occurred between -4 to -5 ft. MLLW, with the exception of Station MP-7, with the boundary was observed at -7 to -8 ft MLLW. Sediment in the nearshore portion of Area C differed from that of the channel stations further offshore. In the nearshore area, sands similar to the surface sands in Area B were found overlaying a moderately compacted silticlay layer, overlaying the ancient Bay sand. A similar sediment composition was observed at the western portion of the channel stations, Station MP- 11. The sediments observed at Stations MP-13 and MP-15 were generally characterized by silts and clays overlaying the ancient Bay sands. Each of the cores was split into an upper and lower section at the boundary with the ancient Bay sands. The upper sections within each area were composited to create an upper Area composite and the lower sections within each area were composited to create a lower Area composite. In addition, the upper and lower sections from each core were either archived for possible future analysis (Areas A and B) or submitted for mercury and grain size analysis (Area C). NEWFIELDS 21 June 2009 Table 3-1. Sample Log Data, Marina Park 2008 Dredged Material Evaluation Marina Park Coordinates Target Actual Core Core Core Latitude Longitude Depth Length Length Site Type (°N) (°W) (ft MLLW) ft(ft)___Comments Area A MP-1 CPT 33° 36.474 117°55.325 +9 to 10 20 20 Upper 4 5 feet MP-2 CPT 33° 36.479 117° 55.338 + 9 to 10 20 20 o above core not Included in analysts; top of 20 ft. core is at +4 to 5 ft MLLW MP-3 CPT 33° 36.469 117° 55.312 + 9 to 10 20 20 MP-4 CPT 33° 36.492 117° 55.310 + 9 to 10 20 20 MP-5 CPT 33° 36.494 117° 55.326 + 9 to 10 20 20 Area t3 MP-6a CPT 33° 36.498 117° 55.325 + 6 20 20 MP-6b CPT 33° 36.495 117° 55.313 + 6 20 20 Surface sediment from beach MP-7 CPT 33° 36.507 117055,312 + 3 to 4 18 18 included in core. MP-8 CPT 330 36.510 117° 55.336 + 3 to 4 18 18 Refusal at 3; MP-9 VC 33° 36.515 117° 55.361 + 1 16 3.0 3 attempts; unable to sample with VC Area C Refusal at -12.0; MP-10 VC 33° 36.525 117° 55.363 - 4.1 10.4 8.0 0.5 ft. sand lost from cutter head MP-11 VC 33° 36.527 117055.362 - 7.5 7.0 7.0 Refusal at -12.0; MP-12 VC 33° 36.519 117° 55.332 -5.0 9.5 7.0 approximately 1.0 ft. of sand lost from cutter head MP=13 VC 33° 36.532 117° 55.335 .8.5 6.5 6.5 Refusal at -11.5; MP-14 VC 33° 36.525 117° 55.308 -5.5 9.0 6.0 0.5 ft. sand lost from cutter head MP-15 VC 33° 36.539 117055.305 -6.5 7.9 7.9 MP-16 I VC 33° 36.521 1 117° 55.327 1 -5.1 9.5 8.5 Refusal at -13.5' NEWFIELDS 22 Dredged Material Evaluation June 2009 Madna Park Depth Area A Area Area C - 2 3 -4 5 6a I 6b 7' 8 10 12 114116 1 11 1 13 1 15 10 — — — 10 9 — — — — 9 8 8 — — — — — — — — 7 — — — — — — — — —7 6 T T 6 4 4 3 3 2 2 0 0 - -2 2 . ...... . . . . . .3 .3 4 T -4 555ig W6; 6 -5 :,1, M T 115R 55 6 -6 ?4n -6 RU -7 .7 -8 -8 T T :�O im .61 -9 -9 *55 R. -10 —olo 61. -181 ••12 .12 6'... .13i�i•-13 -14 -14 Q -15 -15 NS: no sample Sand Wet Silt/Clay Silty Sand Coarse Sand Figure 6. General Characterization of Sediment in Cores from Marina Park. NEwFIELDS 23 June 2009 3.2 PHYSICAL AND CHEMICAL ANALYSIS OF SEDIMENT Dredged Material Evaluation 1 Marina Park Physical characterizations and conventionals analysis of all composites and the reference sample included grain size determination, total organic carbon (TOC) content, percent total solids, oil and grease, total recoverable petroleum, total ammonia and sulfides, and Atterberg limits. Chemical characterizations included metals, organotins, PAH's, chlorinated pesticides, PCB aroclors, and phthalates. Results of these characterizations are summarized in the following sections. 3.2.1 PHYSICAL CHARACTERISTICS AND CONVENTIONAL CHEMICAL ANALYSIS Physical characteristics of composites and the reference sample are shown in Table 3-2. Area A and B composites, as well as Comp C-L, were >95% sand and gravel, with very little fine sediment. Comp C- U was comprised of approximately 78% sand, with approximately 22% silt and clay. The LA-3 Reference site was predominantly silt with 29.6% clay and only 3.2% sand. TOC content was generally low in the A and B composites, ranging from 0.02% - 0.15% TOC. Comp C- U was somewhat higher with 0.68% TOC content. The reference sample had TOC content of 1.8%. Oil and grease and TRPH were below detection levels in all samples. Total ammonia levels were generally low or undetected (<0.1 to 1.2 mg/kg total ammonia) , with the highest concentration in the test composites being 14.8 mg/kg total ammonia in Comp C-U. The total ammonia concentration in the LA- 3 Reference sediment was 4.8 mg/kg total ammonia. Sulfides were detectable only in Comp A-U and Comp B-L, with 7.56 and 4.25 mg/kg respectively. All composites and the reference were analyzed for plasticity using the Atterberg test. Area A and B composites and Comp C-L displayed no plasticity. The Atterberg limits found for the LA-3 Reference and Comp C-U were 30.3 and 16.9 cm respectively. The plasticity index was 11.2% indicating that materials were not highly plastic and would be unlikely to form hardpan surfaces on beaches. Table 3-2. Summary of ConventionaIs, Marina Park 2008 Analyte LA-3 Composites A-U Comp A-L Comp B-U Comp B-L Comp C-U Comp C-L Comp Gravel (%) 0.0 2.2 9.6 2.3 6.2 0.0 3.7 Sand (%) 3.2 93.6 89.7 93.6 93.0 77.9 95.3 Silt (%) 67.2 2.6 0.7 2.7 1.8 10.5 1.0 Clay (%) 29.6 1.6 <1 U 1.5 <1 U 11.6 0.0 Total Organic Carbon (%) 1.8 0.15 0.08 0.02 0,02 0.68 0.05 Total Solids (%) 43.5 84.6 90.3 89.3 86.6 76.2 87.4 Oil and Grease (mg/kg) <450U <230 U <215 U <218 U <226 U <262 U <221 U TRPH (mg/kg) <450U <230 U <215 U <218 U <226 U <262 U <221 U Total Ammonia (mg/kg) 4.8 1.2 0,11 0.2 <0.10 U 14.5 <0.5 Total Sulfides (mg/kg) NM 7.56 <1.20 U <1.16 U 4.25 NM NM Atterberg Limits (cm) 30.3 Not Plastic Not Plastic Not Plastic Not Plastic 16 9 Not Plastic NM: Not Measured U: Undetected. Actual concentration below reported concentration NEWFIELDS 24 June 2009 3.2.2 METALS Dredged Material Evaluation Marina Park The test composites and the reference sample were analyzed for the presence of ten different metals (Table 3-3). Selenium and silver were not detected in any of the samples. With the exception of mercury, all detected metals concentrations in the test composites were below those of LA-3 Reference. With the exception of mercury in Comp C-U and chromium in Comp C-U and LA-3 Reference, metals concentrations in test samples were well below the effects range- low (ERL). Chromium was found at concentrations of 12.4 and 40 mg/kg, above the ERL (8.1 mg/kg), but well below the effects range - median (ERM, 370 mg/kg). The mercury concentration in Comp C-U was 0.36 mg/kg, which was above the ERL (0.15 mg/kg) but below the ERM (0.71 mg/kg). Upper and lower sections from the individual cores in Area C were analyzed for mercury concentrations (Table 3-3). In the upper cores collected from the nearshore stations (MP-10, 12, 14, and 16), mercury concentrations ranged from 0.10 to 0.85 mg/kg. In sediment collected from the channel stations, the mercury concentrations in the upper sections were 1.11 mg/kg and 3.35 mg/kg for Stations MP-13 and MP-15, respectively. Mercury was not detected in any of the lower sections from either the nearshore stations or channel stations. A subsample from Station MP-11 was compromised during shipment and was not available for mercury analysis. r..�.i., a a iilintala in Qarliman4_ Marina Park 2008 IGNIG V-V. ,V Anal'yte ERL � ERM' LA-3 Composites A-U Comp, A-L CompCompCom B-U B-L C-U Com' C-L Comp Arsenic 8.2 70 '5.5 2.0 2.1 2.2 1.9 3.7 2.1 Cadmium 1.2 9.5 0.9 <0.2 U <0.2 U 0.2 <0.2 U 0.4 <0.2 U Chromium 8.1 370 40 4.0 2.2 3.0 3.2 12.4 2.8 Copper 34 270 22 2.0 1.0 3.7 2.4 18.3 1.2 Lead 46.7 218 13 <2 U <2 U 5 <2 U 9.0 <1 U Mercury 0.15 0.71 0.10 <0.05 U <0.06 U 0.05 <0.05 U 0.36 <0.5 U Nickel 20.9 51.6 24 3 <1 U 2 2 9.2 1.9 Selenium NA NA <1 U <0.2 U <0.2 U <0.2 U <0.2 U <0.6 U <0.6 U Silver 1.0 3.<0.4 U <0.3 U <0.3 U <0.3 U <0.3 U <0.2 U <0.2U Zinc 150E41d 63 10 6 11 6 44 6 Section Hg ERL Hg ERM MiarcurvCondentrations,in Cores m /k MP-10 MP-12 MP-14 MP-16 MP-13 MP-15 Upper Section 0.15 0.71 0.10 0.31 0.85 0.07 1.11 3.35 Lower Section 0.15 0.71 <0.06 U <0.07 U <0.06 U <0.05 U <0.05 U <0.05 U U: Undetected. Actual concentration below reported concentration No data for MP-11; no subsample available for analysis. NEWFIELDS 25 June 2009 3.2.3 ORGANOTINS Dredged Material Evaluation t Manna Park Tributyltin was not detected in any of the test composites (Table3-4). No organotins were observed in Comps C-U or C-L, or in the LA-3 Reference. Monobutyltin and dibutyltin was detected in the area A and B composites. Table 3-4.Organotins in Sediment, Marina Park 2008 Analyte LA-3 Com osites A-U Comp A-L Comp B-U Comp B-L ComP C-U Comp C-L Com Tribut Ilin <3.8 U <3.6 U <3.4 U <3:6 U <3.6 U <3.6 U <3.7 U Dibut Itin <5.6 U 14 15 13 19 <5.3 U <5.6 U Monobut Itin <4.0 U 5.5 4.5 <3.4 U 6.1 <3.8 U <4.0 U U: Undetected: Actual concentration below reported concentration 3.2.4 POLYCYCLIC AROMATIC HYDROCARBONS Each of the test composites and the reference sample were analyzed for the presence of PAHs (Table 3- 5). None of the 16 PAHs were detected in either the upper or lower composites from Area A or Comps B-L or C-L. Concentrations of some PAHs were observed above reporting limits in Comps B-U and C- U. However, these concentrations were -quite low and were below the PAHs concentrations observed in sediment from LA-3 Reference. The total detected PAHs were 32.7 µg/kg and 108.1 µg/kg in Comps B- U and C-U, respectively. Concentrations observed in the test composites were well below the ERL (4,022 µg/kg). Table 3.5. PAHs in Sediment. Marina Park 2008 Analyte LA-3 Composites A-U Com A-L Com B-U Com 8-L Com C-U comp C-L comp. Acena hth lane <4.8 U <4.9 U <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Acena hthene <4.8 U <4.9 U' <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Fluorene <4:8 U <4.9 U <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Phenanthrene <4.8 U <4.9 U <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Anthracene <4.8 U <4.9 U <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Fluoranthene 8.7 <4.9 U <4.7 U <4.8 U <4.9 U 15 <4.5 U P rene 11 <4.9 U <4.7 U <4.8 U <4.9 U 19 44.5 U Benz a anthracene <4.8 U <4.9 U <4.7 U <4.8 U <4.9 U 6.3 <4.5 U Chrysene 5.8 <4.9U <4.7U 5.8 <4.9U 7.8 <4.5U Benzo b fluoranthene 5.3 <4.9 U <4.7 U 4.8 <4.9 U 12 <4.5 U Indeno 1,2,3-c,d rene <4.8 U <4.9 U <4.7 U 7.7 <4.9 U 12 <4.5 U Dibenz a,h anthradene <4.8 U <4.9 U <4.7 U <4.8 U <4.9 U <4.8 U <4.5 U Benzo ,h,i a lene 4.8 <4.9 U <4.7 U 9.6 <4.9 U 20 <4.5 U Benzo a rene 5.3 <4.9 U <4.7 U 4.8 <4.9 U 16 <4.5 U Total Detected PAHs 40.9 0 0 32.7 0 108.1 0 U: Undetected. Actual concentration below reported concentration ERL: 4,022 µg/kg NEWFIELDS 26 June 2009 Dredged Material Evaluation Manna Park 3.2.5 CHLORINATED PESTICIDES Each composite and the reference sample were analyzed for a suite of chlorinated pesticides. The results are summarized in Table 3-6. There were no concentrations found above the reporting limits in any of the test composites. Table 3-6. Chlorinated Pesticides in Sediment, Marina Park 2008 Analyte JLA-3 sites Com osites A-U Com A-L Comp B-U Com : Comp C-U Com C-L Comp 2,4'-DDD <2.0 U <2.0 U <2.0 U <2.0 U <2.0 U <2.0 U <1.9 U 2,4-DDE <2.OU <2.OU <2.OU <2.OU <2.OU <2.OU <1.9U 2,4'-DDT <2.0 U <2.0 U <2.0 U <2.0 U <2,0 U <2.0 U <1.9 U 4,4-DDD <2.OU <2.OU <2.OU <2.OU <2.OU <2.OU <1.9U 4,4'-DDE <2.0 U <2.0 U <2.0 U <2.0 U <2.0 U <2.0 U <1.9 U 4,4'-DDT <2.OU <2.OU <2.OU <2.OU <2.OU <2.OU <1.9U Total Detected DDT: 0 0 0 0 0 0 0 Aldrin <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U BHC-al ha <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U BHC-beta <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U BHC-delta <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98,U <0.94U BHC- amma Lindane <0.98 U <0.97U <0.98U <0.99U <0.98U <0:98U <0.94U Chlordane -alpha <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Chlordane -gamma <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Ox chlordane <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Total Detectable Chlordane 0 0 0 0 0 0 0 Dieldrin <2.0 U <0.97U <0.98U <0.99U <0.98U <2.OU <1.9U Endosulfan Sulfate <2.0 U <0.97U <0.98U <0.99U <0.98U <2.01.1 <1.9U Endosulfan-I <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Endosulfan-II <2.0 U <0.97U <0.98U <0.99U <0.98U <2.OU <1.9U Endrin <2.0 U <0.97U <0.98U <0.99U <0.98U <2.OU <1.9U Endrin Aldehyde <2.0 U <0.97U <0.98U <0.99U <0.98U <2.01-1 <1.91.1 Heptachlor <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Heptachlor Epoxide <0.98 U <0.97U <0.98U <0.99U <0.98U <0.98U <0.94U Methox chlor I <9.8 U <9.7 U <9.8U <9.9U <9.8U <9.8U <9.4U Mirex <0.98 U I <0.97U I <0.98U <0.99U I <0.98U I <0.98U <0.94U Toxa hene <98 U 1 <97 U I <98U I <99U I <98U L <98U 1 <9411 U: Undetected. Actual concentration Detow reporwu cunocuuauu„ NEWFIELDS 27 June 2009 Dredged Material EvalUatlon t Marina Park 3.2.6 PCB AROCOLORS Each composite and the reference sample were analyzed for seven PCB aroclots. The results are summarized in Table 3-7. There were no concentrations found above the reporting limits in any of the test composites. 3.2.7 PHTHALATES Each composite and the reference sample were analyzed for 5 phthalates. The results are summarized in Table 3-8. There were no concentrations found above the reporting limits in any of the test composites. Tahla 3.7_ PCR Arnrinrc in Sediment. Marina Park 2008 Analyte LA-3 composites A-U Comp A-L Comp B-U Comp B-L Comp C-U Comp C-L Comp Aroclor 1016 <20 U <20 U <20 U- <20 U <20 U <20 U <19 U Aroclor 1242 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Aroclor 1248 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Aroclor 1254 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Aroclor 1260 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Aroclor 1221 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Aroclor 1232 <20 U <20 U <20 U <20 U <20 U <20 U <19 U Total Detected PCBs 0 0 0 0 0 0 0 U: Undetected. Actual concentration below reported concentration Tnhla q.R Phthnlntac in SadirnPnt. Marina Park 2008 Analyte LA-3 composites A-U Comp A-L Comp B-U Comp B-L Comp C-U Com C-L Comp Dimeth I hthalate <20 U <20 U <19 U <20 U <20 U <19 U <19 U Dieth I hthalate <20 U <20 U <19 U <20 U <20 U <19 U <19 U But Ibenz i hthalate <20 U <20 U <19 U <20 U <20 U <19 U <19 U bis 2-Eth Ihex i hthalate <20 U <20 U <19 U <20 U <20 U <19 U <19 U Di-n-0ci I phthalate <20 U <20 U <19 U <20 U 1 <20 U 1 <19 U I <19 U U: Undetected. Actual concentration below reported concentration 11 11 i' 1, 11 NEWFIELDS 28 11 ' Dredged Material Evaluation June 2009 Marina -Park ' 3.3 RESULTS OF BENTHIC AND WATER -COLUMN BIOASSAYS ' This section presents a summary of bioassays conducted in support of the EIR for the Marina Park project. Results for each replicate, all water quality observations, statistical analysis, and bench sheets for each test are provided in Appendix C. I I I I I I I LJ I I 3.3.1 10-DAY BENTHIC AMPHIPOD TEST The 10-d amphipod test with Ampelisca abdita was initiated on December 19, 2008. A summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-9 to 3- 11. The test was validated by 90% survival in the controls. The LC50 for the cadmium reference -toxicant test was 0.54 mg Cd/L, within the control chart limits (0.13 - 1.09 mg Cd/L), indicating that the test animals were similar in sensitivity to previous populations used at the NewFields laboratory. Temperature and salinity were slightly outside the target range in all treatments except for the control. Deviations were generally less than one unit (°C or ppt) and did not appear to have an effect on the test organism survival. Ammonia levels were below NOEC (approximately 20 mg/L total ammonia) for all treatments. Mean percent survival in LA-3 Reference was 92.0%. In Comp C-U and Comp C-L survival was 87.0 and 89.0% relatively. There was no significant difference between test treatments and the reference. T bl 3-9 Survival Summa for the 10-dav Benthic Test with A. abdita a e Treatment Mean Percentage Survival SD Control 90 3.5 LA-3 Reference 92 2.7 Comp C-U 87 7.6 Comp C-L 89 4.2 a An c...-...........F 1Ah4nr n,snHfv fnr fhP 1n.dav Eenthic Test with A. abdita 111WIV 4- IV. Treatment uUMMGI' Dissolved Oxygen (mg/L) - - Temperature (°C) -- --- - pH'(units) Salinity (ppt) Min Max Mean Min 'Max Mean Min Max Mean Min Max Control 5.3 7.3 19.1 18.6 19.5 8.1 7.7 8.5 2 29.0 32.0 LA-3 Reference6.17 5.7 7.7 19.2 18.3 19.6 8.1 7.8 8.4 6 F32.1 31.0 36.0 Comp C-U 5.5 8.0 19.2 17.8 19.6 8.1 7.7 8.3 31.0 35.0 Comp C-L 6.7 5.8 8.0 19.2 18.0 19.6 8.1 7.8 8.3 .2 31.0 35.0 i NEWFIELDS 1 f4J June 2009 TnhlP 3.11- Test Condition Stimmary for Amoelisca abdita Dredged Material Evaluation Marina Park Test Conditions: A. abdita Sample Identification LA-3 Ref, Comp C-L, Comp C-U Date sampled 12/8/2008 Date received 12/13/2008 Sample storage 4°C, dark Weeks of holding 1 week Control sediment Tomales Bay, California (native sediment) Test Species Ampelisca abdita Supplier John Brezina Date acquired 12/17/2008 Acclimation/holding time 2 days Age class Adult Test Procedures OTMI ITM Regulatory Program OTM/ ITM Test location NewFields Northwest Laboratory Test type/duration 10-Day static Test dates 12/19/2008-12129/200B Control water 0.45 pm -filtered North Hood Canai seawater Test temperature Recommended: 20 t 1 °C Achieved: 17.8 —19.6 °C Test Salinity Recommended: 321: 2 ppt Achieved: 29-36 ppt Test dissolved oxygen Recommended: > 4.6 mg/L Achieved: 5.3- 8.0 mg/L Test pH Recommended: 8.0 t 0.5 Achieved: 7.7-8.5 Control performance standard Recommended: Control < 10% mortality Achieved:10% Reference performance standard Recommended: Reference mortality < 25% Achieved: 8% Reference Toxicant LC50 0.54 mg/L Cd Acceptable Range 0.13 —1.09 mg/L Test Lighting Continuous Test chamber 1-Liter Glass Chamber Replicates/treatment 5 + 2 surrogates for measuring porewater ammonia levels Organisms/replicate 20 Exposure volume 175 mL sediment/ 950 mL water Feeding None Water renewal None Deviations from Test Protocol Salinity and temperature out of range for all except Control In 'I �J LJ I' Lj LJ I lJ IJ' '1 [I u IJ 11 n 1 NEWFIELDs 30 ' Dredged Material Evaluation June 2009 Marina Park ' 3.3.2 10-DAY SOLID -PHASE POLYCHAETE WORM TEST The 10-d polychaete worm test with Neanthes arenaceodentata was initiated on December 19, 2008. A ' summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-12 to 3-14. The test was validated by 92% survival in the controls. The LC50 for the cadmium reference -toxicant test was 10.4 mg Cd/L within the control chart limits (2.87- 16.9 mg Cd/L). Temperature fell slightly below and salinity increased above the target range in all treatments. This did ' not appear to have an effect on the animals as evidenced by the high survival rates in all treatments. Ammonia levels were below NOEC (approximately 5 mg/L) for all treatments. ' Mean percent survival in LA-3 Reference was 92.0%. Mean percent survival in the test treatments was 84.0% for both Comp C-L and Comp C-U. There was no significant difference between treatments and' the reference. T..Ai.. ,-3 c,lmmary for the 1n.dnv Renthic Test with N. arenaceodentata 7 u Lli 1 1 QMI�i � Treatment Mean Percentage Survival SD Control 92.0 11 LA-3 Reference 92 17.9 Comp C-U 84.0 21.9 Comp C-L 84.0 16.7 T_II- 9 AO o............. -4: nl,. mir 9n-nnu Ronthir. Test with N. arenaceodentata I Oulu J-I P.- Treatment Dissolved Oxygen (mg/L) Temperature ('C) pH (units) 1 Salinity (ppt)' Mean Min Max Mean Min I Max ,Mean Min Max Mean Min I Max Control 7.0 6.6 7.9 19.0 18.0 19.6 8.1 7.7 8.2 31.9 31.0 34.0 LA-3 Reference 6.9 6.3 7.3 19.0 18.0 19.5 8.1 7.8 8.2 32.2 31.0 34.0 Comp C-U 6.8 6.4 7.7 19.0 18.3 19.5 8.1 7.8 8.2 31.9 31.0 33.0 CoC-L 6.9 1 6.3 7.9 19.0 18.0 19.6 8.1 7.8 8.2 32.3 31.0 35.0 NEWFIELDS 31 June 2009 Dredged Material Evaluation Marina Park Tnhla 3.4d That Cnnrlifinn summary for Neanthes areanaceodentata Test Conditions: N. arenaceodentata ifi ti LA-3 Ref, Comp C-L, Comp C-U —Sampled Date sampled 1218/2008 Date received 12/13/2008 Sample storage 4°C, dark Weeks of holding 1 week Control sediment Yaquina Bay, Oregon Test Species N. arenaceodentata Supplier Don Reish Date acquired 12/16/2008 Acclimationlholding time 3 days Age class Juvenile Test Procedures OTM/ ITM Regulatory Program OTM/ ITM Test location NewFields Northwest Laboratory Test type/duration 10-Day static Test dates 12/19/2008-12/29/2008 Control water 0.45 pm -filtered North Hood Canal sea water Test temperature Recommended: 20 ± 1 °C Achieved: 17.8 —19.6 °C Test Salinity Recommended: 30 ± 2 ppt Achieved: 29-36 ppt Test dissolved oxygen Recommended: > 4.6 mg/L Achieved: 5.3- 8.0 mg/L Test pH Recommended: 8.0 ± 0.5 Achieved: 7.7-8.5 Control performance standard Recommended: Control < 10% mortality - Achieved: 10% Reference performance standard Recommended: Reference mortality <25% Achieved: 8% Reference Toxicant LC50 10A mg/L Acceptable Range 2.87- 16.9 mg/L Test Lighting Continuous Test chamber 1-Liter Glass Chamber Replicates/treatment 5 + 2 surrogates for measuring porewater ammonia levels Organisms/replicate 5 Exposure volume 175 mL sediment/ 950 mL water Feeding None Water renewal None Deviations Salinity and temperature out of range for all except Control i I I I i I I I i I 1J I I I I I I NtwRELDS 32 I I I I I L i I j I i I �J Dredged Material Evaluation June 2009 Marina Park 3.3.3 RESULTS OF THE WATER -COLUMN TEST WITH MENIDIA BERYLLINA The water -column test with M. beryllina was initiated on January 7, 2009. A summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-15 to 3-17. The test was validated by 96% survival in the controls. The LC50 for the copper reference -toxicant test was 227 µg Cu/L, and was inside the control chart limits (91.4 - 454 mg Cu/L), indicating that the population of test organisms used in this test were similar in sensitivity to those previously tested at the NewFields laboratory. Bench sheets, including survival in each of the treatment replicates, are presented in Appendix D. Salinity levels were slightly out of the target range for all treatments, but were within the tolerance range for this species and did not appear to have no effect as evidenced by the high survival rates. Ammonia levels were below NOEC for all treatments. Mean percentage survival in the 100% SPP for Comp C-U and Comp C-L samples were 88% to 98% relatively. There was no significant difference between test treatments and control survival, and the estimated LC50 for both treatments was >100%. Table 3-15. Summary of Results for the Water -column Test with M. beryllina Treatment SPP % Mean Percentage Survival SIP LC50 Control 0 96 8.9 NA Site Water 0 96 8.9 NA Comp C-U 10 92 17.9 >100% 50 94 5.5 100 88 8.4 Comp C-L 10 88 11.0 >100% 50 94 5.5 100 98 4.5 Table 3-16 Summary of Water Quality for the Water -column Test with M. beryllina Treatment SPP Dissolved Oxygen (mg1L) Temperature (°C) Salinity (ppt) pH ('units) ;Mean Min FMax Mean ,Min Max Mean Min Max Mean Min Max Control 0 7.3r6. 7.9 19.2 18.6 19.8 32.8 32.0 34.0 7.6 7.4 8.0 Site Water 0 7.4 9.0 19.4 19.1 19.8 35.3 34.0 37.0 7.8 7.6 7.9 Comp C-U 10 50 100 7.3 8.0 19.3 18.8 19.9 33.3 32.0 36.0 7.9 7.7 8.0 7.2 7.7 19.5 19.0 19.9 33.9 33.0 35.0 7.9 7.7 8.0 6.9 7.4 19.5 19.3 19.9 35.2 34.0 36.0 7.9 7.7 8.2 Comp C-L 10 50 100 7.1 8.2 19.4 18.7 19.9 32.8 32.0 34.0 7.9 7.7 7.9 7.2 6.6 8.0 19.4 18.7 19.9 34.6 33.0 36.0 1 7.8 7.7 8.0 1 7.3 6.9 8.0 19.5 19.2 19.9 34.7 34.0 36.0 7.9 7.8 8.0 1 NEWFIELDS 1 33 Dredged Material Evaluation June 2009 Marine Park Table 3-17. Test Condition Summary for Menidia betyllina Test Conditions: M. beryllina Identification LA-3 Ref, Comp C-L, Comp C-U Date sampled 12/8/2008 Date received 12/13/2008 , Sample storage 4°C, dark Weeks of holding 3 weeks Test Species M. beryllina Supplier Aquatic BioSystems Date acquired 1/6/2009 Acclimation/holding time 1 day Age class 10 days old Test Procedures OTM/ ITM Regulatory Program OTM/ ITM Test location NewFields Northwest Laboratory Test type/duration 96-hour SPP Test dates 1/712009-1/11/2009 Control Water 0.2Nm-filtered North Hood Canal sea water Test temperature Recommended: 20 t 1 °C Achieved: 18.6—19.9°C Test Salinity Recommended: 31 t 2 ppt Achieved: 32- 37 ppt , Test dissolved oxygen Recommended: > 3.7 mg/L Achieved: 6.5- 9.0 mg/L Test pH Recommended: 7.8 t 0.5 Achieved: 7.4-8.2 Control performance standard Recommended: Control < 10% mortality Achieved: 4% Reference Toxicant LC50 307 pg Cu/L , Acceptable Range 89.6- 443 pg Cu/L Test Lighting 16- hours light, 8-hours dark Test chamber 600mL Glass Chamber Replicates/treatment 5 Organisms/replicate 10 , Exposure volume 250 mL Feeding Once at 48 hours Water renewal Deviations NEWPiuD9 None Salinity out of range in all treatments 34 ' ' Dredged Material Evaluation June 2009 Marina Park 1 II u I II 3.3.4 RESULTS OF THE WATER -COLUMN TEST WITH AMERICAMYSIS BAHIA The water -column test with A. bahia was initiated on January 7, 2009. A summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-18 to 3-19. The test was validated by 98% survival in the controls. The LC50 for the copper reference -toxicant test was 233 µg Cu/L, and was inside the control chart limits (140 - 406 mg Cu/L), indicating that the population of test organisms used in this test were similar in sensitivity to those previously tested at the NewFields laboratory. Bench sheets, including survival in each of the treatment replicates, are presented in Appendix D. Salinity levels were out of range for all treatments, but did not appear to have affected survival as evidenced by the high survival rates. Ammonia levels were below NOEC for all treatments. Mean percentage survival in the 100% SPP for Comp C-U and Comp C-L samples were both 98%, and the estimated LC50 for each of the test treatments was >100%. n. 1GVIC J'1V. Vl Treatme Contro Site Wat Comp C Comp C 1 dulu a- IV. JI Treatment Control Site Water Comp C-U Comp C-L NEWFIELDS A-A;- June 2009 Table 3-20. Test Condition Summary for Americamvsis bahia Dredged Material Evaluation , Marine Park ----- - --- - - Test Conditions: A. bahia Sample Identification LA-3 Ref, Comp C-L, Comp C-U Date sampled 12/8/2008 Date received 12/13/2008 Sample storage 4°C, dark Weeks of holding 3 weeks Test Species Americamysis bahia Supplier Aquatic BioSystems Date acquired 1/6/2009 Acclimation/holding 1 day Age class 3 days old Test Procedures OTM/ ITM Regulatory Program OTM/ ITM Test location NewFields Northwest Laboratory - Test type/duration 96-hour SPO Test dates 1/7/2009-1/11/2009 Control water 0.2pm-filtered North Hood Canal sea water Test temperature Recommended: 20 + 1 °C Achieved: 18.6—19.9°C Test Salinity Recommended: 31 + 2 ppt Achieved: 32- 37 ppt Test dissolved oxygen Recommended: > 3.7 mg/L Achieved: 6.5- 9.0 mgtL Test pH Recommended: 7.8+0.5 Achieved: 7.4-8.2 Control performance standard Recommended: Control < 10% mortality — Achieved: 4% Reference Toxicant LC50 233 pg Cu/L Acceptable Range 140- 406 pg Cu/L Test Lighting 16- hours light, 8-hours dark Test chamber 600mL Glass Chamber Replicates/treatment 5 Organisms/replicate 10 Exposure volume 250mL Feeding Twice daily Water renewal None Deviations from Test Protocol Salinity out of range in all treatments I [1 I 1 NEWFIELDS 36 ' Dredged Material Evaluation June 2009 Marina Park ' 3.3.5 RESULTS OF THE WATER -COLUMN TEST WITH MYTILUS SP. The bivalve larval test was conducted on January 7, 2009 and was validated by 96.8% mean normal ' development in the controls. The EC50 for the copper reference -toxicant test was 9.69 µg Cu /L for normal development, which was within control chart limits (3.60 - 18.0 µg Cu/L). A summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-21 to 3- 23. Bench sheets, including survival in each of the treatment replicates, are presented in Appendix D. Salinity was out of range for Comp C-U 50 and 100% as well as Comp C-L 50 and 100%. There was no adverse effect on the animals as evidenced by high normal development percentages. Ammonia levels were below NOEC for all treatments. Mean percentage normal survival in the Site Water control was 98.1%, while mean percentage normal in 100% SPP for Comp C-U and Comp C-L were 97.2% and ' 97.6%, respectively. There were no significant differences between mean normal survival in the 100% SPP for either test composite, relative to the control and the estimated EC50 for both treatments was >100% SPP. 1 r LJ 1 I � ee c.........,.....f @nmdfc fnr 4ha WafPr.Cnhlmn Test with MVHIUS SP. Treatment SPP % Mean Normal Development SD EC50 %SPP, Control 0 96.8 1.3 NA Site Water 0 98.1 0.6 NA Comp C-U 1 96.5 0.6 >100 10 97.5 0.7 50 97.0 0.9 100 97.2 1.4 Comp C-L 1 97.9 0.5 >100 10 97.3 0.9 50 97.3 0.9 100 97.6 0.6 T bi 3 22 S ma of Water Qualit Observations Water -column Test with M tilus sp. a e - Treatment um SPP ( /o) Dissolved Oxygen (mglL) I Temperature (°C) pH (units) Salinity (ppt) Mean Min Max Mean Min Max Mean Min Max 'Mean Mln Max Control 0 7.6 7.5 7.9 16.0 15.5 16.8 7.8 7.8 7.9 32.0 31.0 33.0 Site Water 0 7.9 7.3 9.0 16.0 15.6 16.3 7.8 7.8 7.9 35.0 34.0 36.0 1 7.6 7.2 8.3 16.0 16.4 7.9 7.9 8.0 32.3 32.0 33.0 10 7.5 7.1 8.1 16.1 16.6 7.9 .3 32.0 33.0 Comp C-U 50 7.2 6.8 7.5 15.9 r15.6 16.5 8:0 4.0 33.0 35.0 100 6.9 6.6 7.1 15.9 16.6 8.1 5.3 34.0 37.01 7.3 6.9 7.9 16.0 16.5 8.1 M8.335.3 2.3 32.0 33.0 10 7.6 7.3 8.0 15.9 16.6 8.0 2.7 32.0 33.0 Comp C-L 50 7.6 7.3 8.0 15.8 15.4 16.6 8.0 4.7 33.0 36.0 100 7.6 7.3 8.0 161 15.5 16.9 7.9 5.0 3") 36.0 NEWFIELDS 37 Dredged Material Evaluation Marina Park June 2009 Tahie 3.23. Test Condition Summary for Mvtilus SD Test Conditions; Mytilus sp. Sample Identification LA-3 Ref, Comp C-L, Comp C-U Date sampled 12/8/2008 Date received 12/13/2008 Sample storage 4°C, dark Weeks of holding 3 weeks Test Species Mytilus sp. Supplier Carlsbad Aquafarms Date acquired 1/6/2009 Acclimation/holding Broodstock held for 1 day Age class Larval Age of test animals <4 hours Test Procedures OTM/ ITM Regulatory Program OTM/ ITM Test location NewFields'Northwest Laboratory Test type/duration 48-hour SPP Test dates 1/7/2009-1/9/2009 Control water 0.2pm-filtered North Hood Canal sea water Test temperature Recommended: 16 ± 1 °C Achieved: 15.4—16.9°C Test Salinity Recommended: 31 ± 2 ppt Achieved: 31- 36 ppt Test dissolved oxygen Recommended: > 4.0 mg/L Achieved: 6.6- 8.1 mg/L Test pH Recommended: 8.0 ± 1, Achieved: 7.8-8.3 Control performance standard Recommended: Control < 10% mortality Achieved: 3.2% Reference Toxicant LC50 9.69 pg Cu/L Acceptable Range 3.60-18.0 pg Cu/L Test Lighting 16- hours light, 8-hours dark Test chamber 1-L Glass Chamber Replicates/treatment 5 Organisms/replicate Stocking density = 288.6 embryos per chamber Exposure volume 10mL Feeding None Water renewal None Deviations Salinity out of range in all treatments I I I I I 11 I I I I I I I I i NEWFIELDS 38 1 ' Dredged Material Evaluation June 2009 Marina Park I I I u [i i I 1 r 3.3.6 SIOACCUMULATION TEST RESULTS Bioaccumulation tests were initiated on December 16, 2008 using the polychaete worm, Nephrys caecoides, and the bent nose clam, Macoma nasuta. A summary of test results, water quality observations and an overall summary of the test are presented in Tables 3-24 to 3-26. Bench sheets, including survival in each of the treatment replicates, are presented in Appendix E. The bioaccumulation tests were validated by 95.0% survival in the N. caecoides control and 93.6% survival in the M. nasuta control. Both species were tested in the same test chambers, therefore only one set of water quality observations are recorded. All water quality parameters were within range. Mean percentage survival in LA-3 Ref was 96.8% for M. nasuta and 86.3% for N. caecoides. Mean percentage N. caecoides survival were 86.3 and 90.3% for Comp C-L and Comp C-U relatively. Mean percentage M. nasuta survival were 64.8 and 99.2% for Comp C-L and Comp C-U. The higher mortality rate for clams in Comp C-L may have been due to the higher percent sand and very low TOC content of 0.05%. However, sufficient tissue was available for all tissue analyses. �.. .. : ee �..*� ..,a Alraucnir�lac Survival 28-d Bioaccumulation Test au;c a-��r. uuu.... ..................... Treatment Macoma nasuta Ne ht s caecoides Mean Percentage Survival. SD Mean Percentage 'Survival SD Control 93.6 3.6 95.0 4.2 LA-3 Ref 96.8 3.3 86.3 4.9 Comp C-L 64.8 13.7 86.3 3.8 Comp C-U 99.2 1.8 90.3 4.8 _._._ n nv o..�........ -9 ur..a..r ru.�Iif.. fnr 4ha 9A. rlav Rinnrrumulation Test l aide a -La. Dissolved Ox en m /L Temperature °C Salinity t H H units Flow mL130 sec Treatment Mean Min Max, Mean Min Max Mean Min 'Max Mean Min Max Mean Min Max Control 7.1 5.8 8.0 15.6 15.1 16.1 31.T731 33 7.6 17.318.1 40 38 42 LA-3 Ref 7.1 6.1 8.0 15.6 15.0 16.2 31.7 31 33 7.7 7.3 8.0 40 38 1 42 Comp C-L 7.1 5.8 7.9 15.5 14.9 15.8 31.7 31 33 7.7 7.3 8.0 40 38 42 mp C-U 7.1 5.5 7.8 15.5 15.0 15.9 31.7 31 33 7.7 7.4 8.3 40 38 42 NEWFIELD5 61d Dredged Material Evaluation June 2009 Marina Park Table 3-26. Test Condition Summary for Macotna nasuta and Ne ht s caecoides 1 Test Conditions Samole IdentificationLA-3 Ref, Comp C-L, Comp C-U Date sampled 12/8/2008 Date received 12/13/2008 Sample storage 4°C, dark ' Weeks of holding 1 week Test Species Macoma nasuta and Nephtys caecoides Supplier J & G Gunstone provided clams and John Brezina provided worms Date acquired 1/6/2009 Acclimation/holding 4 days , time Age class Adult , Test Procedures OTM/ ITM Regulatory Program OTM/ ITM Test location NewFlelds Northwest Laboratory Test type/duration 28-Day Bioaccumulation Test dates 12/16/2008-1/13/2009 Control water 0.2pm-filtered North Hood Canal sea water Test temperature Recommended: 15 ± 1 °C Achieved: 14.9—16.2°C Test Salinity Recommended: 32 ± 2 ppt Achieved: 31- 33 ppt Test dissolved oxygen Recommended: > 4.5 mg/L Achieved: 5.5- 8.0 mg/L Test pH Recommended: 7.8 ± 0.5 Achieved: 7.3-8.3 Achieved: M. nasuta— Achieved: Control performance Control < 10% mortality 6.4% standard N. caecoides — 5.0% Test Lighting 16- hours light, 8-hours dark Test chamber 10 Gallon Glass Aquarium Replicates/treatment 5 Organisms/replicate 25 clams, 60 worms ' Exposure volume 5 cm of sediment, 30 L seawater Feeding Water renewal None Flow -Through , Deviations None NEWFIELDS 40 ' Dredged Material Evaluation June 2009 Marina Park ' 3.4 TISSUE CHEMICAL ANALYSIS ' Bioaccumulation tests were conducted using Comp C-U and Comp C-L, as well as sediment collected from the LA-3 Reference site. The analyte list for tissue residue analysis was based on the chemical concentrations found in the sediments. Based on the sediment chemistry, tissues from the ' bioaccumulation exposures were analyzed for mercury and lipids. Concentrations found for each replicate in the test treatments and the reference sample are presented in Table 3-26. No mercury was observed in reference sample. Mercury was detectable in N. caecoides from Comp C-U and in M. nasuta from Comp C-L; however, concentrations found were only slightly above reporting values. There was a significant difference between the concentration of mercury in the clam tissues exposred to Comp C-U, relative to the LA-3 Reference. However, this was likely to the absence of mercury in the LA-3 Reference clam tissues. I I I I 1 t I I ,r-we a-oa S.,mmani of Marenry r nnep_ntrations in Tissues Macoma nasuta Nephtys caecoides Mean Mercury Mean Mercury Mercury Concentration Mercury Concentration, Treatment Replicate (mg/kg) (mg/kg) (mg/kg) (mg/kg) 1 0.01 U 0.01 U 2 0.009 U 0.01 U LA-3 3 0.009 U 0.010 0.01 U 0.010 Reference 4 0.01 U 0.01 U 5 0.01 U 0.009 U 1 0.011 0.009 2 0.013 0.01 U Comp C-U 3 0.011 0.011 0.011 0.010 4 0.011 0.01 U 5 0.01 0.009 U 1 0.009 U 0.01 U 2 0.009 U 0.009 U Comp C-L 3 0.01 U 0.009 0.009 U 0.0 4 0.009 U 0.009 U 5 0.01 U 0.01 U NEWFIELDS 41 Dredged Material Evaluation June 2009 Marina Park 4 DISCUSSION 11 As part of the planning process for Marina Park, NewFields LLC conducted an evaluation of the , proposed dredged material from arca-of the proposed marina. The objective of this sampling and analysis program was to characterize the dredged materials from three dredged material management areas (Areas A, E, and C) within the Marina Park marina project area. The primary disposal options under ' consideration for the dredged materials are 1) beach nourishment under Regional General Permit Number 67 or an individual permit for unconfined aquatic disposal alternative as governed by the U.S. Army Corps of Engineers (USACE)/U.S. Environmental Protection Agency (USEPA) guidelines set forth in the Inland Testing Manual (ITM; USACE/USEPA 1998), and 2) ocean disposal at disposal site LA-3 based on guidance provided by the Ocean Testing Manual (OTM; USACE/USEPA 1991). Evaluation criteria were based on the ITMIRGP-67 guidance for nearshore disposal and OTM guidance ' for open ocean disposal at the LA-3 disposal site. Under the RGP-67 and ITM, sediment is suitable for beach nourishment projects or nearshore placement if the sediment is >80% sand and gravel, is free from chemical contamination, is not plastic (a measure of cohesiveness), and is not likely cause adverse ' aesthetic effects. In order to determine whether test sediments were free of chemical contamination, chemical concentrations in test sediments were compared to National Oceanographic and Atmospheric Administration (NOAA) effects -based guidance values called Effects -Range Low (ERL) and Effects - Range Median (ERM). The ERL represents the 10'h percentile in NOAA effects data base and the ERM represents the 50'h percentile. While not criteria, these guidance values provide an indication of whether chemical concentrations are sufficient to predict benthic community effects. If the ERL/ERM values are exceeded, further biological testing might be required'as directed by the ITM. Under the OTM, sediment is suitable for placement in an open -ocean disposal site if it does not exceed the limiting permissible concentration (LPC) for the disposal site. The LPC is based on the sediment chemistry results, toxicity tests, and bioaccumulation test and comparisons to the disposal site reference site (in this case LA-3 Reference). As above, chemical concentrations were screened using the NOAA ERL and ERM values. For benthic toxicity tests, the LPC was defined as: no significant toxicity, relative to the LA-3 Reference and survival within 10% of the reference for the polychaete test and 20% for the amphipod test. For the SPP tests, the LPC was based on a comparison of survival or normal development (larval test only) in the 100% SPP of the test treatments with that of the control seawater. If there is a significant difference, then the median lethal concentration (LC50) for the test treatments is compared with a modeled concentration of SPP at the boundary of the disposal site. Concentrations of targeted chemical analytes in the tissues exposed to test sediments are first compared to the tissues exposed to the LA-3 Reference sediment and second compared to guidance values from the Food and , Drug Administration (FDA) and USEPA (2000). Sediment treatments that do not exceed the LPC for the LA-3 disposal site would meet the requirements for disposal at LA-3. ' The following discussion evaluates the physical, chemical, and biological data for each composite relative to the two disposal options. In each case the USACE and EPA will make a final determination. i NEWDEI.DS 42 ' Dredged Material Evaluation June 2009 Marina Park ' Area A Composites (Comp A-U and Comp A-L): ' Area A included that portion of the site currently occupied by the mobile home park. Sediments in the upper composite represented that material from 5 feet below the ground surface (approximately +5 ft. MLLW) to a depth of approximately -4 to 5 ft. MLLW. Soils above +5 ft. MLLW will be used as construction -fill on -site. Sediments in the lower composite represented that material from -4 to -5 MLLW to -14 Ft. MLLW and appeared to represent the ancient Bay sands that underlay much of Lower Newport Bay. Sediment in the Comp A-U was characterized by 96% sand and gravel, with 0.15% TOC. Sands were not plastic, had very low levels of sulfides and ammonia, and no detectable oil and grease. Metals were either undetected (cadmium, lead, mercury, selenium, and silver) or detected at concentrations well below ERL values (arsenic, chromium, copper, nickel and zinc). All metals concentrations were well below those of the LA-3 Reference sediment. PAHs, pesticides, PCBs, phthalates, and tributyltin were not detected in the Comp A-U sediment. ' Sediment in the Comp A-L was characterized by 99% sand and gravel, with 0.08% TOC. Sands were not plastic, had very low levels of ammonia, and no detectable oil and grease or sulfides. Metals were either undetected (cadmium, lead, nickel mercury, selenium, and silver) or detected at concentrations well below ERL values (arsenic, chromium, copper, and zinc). All metals concentrations were well below those of the LA-3 Reference sediment. PAHs, pesticides, PCBs, phthalates, and tributyltin were not detected in the Comp A-L sediment. The upper and lower sediments of Area A from +5 ft. MLLW to -14 ft. MLLW would meet the criteria for the RGP-67 and ocean disposal at LA-3, as defined above. Area B Composites (Comp B-U and Comp B-L): Area B included the beach in front of the mobile home park to the 0 ft. MLLW tide line. The upper composite represented sediment from the beach face to a depth of -4 to -7 ft. MLLW and included hydraulic -fill sands (Terra Costa 2008). Sediments in the lower composite represented that material from -4 to -5 MLLW to -14 Ft. MLLW and were similar to the ancient Bay sands found in lower portion of Area A. Sediment in the Comp B-U was characterized by 96% sand and gravel, with 0.02% TOC. Sands were not plastic, had very low levels of ammonia, and no detectable oil and grease or sulfides. Metals were either undetected (selenium, and silver) or detected at concentrations well below ERL values (arsenic, cadmium, chromium, copper, lead mercury, nickel and zinc). All metals concentrations were well below those of the LA-3 Reference sediment. Some PAHs were detected in Comp B-U sediment, however, total PAHs were three orders of magnitude below the ERL. Pesticides, PCBs, phthalates, and tributyltin were not detected in the Comp B-U sediment. Sediment in the Comp B-L was characterized by 98% sand and gravel, with 0.08% TOC. Sands were not plastic, had very low levels of ammonia, and no detectable oil and grease or sulfides. Metals were either undetected (cadmium, lead, mercury, selenium, and silver) or detected at concentrations well ' below ERL values (arsenic, chromium, copper, nickel, and zinc). All metals concentrations were well below those of the LA-3 Reference sediment. PAHs, pesticides, PCBs, phthalates, -and tributyltin were not detected in the Comp B-L sediment. ' The upper and lower portions of Area B would meet the criteria for the RGP-67 and ocean disposal at LA-3, as defined above. NEWFIELDS 43 Dredged Material Evaluation June 2009 Marina Park Area C Composites (Comp C-U and Conip C-L): Area C included that portion of the site below the 0 ft. MLLW tide line. Area C included a nearshore component (0 ft. to approximately -5 ft, MLLW) where the bulk of the proposed dredge volume is located and a channel component (-6 ft. to approximately -10 ft. MLLW). The upper Area C composite represented that portion of the cores from the sediment surface to -10 ft. to -12 ft. MLLW. Sediment in the upper segment in the nearshore area was comprised of a sand layer, overlaying a two to three foot layer of silt and was bounded at the bottom by the ancient Bay sands. The upper segment of the channel cores was comprised of silts and clays. The lower segment was similar throughout the Area and was comprised of the ancient Bay sands that were observed in Areas A and B. The lower segment represented that portion of the cores from -10 to - 12 ft. MLLW to project depth. Sediment in the Comp C-U was characterized by 78% sand and gravel, with 0.68% TOC. Sediment was slightly plastic, with an Atterberg Limit of 16 cm, low levels of ammonia, and no detectable oil and grease or sulfides. While there was some measurable plasticity in the Comp C-U sediment, the plasticity index was relatively low and would not necessarily predict that sediments would form a hardpan during placement, particularly if placed in the surf zone. With the exception of mercury, metals were either undetected (selenium and silver) or detected at concentrations below ERL values (arsenic, cadmium, chromium, copper, lead, nickel and zinc) and below those of the LA-3 Reference sediment. Mercury was detected in Comp C-U at a concentration of 0.36 mg/kg, which is slightly above that of the LA-3 Reference site (0.10 mg/kg) and the ERL of 0.24 mg/kg, but below the ERM of 0.76 mg/kg. Some PAHs were detected in Comp C-U sediment; however, total detected PAHs were 108 µg/kg, less than 3% of the ERL (4,022 µg/kg). Pesticides, PCBs, phthalates, and tributyltin were not detected in the Comp C-U sediment. Upper and lower segments of individual cores from Area C were also analyzed for mercury and sediment grain size. The upper segment from the cores in the nearshore portion of Area C was characterized as a mixture of sand and silt. Mercury concentrations ranged from undetected to 0.85 mg/kg. The upper segment of cores from the offshore portion.of Area C was dominated by fine-grained silts and clays and mercury concentrations were higher, ranging from 1.11 to 3.35 mg/kg. The lower segments for both the nearshore and offshore stations were similar, dominated by sand with concentrations of mercury that were either undetected or detected at concentrations very near the detection limit. The upper silt layer that occurred in each of the cores was 2 to 3 ft thick and comprised relatively small portion of the material in the Area C-U composite. Sediment from the lower Area C composite was very similar to the lower composites from Areas A and B, with 99% sand and 0.05% TOC. Metals were either undetected or detected very near the detection limits. Pesticides, PCBs, tributyltin, TRPH, oil and grease, phthalates, and PAHs were not detected in the Comp C-L. No toxicity was observed in either of the benthic tests. Survival in the amphipod test ranged from 87- 92%. Control survival met the standard, proving a valid test, and there was no significant difference between test treatments and the reference, Survival in the polychaete test for both test treatments was 84%. Similarly, control survival met the standard and there was no significant difference between test treatments and the reference site. There was also no indication of toxicity in the water -column tests. For the fish and mysid tests, survival was >88% in the 100% SPP and there were not significant differences between the 0% and 100% SPP. Mean normal development of larval mussels was slightly greater in the test treatments than in the dilution water and there were no significant differences between the 0% and 100% SPP treatments. As NwFIEws 44 Dredged Material Evaluation June 2009 Marina Park ' outlined in the ITM, dredged material does not exceed the water -column LPC if survival in 100% elutriate is not >10% less than that of dilution water (USEPA 1998). None of the treatments exceeded 1 these guidelines. Area C composites and the LA-3 Reference site were evaluated for bioaccumulation potential. The chemistry analyte list for tissues exposed to the Area C composites included mercury and lipids. No ' mercury was detected in either the reference material or in Comp C-L. Mercury was either undetected or detected at the detection limit (0.01 to 0.013 mg/kg) in tissues exposed to Comp C-U. The mean tissue concentrations in clams and worms exposed to Comp GU were within 20% of the detection limit, the ' standard margin of error for this analytical method. The tissues concentrations of mercury were also well below the FDA limit of 1.0 mg/kg and the risk -based guidance value of 0.3 mg/kg (USEPA 2000). ' Sediment from the Area C upper composite would not meet the requirement for beach nourishment, with <80% sand and gravel. Sediment from nearshore portion of the Area C upper composite (that area represented by Stations 10, 12, and 16) would meet the requirements for open -ocean disposal, or ' nearshore placement in the surf zone, which allows 15% to 45% fines. With the exception of mercury, concentrations for chemicals of potential concern were either not detected or detected at concentrations below those of the LA-3 Reference site. Mercury was detected above the ERL, but below the ERM. No ' significant toxicity was observed in any of the biological tests and no significant bioaccumulation of mercury was observed in the bioaccumulation tests. ' The upper portions of Area C corresponding to cores MP-11, 13, 14, and 15 would not be suitable for unconfined disposal in either the nearshore zone or the open ocean disposal site due to mercury concentrations in the sediment from the individual cores. Alternative disposal options may include upland disposal or placement in a confined aquatic disposal facility. Sediment from the lower Area C composite met the requirements for beach nourishment and ocean disposal. However, this layer occurs close to the proposed dredge depth of -12 ft. MLLW and it is ' unlikely that the layer could be easily separated from the overlying sediment during dredging. If the lower portion of Area C represented by Stations 11, 13, 14, and 15 are disposed of separately from the upper portion, the dredged material will be monitored for grain size during removal to ensure that no ' surface sediments are placed in nearshore or open -ocean waters. Because the demarcation from the overlying silt/clay layer and the underlying clean sands is distinct, dredging for upland disposal will be considered complete when field monitoring indicates that the remaining sediment face is >80% sand. 1 1 1 1 1 NEWFIELDS 45 1 Dredged Material Evaluation June 2009 Marina Park Figure 7. Portion of Area C for which the upper portion is not considered to be suitable ' for beach nourishment or open -ocean disposal (area represented by pink hatching). 1 1 t 1 1 1 NEWFIELDS 46 ' Dredged Material Evaluation June 2009 Marina Park REFERENCES ' APHA/AWWA (American Public Health Association/American Water Works Association). 1998. Standard Methods for the Examination of Water and Wastewater (20th Edition). Edited by Lenore S. Clesceri, Arnold E. Greenberg and Andrew D. Eaton. APHA Phildelphia PA. ' American Society for Testing and Materials. 2003a. E724-98 Standard Guide for Conducting Static Acute Toxicity Tests Starting with Embryos of Four Species of Saltwater Bivalve Molluscs. In ' Annual Book of Standards, Vol. 11-05. West Conshohocken, Penn. 2003c. E1367-99 Standard Guide for Conducting 10-day Static Sediment Toxicity Tests with Marine and Estuarine Amphipods. In Annual Book of Standards, Vol. 11-05. West Conshohocken, ' Penn 2003d. E1611-00 Standard Guide for Conducting Sediment Toxicity Tests with Marine and ' Estuarine Polychaetous Annelids. In Annual Book of Standards, Vol. 11-05. West Conshohocken, Penn. ' Krone, C.A., D.W. Brown, D.G. Burrows, R.G. Bogar, S.L. Chan, and U. Varanasi. 1989. A method for analysis of butyltin species in measurement of butyltins in sediment and English sole livers from Puget Sound. Marine Environmental Research 27:1-18. ' Lee, D. R. 1980. Reference toxicants in quality control of aquatic bioassays. In Aquatic Invertebrate Bioassays, ASTM STP 715. American Society for Testing and Materials. Philadelphia, PA. Long, E. R., D. D. MacDonald, S. L. Smith, and F. D. Calder. 1995. Incidence of Adverse Biological Effects within Ranges of Chemical Concentrations in Marine and Estuarine Sediments. Environmental Management, Vol 19, No. 1, pp 81-97. NewFields. 2007. Mercury study of West Lido Channel and Balboa Peninsula. Prepared for City of Newport Beach. Plumb, R. H., Jr. 1981. Procedure for handling and chemical analysis of sediment and water samples. Technical Report EPA/CE-81-1. U.S. Environmental Protection Agency/U.S. Army Corps of ' Engineers Technical Committee on criteria for dredged and fill material, U.S. Army Waterways Experimental Station. Vicksburg, MS. ' TerraCosta Consulting Group, Inc. 2008. Geotechnical Investigation, Marina Park Project, Newport Beach, California. Prepared for City of Newport Beach, August. USEPA 1993. Guidance Manual Bedded Sediment Bioaccumulation Tests. EPA/600/R-93/183. USEPA ' Office of Research and Development. USEPA. 1994. Method 7471A: Mercury in Solid or Semisolid Waste. U.S. Environmental Protection Agency, Office of Solid Waste and Emergency Response, Washington, DC. . 2001. SW-846 On-line, Test Methods for Evaluating Solid Waste, Physical/Chemical Methods. ' URL: <http://www.epa.gov/epaoswer/hazwaste/test/sw846.htm>. Office of Solid Waste. USEPA/USACE 1991. Evaluation of Dredged Material Proposed for Ocean Disposal: Testing Manual. EPA 503/8-91/001. USEPA Office of Water. February. NEwFtELDs 47 June 2009 Dredged Material Evaluation Marina Park 1998. Evaluation of Dredged Material Proposed for Discharge in Waters of the U.S: - Testing , Manual. EPA 823-B-98-004. USEPA Office of Water. February. J 11 I I 7 11 1 NEWFiEns 48 I 1 i 1 1 1 1 i 1 n 1 1 LJ i 1 �J i Appendix A Field Logs and Core Photographs 1 NT=_�w.[-tJ=LAs SEDIMENT CORING LOG r7 11 PROJECTISURVEY DATE PROJECT MANAGER RECORDER Newrx�rl- Cftwnna. 1Cck'� I!i c,�e B.G-2.rd•i�er T.`Xliu�) STATION ID NAY DATUM LATITUDE LONGITUDE ,.4 NAD83 ?j�j` 3(o- L{� �(' (1� 0 v•3oZ S � N� WATER DEPTH (FT) TIDEWTI MLLW(FTI-WATER DEPTH -TIDE SAP DEPTH IFT) TARGET CORE LENGTH (FTI (SAP DEPTH- MLL FINAL h" CORE LENGTH(FT) PENETRATION(FT) CORE LENGTH COLLECTED FOR ANALYSIS IF COREDIAMETERIIN) 11/2 ATTEMPT TIMESTARTED I of I I�' TIME FINISHED DEP.(FT) DEP.(FT) SEDIMENT TYPE ODOR COLOR (HUE VALUE/CHROMA) SPHPLE ID BY DEPTH ISC 3 3 j(t✓^.Gl lam"'\L �Q✓LAt.0-11 4 4 t&�I . 3 -Lj.s M.IS:s r VI�Q'I U� 5 5 6 6 7 7 8 8 j 9 9 cy q yl , �-s, 10 10 11 11 ; 12 12 1 , I 13 13 � I 15 15�� I i J(vr'•>'Y1 16 16 17 17 I 18 18 �' 19 19 �t�d1 �r + 20 20771 __ aaNSEDIMENT CORING LOG ' PROJECTISURVEY N 0,,o voc k rna rk na, �a.� - DATE 1 k 12( o s PROJECTMANAGER RECORDER P). e e AYU 0 Y STATIONID Mf-2 NAV DATUM LATITUDE NAD83 3qG%. N:9' N LONGITUDE 11�° SS.338' W WATERDEPTH(PT) TIOEIFT) MLLW(FT) -WATER DEPTH•TIOE 5APDEFTHIFT) TARGET CORE LENGTH (FT) (SAP DEPTH• MLL 017 ' FINALCORE LENGTH IFTI PENETRATIONIFTI a. ?a CORE LENGTH COLLECTED FOR ANALYSIS( 2Gi CORE DIAMETER 110 1112 ATTEMPT 71ME5TARTED of I 1230 TIMEFINISHED I IS DEP.(FT) DEP.(FT) SEDIMENTTYPS OODR COLOR HUE VALUEICHROMA) SAMPLEIDSYDEPTH MISC ' l N✓✓7.�t �(, Id i1u�/�%CS.� l7 / C.�1'✓'h�rft -2-' Q„rL,' 2 2 J 3 3 ` jlg` I I ` LUTA% dl-6 4 4 I C( rx 11 1 5 5 I I. I I nn 6 6 � �• 7 7 G "� v6p x ^ Ul 8 8 10 10 12 12�. U ."krn.a r (. 2w 'Ll& 1-r3T,4 .. 13 13 14 14 1 y— 15 15 I 16 16 17 17 18 1D t i 19 19 i I O1E. C .\•....... .......... ... ...................r....w... ..i..�..7 .C..0 .....u..�.....•.••nn'......u..u...........u......u1...••...........••..o......nu.............................�n.............u.................................... . ' ...............w.......................u...................u............................n..... ...4..................N........ w u...M..0•u.,u.................N.............r. ............. ................... ...... u......................... ......w................. u.......................u....................«........................ ' I-TJaw V IJaI_us SEDIMENT CORING LOG 11 1 1 , PROJECTISURVEY DATE PROJECT MANAGER RECORDER N STATIONID NAV DATUM LATITUDE 'LONGITUDE (!. NAD83 3 3° AP I Al w*� • 312 �yj WATER DEPTH (FT) TIDEIFTI MLLW(FT)=WATER DEPTH -TIDE SAPOEPTH(FTI TARGET CORE LENGTH(FT)(SAP DEPTH. MLL FINAL CORE LENGTH PENETRATION(FT) CORE LENGTH COLLECTED FOR ANALYSIS IF a5' aO e � ac) CORE DIAMETER (IN) ATTEMPT I TIMESTARTED i W TIMEFINISHED 1 112 I of DEP.(FT) bEP.{FT) SEDIMENT TYPE ODOR COLOR (HUE VALUEICHROMA) SAMPLEIDBYDEPTH MISC C.b�rS�. v�•�i� j�r.�.c�: 2 2 d.GLn Jl 3 3 4 5 5 6 6 -- 7 8 8 C/-1b wl,u5S..Ar 9 J 12 12 13 13 - )n l I' L. 14 14�i ; I 15 15 16 16 I I 17 17 18 18 19 19 I 20 26 1 c� . ; S ;i ; (/v 7 t �. �(Ur✓krl —2 v;:. e� u 'r SEDIMENT CORING LOG PROJECTISURVEY I\�ej-&) ox i. - ff1. '1n ,r i DATE itlaro'c7 PROJECTMANAGER 3.�c�� t:)R s~ RECORDER T•l-�c�tkl'1, STATION 10' NAV DATUM LATITUDENAD83 950 5&^ 444y� LONGITUDE � SS.3Z�I'CAI WATER DEPrH(FT) TIDE(FT) MLLW(FTI°WATER OEM -TIDE SAP DEPTHIFT) TARGET CORE LENGTH IFT116AP DEPTH• MLL FINAL CORE LENGTH (FT) PENETRATIONIPTI CORE LENGTH COLLECTED FORANALYSIS(F CORE DIAMETER (IN) ATTEMPT ! of TIME STARTED TIMEFINISHED DEPAFT) SEDIMENT TYPE DOOR COLOR HUE VALUEICHRGMA SAMPLE ID BY DEPTH MISC 1 1 G ~.,, ..i•1.34t�.� -� r11/2 r 3 3 `� iJ-,uo-'1 5 6 l y �••� 6 7 7 / i! 6 8 ' 9 9 10 10 11 11 12 12 1 y 13 13 r 14 14 �� ' ALL 16 16 s 17 17 ly 18 18 19 19 J 20 20 I [1 I I I n .... I ... ........ ........... .................... ............. ............. _................. .... ................... .,.......... .... ................... ............. ........... ....... ............ ............ ........_....... ........... .. 1 SEDIMENT CORING LOG PROJECTISUAVEY GATE PROJECTMANAGER RECORDER SYiG.7('iU-"GlF' �iliGo.i IJ.(;;Ci�C1'1G' STATION 10 NAY DATUM LATITUDE � LONGTfUDE 3�i 4AIR o (n� �j Or. NAD83 $3 � �a 32S WATERDEPTH(FTI TIDE(FTI MLLW(FTI=WATER DEPTH -TIDE SAPDEPTH(FT) ' TARGET CORE LENGTH (FT)(SAP DEPTH- MILL FINAL CORE LENGTH (FT) PENETRATION(FTI CORE LENGTH COLLECTED FOR ANALYSIS IF CORE DIAMETERON) ATTEMPT TIME STARTED TIME FINISHED 1112 of aC, ig50 COLOR I�_ DEP.(FT) DEP.(FT) SEDIMENTTYPE ODOR (HUE VALUEICHROMA) SAMPLE ID BY DEPTH MISC 1 1IbVA 2 2 U6trb54- j 3 3n ' 4 4 �IllUf1SG Yii ©I-vp�+a" 5 5 �•2i� n...a, ' 6 6 v ^ �A {YtISSi ' 7 7k� 8 8 ' 9 9 ' 10 10 11 11 j ' 12 12 h i ' 13 13 < D ��)a 1 . If 14 14AP YAP tnCR." �a�✓ ' 15 15 16 16 ' 17 17 !- 18 18 19 19 %OIL t.O y R" ,'Pht zo zo NOTES {...........^.........j..:. . .........�G.a..,.......5,?,.'....... .c........ ... tiC,:! .1.iC,.. .. ?�.. ..%r!... %.�lCi�......... v..SX,.' � ....Nr......... a....1. ....................... ..��. ......:.ifMC.: ........ .. ��:::..5 �........... �' . �..... l IL \ .: �'C�. � '......... :.` i r �ct:l.. sl........... ``..... �...i..... _. a.c ... .� .0 ._..... t ........n (a�.... )... �,.7............ », SEDIMENT CORING LOG PROJECT)SURVEY ^ t��iTtJ,rY'Y1- t�ti(ll'1ao, DATE 1 ?(,)C7$ PROJECTMANAGER RECORDER .Gc.!lIL.; �G'.r' srnnD M DATUM NAD83 LATITUDE 6. 4 416 4 LONGITUDE 1HI1O 1K. WATERDEPTHIFT) TIOEIPT) MLLW(FTI-WATER DEPTH•71DE SAP DEPTHIFT) TARGET CORE LENGTH (FT)(SAP DEPTH:MLL FINAL CORE ��LENGTH (FTI PENETRATION(FT) CORE LENGTH COLLECTED FOR ANALYSIS IF COREDIAMETERIINI 1 112 ATTEMPT 1 of TIMESTARTED TIMEFINISHED DEP.(FT) DEP.(FT) SEDIMENTTYPE ODOR COLOR HUE VALUE,CHROMA SAMPLE ID DY DEPTH MISC — .Lt � 2 2 Cr 3 3 }�fB✓� 4 4 GM.,A{,en iJIW • Lim i,�, 5 6 �evniS S - 1 Sn 7 7 6 l 8 8 10 10 11 11 12 12(Z,l tSSt 13 13 ��L41�'(� QV 14 14 16 16 16 16 17 17 & se-c 18 18'A� �' ( l b'. 19 19 &� 20 20 1 I I i SEDIMENT CORING LOG y- moI�-r4v l SuotP ,1V J3WA:�TIELIDS k&C.�'N I LV\ { •- PROJECTISURVEY I\3 e uo r oa. S'l, r�C.+ DATE I 12L,106 PROJECT MANAGER �J .c�'L-Ln`�•l�•l4?.)� RECORDER (• . ;_>L.L(Lt�1i STATION ID YY1P- NAY DATUM NAD83 LATITUDE 33° 3�•5��' n1 LONGITUDE 11-409'-312 � WATER DEPTH (FT) TIOE(FTI MLLW(FT)-WATER DEPTH -TIDE SAP DEPTH IFT) TARGET CORE LENGTH (FT)(SAP DEPTH- MLL FINAL CORE LENGTH(FTI PENETRATIONOT) CORE LENGTH COLLECTED FOR ANALYSIS IF rxl CORE DIAMETER (IN) ATTEMPT 1 TIME STARTED l5�( o TIMEFINISHED lo?x' 1112 of SEDIMENTTYPE ODOR COLOR (HUE VALUE/CHROMA) SAMPLE ID BY DEPTH MISC m u3� 1 — 14 .2 - 2.6 ✓/b16d<f vUoll"k J tt .Nzvl) 4 4 6 6 7 "�D ✓rltSSr� 8 8S 9 J7 9 10 10 11 11 { S ,viI r 12 12 13 13 f I 14 14 15 15IA (/a �Jr 01�A1. U 16 16 +tiJ ., 17 17 18 18 19 19 20 20 v11 1 L, Ill s SEDIMENT CORING LOG vj PftOJECTISURVEY Mart �o DATE PROJECT MANAGER RECORDER .S.G-avcue r -r, STATIONID MF- NAVOATUM LATITUDE NAD83 -5-50 &.51o' lJ LONGITUDE tl.4 °SS. WATER DEPTH IFTI TIDE (PTI MLLW(FT)-WATER DEPTH -TIDE SAPDEPTHIFT) TARGET CORE LENGTH IFTI IBM UEPTH•MLL FINAL CORE LENGTH IFTI PENETRATIONIFTI CORE LENGTH COLLECTED FOR ANALYSIS IF CORE DIAMETERIINI 1112 ATTEMPT TIME I of 1 STARTED 1040 TIMEFINISHED DEP.(FT) DEPAPT) SEDIMERTTYPE ODOR COLOR (TRUE VALUFJCHROMA SAMPLER) 13YDEPTH MISC 1 1 �Q11 ire. i46D�5e�! {YU5511LrJ�pperbu 2 2 10M S-S 3 3 4 4 IMP 5 5 6 6 7 7 9 9 ILdA .dG 10 10 11 11 mP 12 12 13 13 'aj 14 14 0 QL 15 15 I C4.1 If 1`14A 16 16 17 17 1 18 18 19 19 20 20 V .... I ......................... r............... .................... w......... ..................... I ....... ..... ............... .. i...... w...... .................................................. ............. I............ Iw............... I .... .......... I. ......... ............ w.......... u.u......u........ M............ w..... .,.... .................. .... ........ 1...w............................. .w....... x.............................u............................... u ......... ...................... I 11 11 I 1 1 1 1 Nsvcr�aa?aAlu� SEDIMENT CORING LOG I [1 1 i 1 I I LI PROJECTISURVEY DATE b PROJ TMANAGER RECOA R STATIOHAV NID MP WATER DEP�H (FTl iu TIDE r b DATUM NAD83 q v LATITUDE 33 MLLW(FTI=WATER DEPTH •TIDE -f- - O LONGITUDE ) 1 7 S. (o4 SAPDEP H FT) TARGET CORE LENGTH( (SAP DEPTH-MLL FINAL CORE LENGTH IFT) PENETRATIONWTI CORE LENGTH COLLECTED FOR ANALYSIS( CORE DIAMETER(IN) 1112 ATTEMPT of TIMESTARTEO n r �'o TIME FINIEHED DEP.(FT) DEP.(FT) SEDIMENTTYPE ODOR COLOR (HUE VALUEICHROMA) SAMPLEID BYDEPTH WIN; 1 1 ( i 2 2 ��.. 3 3 i 4 4 5 5 ,6 6 7 7 8 8 9 9 10 10 11 11 12 12 13 13 14 14 15 15 16 16 17 17 18 18 19 19 20 20 (�V ICJ r..r...................... r.rrr.rr.....r.............r......r.....................r.r..................r............—.....n.............x.........................n..m...rrrrwu..............x.........r.... rr.r rrr .x.xx.x.--...rx..x.rx.rx.r.x.n..r......r.............x............................................. x.x....x...rr..x...x.x.xxr........xx..xrxxxxx...xx.xxx.......... xxxx.xxrrxr. 1�T13�C/Tr11nLlU6 SEDIMENT CORING LOG ' r t PROJECTISURVEY DATE 12 •- g - 0 8 PROJECTMANAGER RECORDF �,,,-� I/Q�"L.JF,�yT' STATIONID Yn P - l a NAV DATUM NAD83 LATITUDE 2, 7i� 5 ZS LONGITUDE 117 Ste. WATERDEPTH(FT) -3 TIDB(FTI -(•b MLLWIFT)• WATER DEPTH -TIDE 14.( SAPDEPTH(FT) 1H.S TAR GET CORE LENGTH(FTI(SAP DEPTH • SILL In, FINAL CORE LENGTH (FT) 9'•o PENETRATIONIFT) ;Z•o CORE LENGTH COLLECTED FOR ANALYSIS IF &S.v (7.7 CORE DIAMETER/WI 1112 ATTEMPT Of TIMESTARTED TIMEFINISHED ' DEP.(Fi) OEP.(FT) SEDIMENTTYPE ODOR C (HUE VALUEICHROMA) SAMPLEIDBYDEPTH MISC 1 rMJ 2 2 �(L 3 3 4 4 t,) J b b 6 6 7 7 8 8 �jll-FEI ��Lt LAgi' '�1 tv�i�.e.✓ -- �1`-Q,l C DO. 9 9 10 10 11 11 11 2 12 13 13 14 14 15 15 16 16 17 17 18 18 E2O20 19 n�ma ............»....................... «.......... »................ ............ ..... ............. ».... ............ .«..... »»............... «.... »..».»..»..».......... .......... »... »....w......... »» »...».....»»..... ..»..... ......... «».»........... oo.......00u.».............. »... .»1..».... »..... »»»........ »....... »o......»........»......... ...»........ ».... ..»............. ....... .».... ................ »...».».......... ..... ... .».»...»...... ..«nwn».»u.n..»»u......»... u.......... b»...».n»u»»»»....... ...Pn...»»»u...»....«........».............»........................»....»».».».»»»n..».»A..«......... 7�7>=WF1LI.US SEDIMENT CORING LOG PROJECTISURVEY DATE !r,•ovil,,t�, PROJECT MANAGER RECORDER (/9 STATION ID NAV WATER 01 PTHIFT) _ TIDE TARGET GORE LENGTH(FT)(SAP DEPTH- MLL FINALCORE_LE�NNGGlTH(FT) • O CORE Of 1 112 DATUM NAD83 (FT) 0.0 -7• V ATTEMPT Of LATITUDE MLLWIFTI^ WATER DEP TIDE �' PENETRATION(FTI `` 4 Q o .V TIMESTARTED - LONGITUDE 117. SAPDEPTH I,�FTI 'J1-r� CORE LENGTH COLLECTED FOR ANALYSISIFT -1, b TIME FINISHED OEP.(FI) DEP.(FT) SEDIMENTTYPE ODOR COLOR (HUF VALUEICHROMA) SAMPLE ID BY DEPTH MISC 2 2 ra�`� mp Il o 3 3 1 4 4 5 5 <A 6 6 GO - r �` 7 7 8 8 9 9 10 10 11 11 12 12 13 13 14 F15 15 16 17 17 18 18 19 19 20 20 ............................................,.,,.............................................................................................................................. _.... -...............................,,,.,...........,,.........,......,..........._.................,........._.,..._..............,..,..............._..._.........",.....,."._....,....,....................,.. . .... .................. ....... ................. ........ ... ................................ ........... ................ ....... .............. .......... ........ ........ ....... .,.... ................,,.,....,.....,.,,..............,.,..., ............................... ........................... ...... ........ .................. ,...... ............ _.............. ...,,........................ ........ .......................... ....................... I ...... I ............... - . NWAI3LDS SEDIMENT CORING LOG ' U PROJECTISURVEY ,,M A-. DATE PROJECT MANAGERRCOR &Jib � STATION ID NAV Vl'1 Q -12 DATUM NAD83 LATITUDE LONGITUDE WATERDEPTH(FT) TIDE(FT) MLLWIPTI-WATERDEPFH.TIDE LI .5 SAPDEPTHIFT) TARGET CORE LENGTH IFTI(SAP DEPTH•MLL ul--Azr l3 FIHAI. CORE LE-NNGTHIFT) 4 PENETRATION(FT) j CORE LENGTH COLLECTEDFOR ANALYSIS IF CORPOIAMETERANI 1 112 ATTEMPT of TIMESTARTED ' TIMEFINISHED FW DEP.(FT) DEP.{PT) SEDIMERTTYPE ODOR COLOR RRIM VV�ALUFJCHROMA) SAMPLE ID BY DEPTH MISC 2 2 ' aA (L 3 3 T Vey" 4 4) 5 5 jet-tJ 6 6 e', 7 7 � 4 8 8 'dv 9 9 10 10 S 11 11 12 12 13 13 14 14 15 15 16 16 17 17 18 18 19 19 20 20 NOTES .»..».»»«....., w....,»........... ...... ......... ....».,.....„................................................... ......,..............................................»»...«...«.......«................. ........ .... .«»... ..,,.....,»...»..,.».».................................................... .............. .............. ............ ... .................... .... ............ w..................... ............................ »........... ...... ...... .....,..«..............................,....»......................,.,...,....,.................,....»,..,.....................................................,,,...,......,...................«.............................»... ' ..»..»»..»...,..«».»»»..»,... »... .............. ..................... ........ »»............. «.».».....»»..»,...»...... ..... .......... ............ ................ ,.......... .............. ».......... ....».......» J,zJr W r-AJ=L.11 E; SEDIMENT CORING LOG PROJECTISURVEYWAAi/4,_ � DATE 0 PROJ£ ANAGER REC DER STATION ID NAVDATUM TID TARGET CORE LENGTH IFT)ISAP DEPTH- Li FINALC CORE DIAMETER ON) 1 112 NAD83 (FT) t. RO ELEN 1H(FT) ATTEMPT .b Of LAT�7W �Z�2� MLLATER OEPTH•TIDE PEW AND TIME STARTED LONGITUDE .3�WATERDEPTHIFT) SAP DEP (FT) .� CORE LENGTH COLLECTED FOR ANALYSISIFT TIME FINISHED DEP.(FT) DERIFT) SEOIMENI'TYPE ODOR COLOR (HUE_VALUEICHROMA) SAMPLEIDSYDEPTH MISC 1 1 4 3 3� % 4 4 5 5 J(� Or52 j�Y� P b?� L. 6 6 1 7 7 8 8 9 9 10 10 11 11 12 12 13 13 14 14 15 15 16 16 17 17 18 18 19 19 20 20 k�x Lra uE SEDIMENT CORING LOG ' D I PROJECTISURVEY 1'r OAlka. ,4&L, DATE Iz o$ PROJECTM DER RECO OER 1wc STATIONIO NAY m,P DATUM NAD83 LATITUDE LONGITUDE WATERDEPTH(FT) ' TIDE(FT)' I S MLLWIFT)aINATT RDEPTH41DE SS SAPDE fH(FT) C TARGET CORE LENGTH (PT)(SAP DEPTH • MU FINALCORE LENGTH(FT) S PENETRATION(FT) l CORE LENGTH COLLECTED FORANALYSISIFI COREDIAMETERAH) 1 112 ATTEMPT Of TIMESTARTED TIkEFINISHED DEP.(F7) DEP.(FT) SEDIMENT7YPE ODOR COLOR NUE YALUEICHIIOMA) SAMPLE ID EYDEPTH MISC 2 2 `� s s p u I"1 3 4 4 5 6 6 1 7 8 r7 8 9 9 10 10 11 11 12 12 13 13 14 14 15 15 16 16 17 17 18 18 19 19 20 20 ................................................w............. ................. ........ .................................................... ............................. ..... .......... ........ . x........ n...... ............ .................... ............n..wn.................n.n............. ......................... w....nn................. .....4u..b.................... uu....................... .,.......ntl........ vu....................... ................... ..........................................................................................................................................................b.................................................................4........... j�7�W�1lLJ.)S SEDIMENT CORING LOG PROJECTISURVEY DATE g" PROJECT GER RECC ER G STATIONID NAV 0/1 Q t!!� WATER DEPTHIFT) TIDE(FT) S .S DATUM NAD83 - .1 LATITUDE 3s 36. S'j MLLW(FT)=WATER DEPTH -TIDE 6• LONGITUDE 1 I SS•�a�� SAP DEPTH(FT) ► -s TARGET CORE LENGTH (FT) (SAP DEPTH•MLL FINAL CORE DIAMETER (IN) 11/2 CORE LENGTH(FTI r,b ATTEMPT I of PENETRATIONIFTI ( •S TIMESTARTED 330 CORE LENGTH COLLECTED FOR ANALYSIS IF* S. TIMEFINISHED DEP.(FT) DEP.(FT) SEDIMENTTYPE ODOR COLOR (HUE VALUEICHROMA) SAMPLEIDDYDEPTH MISC 2 2 3 3 4 4 If 11 5 5 <,q 6 6 7 7 g 9 1D 10 11 11 12 12 13 13 14 14 15 15 16 16 17 E1917 18 19 20 20 HY�t> ................................................ ....................... ........................ ................................................. _....... .............. ,....................... I ...... ........ .............................................. ............. _................ ............................... _............. _..... ,............................ ,.,............. _...................... ..................... .... .... I.................................. .............. ................ ....,.,....................... ,............................ ..... _._.... ..................... .................. ............. ....... I ............................ , Nfi.Vir.L 'T SEDIMENT CORING LOG ' PROJECTISURVEY O P� (L DATE PROJEC MANAGER RECORDER n ( NAVDATUM1 bTAT10NID mp�166 NAD83 IAmuD3� �5�! LaxclrlD55.?✓-Z , WA7EROEPTR IFTI n L�(. TIDEMFTI MLLWIPTI^WATER DEPTH -TICS SAP DEPTH(FT) ' TMG CORE LENGT IFTIISAPOEPTH•MLL FINAL CORELEN67HIFTI PENETRATIONITI CORE LENGTH COLLECTED FORANALYSISIF COREDIAMETER() ATTEMPT TIMESTARTED 1 1/2 of TIMEFINISHED SAMPLE 10 DY DEPTH COLOR DEP4PT) DEP4FT) SEDIMENTTYPE ODOR HUEVALUFJCNROMA 1 1 ) MISC 2 2t A '^ 3 3 V „ 4 4 , ij ' J/ 5 5 i 6 6 , 7 7 ("UQdS•�- 1 1 8 8 l 4 r9 ' 10 10 11 11 12 12 ' 13 13 14 14 15 15 ' 18 16 17 17 , 18 18 E20 , 19 19 t 20 NOTES w........... ......«.«...«.«.W. .¢YMLTnI««. (1.,.r,1.Gw��,.. ....u«..«... «....«........4F..J?»IfN` .m,,. ... /.m.T•.�ry.. .Y.Y1d1C�w.R.'..`^..••«.'w"..' ............. «.».«.«.«.w.«..« «w...«.««.....««w.«........«.....o ' ................1.....««.... ........ •oo......................... ..«....«... «.o».uopu««0ouo««o««. ................. «.w...«..........w.«..«.«...w..........................................000...................«....«...........w........«..«.............«.w........................................««........«o...a........... .............w.«.«.w«e.n...»..e«..o...«..«..........« ...... .w.,«« ... ... ' o «««« 0 ft. (+7 ft. MLLW) 8 ft. (-1 ft. MLLW) 14 ft. (-9 ft. MLLW) 2 ft. (+5 ft. MLLW) 10 ft. (-3 ft. MLLW) 16 ft. (-11 ft. MLLW) MP-1 4 ft. (+3 ft. MLLW) 6 ft. 8 ft. (+1 ft. MLLW) (+1 ft. MLLW) 18 ft. (-13 ft. MLLW) 12 ft. (-6 ft. MLLW) 20 ft. (-15 ft. MLLW) (MIIW 'u 9L-) (MIIW 'u £l-) (MIIW 'u l l ) 'u oz 'u e� u e� :.f WIWI .4 L-) (MIIW 'u 4-) ua� 'uN (MIIW .0 l6 ) 49 aldmuS oK (MIIW 'u l+) uv (MIIW 'u 6-) (MIIW 'u L-) urn 4ZI ologd ou `ajduieS (MIIW 'u £-) (MIIW 'u l ) Ile 'lie (MIIW 'u £+) (MIIW .0 9+) uz 110 aidmus oK W7- 0 ft. 2 ft. (+5 ft. MLLW) (+3 ft. MLLW) 6 ft. (-1 ft. MLLW) 8 ft. (-3 ft. MLLW) MP-3 12 ft. 14 ft. 16 ft. (-7 ft. MLLW) (-9 ft. MLLW) (-11 ft. MLLW) Sample, no photo 4ft. 6ft. (+1 ft. MLLW) (-11 ft. MLLW) 10 ft. (-5 ft. MLLW) 18 ft. (-13 ft. MLLW) 12 ft. (-7 ft. MLLW) 20 ft. (-15 ft. MLLW) (MIIW '1J 90 (MIIW '14 £l-) (MIIW .0 6 H (MIIW 116-) (MIIW IJ L-) '4 OZ 'lJ 8l u 9L 'lj bl 'll U F. (MIIW 11 L-) (MIIW '8 9-) (MIIW 'li E ) 8ZL uOl 1;8 (MlIA'U (MIIW .34 b 6-) (MIIW .8 6+) (MIIW 'u E+) (WIN _0 9+) 'u9 11h 'uZ 110 tb-d W m= r m i r===== m = = � m m m MP-5 Oft. 2ft. 4ft. 6ft. (+5 ft. MLLW) (+3 ft. MLLW) (+1 ft. MLLW) (-11 ft. MLLW) 6 ft. g ft. 10 ft. (-1 ft. MLLW) (-3 ft. MLLW) (-5 ft. MLLW) 12 ft. (-7 ft. MLLW) 12 ft. 14 ft. (-7 ft. MLLW) 16 ft. 18 ft. 20 ft. (-9 ft. MLLW) (-11 ft. MLLW) (-13 ft. MLLW) (-15 ft. MLLW) (Mllw 'u E L-) u9L u9L (Mllw 'u 6-) li 4L (Mllw Vu L-) 1) ZI Mllw .1) L-) (WIN A 9-) (Mllw .)4 £) (Mllw 'u L-) uZL uOL 49 u9 (Mllw'u L) (MIIw')j L+) 14 9 u 4 (milvq,lj Z E+) (MIIW 'u S+) u0 e9-d W 0 ft. (+7 ft. MLLW) 2 ft. (+5 ft. MLLW) 8 ft. (-1 ft. MLLW) 10 ft. (-3 ft. MLLW) A' •• 4 ft. (+3 ft. MLLW) 12 ft. (-5 ft. MLLW) 6 ft. (+1ft. MLLW) 14 ft. (-7 ft. MLLW) 41 6 j` 'l 14 ft. 16 ft. 18 ft. 20 ft. (-9 ft. MLLW) (-11 ft. MLLW) (-13 ft. MLLW) (-15 ft. MLLW) 8 ft. (-1 ft. MLLW) (MII" 'u bL-) (MIIW 'u Z1 ) '14 9 L 491 (MIIW '1; OH 'a bL (MII W '14 9-) 4ZL (MIIW '11 H (MIIW '1; Z-) (MIIW Ii 8-) _0 9 'N 9 l; ZL (MIIW 'll 9-) SOL (MIIW '11 Z-) (MIIW ')10) (MIIW 'u Z+) (MIIW 11 ti+) 149 ')117 .0Z I10 L-d W mm 0 ft. 2 ft. 4 ft. 6 ft. (+5 ft. MLLW) (+3 ft. MLLW) (+1 ft. MLLW) (-1 ft. MLLW) Eft. 8ft. 10ft. 12ft. (-1 ft. MLLW) (-3 ft. MLLW) (-5 ft. MLLW) (-7 ft. MLLW) �V a: 12ft. 14ft. 16ft. 18ft. (-9 ft. MLLW) (-11 ft. MLLW) (-13 ft. MLLW) (-15 ft. MLLW) (MIIW '8 9'9-) (MIIW '8 S'L-) (MIIW '8 9'6-) (AM IW '13 Sl l ) '110 '11 Z li b 11 9 (MIIW I10'S-) '4 0 (WIN .0 b-) 10 (MIIW 80'L-) 11 7 (MIIW '8 9-) 'u z VVdW Z6-dW (MIIW ')48-) 'a 17 06-dW (MI -IN '110'6-) 'a r (MIIW -8 OH '119 (MIIW'110'6l ) '119 (MIIW '8 Zl-) 'u 9 � m m i m m m = ! t r m m m m m S = r (-13.5 ft. MLLW) MP-11 MP-13 2 ft. 0 ft. 6 ft. 4 ft. (-14.3 ft. MLLW) (-12.3 ft. MLLW) (-10.3 ft. MLLW) (-8.3 ft. MLLW) MP-15 6 ft. 4 ft. (-12.6 ft. MLLW) (-10.6 ft. MLLW) 2 ft. 0 ft. (-8.6 ft. MLLW) (-6.6 ft. MLLW) (MIIW '116-) (MIIW 'B l l) (MIIW .0 66-) li 'u9 49 (MIIW '8 S-) (MIIW 'u L-) (MIIW '8 6-) u0 uZ ub 9 6-M I I I I J 1 1 I [] 1 I Appendix B Chemistry Data Newfields Northwest Marina Park Apparent Grain Size Distribution Summary Percent Finer Than Indicated Size Sample No. Gravel Very Coarse Sand Coarse Sand Medium Sand Fine Sand Very Fine Sand Sill Clay Phi Size -3 -2 -1 0 1 2 3 4 5 6 7 8 9 10 Sieve Size microns 3f8„ #10 2000 #18 1000 #35 500 #60 250 #120 126) #230 62 31.00 15.60 7.80 3.90 200 1.00 REF-05 100.0 100.0 99.9 99.7 99.4 98.9 98.1 94.3 73.3 57.2 42.7 33A 28.2 17.7 REF-05 100.0 100.0 99.7 99.5 99.1 98.5 97.7 93.9 80.7 58.9 42.8 33.5 28.4 17.8 REF-05 100.0 100.0 100.0 99.6 99.3 98.7 97.9 93.8 76.8 58A 43.0 33.6 28A 17.9 COMP A-U 100.0 99.6 97.8 91.6 76.0 48.4 16.2 4.2 2.9 2.4 2.1 1.6 1.4 COMP A-L 100.0 98.3 90.4 69.8 31.1 4.7 1.1 0.7 NA NA NA NA NA COMP 100.0 99.9 97.7 90.5 71.9 40.5 14.6 4.2 2.5 2.1 1.8 1.5 1.3 NEN p COMP B-L 100.0 99.0 94.a81.5 56.2 25.6 8.2 1.1 NA NA NA NA NA Notes to the Testing: 1. Organic matter was not removed prior to testing, thus the reported values are the "apparent" grain size distribution. See narrative for discussion of the testing. OC80 Newfields Northwest Marina Park Apparent Grain Size Distribution Summary Percent Retained in Each Size Fraction Sample No. Gravel Very Coarse Sand Coarse Sand Medium Sand Fine Sand Very Fine Sand Coarse Silt Medium Sift Fine Silt Very Fine Silt Clay Total Fines Phi Size >-1 -1 too Oto1 1to2 2to3 3to4 4to5 5to6 6to7 7to8 8to9 9to 10 <10 <4 Sieve Size (microns) >910 (2000) 101018 (z66o-1b96) 18-35 (1000-500) 35-60 (506-250) 60.120 (256-125) 12A-230 (125-62) 62. 31.0 31.0g5.6 �5A67.8 7.8-3.9 3.9-2.0 20.L0 <1.0 � (wz) REF-05 0.1 0.2 0.3 0.5 0.8 3.8 21.0 16.1 14.6 9.3 5.1 10.6 17.7 94.3 REF-05 1 0.3 1 0.2 1 0.3 1 0.6 1 0.8 1 3.9 13.2 1 21.8 1 16.2 1 9.3 1 5.0 10.6 17.8 93.9 REF-05 0.0 1 0.4 1 0.3 0.6 1 0.8 1 4.1 17.0 18.4 15.4 9.4 5.3 10.4 17.9 93.8 COMP A•U 2.2 6.2 15.6 27.7 32.2 12.0 1.3 0.4 0.4 0.4 0.2 0.5 0.9 4.2 COMP A-L 9.6 20 6 38.7 26.4- 3.7 1 0.4 -1 NA I NA I NA NA NA NA NA 0.7 COMP &U 2.3 7.3 18.6 31.3 26.0 10.4 1.7 0.3 0.3 0.3 0.2 0.3 1.0 4.2 COMP B-L 5.2 13.2 25.3 30.6 1 17_4 1 7.1 1 NA I NA I NA I NA I NA I NA I NA 1.1 Notes to the Testing: 1. Organic matter was not removed prior to testing, thus the reported values are the 'apparent' grain size distribution. See narrative for discussion of the testing. OC80 QASUMMARY Client: Newfields Northwest Project No.: Manna Park ARI Trip. Sample ID: OB99C Batch No.: OC80-1 Client Trip. Sample ID: REF-05 Page: 1 of 1 Rolafiva SlandaM rlovialinn R. Phi Sivc Sample ID -3 -2 -1 0 1 2 3 4 5 6 7 8 9 10 REF-05 100.0 100.0 99.9 99.7 99.4 98.9 98.1 94.3 73.3 57.2 42.7 33A 28.2 17.7 REF-05 100.0 100.0 99.7 99.5 99.1 98.5 97.7 93.9 80.7 58.9 42.8 33.5 28.4 17.8 REF-05 100.0 100.0 100.0 99.6 99.3 98.7 97.9 93.8 76.8 58.4 43.0 33.6 28A 17.9 AVE NA 100.00 99.86 i 99.61 99.29 98.72 97.91 94.00 76.93 58.16 42.80 33.48 2834 17.81 STDEV NA 0.00 0.18 0.13 0.15 0.18 0.18 0.29 3.70 0.87 0.17 0.14 0.10 0.12 %RSO NA 0.00 0.18 0.13 0.15 0.18 0.18 0.31 4.81 1.49 0.39 0.41 0.36 0.70 The TrinU-ln Cnnliae Tn Th. Fnllnwinn Camnlac Client ID Date Sampled Date Extracted Dale Complete QA Ratio (95-105) Data Qualifiers Pipette Portion (5.0- 25.0 REF-05 12/212008 12111/2008 12/2412008 99.2 148 REF-05 12/212008 12M 112008 1212412008 100.0 14.6 REF-05 ` 1212/2008 1211112008 12/24/2008 100.3 14.7 COMP A-U 12/5/2008 12112/2008 1212412008 100.5 6.5 COMP A-L 1215/2008 12/1212008 12124/2008 100.1 SS 0.9 COMP B-U 12/5/2008 12/12/2008 1212412008 100.8 5.4 COMP 5-L 12/5/2008 12112/2008 12/24/2008 99.1 SS 2.5 ARI Internal QA limits = 95-105 Notes to the Testing: 1. Organic matter was not removed prior to testing, thus the reported values are the "apparent" grain size distribution. See narrative for discussion of the testing. OC80 PSEP Grain Size Distribution Triplicate Sample Plot GRAVEL SAND SILT CLAY 100 90 80 70 60 m m 50 m 40 ' 30 20 10 M71 0 10000 1000 100 10 1 Particle Diameter (microns) -+-REF-05 -♦-REF-05 -*-REF-05 M PSEP Grain Size Distribution GRAVEL SAND SILT CLAY 100 so eo 70 so m 'n m Sll ,�.. T 3 m 40 ' 30 20 10 .0 10000 1000 100 10 1 Particle Diameter (microns) +COMP A-U COMP A-L --t—COMP B-U—o--COMP B-L I Newflelds Northwest Marina Park Atterberg Limits 80 7o 60 x CH or OH d 50 40 v a+ U) 30 fi MH or OH 20 CL or OL X 10 1 Lldd�� ML or OL 0 0 20 40 60 80 100 Liquid Limit �COMPA-U ♦COMPA-L ■ COMP B-U 000MPBL Sample Identification Plasticity Index Liquid Limit Plastic Limit USCS COMP A-U NA NA NA Non -Plastic COMP A-L NA NA NA Non -Plastic COMP B-U NA NA NA Non -Plastic COMP B-L NA NA NA Non -Plastic — • e ' SAMPLE RESULTS-CONVENTIONALS OC80-Newfields Northwest ' Matrix: Sediment Project: MARINA PARK Data Release Authorizedir Event: NA Reported: 01/02/09 11 Date Sampled: Date Received: 11/26/08 12/05/08 ' Client ID: COMP A-U ARI ID: 08-32709 OC80A Analy Date Method Units RL ' Total Solids 12/08/08 EPA 160.3 '120808#3 Preserved Total Solids 12/09/08 EPA 160.3 120908#2 ' N-Ammonia 12/11/08 EPA 350.1M 121108#1 Sulfide 12/08/08 EPA 376.2 ' 120808#1 Total Organic Carbon 12/11/08 Plumb,1981 121108#1 HEM Oil & Grease 12/30/08 9071 B 123008#1 ' HEM-ST NP Oil & Grease 12/30/08 9071 B HEM Polar Oil & Grease 12/30/08 9071 B ' RL Analytical reporting limit U Undetected at reported detection limit ' 2N KC1 extracts. Ammonia determined on 1 Soil Sample Report-OC80 ANALYTICAL RESOURCES INCORPORATED Sample Percent 0.01 84.60 Percent 0.01 82.80 mg-N/kg 0.12 1.20 mg/kg 1.18 7.56 Percent 0.020 0.151 mg/kg 230 < 230 U mg/kg 230 < 230 U mg/kg 230 < 230 U SAMPLE RESULTS-CONVENTIONALS OC80-New£ields Northwest Matrix: Sediment O Project: MARINA PARK Data Release Authorized Event: NA Reported: 01/02/09 Date Sampled: 11/26/08 Date Rgceived: 12/05/08 Client ID: COMP A-L ARI ID: 08-32710 OC80B Analyte Date Method Units RL Total Solids 12/08/08 EPA 160.3 Percent 0.01 120808#3 Preserved Total Solids 12/09/08 EPA 160.3 Percent 0.01 120908#2 N-Ammonia 12/11/08 EPA 350.1M mg-N/kg 0.11 121108#1 Sulfide 12/08/08 EPA 376.2 mg/kg 1.20 120808#1 Total Organic Carbon 12/11/08 Plumb,1981 Percent 0.020 121108#1 HEM Oil s Grease 12/30/08 9071 B mg/kg 215 123008#1 HEM-ST NP Oil 6 Grease 12/30/08 9071 B mg/kg 215 HEM Polar Oil s Grease 12/30/08 9071 B mg/kg 215 RL Analytical reporting limit U Undetected at reported detection limit Ammonia determined on 2N KC1 extracts. ANALYTICAL RESOURCEs( INCORPORATED 1 1 Sample t 90.30 82.00 ! < 0.11 U ' { i < 1.20 U ' 0.076ii < 215 U I i i < 215 U , < 215 U i 4 t i 4 I Soil Sample Report-OC80 SAMPLE RESULTS-CONVENTIONALS OC80-Newfields Northwest ' Matrix: Sediment nJ(J� Project: MARINA PARK Data Release Authorized Event: NA Reported: 01/02/09 UU Date Sampled: Date Received: 11/26/08 12/05/08 Client ID: COMP B-U ARI ID: 08-32711 OC80C Analyte Date Method Units RL ' Total Solids 12/08/08 EPA 160.3 '120808#3 Preserved Total Solids 12/09/08 EPA 160.3 120908#2 ' N-Ammonia 12/11/08 EPA 350.1M 121108#1 Sulfide 12/08/08 EPA 376.2 ' 120808#1 Total Organic Carbon 12/11/08 Plumb,1981 121108#1 HEM Oil & Grease 12/30/08 9071 B 123008#1 ' HEM-ST NP Oil & Grease 12/30/08 9071 B HEM Polar Oil & Grease 12/30/08 9071 B RL Analytical reporting limit U Undetected at reported detection limit determined on 2N KC1 extracts. Ammonia Soil Sample Report-OC80 ANALYTICAL RESOURCES INCORPORATED Sample Percent 0.01 89.30 Percent 0.01 83.60 mg-N/kg 0.10 0.17 mg/kg 1.16 < 1.16 U Percent 0.020 0.055 mg/kg 218 < 218 U mg/kg 218 < 218 U mg/kg 218 < 218 U SAMPLE RESULTS-CONVENTIONALS OC80-Newfields Northwest Matrix: Sediment r,�% Project: MARINA PARK Data Release Authorized AUlIV1 Event: NA Reported: 01/02/09 Y Date Sampled: 11/26/08 Date Received: 12/05/08 Client ID: COMP B-L ARI ID: 08-32712 OC80D Analyte Date Method Units RL Total Solids 12/08/08 EPA 160.3 Percent 0.01 120808113 Preserved Total Solids 12/09/08 EPA 160.3 Percent 0.01 120908#2 N-Ammonia 12/11/08 EPA 350.1M mg-N/kg 0.10 121108#1 Sulfide 12/08/08 EPA 376.2 mg/kg 1.15 120808#1 Total Organic Carbon 12/11/08 Plumb,1981 Percent 0.020 121108#1 HEM Oil & Grease 12/30/08 9071 B mg/kg 226 123008#1 HEM-ST NP Oil & Grease 12/30/08 9071 B mg/kg 226 HEM Polar Oil & Grease 12/30/08 9071 B mg/kg 226 RL Analytical reporting limit U Undetected at reported detection limit Ammonia determined on 2N KC1 extracts. ANALYTICAL , RESOURCES* INCORPORATED i Sample 86.60 , 85.70 ' < 0.10 U , 9.25 0.071 i I < 226 U i < 226 U f < 226 U 1 I t Soil Sample Report-OC80 ' METHOD BLANK RESULTS-CONVENTIONALS OC80-Newfields Northwest Matrix: Sediment ' Data Release Authorized Reported: 01/02/09 ' Analyte ' Total Solids Preserved Total Solids ' N-Ammonia 'Sulfide Total Organic Carbon ' HEM Oil & Grease 1 Project: MARINA PARK Event: NA Date Sampled: NA Date Received: NA Date Units Blank 12/08/08 Percent < 0.01 U 12/09/08 Percent < 0.01 U 12/11/08 mg-N/kg < 0.10 U 12/11/08 < 0.10 U 12/08/08 mg/kg < 1.00 U 12/11/08 Percent < 0.020 U 12/30/08 mg/kg 260 ANALYTICAL RESOURCES INCORPORATED ' Soil Method Blank Report-OC80 Matrix: Sediment Data Release Authorized Reported: 01/02/09 Analyte LAB CONTROL RESULTS-CONVENTXONALS ANALYTICAL OC80-Newfields Northwest RESOURCES Date Unite INCORPORATED ' 1 Project: MARINA PARK Event: Date Sampled: NA NA ' bate Received: NA Spike ' LCS Added Recovery i Sulfide 12/08/08 mg/kg 119 114 104.8% ' Total Organic Carbon 12/11/08 Percent 0.489 0.500 97.8% e �1 �I l Soil Lab Control Report-OC80 t ' ' ' STANDARD REFERENCE RESULTS-CONVENTIONALS OC80-Newfields Northwest Matrix: Sediment Project: Data Release Authorize Event: Reported: 01/02/09 Date Sampled: Date Received: Analyte/SRM ID Date Units SRM MARINA NA NA NA True Value ANALYTICAL O RESOURCES INCORPORATED PARK Recovery N-Ammonia 12/11/08 mg-N/kg 94.6 100 94.6% SPEX 28-24AS 12/11/08 102 100 102.0% Total Organic Carbon 12/11/08 Percent 3.04 3.35 90.7% ' NIST #8704 HEM Oil & Grease 12/30/08 mg/kg 8,180 8,000 102.2% ' Env. Exp. *104129 ' Soil Standard Reference Report-OC80 Matrix: Sediment Data Release Authorized Reported: 01/02/09 Analyte REPLICATE RESULTS-CONVENTIONALS OC80-Newfields Northwest �1 1J Project: Event: Date Sampled: Date Received: Date Units Sample MARINA PARK NA 11/26/08 12/05/08 Replicate(s) ANALYTICAL ® RESOURCES INCORPORATED RPD/RSD , t ARI ID: OC80A Client ID: COMP A-U ' Total Solids 12/08/08 Percent 84.60 83.90 0.6% 83.70 , Preserved Total Solids 12/09/08 Percent 82.80 83.10 0.3% B3.30 N-Ammonia 12/11/08 mg-N/kg 1.20 1.06 9.1% 1.27 12/08/08 7.56 3.00 86.4% Sulfide mg/kg Total Organic Carbon 12/11/08 Percent 0.151 0.127 15.9% 0.110 HEM Oil & Grease 12/30/08 mg/kg < 230 < 231 NA t i t r t t r 1 I Soil Replicate Report-OC80 ' ' MS/MSD RESULTS-CONVENTIONALS OC80-Newfields Northwest Matrix: Sediment Data Release Authorized: Reported: 01/02/09 Analyte Date Units Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Spike Sample Spike Added ANALYTICAL RESOURCES INCORPORATED Recovery ARI ID: OC80A Client ID: COMP A-U N-Ammonia 12/11/08 mg-N/kg 1.20 110 115 94.8% Sulfide 12/08/08 mg/kg 7.56 139 136 96.6% Total Organic Carbon 12/11/08 Percent 0.151 0.710 0.578 96.7% ' HEM Oil & Grease 12/30/08 mg/kg < 230 1,970 2,310 85.3% 1 Soil MS/MSD Report-OC80 ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP A-U Page 1 of 1 SAMPLE Lab Sample ID: OC80A QC Report No: OC80-Newfields Northwest LIMS ID: 08-32709 Project: MARINA PARK Matrix: Sediment Data Release Authorized • Date Sampled: 11/26/08 Reported: 12/17/08 Date Received: 12/05/08 Percent Total Solids: 6 .08 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte 3050B 12/10/08 6010B 12/15/08 7440-38-2 Arsenic 3050B 12/10/08 6010B 12/15/08 7440-43-9 Cadmium 3050E 12/10/08 6010B 12/15/08 7440-47-3 Chromium 3050E 12/10/08 6010B 12/15/08 7440-50-8 Copper 3050E 12/10/08 6010B 12/15/08 7439-92-1 Lead CLP 12/10/08 7471A 12/15/08 7439-97-6 Mercury 3050E 12/10/08 6010E 12/15/08 7440-02-0 Nickel 3050E 12/10/08 7740 12/15/08 7782-49-2 Selenium 3050E 12/10/08 6010B 12/15/08 7440-22-4 Silver 3050B 12/10/08 6010B 12/15/08 7440-66-6 Zinc U-Analyte undetected at given RL RL-Reporting Limit u a;;. RL mg/kg-dry Q 6 6 U 0.2 0.2 U 0.6 4.8 0.2 2.8 2 2 U 0.05 0.05 U 1 3 0.2 0.2 U 0.3 0.3 U 1 10 FORM -I ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP A-U ' Page 1 of 1 DUPLICATE Lab Sample ID: OC80A QC Report No: OC80-Newfields Northwest 'LIMS ID: 08-32109 Project: MARINA PARK Matrix: Sediment Data Release Authorize Date Sampled: 11/26/08 Reported: 12/17/08 Date Received: 12/05/08 MATRIX DUPLICATE QUALITY CONTROL REPORT ' Analysis Control Analyte Method Sample Duplicate RPD Limit 'Arsenic 6010B 6 U 6 U 0.0% Cadmium 6010B 0.2 U 0.2 U 0.0% 601011 4.8 4.9 2.1% 'Chromium Copper 6010B 2.8 2.5 11.3% Lead 6010B 2 U 2 U 0.0% Mercury 7471A 0.05 U 0.05 U 0.0% 6010B 3 2 40.0% 'Nickel Selenium 7740 0.2 U 0.2 U 0.0% Silver 6010B 0.3 U 0.3 U 0.0% ' Zinc 6010B 10 10 0.0% Reported in mg/kg-dry *-Control Limit Not Met L-RPD Invalid, Limit = Detection Limit FORM -VI ANALYTICAL RESOURCES INCORPORATED Q +/- 6 L +/- 0.2 L +/- 20% +/- 20% +/- 2 L +/- 0.05 L +/- 1 L +/- 0.2 L +/- 0.3 L +/- 20% INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sedimen Data Release Autt horize Reported: 12/17/08 80 ANALYTICAL /� RESOURCES v INCORPORATED Sample ID: COMP A-U MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 MATRIX SPIKE QUALITY CONTROL REPORT Analyte Analysis Method Sample Spike Spike Added % Recovery Q Arsenic 6010B 6 U 240 230 104% Cadmium 6010B 0.2 U 56.7 57.6 98.4% Chromium 6010B 4.8 59.4 57.6 94.8% Copper 6010B 2.8 63.4 57.6 105% Lead 6010B 2 U 229 230 99.6% Mercury 7471A 0.05 U 0.55 0.496 111% Nickel 6010B 3 58 57.6 95.5% Selenium 7740 0.2 U 12.5 11.8 106% Silver 6010B 0.3 U 61.5 57.6 107% Zinc 6010B 10 67 57.6 99.0% Reported in mg/kg-dry N-Control Limit Not Met H-% Recovery Not Applicable, Sample Concentration Too High NA -Not Applicable, Analyte Not Spiked Percent Recovery Limits: 75-125% FORM-V II INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 'Matrix: Sediment Data Release Authorize Reported: 12/17/08 Percent Total Solids: 88.6% ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 ' Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-dry Q 3050B 12/10/08 6010B 12/15/08 7440-38-2 Arsenic 6 6 U 3050B 12/10/08 6010B 12/15/08 7440-43-9 Cadmium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-47-3 Chromium 0.6 2.2 3050B 12/10/08 6010B 12/15/08 7440-50-8 Copper 0.2 1.0 3050B 12/10/08 6010B 12/15/08 7439-92-1 Lead 2 2 U CLP 12/10/08 7471A 12/15/08 7439-97-6 Mercury 0.06 0.06 U 1 U 3050B 12/10/08 6010B 12/15/08 7440-02-0 Nickel 1 3050B 12/10/08 7740 12/15/08 7782-49-2 Selenium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-22-4 Silver 0.3 1 0.3 U 6 3050E 12/10/08 6010B 12/15/08 7440-66-6 Zinc 'U-Analyte undetected at given RL RL-Reporting Limit II II II INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OC80C LIMS ID: 08-32711 Matrix: Sediment Data Release Authorize Reported: 12/17/08 Percent Total Solids: 86.8% ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 .Prep Prep Analysis Analysis Meth Date Method Date CAS Number Ahalyte RL mg/kg-dry Q 3050B 12/10/08 6010B 12/15/08 7440-38-2 3050B 12/10/08 6010B 12/15/08 7440-43-9 3050E 12/10/08 6010E 12/15/08 7440-47-3 3050B 12/10/08 6010B 12/15/08 7440-50-8 3050B 12/10/08 6010B 12/15/08 7439-92-1 CLP 12/10/08 7471A 12/15/08 7439-97-6 3050E 12/10/08 6010B 12/15/08 7440-02-0 3050B 12/10/08 7740 12/15/08 7782-49-2 3050B 12/10/08 6010B 12/15/08 7440-22-4 3050E 12/10/08 6010B 12/15/08 7440-66-6 U-Analyte undetected at given RL RL-Reporting Limit Arsenic 5 6 Cadmium 0.2 0.2 Chromium 0.5 3.8 Copper 0.2 3.7 Lead 2 5 Mercury 0.05 0.05 Nickel 1 2 Selenium 0.2 0.2 Silver 0.3 0.8 Zinc 1 11 U A FORM -I INORGANICS ANALYSIS DATA SHEET TOTAL METALS ' Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 11-32712 Matrix: Sediment Data Release Authoriz Reported: 12/17/08 Percent Total Solids: 4.0 ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-dry Q ' 3050B 12/10/08 6010B 12/15/08 7440-38-2 Arsenic 6 6 U 3050B 12/10/08 6010B 12/15/08 7440-43-9 Cadmium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-47-3 Chromium 0.6 3.2 3050B 12/10/08 6010B 12/15/08 7440-50-8 Copper 0.2 2.4 3050B 12/10/08 6010B 12/15/08 7439-92-1 Lead 2 2 U 'CLP 12/10/08 7471A 12/15/08 7439-97-6 Mercury 0.05 1 0.05 2 U 3050B 12/10/08 6010B 12/15/08 7440-02-0 Nickel 3150B 12/10/08 7740 12/15/08 7782-49-2 Selenium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-22-4 Silver 0.3 1 0.3 6 U 3050E 12/10/08 6010B 12/15/08 7440-66-6 Zinc U-Analyte undetected at given RL RL-Reporting Limit i I FORM -I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OC80MB LIMS ID: 08-32710 Matrik: Sediment Data Release Authorize Reported: 12/17/08 Percent Total Solids: NA ANALYTICAL RESOURCES® INCORPORATED Sample ID: METHOD BLANK QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-dry Q 3050E 12/10/08 6010B 12/15/08 7440-38-2 Arsenic 5 5 U 3050E 12/10/08 6010B 12/15/08 7440-43-9 Cadmium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-47-3 Chromium 0.5 0.5 U 3050B 12/10/08 6010B 12/15/08 7440-50-8 Copper 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7439-92-1 Lead 2 2 U CLP 12/10/08 7471A 12/15/08 7439-97-6 Mercury 0.05 0.05 U 3050B 12/10/08 6010E 12/15/08 7440-02-0 Nickel 1 1 U 3050B 12/10/08 7740 12/15/08 7792-49-2 Selenium 0.2 0.2 U 3050B 12/10/08 6010B 12/15/08 7440-22-4 Silver 0.3 0.3 U 3050B 12/10/08 6010B 12/15/08 7440-66-6 zinc 1 1 U U-Analyte undetected at given RL RL-Reporting Limit I ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS ' Page 1 of 1 Lab Sample ID: OC80LCS LIMS ID: 08-32710 'Matrix: Sediment Data Release Authorize Reported: 12/17/08 ' Analyte Arsenic Cadmium Chromium 'Copper Lead Mercury INickel Selenium Silver ANALYTICAL RESOURCES INCORPORATED Sample ID: LAB CONTROL QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA BLANK SPIKE QUALITY CONTROL REPORT Analysis Spike Spike Method Found Added 6010B 6010B 6010B 6010B 6010B 7471A 6010B 7740 6010B Zinc 6010B Reported in mg/kg-dry 'N-Control limit not met NA -Not Applicable, Analyte Not Spiked Control Limits: 80-120% I II II II II Recovery Q 198 200 99.0% 49.0 50.0 98.0% 46.9 50.0 93.8% 50.1 50.0 100% 200 200 100% 1.14 1.00 114% 46 50 92.0% 9 10 90.0% 54.1 50.0 108% 47 50 94.0% ' FORM-VII ANALYTICAL' RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP A-U Page 1 of 1 SAMPLE Lab Sample ID: OF16A QC Report No: OF16-Newfields Northwest LIMS ID: 08-34349 Project: MARINA PARK Matrix: Sediment i Data Release Authoriz Date Sampled: 11/26/08 Reported: 12/29/08 Date Received: 12/05/08 Percent Total Solids: 3.36 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL 3050B 12/23/08 200.8 12/26/08 7440-38-2 Arsenic U-Analyte undetected at given RL RL-Reporting Limit mg/kg-dry Q 0.2 2.0 FORM -I 1 1 INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP A-L 'Page 1 of 1 SAMPLE Lab Sample ID: OF16B QC Report No: OF16-Newfields Northwest LIMS ID: 08-31350 Project: MARINA PARK 1 Matrix: Sediment Date Sampled: 11/26/08 Data Release Authorized• Reported: 12/29/08 Date Received: 12/05/08 Percent Total Solids: 86.3% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL 3050B 12/23/08 200.8 12/26/08 7440-38-2 Arsenic U-Analyte undetected at given RL RL-Reporting Limit I 1 1 1 1 1 1 1 i 1 FORM -I ANALYTICAL RESOURCES INCORPORATED mg/kg-dry Q 0.2 2.1 ANALYTICAL /� RESOURCES V INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP B-U Page 1 of 1 SAMPLE Lab Sample ID: OF16C QC Report No: OF16-Newfields Northwest LIMS ID: 08-34351 Project: MARINA PARK Matrix: Sediment Data Release Authorize Date Sampled: 11/26/08 Reported: 12/29/08 Date Received: 12/05/08 Percent Total Solids: 87.3% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte 3050B 12/23/08 200.8 12/26/08 7440-38-2 Arsenic U-Analyte undetected at given RL RL-Reporting Limit RL mg/kg-dry 0.2 2.2 F, FORM -I ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: COMP B-L ' Page 1 of 1 SAMPLE Lab Sample ID: OF16D QC Report No: OF16-Newfields Northwest LIMS ID: 08-31352 Project: MARINA PARK Matrix: Sediment Data Release Authorize .' Date Sampled: 11/26/08 Reported: 12/29/08 Date Received: 12/05/08 ' Percent Total Solids: 85.2% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL 3050B 12/23/08 200.8 12/26/08 7440-38-2 Arsenic U-Analyte undetected at given RL RL-Reporting Limit FORM -I ANALYTICAL RESOURCES INCORPORATED mg/kg-dry Q 0.2 1.9 ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample 'ID: METHOD BLANK Page 1 of 1 Lab Sample ID: OF16MB QC Report No: OF16-Newfields Northwest LIMS ID: 08-34349 Project: MARINA PARK Matrix: Sediment Data Release Authorized Date Sampled: NA Reported: 12/29/08 Date Received: NA Percent Total Solids: Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-dry Q 3050B 12/23/08 200.8 12/26/08 7990-38-2 Arsenic 0.2 0.2 U U-Analyte undetected at given RL RL-Reporting Limit FORM -I � I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page I of 1 Lab Sample ID: OF16LCS LIMS ID: 08-34349 Matrix: Sediment Data Release Authoriz Reported: 12/29/ 01 e U, Analyte Arsenic ANALYTICAL RESOURCES# INCORPORATED Sample ID: LAB CONTROL QC Report No: OF16-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA BLANK SPIKE QUALITY CONTROL REPORT Analysis Method 200.8 Reported in mg/kg-dry N-Control limit not met NA -Not Applicable, Analyte Not spiked Control Limits: 80-120% , I I A I I I I 1 11 Spike Found 26.3 Spike % Added Recovery 25.0 105% � I FORM-VII Matrix: Sediment ' ANALYTICAL O RESOURCES INCORPORATED TBT SURROGATE RECOVERY SUMMARY QC Report No: OC80-New£ields Northwest Project: MARINA PARK Event: NA Client ID TPRT TPNT TOT OUT COMP A-U 103% 226%* 1 COMP A-L 84.1% 92.8% 0 COMP B-U 102% 106% 0 MB-120908 83.9* 170%* 1 LCS-120908 94.6* 268%* 1 COMP B-L 101% 185%* 1 COMP B-L MS 96.0% 102% 0 COMP B-L MSp 97.3% 106* 0 LCS/MB LIMITS QC LIMITS (TPRT) = Tripropyl Tin Chloride (30-160) (30-160) (TPNT) = Tripentyl Tin Chloride (30-160) (30-160) Prep Method: SW3546 Analytical Method: TBT (Hexyl) Krone 1988 Log Number Range: 08-32709 to 08-32712 FORM -II TBT Page 1 for OC80 It It I II II It II It ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized: Reported: 12/15/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 17:37 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyte TBT_ION Tributyltin Ion DBT_ION Dibutyltin Ion BT ION Butyltin Ion ANALYTICAL RESOURCES INCORPORATED Sample I•D: COMP A-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.55 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 15.1% RL Result Q Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 103% Tripentyl Tin Chloride 226% 3.5 < 3.5 U 5.2 16 3.7 5.5 11 FORM I ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized! Reported: 12/15/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 17:56 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.61 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 12.8% RL Result Q TBT ION Tributyltin Ion 3.4 < 3.4 U DBT__ION Dibutyltin Ion 5.2 15 BT ION Butyltin Ion 3.6 4.8 Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 84.1$ Tripentyl Tin Chloride 92.8% I FORM I I I I I I I r r I 1 ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIX GC/MS Page 1 of 1 Lab Sample ID: OC80C LIMS ID: 08-32711 Matrix: Sediment Data Release Authorized: /15( Reported: 12/15/08 Date Extracted: 12/09/06 Date Analyzed: 12/11/08 18:16 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.40 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 13.7% RL Result Q TBT ION Tributyltin Ion 3.6 DST ION Dibutyltin Ion 5.4 BT_ION Butyltin Ion 3.8 Reported in yg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 102% Tripentyl Tin Chloride 106% 3.6 U 13 < 3.8 U r FORM I ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIX GC/MS Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized Reported: 12/15/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 18:35 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyse ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.47 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 15.7* RL Result Q TBT ION Tributyltin Ion 3.5 < 3.5 U DBT_ION Dibutyltin Ion 5.3 19 BT ION Butyltin Ion 3.7 6.1 Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 101% Tripentyl Tin Chloride 185% FORM I I ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 �1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment 'Data Release Authorized: . Reported: 12/15/08 Date Extracted MS: 12/09/08 Date Analyzed MS: 12/11/08 18:55 MSD: 12/11/08 19:14 Instrument/Analyst MS: NT2/VTS MSD: NT2/VTS Silica Gel Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount MS: 5.21 g-dry-wt MSD: 5.29 g-dry-wt Final Extract Volume MS: 0.5 mL MSD: 0.5 mL Dilution Factor MS: 1.00 MSD: 1.00 Alumina Cleanup: Yes Moisture: 15.7% Analyte Sample MS Spike MS Added -MS Recovery MSD Spike Added-MSD MSD Recovery ' RPD Tributyltin Ion < 3.5 U 35.6 42.8 83.29s 36.7 42.1 87.2% 3.0% Dibutyltin Ion 18.8 40.6 36.8 59.2% 55.3 36.2 101% 30.7% Butyltin Ion 6.1 21.6 29.9 51.84; 27.4 29.4 72.4% 23.7% Results reported in RPD calculated using µg/kg sample concentrations per SW846. I I 11 I I 11 I I I FORM III ORGANICS ANALYSIS DATA SHEET Tributyl Tine by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OCSOD LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized Reported: 12/15/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 18:55 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number TBT ION DBT ION BT ION Analyte Tributyltin Ion Dibutyltin Ion Butyltin Ion Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 96.0% Tripentyl Tin Chloride 102% ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.21 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 15.7% RL Result Q 3.7 --- 5.6 --- 3.9 --- FO] 0ya II ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIX GC/MS Page 1 of 1 �Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized: Reported: 12/15/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 19:14 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyte TBT_ION Tributyltin Ion DBT_ION Dibutyltin Ion BT_ION Butyltin Ion Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride Tripentyl Tin Chloride 97.3% 106% ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L MATRIX SPIKE DUP QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 5.29 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 15.7% RL Result Q 3.7 --- 5.5 --- 3.9 --- FORM I 11 ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIX dC/MS Page 1 of 1 Lab Sample ID: MB-120908 LIMS ID: 08-32712 Matrix: Sediment �y Data Release Authorized: /// Reported: 12/15/08 fl Date Extracted: 12/09/08 Date Analyzed: 12/11/08 16:58 Instrument/Analyst: NT2/VTS Silica Gel Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: MB-120908 METHOD BLANK QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: NA Date Received: NA Sample Amount: 5.00 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes RL Result Q TBT ION Tributyltin Ion 3.9 < 3.9 U DBT`_ION Dibutyltin Ion 5.8 < 5.8 U BT ION Butyltin Ion 4.1 < 4.1 U Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 83-.9W Tripentyl Tin Chloride 170$ 19 FORM I II ANALYTICAL RESOURCES ORGANICS ANALYSIS DATA SHEET Sample INCORPORATED ID: LCS-1 8 Tributyl Tins by Krone 1988 SIX GC/MS LAB CONTROL SAMPLE Page 1 of 1 Lab Sample ID: LCS-120908 QC Report No: OC80-Newfields Northwest LIMS ID: 08-32712 Project: MARINA PARK Matrix: Sediment Data Release Authorized: /10 Date Sampled: Date Received: NA NA Reported: 12/15/08 Date Extracted LCS: 12/09/08 Sample Amount LCS: 5.00 g-dry-wt Date Analyzed LCS: 12/11/08 17:18 Final Extract Volume LCS: 0.50 mL Instrument/Analyst LCS: NT2/VTS Dilution Factor LCS: 1.00 Silica Gel Cleanup: No Alumina Cleanup: Yes Spike Analyte LCS Added Recovery Tributyltin Ion 35.8 44.6 80.3% Dibutyltin Ion 26.7 38.4 69.596 Butyltin Ion 23.7 31.2 76.0% Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride Tripentyl Tin Chloride 94.6% 268% FORM III ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized: V Reported: 12/11/08 Date Extracted: 12/09/08 Date Analyzed: 12/10/08 14:57 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 15.1% CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21,9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 85.2% Tetrachlorometaxylene 89.2% C I'l FORM I 1] I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: MB-120908 LIMS ID: 08-32710 Matrix: Sediment 'Data Release Authorized: �1 Reported: 12/11/08 V Date Extracted: 12/09/08 Date Analyzed: 12/10/08 14:05 Instrument/Analyst: ECDS/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: NB-120908 METHOD BLANK QC Report No: OCSO-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA Sample Amount: 25.0 g Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: NA CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 20 U U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 84.84; Tetrachlorometaxylene 85.5% I I 1, U I 11 I I FORM I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: 05 Reported: 12/11/08 Date Extracted: 12/09/08 Date Analyzed: 12/10/08 15:14 Instrument/Analyst: ECDS/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL /� RESOURCES V INCORPORATED Sample IDs COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.4 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 12.8* CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U ,11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 78.08 Tetrachlorometaxylene 81.5% �l I FORM I �I n ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment \� Data Release Authorized: V `" Reported: 12/11/08 Date Extracted: 12/09/08 Date Analyzed: 12/10/08 15:31 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes ' Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.3 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 12.8% CAS Number Analyte RL Result _ 12674-11-2 Aroclor 1016 20 20 U 53469-21-9 Aroclor 1242 20 < U 12672-29-6 Aroclor 1248 20 <-20 20 U 11097-69-1 Aroclor 1254 20 < 11096-82-5 Aroclor 1260 20 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < Reported in Mg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 85.5% Tetrachlorometaxylene 86.8% ,I I FORM I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: r Jc Reported: 12/11/08 Date Extracted: 12/09/08 Date Analyzed: 12/10/08 15:48 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL /� RESOURCES v INCORPORATED Sample ID: COMP A-L MATRIX SPIKE DDP QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.4 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 12.-S$ CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 --- 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 --- 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 84.0!k Tetrachlorometaxylene 86.8$ FORM I I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80C LIMS ID: 08-32711 Matrix: Sediment Data Release Authorized: Reported: 12/11/08 Date Extracted: 12/09/08 'Date Analyzed: 12/10/08 16:05 i Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.1 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 13.7t CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U - 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 20 U U 11104-28-2 Aroclor 1221 20 < 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 83.5% Tetrachlorometaxylene 86.0% FORM I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized: Reported: 12/11/08 Date Extracted: 12/09/08 Date Analyzed: 12/10/08 16:23 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L SAMPLE QC Report No: OC80-NewfieldS Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.4 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 15.7% CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 84.296 Tetrachlorometaxylene 88.06 I I .I FORM I I SW8082/PCB SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OC80-Newfields Northwest Project: MARINA PARK DCBP DCBP TCMX TCMX Client ID % REC LCL-UCL % REC LCL-UCL 'TOT OUT COMP A-U 85.2% 43-148 89.2% 48-123 0 MB-120908 84.8% 65-117 85.5% 63-119 0 LCS-120908 86.5% 65-117 82.5% 63-119 0 COMP A-L 78.0% 43-148 81.5% 48-123 0 COMP A-L MS 85.5% 43-148 86.8% 48-123 0 COMP A-L MSD 84.0% 43-148 86.8% 48-123 0 COMP B-U 83.5% 43-148 86.0% 48-123 0 COMP B-L 84.2% 43-148 88.0% 48-123 0 PSDDA Control Limits Prep Method: SW3550B Log Number Range: 08-32709 to 08-32712 FORM -II SW8082 Page 1 for OC80 I ANALYTICAL RESOURCES INCORPORATED F1 ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/BCD Page 1 of 1 Lab Sample ID: OC8013 LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: Reported: 12/11/08 Date Extracted MS/MSD: 12/09/08 Date Analyzed MS: 12/10/08 15:31 MSD: 22/10/08 15:48 Instrument/Analyst MS: ECDS/JGR MSD: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No Analyse Sample MS ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L MS/MSD QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount MS: 25.3 g-dry-wt MSD: 25.4 g-dry-wt Final Extract Volume MS: 5.0 mL MSD: 5.0 mL Dilution Factor MS: 1.00 MSD: 1.00 Silica Gel: No Percent Moisture: 12.8W Spike MS Spike MSD Added -MS Recovery MSD Added-MSD Recovery RPD Aroclor 1016 < 19.7 U 86.6 98.8 87.7% 87.7 98.3 Aroclor 1260 < 19.7 U 94.4 98.8 95.5pd 93.4 98.3 Results reported in µg/kg (ppb) RPD calculated using sample concentrations per SW846. 89.28 1.3% 95.08 1.1t FORM III ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: LCS-120908 LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: U Reported: 12/11/08 �J 'Date Extracted: 12/09/08 Date Analyzed: 12/10/08 14:22 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No Analyte Aroclor 1016 Aroclor 1260 I 1 ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-120908 LAB CONTROL QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA Sample Amount: 25.0 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: NA Lab Spike Control Added Recovery 84.9 100 84.9% 100 100 100% PCB Surrogate Recovery Decachlorobiphenyl 86.5% Tetrachlorometaxylene 82.5% Results reported in µg/kg (ppb) If I IFORM III ANALYTICAL RESOURCES INCORPORATED SW8081 PESTICIDE SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OC80-Newfields Northwest Project: MARINA PARK Client ID DCBP TCMX TOT OUT COMP A-U 78.5% 78.5% 0 COMP A-L 79.2% 77.5% 0 MB-120908 79.8% 78A % 0 LCS-120908 79.5% 84.0% 0 COMP B-U 80.5% 80.8% 0 COMP B-U MS 78.2% 84.5% 0 COMP B-U MSD 88.0% 85.2% 0 COMP B-L 79.8% 82.8% 0 LCS/MB LIMITS QC LIMITS (DCBP) = Decachlorobiphenyl (65-125) (52-143) (TCMX) = Tetrachlorometaxylene (53-112) (43-128) Prep Method: SW3550B Log Number Range: 08-32709 to 08-32712 FORM -II SW8081 Page 1 for OC80 ' ANALYTICAL O RESOURCES ORGANICS ANALYSIS DATA SHEET INCORPORATED PSDDA Pesticides/PCB by GC/ECD Sample ID: COMP A-U Page 1 of 1 SAMPLE Lab Sample ID: OC80A QC Report No: OC80-Newfields PARK Northwest LIMS ID: 08-32709 Project: MARINA Matrix: Sediment Data Release Authorized: DatDateeReceived: Reported: 12/12/08 12/05/08 Date Extracted: 12/09/08 Sample Amount: 25.7 g-dry-wt Date Analyzed: 12/11/08 11:55 Final Extract Volume: 5.0 mL Instrument/Analyst: ECD4/AAR Dilution Factor: 1.00 GPC Cleanup: No Silica Gel: Yes Sulfur Cleanup: Yes Percent Moisture: 15.1$ �y Florisil Cleanup: No Acid Cleanup: No CAS Number Analyte RL Result 319-84-6 alpha-BHC 0.97 < 0.97 U 319-85-7 beta-BHC 0.97 < 0.97 U 319-86-8 delta-BHC 0.97 < 0.97 U 58-89-9 gamma-BHC (Lindane) 0.97 < 0.97 U 76-44-8 Heptachlor 0.97 < 0.97 U 309-00-2 Aldrin 0.97 < 0.97 U 1024-57-3 Heptachlor Epoxide 0.97 < 0.97 U 959-98-8 Endosulfan I 0.97 < 0.97 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,4'-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.7 < 9.7 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U 5103-74-2 gamma Chlordane 0.97 < 0.97 U 5103-71-9 alpha Chlordane 0.97 97 < 0.97 < 97 U U 8001-35-2 Toxaphene 2.0 U 789-02-6 2,4'-DDT 2.0 2.0 < < 2.0 U 3424-82-6 53-19-0 2,4'-DDE 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Pest/PCB Surrogate Recovery Decachlorobiphenyl 78.5% Tetrachlorometaxylene 78.5& A FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 12:15 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisturet 12.8% CAS Number Analyte RL Result 319-84-6 alpha:BHC 0.98 < 0.98 U 319-85-7 beta-BHC 0.98 < 0.98 U 319-86-8 delta-BHC 0.98 < 0.98 U 58-89-9 gamma-BHC (Lindane) 0.96 < 0.98 U 76-44-8 Heptachlor 0.98 < 0.98 U 309-00-2 Aldrin 0.98 < 0.98 U 1024-57-3 Heptachlor Epoxide 0.98 < 0.98 U 959-98-8 Endosulfan 1 0.98 < 0.98 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,41-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,4'-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.8 < 9.8 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U 5103-74-2 gamma Chlordane 0.98 < 0.98 U 5103-71-9 alpha Chlordane 0.98 < 0.98 U 8001-35-2 Toxaphene 98 < 98 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Peat/PCB Surrogate Recovery Decachlorobiphenyi 79.2% Tetrachlorometaxylene 77.5* FORM I ANALYTICAL ORGANICS ANALYSIS DATA SHEET RESOURCES INCORPORATED PSDDA Pesticides/PCB by GC/ECD Sample ID: COMP B-U Page 1 of 1 SAMPLE Lab Sample ID: OC80C QC Report No: OC80-Newfields Northwest LIMS ID: 08-32711 Project: MARINA PARK Matrix: Sediment Data Release Authorized Date ///"``"""" Date Sampled: 11/.26/08 Received: 12/05/08 Reported: 12/12/08 Date Extracted: 12/09/08 Sample Amount: 25.2 g-dry-wt ' Date Analyzed: 12/11/08 12:35 Final Extract Volume: 5.0 mL Instrument/Analyst: ECD4/AAR Dilution Factor: 1.00 GPC Cleanup: No Silica Gel: Yes ' Sulfur Cleanup: Yes Florisil Cleanup: No Percent Moisture: 13.7% Acid Cleanup: No CAS Number Analyte RL Result ' 319-84-6 alpha-BHC 0.99 < 0.99 U 319-85-7 beta-BHC 0.99 < 0.99 U 319-86-8 delta-BHC 0.99 < 0.99 U ' 56-89-9 gamma-BHC (Lindane) 0.99 < 0.99 U 76-44-8 Heptachlor 0.99 < 0.99 U 309-00-2 Aldrin 0.99 < 0.99 U 1024-57-3 Heptachlor Epoxide 0.99 < 0.99 U ' 959-98-8 Endosulfan I 0.99 < 0.99 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U ' 50-29-3 4,4'-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.9 < 9.9 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U ' 5103-74-2 5103-71-9 gamma Chlordane alpha Chlordane 0.99 0.99 < 0.99 < 0.99 U U 8001-35-2 Toxaphene 99 < 99 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4--DDE 2.0 < 2.0 U ' 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) ' Peat/PCB Surrogate Recovery Decachlorobiphenyl 80.5% ' Tetrachlorometaxylene 80.8% ' FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/BCD Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 14:21 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: 140 ' ANALYTICAL© RESOURCES INCORPORATED ' Sample IDs COMP H-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 , Sample Amount: 25.5 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: 15.7% CAS Number Analyte RL Result 319-84-6 alpha-BHC 0.98 < 0.98 U 319-85-7 beta-BHC 0.98 < 0.98 U 319-86-8 delta-BHC 0.98 < 0.98 U 58-89-9 gamma-BHC (Lindane) 0.98 < 0.98 U 76-44-8 Heptachlor 0.98 < 0.98 U 309-00-2 Aldrin 0.98. < 0.98 U 1024-57-3 Heptachlor Epoxide 0.98 < 0.98 U 959-98-8 Endosulfan I 0.98 < 0.98 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-SS-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,41-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.8 < 9.8 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U 5103-74-2 gamma Chlordane 0.98 < 0.98 U 5103-71-9 alpha Chlordane 0.98 < 0.98 U 8001-35-2 Toxaphene 98 < 98 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Peat/PCB Surrogate Recovery Decachlorobiphenyl 79.8% Tetrachlorometaxylene 82.8% FORM I I 'ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 'Lab Sample ID: OCOOC LIMS ID: 00-32711 Matrix: Sediment Data Release Authorized Reported: 12/12/08 Date Extracted MS/MSD: 12/09/08 ' Date Analyzed MS: 12/11/08 13:41 MSD: 12/11/08 14:01 Instrument/Analyst MS: ECD4/AAR ' GPC Cleanup: No MSD: ECD4/AAR Sulfur Cleanup: Yes ' Florisil Cleanup: No Analyte Sample ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U MS/MSD QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount MS: MSD: Final Extract Volume MS: MSD: Dilution Factor MS: MSD: Silica Gel: 25.2 g-dry-wt 25.0 g-dry-wt 5.0 mL 5.0 mL 1.00 1.00 Yes Percent Moisture: 13.7% Spike MS Spike MSD MS Added -MS Recovery MSD Added-MSD Recovery RPD 'alpha-BHC < 0.991 0.991 3.38 3.64 3.97 3.97 85.1% 91.7% 3.59 3.97 3.99 3.99 90.0% 99.5% 6.09d 8.7% beta-BHC < 78.6% 3.77 3.99 94.5% 18.99d delta-BHC (Lindane) < 0.991 < 0,991 3.12 3.38 3.97 3.97 85.1% 3,69 3,99 92.5% 8.8% gamma-BHC < 0.991 3.30 3.97 83.1% 3.93 3.99 98.5% 17.4% 'Heptachlor Aldrin < 0.991 3.24 3.97 81.6% 3.87 3.99 97.0% 17.7% Heptachlor Epoxide < 0.991 3.54 3.97 89.2% 4.07 3.99 102% 95.0% 13.9% 10.8% Endosulfan I < 0.991 3.40 3.97 85.6% 3.79 3.99 7.98 97.7% 8.4% Dieldrin < 1.98 7.17 7.95 90.2% 7.80 7.98 102% 8.35k 4,4'-DDE < 1.98 7.49 7.95 94.2% 85.9% 8.14 7.35 7.98 92.1% 7.39d Endrin < 1.98 1.98 6.83 6.95 7.95 7.95 87.496 7.41 7.98 92.9% 6.4% Endosulfan II < 1.98 6.79 7.95 85.4% 7.19 7.98 90.1% 5.7% 4,41-DDD Sulfate < < 1.98 5.54 7.95 69.7% 6.17 7.98 77.3% 10.8% 'Endosulfan 4,4--DDT < 1.98 7.13 7.95 89.7% 7.60 7.98 95.24; 6.4% Methoxychlor < 9.91 32.8 39.7 82.6% 35.7 39.9 7.98 89.5% 68.0% 8.5% 0.9% Endrin Aldehyde Chlordane < 1.98 < 0.991 5.38 3.54 7.95 3.97 67.7% 89.2% 5.43 3.93 3.99 98.596 92.5% 10.49a 9.4% 'gamma 0.991 3.36 3.97 84.6% 3.69 3.99 alpha Chlordane < Reported in jig/kg (ppb) ' RPD calculated using sample concentrations per SW846. IFORM III ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/BCD Page 1 of 1 Lab Sample ID: OC80C LIMS ID: 08-32711 Matrix: Sediment Data Release Authorized Reported: 12/12/OB Date Extracted: 12/09/08 Date Analyzed: 12/11/08 13:41 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.2 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: 13.7% CAS Number Analyte RL Result 319-84-6 alpha-BHC 0.99 "' 319-85-7 beta-BHC 0.99 --- 319-86-8 delta-BHC 0.99 --- 58-89-9 gamma-BHC (Lindane) 0.99 --- 76-44-8 Heptachlor 0.99 --- 309-00-2 Aldrin 0.99 --- 1024-57-3 Heptachlor Epoxide 0.99 --- 959-98-8 Endosulfan I 0.99 '-- 60-57-1 Dieldrin 2.0 --- 72-55-9 4,4'-DDE 2.0 --- 72-20-8 Endrin 2.0 --- 33213-65-9 Endosulfan lI 2.0 --- 72-54-8 4,4'-DDD 2.0 --' 1031-07-8 Endosulfan Sulfate 2.0 --- 50-29-3 4,4'-DDT 2.0 --- 72-43-5 Methoxychlor 9.9 --- 7421-93-4 Endrin Aldehyde 2.0 --- 5103-74-2 gamma Chlordane 0.99 --- 5103-71-9 alpha Chlordane 0.99 --- 8001-35-2 Toxaphene 99 < 99 U 789-02-6 2,4'-DDT 2.0 t 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Past/PCB Surrogate Recovery Decachlorobiphenyl 78.2$ Tetrachlorometaxylene 84.596 11 11 FORM I I ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/BCD Page 1 of 1 ' Lab Sample ID: OC80C LIMS ID: 08-32711 ' Matrix: Sediment Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/11/08 14:01 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-D MATRIX SPIKE DUP QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.0 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: 13.7% CAS Number Analyte RL Result 319-84-6 alpha-BHC 1.0 --- 319-65-7 beta-BHC 1.0 --- 319-86-8 delta-BHC 1.0 --- 58-89-9 gamma-BHC (Lindane) 1.0 --- 76-44-8 Heptachlor 1.0 --- 309-00-2 Aldrin 1.0 --- 1024-57-3 Heptachlor Epoxide 1.0 --- 959-98-8 Endosulfan I 1.0 --- 60-57-1 Dieldrin 2.0 --- 72-55-9 4,4'-DDE 2.0 --- Endrin 2.0 --- ,72-20-8 33213-65-9 Endosulfan II 2.0 '-- 72-54-8 4,4'-DDD 2.0 --- 1031-07-8 Endosulfan Sulfate 2.0 --- 50-29-3 4,4'-DDT 2.0 --- 72-43-5 Methoxychlor 10 --- 7421-93-4 Endrin Aldehyde 2.0 --- 5103-74-2 gamma Chlordane 1.0 --- 5103-71-9 alpha Chlordane 1.0 --- 8001-35-2 Toxaphene 100 < 100 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) ' Peat/PCB Surrogate Recovery Decachlorobiphenyl 88.0% Tetrachlorometaxylene 85.2% ' FORM I ' ANALYTICAL ORGANICS ANALYSIS DATA SHEET RESOURCESQ INCORPORATED ' PSDDA Pesticides/PCB by GC/ECD Sample ID: MB-120908 Page 1 of 1 METHOD BLANK Lab Sample ID: MB-120908 QC Report No: OC80-Newfields Northwest ' LIMS ID: 08-32711 Project: MARINA PARK Matrix: Sediment Data Release Authorized: Date Sampled: NA Reported: 12/12/08 !!!%%% Date Received: NA Date Extracted: 12/09/08 Sample Amount: 25.0 g-dry-wt ; Date Analyzed: 12/11/08 11:14 Final Extract Volume: 5.0 mL Instrument/Analyst: ECD4/AAR Dilution Factor: 1.00 GPC Cleanup: No Silica Gel: Yes Sulfur Cleanup: Yes Florisil Cleanup: No Percent Moisture: NA ' Acid Cleanup: No CAS Number Analyte RL Result 319-84-6 alpha-BHC 1.0 < 1.0 V 319-85-7 beta-BHC 1-.0 < 1.0 U 319-86-8 delta-BHC 1.0 < 1.0 U 58-89-9 gamma-BHC (Lindane) 1.0 < 1.0 U ' 76-44-8 Heptachlor 1.0 < 1.0 U 309-00-2 Aldrin 1.0 < 1.0 U 1024-57-3 Heptachlor Epoxide 1.0 < 1.0 U 959-98-8 Endosulfan I 1.0 < 1.0 U , 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U , 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,4--DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 10 < 10 U ' 7421-93-4 Endrin Aldehyde 2.0 < 2.0 (T 5103-74-2 gamma Chlordane 1.0 < 1.0 U 5103-71-9 alpha Chlordane 1.0 < 1.0 U , + 8001-35-2 Toxaphene 100 < 100 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U ' Reported in µg/kg (ppb) Pest/PCB Surrogate Recovery Decachlorobiphenyl 79.8W Tetrachlorometaxylene 78.5% , s t i FORM I ' 'ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 ' Lab Sample ID: LCS-120908 LIMS ID: 08-32711 Matrix: Sediment 'Data Release Authorized: Reported: 12/12/08 ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-120908 LAB CONTROL QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 'Date Date Extracted: 12/09/08 Sample Amount: Analyzed: 12/11/08 11:35 Final Extract Volume: Instrument/Analyst: ECD4/AAR Dilution Factor: GPC Cleanup: No Silica Gel: Sulfur Cleanup: Yes Florisil Cleanup: No Percent Moisture: Lab Spike Control Added 25.0 g-dry-wt 5.0 mL 1.00 Yes NA Recovery 'Analyte alpha-BHC 3.48 4.00 87.0% beta-BHC 3.70 4.00 92.5% 3.62 4.00 90.5& tdelta-BHC gamma-BHC (Lindane) 3.66 4.00 91.5-W Heptachlor 3.80 4.00 95.0% Aldrin 3.82 4.00 95.5$ Epoxide 3.92 4.00 98.0% 'Heptachlor Endosulfan I 3.74 4.00 93.5% Dieldrin 7.64 8.00 95.5% 4,4'-DDE 7.98 8.00 99.8% Endrin 7.16 8.00 89.5& Endosulfan II 7.06 8.00 88.2% 4,4'-DDD 6.90 8.00 86.2% Endosulfan Sulfate 5.86 8.00 73.24; 7.28 8.00 91.04; '4,4'-DDT Methoxychlor 34.4 40.0 86.0% Endrin Aldehyde 4.98 8.00 62.2% Chlordane 3.82 4.00 95.596 'gamma alpha Chlordane 3.68 4.00 92.0% Pest/PCB Surrogate Recovery Decachlorobiphenyl 79.596 Tetrachlorometaxylene 84.0% ' Reported in µg/kg (ppb) I II IFORM III ANALYTICAL RESOURCES INCORPORATED SIX SW8270 SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OC80-Newf1elds Northwest Project: MARINA PARK Client ID XNP DBA TOT OUT MB-120908 58.3% 81.0% 0 LCS-120908 62.OB 83.0% 0 COMP A-U 58.3% 83.3% 0 COMP A-U MS 62.3% 78.3% 0 COMP A-U MSD 63.0% 79.79s 0 COMP A-L 59.7% 75.7% 0 COMP B-U 58.7% 76.3% 0 COMP B-L 58.7% 74.0% 0 LCS/MB LIMITS QC LIMITS (MNP) - d10-2-Methylnaphthalene (44-100) (37-106) (DBA) = dl4-Dibenzo(a,h)anthracene (46-121) (16-118) Prep Method: SW3546 Log Number Range: 08-32709 to 08-32712 FORM -II SIM SW8270 Page 1 for OC80 'ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIX GC/XS Page 1 of 1 ' Lab Sample ID: OC80A LIME ID: 08-32709 Matrix: Sediment 'Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 12:03 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 10.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1% CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.9 < 4.9 U 86-73-7 Fluorene 4.9 < 4.9 U 85-01-8 Phenanthrene 4.9 < 4.9 U 120-12-7 Anthracene 4.9 < 4.9 U 206-44-0 Fluoranthene 4.9 < 4.9 U 129-00-0 Pyrene 4.9 < 4.9 U 56-55-3 Benzo(a)anthracene 4.9 < 4.9 U 218-01-9 Chrysene 4.9 < 4.9 U 205-99-2 Benzo(b)fluoranthene 4.9 < 4.9 U 50-32-8 Benzo(a)pyrene 4.9 < 4.9 U 193-39-5 Indeno(1,2,3-cd)pyrene 4.9 < 4.9 U 53-70-3 Dibenz(a,h)anthracene 4.9 < 4.9 U 191-24-2 Benzo(g,h,i)perylene 4.9 < 4.9 U Reported in µg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 58.3% d14-Dibenzo(a,h)anthracen 83.3% FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIX OC/MS Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 13:18 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No V ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 10.7 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 12.8* CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.7 < 4.7 U 86-73-7 Fluorene 4.7 < 4.7 U 85-01-8 Phenanthrene 4.7 < 4.7 U 120-12-7 Anthracene 4.7 < 4.7 U 206-44-0 Fluoranthene 4.7 < 4.7 U 129-00-0 Pyrene 4.7 < 4.7 U 56-55-3 Benzo(a)anthracene 4.7 < 4.7 U 218-01-9 Chrysene 4.7 < 4.7 U 205-99-2 Benzo(b)fluoranthene 4.7 < 4.7 U 50-32-8 Benzo(a)pyrene 4.7 < 4.7 U 193-39-5 Indeno(1,2,3-cd)pyrene 4.7 < 4.7 U 53-70-3 Dibenz(a,h)anthracene 4.7 < 4.7 U 191-24-2 Benzo(g,h,i)perylene 4.7 < 4.7 U Reported in µg/kg (ppb) Six Semivolatiie Surrogate Recovery d10-2-Methylnaphthalene 59.78 dl4-Dibenzo(a,h)anthracen 75.7% I 1 1I 1 I FORM I 'ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 ' Lab Sample ID: OC80C LIMS ID: 08-32711 'Matrix: Sediment] Data Release Authorized: Reported: 12/12/08 .// ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date sampled: 11/26/08 Date Received: 12/05/08 'Date Date Extracted: 12/09/08 Sample Amount: Analyzed: 12/12/08 13:42 Final Extract Volume: Instrument/Analyst: NT1/YZ Dilution Factor: GPC Cleanup: No Percent Moisture: Silica Gel Cleanup: Yes Alumina Cleanup: No CAS Number Analyte RL 10.4 g-dry-wt 0.5 mL 1.00 13.7% Result 83-32-9 Acenaphthene 4.8 < 4.8 < 4.8 U U 86-73-7 Fluorene 4.8 • 85-01-8 Phenanthrene 4.8 < 4.8 U 120-12-7 Anthracene 4.8 < 4.8 U ' 206-44-0 Fluoranthene 4.8 < 4.8 U 129-00-0 Pyrene 4.8 < 4.8 U 56-55-3 Benzo(a)anthracene 4.6 < 4.8 U 218-01-9 Chrysene 4.8 5.8 ' 205-99-2 Benzo(b)fluoranthene 4.8 4.8 50-32-8 Benzo(a)pyrene 4.8 4.8 193-39-5 Indeno(1,2,3-cd)pyrene 4.8 7.7 53-70-3 Dibenz(a,h)anthracene 4.8 4.8 < 4.8 9.6 U 191-24-2 Benzo(g,h,i)perylene Reported in µg/kg (ppb) ' Surrogate Recovery SIM Semivolatile dlo-2-Methylnaphthalene 58.7%* ' dl4-Dibenzo(a,h)anthracen 76.3% FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIX GC/MS Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized: Reported: 12/12/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 14:07 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 10.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.7* CAS Number Anaiyte RL Result 83-32-9 Acenaphthene 4.9 < 4.9 U 86-73-7 Fluorene 4.9 < 4.9 U 85-01-8 Phenanthrene 4.9 < 4.9 U 120-12-7 Anthracene 4.9 < 4.9 U 206-44-0 Fluoranthene 4.9 < 4.9 U 129-00-0 Pyrene 4.9 < 4.9 U 56-55-3 Benzo(a)anthracene 4.9 < 4.9 U 218-01-9 Chrysene 4.9 < 4.9 U 205-99-2 Benzo(b)fluoranthene 4.9 < 4.9 U 50-32-8 Benzo(a)pyrene 4.9 < 4.9 U 193-39-5 Indeno(1,2,3-cd)pyrene 4.9 < 4.9 U 53-70-3 Dibenz(a,h)anthracene 4.9 < 4.9 U 191-24-2 Benzo(g,h,i)perylene 4.9 < 4.9 U Reported in µg/kg (ppb) SIX Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 58.7% dl4-Dibenzo(a,h)anthracen 74.0$ 1. I FORM I r..r��.�..-�.-��.�.+�a..a�r...l..+.a.r*'.w-nu ��.A��X.L: .. y�invuw.r..r -..-.utfa.vv.nvur......vu.n unw..u..-w...w..a��..-..r".. ✓i. .-. �.�.-..-� ANALYTICAL O RESOURCES 'ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIN GC/MS Page 1 of 1 Sample ID: COMP A-U MATRIX SPIKE INCORPORATED 'Lab ' Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment /� Data Release Authorized:/l� Reported: 12/12/08 !� QC Report No: OC80-Newfields Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Northwest 'MSD: ' Date Extracted MS/MSD: 12/09/08 Date Analyzed MS: 12/12/08 12.:28 MSD: 12/12/08 12:53 Instrument/Analyst MS: NT1/YZ MSD: NT1/YZ Sample Amount MS: 10.3 10.5 Final Extract Volume MS: 0.50 MSD: 0.50 Dilution Factor MS: 1.00 MSD: 1.00 g-dry-wt g-dry-wt mL mL Sample MS Spike MS Spike Added -MS Recovery MSD Added-MSD MSD Recovery RPD 'Analyte 'Phenanthrene 'Chrysene 'Dibenz(a,h)anthracene Acenaphthene Fluorene Anthracene Fluoranthene Pyrene Benzo(a)anthracene Benzo(b)fluoranthene Benzo(a)pyrene Indeno(1,2,3-cd)pyrene Benzo(g,h,i)perylene < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U < 4.9 U 86.9 88.3 93.2 95.1 105 106 100 99.0 89.3 107 100 103 102 146 59.59t 89.0 146 60.5% 91.9 146 63.8% 92.4 146 65.1% 93.3 146 71.9% 105 146 72.6% 105 146 68.5% 98.1 146 67.8% 99.0 146 61.2t 95.2 146 73.3% 107 146 68.5% 101 146 70.5% 102 146 69.94; 100 143 143 143 143 143 143 143 143 143 143 143 143 143 62.2% 64.316 64.6% 65.2% 73.4$ 73.42% 68.6% 69.2% 66.6% 74.8% 70.6% 71.396 69.9% 2.4% 4.0% 0.9% 1.9% 0.0% 0.9% 1.9% 0.0% 6.4% 0.0% 1.0% 1,096 2.0%; Reported in µg/kg (ppb) ' RPD calculated using sample concentrations per SW846. 1 I' i II FORM III ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIX GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized; Reported: 12/12/08 4 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 12:28 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A -II MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 10.3 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1% CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.8 --- 86-73-7 Fluorene 4.8 --- 85-01-8 Phenanthrene 4.8 --- 120-12-7 Anthracene 4.8 --- 206-44-0 Fluoranthene 4.8 --- 129-00-0 Pyrene 4.8 --- 56-55-3 Benzo(a)anthracene 4.8 --- 218-01-9 Chrysene 4.8 --- 205-99-2 Benzo(b)fluoranthene 4.8 --- 50-32-8 Benzo(a)pyrene 4.8 --- 193-39-5 Indeno(1,2,3-cd)pyrene 4.8 --- 53-70-3 Dibenz(a,h)anthracene 4.8 --- 191-24-2 Benzo(g,h,i)perylene 4.8 --- Reported in µg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 62.3$ d14-Dibenzo(a,h)anthracen 78.3% MI 11 FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment /� Data Release Authorized: /i_� Reported: 12/12/08 /� Date Extracted: 12/09/08 Date Analyzed: 12/12/08 12:53 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U MATRIX SPIKE DUPLICATE QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 10.5 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1% CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.8 --- 86-73-7 Fluorene 4.8 --- 85-01-8 Phenanthrene 4.8 --- 120-12-7 Anthracene 4-8 --- 206-44-0 Fluoranthene 4.8 --- 129-00-0 Pyrene 4.8 --- 56-55-3 Benzo(a)anthracene 4.8 --- 218-01-9 Chrysene 4.8 --- 205-99-2 Benzo(b)fluoranthene 4.8 --- 50-32-8 Benzo(a)pyrene 4.8 --- 193-39-5 Indeno(1,2,3-cd)pyrene 4.8 --- 53-70-3 Dibenz(a,h)anthracene 4.8 --- 191-24-2 Benzo(g,h,i)perylene 4.8 --- Reported in kg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 63.0% dl4-Dibenzo(a,h)anthracen 79.7% FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW827OD-SIX GC/MS Page 1 of 1 Lab Sample ID: MB-120908 LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized Reported: 12/12/08 4��_ Date Extracted: 12/09/08 Date Analyzed: 12/12/08 11:14 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample IDs MB-120908 METHOD BLANK QC Report No: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: NA Date Received: NA Sample Amount: 10.0 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: NA CAS Number Analyte RL Result 83-32-9 Acenaphthene 5.0 < 5.0 U 86-73-7 Fluorene 5.0 < 5.0 U 85-01-8 Phenanthrene 5.0 < 5.0 U 120-12-7 Anthracene 5.0 < 5.0 U 206-44-0 Fluoranthene 5.0 < 5.0 U 129-00-0 Pyrene 5.0 < 5.0 U 56-55-3 Benzo(a)anthracene 5.0 < 5.0 U 218-01-9 Chrysene 5.0 < 5.0 U 205-99-2 Benzo(b)fluoranthene 5.0 < 5.0 U 50-32-8 Benzo(a)pyrene 5.0 < 5.0 U 193-39-5 Indeno(1,2,3-cd)pyrene 5.0 < 5.0 U 53-70-3 Dibenz(a,h)anthracene 5.0 < 5.0 U 191-24-2 Benzo(g,h,i)perylene 5.0 < 5.0 U Reported in µg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 58.3% d14-Dibenzo(a,h)anthracen 81.0% FORM I ' ORGANICS ANALYSIS DATA SHEET PNAS by SW827OD-SIX GC/MS Page 1 of 1 ' Lab Sample ID: LCS-120908 LIMS ID: 08-32709 'Matrix: Sediment Data Release Authorized Reported: 12/12/08 ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-120908 LAB CONTROL SAMPLE QC Report NO: OC80-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: NA Date Received: NA Extracted: 12/09/08 Sample Amount LCS: 'Date Date Analyzed LCS: 12/22/08 11:39 Final Extract Dilution Volume LCS: Factor LCS: Instrument/Analyst LCS: NT1/YZ Spike ' Analyse LCS Added Recovery Acenaphthene 90.5 150 60.3% Fluorene 95.5 150 63.7% Phenanthrene 97.0 150 64.7% Anthracene 102 150 68.0% Fluoranthene 112 150 74.7% Pyrene 116 150 77.3% Benzo(a)anthracene 110 150 73.3% Chrysene ill 150 74.0% Benzo(b)fluoranthene 104 150 69.3% 114 150 76.0% 'Benzo(a)pyrene Indeno(1,2,3-cd)pyrene 108 ISO 72.04; Dibenz(a,h)anthracene 110 150 73.3% Benzo(g,h,i)perylene 107 150 71.3% ' Reported in µg/kg (ppb) ' SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 62.0% d14-Dibenzo(a,h)anthracen 83.0% ' 10.o g-dry-wt 0.50 mL 1.00 FORM III ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SN8270 GC/MS Page 1 of 1 Lab Sample ID: MB-120908 LIMS ID: 08-32709 Matrix: Sediment ��r Data Release Authorized: Reported: 22/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 18:21 Instrument/Analyst: NT4/PK GPC Cleanup; No Sample IDt MB-120908 METHOD BLANK ANALYTICAL RESOURCES INCORPORATED E f QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: NA Date Received: NA Sample Amount: 25.0 g Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture; NA CAS Number Analyse 131-11-3 Dimethylphthalate 84-66-2 Diethylphthalate 85-68-7 Butylbenzylphthalate 117-81-7 bis(2-Ethylhexyl)phthalate 117-84-0 Di-n-Octyl phthalate Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 2-Fluorobiphenyl d14-p-Terphenyl d4-1,2-Dichlorobenzene 49.2W 60.8W 65.29d 58. 89r RL Result 20 < 20 U 20 < 20 U 20 < 20 U 20 < 20 U 20 < 20 U I ail i 1' 1I i CI it 1 �1 i FORM I F ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized: Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 19:28 Instrument/Analyst: NT4/PK GPC Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1& CAS Number Analyte RL Result ' 131-11-3 Dimethylphthalate 20 < 20 U 84-66-2 Diethylphthalate 20 < 20 U 85-68-7 Butylbenzylphthalate 20 < 20 U ' 117-81-7 bis(2-Ethylhexyl)phthalate 20 < 20 U 117-84-0 Di-n-Octyl phthalate 20 < 20 U Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 53.6% ' 2-Fluorobiphenyl 66.4% d14-p-Terphenyl 66.8% d4-1,2-Dichlorobenzene 57.6% ' I ' FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 20:02 Instrument/Analyst: NT4/PK GPC Cleanup: No CAS Number 131-11-3 84-66-2 85-68-7 117-81-7 117-84-0 ANALYTICAL RESOURCES INCORPORATED Sample IDt COMP A-U MATRIX SPIKE QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1% Analyte Dimethylphthalate Diethylphthalate Butylbenzylphthalate bis(2-Ethylhexyl)phthalate Di-n-Octyl phthalate Reported in kg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 65.2% 2-Fluorobiphenyl 72.8% d14-p-Terphenyl 70.4% d4-1,2-Dichlorobenzene 64.44r RL Result 20 --- 20 --- 20 --- 20 --- 20 --- Fd•F3Yf3 I I ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS ID: 08-32709 Matrix: Sediment l��W Data Release Authorized: Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 20:36 Instrument/Analyst: NT4/PK GPC Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U MATRIX SPIKE DUPLICATE QC Report NO: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 26.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.1* CAS Number Analyte RL Result 131-11-3 Dimethylphthalate 19 84-66-2 Diethylphthalate 19 --- 85-68-7 Butylbenzylphthalate 19 --- ' 117-81-7 bis(2-Ethylhexyl)phthalate 19 117-84-0 Di-n-Octyl phthalate 19 Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 66.0% 2-Fluorobiphenyl 72.8% d14-p-Terphenyl 69.6% d4-1,2-Dichlorobenzene 65.6% ' I I FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80B LIMS ID: 08-32710 Matrix: Sediment Data Release Authorized: "n� Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 21:10 Instrument/Analyst: NT4/PK GPC Cleanup: No CAS Number 131-11-3 84-66-2 85-68-7 117-81-7 117-84-0 ANALYTICAL RESOURCES INCORPORATED Sample IDs COMP A-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.7 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 12.8% Analyte Dimethylphthalate Diethylphthalate Butylbenzylphthalate bis(2-Ethylhexyl)phthalate Di-n-Octyl phthalate Reported in µg/kg (ppb) Semivolatile Surrogate-Recovary d5-Nitrobenzene 62.0% 2-Fluorobiphenyl 80.4% d14-p-Terphenyl 69.2% d4-1,2-Dichlorobenzene 67.2% RL Result 19 < 19 U 19 < 19 U 19 < 19 U 19 < 19 U 19 < 19 U �i AI 1!I FORM I I 'ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80C LIMS ID: 08-32711 Matrix: Sediment Data Release Authorized:� Reported: 12/16/08 Date Extracted: 12/09/08 'Date Analyzed: 12/12/08 21:43 Instrument/Analyst: NT4/PK GPC Cleanup: No ANALYTICAL . RESOURCES INCORPORATED Sample ID: COMP B-U SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.4 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 13.7!k CAS Number Analyte RL- Result 131-11-3 Dimethylphthalate 20 < 20 U 84-66-2 Diethylphthalate 20 < 20 U 85-68-7 Butylbenzylphthalate 20 < 20 U 117-81-7 bis(2-Ethylhexyl)phthalate 20 < 20 U 117-84-0 Di-n-Octyl phthalate 20 < 20 U Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 58.8% , 2-Fluorobiphenyl 70.8-W dl4-p-Terphenyl 72.4$ d4-1,2-Dichlorobenzene 65.29a FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80D LIMS ID: 08-32712 Matrix: Sediment Data Release Authorized, Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/08 22:17 Instrument/Analyst: NT4/PK GPC Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP B-L SAMPLE QC Report No: OC80-Newfields Northwest Project: MARINA PARK NA Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.5 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 15.7% CAS Number Analyte RL Result 131-11-3 Dimethylphthalate 20 < 20 U 84-66-2 Diethylphthalate 20 < 20 U 85-68-7 Butylbenzylphthalate 20 < 20 U 117-81-7 bis(2-Ethylhexyl)phthalate 20 < 20 U 117-84-0 Di-n-Octyl phthalate 20 < 20 U Reported in µg/kg (ppb) Semivolatile Surrogate Recovery, d5-Nitrobenzene 62.0$ 2-Fluorobiphenyl 68.8% dl4-p-Terphenyl 70.0%; d4-1,2-Dichlorobenzene 65.2W I FORM I II SW8270 SEMIVOLATILES SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OC80-Newfields Northwest Project: MARINA PARK Client ID NBZ FBP TPH DCB TOT OUT MB-120908 49.2% 60.8% 65.2% 58.8% 0 LCS-120908 51.2% 71.6% 70.8% 62.4% 0 COMP A-U 53.6% 66.4% 66.8% 57.6% 0 COMP A-U MS 65.2% 72.8% 70.4% 64.4% 0 COMP A-U MSD 66.0% 72.8% 69.6% 65.6% 0 COMP A-L 62.0% 80.4% 69.2% 67.2% 0 COMP B-U 58.8% 70.8% 72.4% 65.2% 0 COMP B-L 62.0% 68.8% 70.0% 65.2% 0 LCS/MB LIMITS QC LIMITS 29 87) (NBZ) = d5-Nitrobenzene (37-85) (39-82) ( - (32-88) (FBP) (TPH) = 2-Fluorobiphenyl = d14-p-Terphenyl (38-105) (21-97) (J)CB) = d4-1,2-Dichlorobenzene (33-79) (25-82) II I! II It II II It II Prep Method: SW3550B Log Number Range: 08-32709 to 08-32712 ANALYTICAL RESOURCES INCORPORATED FORM -II SW8270 Page 1 for OC80 ORGANICS ANALYSIS DATA SHEET PsDDA Samivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OC80A LIMS Ip: 08-32709 Matrix: Sediment Data Release Authorized: Reported: 12/16/08 Date Extracted MS/MSD: 12/09/08 Date Analyzed MS: 12/12/08 20:02 MSD: 12/12/08 20:36 Instrument/Analyst MS: NT4/PK MSD: NT4/PK GPC Cleanup: NO ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP A-U MS/MSD QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount MS: 25.6 g-dry-wt MSD: 26.2 g-dry-wt Final Extract Volume MS: 0.5 mL MSD: 0.5 mL Dilution Factor MS: 1.00 MSD: 1.00 Percent Moisture: 15.1 W spike Ms Analyse Sample MS Added -MS Recovery Dimethylphthalate < 19.6 397 489 81.25 Diethylphthalate < 19.6 399 489 81.69k Sutylbenzylphthalate < 19.6 356 489 72.896 bis(2-Ethylhexyl)phthalate < 19.6 412 489 84.36 Di-n-Octyl phthalate < 19.6 405 489 82.8%; Results reported in µg/kg RPD calculated using sample concentrations per SW846. Spike MSD MSD Added-MSD Recovery RPD 369 478 77.29d 7.3% 373 478 78.096 6.78 336 478 70.38 5.88 381 478 79.7% 7.8$ 368 478 77.0% 9.61k FORM III II ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: LCS-120908 LIMS ID: 08-32709 Matrix: Sediment Data Release Authorized: Reported: 12/16/08 Date Extracted: 12/09/08 Date Analyzed: 12/12/06 18:55 Instrument/Analyst: NT4/PK GPC Cleanup: NO ANALYTICAL O RESOURCES INCORPORATED Sample ID: LCS-120908 LAB CONTROL QC Report No: OC80-Newfields Northwest Project: MARINA PARK Date Sampled: 11/26/08 Date Received: 12/05/08 Sample Amount: 25.0 g Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: NA Analyte Lab Control Spike Added Recovery Dimethylphthalate 393 500 78.6% Diethylphthalate 405 500 81.0% Butylbenzylphthalate 359 500 71.8% bis(2-Ethylhexyl)phthalate 385 500 77.0% Di-n-Octyl phthalate 375 500 75.01e Semivolatile Surrogate Recovery d5-Nitrobenzene 51.2% 2-Fluorobiphenyl 71.6% dl4-p-Terphenyl 70.8% d4-1,2-Dichlorobenzene 62.4% Results reported in µg/kg r IFORM III ANALYTICAL GEOTECHNICAL ANALYSIS DATA SHEET RESOURCES O Moisture Content by Method ASTM D2916 INCORPORATED Data Release Authorized: QC Report No: OF06-Newfields Northwest Reported: 01/09/09 Project: Marina Park Date Received: 12/17/08 Page 1 of 1 Client/ Date Analysis ARI ID Sampled Matrix Date Result Comp CD 12/08/08 Sediment 01/07/09 12:56 28.86 OF06A 08-34190 Comp CL 12/08/08 Sediment 01/07/09 12:56 17.21 OF06B 08-34191 LA-3 Ref 12/08/08 Sediment 01/07/09 12:56 111.7 OF06C 08-34192 Reported in Percent Report for OF06 Newfields Northwest Atterberg Limits 80 70 60 K CH or OH d 50 ■ 40 v 30 to 0. MH or OH 20 CL or OL 10 ML or OL 0 0 20 40 60 80 100 Liquid Limit • NA Comp CU NA ■ NA LA-3 Ref NA Boring Depth (ft) As-Moistue PlInd Liqui Plastic Limit USCS Number Number Con ent xiry Limit NA Comp CU NA 28.86 11.2 28.0 16.9 CL NA Com CL NA 17.21 NA NA NA NP NA LA-3 Ref NA 111.70 48.2 78.5 30.3 CH OF06 ' Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number., 399 Page 1 Sample ID: Comp CU Operator. gs Client: Newfields Northwest File: C:1...1OF061OF06A.SMP Material/Liquid: Sediment/ 0.05% Sodium Metaphosphate (w/w) Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Ad)) Analyzed: 1/9/2009 11:16:09AM Run Time: 0:10 hrs:min Reported: 1/9/2009 12:42:35PM Sample Density. 2.650 g/cm' ' Liquid Visc: 0.7230 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 102 kCnts/s Reynolds Number 0.43 Report by Sieve Size ' Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (PM) (Percent) (Percent) it No.4 4750.0 100.0 0.0 No.60 250.0 57.2 17.9 No.10 2000.0 99.1 0.9 No.120 125.0 36.7 20.5 No.18 1000.0 92.5 6.6 No.230 63.0 22.1 14.6 No.35 500.0 75.1 17.4 No.635 20.0 20.2 1.9 t r i t f F Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: Comp CU Page 2 Operator: gs Client: Newfields Northwest File: C:\...\OF06\OF06A.SMP ; Material/Liquid: Sediment / 0.05% Sodium Metaphosphate (w/w) Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analysis Type: High Speed(Adj) I Analyzed: 119/2009 11:16:09AM Run Time: 0:10 hrs:min Reported: 1/9/2009 12:42:35PM Sample Density: 2.650 g/cm' Liquid Vise: 0.7230 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.43 Report by Size Table High Diameter Cumulative Cumulative Mass Mass High Mass Finer Frequency Diameter Finer Mass Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) ' 300.0 57.2 4.7 15.00 18.3 1.1 i j 250.0 50.9 6.3 10.00 17.5 0.8 IF 200.0 42.1 8.8 8.000 16.5 1.1 150.0 100.0 30.3 11.8 6.000 15.7 24.9 5.4 5.000 14.6 0.7 1.1 80.00 22.0 2.8 4.000 13.3 1.2 60.00 21.7 0.3 3.000 11.6 1.7 �. 50.00 40.00 21.5 0.3 2.000 10.5 21.0 0.5 1.500 8.8 1.1 1.6 30.00 20.6 0.3 1.000 8.0 0.9 25.00 20.2 0.5 0.800 6:8 1.2 20.00 19.5 0.7 0.600 6.1 0.7 1. r C i. 1 1 Analytical Resources, Inc. III Sed' ra h 1 iG p V .04 Unit 1 Serial Number: 399 Page 3 9 � Sample ID: Comp CU Operator: gs Client: Newfields Northwest File: C.\... \OF06\OF06A.SMP Material/Liquid: Sediment/ 0.06% Sodium Metaphosphate (w/w) Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Bases law of extinction Test Number. 1 Analysis Type: High Speed(Adj) Analyzed: 1/9/2009 11:16:09AM Run Time: 0:10 hrs:min Reported: 1/9/200912-42:35PM Sample Density: 2.650 g/cm' Liquid Visc: 0.7230 cp Liquid Density: 0.9941 g/cm2 Analysis Temp: 35.0 °C Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.43 Report by Mass Percent ` Cumulative Cumulative High Mass Mass High Mass Mass 'I Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 4750 100.0 0.0 230.5 50.0 5.0 4750 95.0 5.0 194.2 45.0 5.0 it 1130 90.0 5.0 165.0 40.0 5.0 901.6 85.0 5.0 140.0 35.0 5.0 737.0 80.0 5.0 117.8 30.0 5.0 605.2 75.0 5.0 98.94 25.0 5.0 l' 498.1 70.0 5.0 80.58 20.0 5.0 410.0 65.0 5.0 18.64 15.0 5.0 337.6 60.0 5.0 4.34-1 10.0 5.0 278.4 55.0 5.0 1.334 5.6 5.0 i t k I� i l 1: Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 4 Sample ID: Comp CU Operator: gs Client: Newfields Northwest File: C:\...\OF06\OFO6A.SMP Material/Liquid: Sediment / 0.05% Sodium Metaphosphate (w/w) Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analysis Type: High Speed(Adj) Analyzed: 1/9/2009 11:16:09AM Run Time: 0:10 hrs:min Reported: 1/9/2009 12:42:35PM Sample Density: 2.650 g/cm' Liquid Viso: 0.7230 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.43 Cumulative Finer Mass Percent vs. Diameter e Test 100 i 90 I i 80 I �. 70 c U f. �- m 60 N l0 LL ca 50 U 40 30 20 10 i t. ' 0 I' 1,000 10 0.1 Particle Diameter (pm) i� SediGraph III V1.04 Analytical Resources, Inc. Unit 1 Serial Number: 399 Sample ID: Comp CL Operator: gs Client: Newtields Northwest File: C.\...\OF06\OF06B.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analyzed: 1/9/2009 11:47:07AM Reported: 1 /9/200912:46:53PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 107 kCnts/s Reynolds Number. 0.30 Report by Sieve Size Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number. 399 Sample ID: Comp CL Operator: gs Client: Newfields Northwest File: Q\... \OF06\OF06B.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /9/2009 11:47:07AM Reported: 1 /9/2009 12:46:53PM Liquid Vise: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 107 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 7.1 3.7 20.00 0.7 0.0 250.0 4.8 2.3 15.00 0.7 0.0 200.0 3.0 1.8 10.00 0.7 0.0 150.0 1.7 1.3 8.000 0.7 0.0 100.0 1.1 0.6 6.000 0.7 0.0 80.00 0.8 0.3 5.000 0.6 0.0 60.00 0.8 0.0 4.000 0.6 0.0 50.00 0.8 0.0 3.000 0.5 0.0 40.00 • 0.8 0.0 2.000 0.5 0.0 30.00 0.8 0.0 1.500 0.5 0.0 25.00 0.7 0.0 II i E v [] Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: Comp CL Operator. gs Client: Newfields Northwest File: C:\...\OFO6\OF06B.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analyzed: 1 /9/2009 11:47:07AM Reported: 1 /9/2009 12:46:53PM Liquid Viso: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 107 kCnts/s Reynolds Number. 0.30 Page 3 1 1 Report by Mass Percent Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 1 9500 100.0 0.0 808.4 50.0 5.0 9500 95.0 5.0 735.7 45.0 5.0 3928 90.0 5.0 670.8 40.0 5.0 2514 85.0 5.0 610.8 35.0 5.0 1833 80.0 5.0 553.5 30.0 5.0 1505 75.0 5.0 496.5 25.0 5.0 1292 70.0 5.0 442.2 20.0 5.0 1129 65.0 5.0 392.1 15.0 5.0 997.6 60.0 5.0 343.5 10.0 510 892.9 55.0 5.0 291.3 5.0 5.0 1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: Comp CL Operator: gs Client: Newflelds Northwest File: CA ... \OF06\OF06B.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /912009 11:47:07AM Reported: 1/9/2009 12:46:53PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 107 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Diameter (um) Page 4 i Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: LA-3 Ref Operator. gs Client: Newfieids Northwest File: C:\...\OFO6\OF06C.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analyzed: 1 /9/2009 12:52:45PM Reported: 1/9/2009 1:03:57PM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05-hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 77 kCnts/s Reynolds Number. 0.30 Report by Sieve Size I. Page 1 c Cumulative Cumulative Sieve Aperture Mass Mass Steve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) I (pm) (Percent) (Percent) No.4 4750.0 100.0 0.0 No.60 250.0 99.2 0.4 No.10 2000.0 99.9 0.1 No.120 125.0 97.8 1.4 No.18 1000.0 99.8 0.1 No.230 63.0 92.1 6.7 No.35 500.0 99.6 0.2 No.635 20.0 63.4 28.7 11 .- . Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 2 Sample ID: LA-3 Ref Operator: gs Client: Newfields Northwest File: C:\...\OF06\OF06C.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analyzed: 1 /9/2009 12:52:45PM Reported: 1/9/2009 1:03:57PM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 77 kCnts/s Reynolds Number: 0.30 Report by Size Table Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (um) (Percent) (Percent) (Nm) (Percent) (Percent) 300.0 99.2 0.1 20.00 55.4 8.0 250.0 98.9 0.3 16.00 46.1 9.3 200.0 98.3 0.6 10.00 41.8 4.3 150.0 96.2 2.1 8.000 37.8 4.0 100.0. 93.7 2.5 6.000 35.5 2.3 80.00 92.1 1.6 5.000 32.8 2.7 60.00 91.5 0.6 4.000 29.6 3.3 50.00 87.6 3.9 3.000 25.9 3.7 40.00 77.3 10.2 2.000 23.8 2.0 30.00 70.7 6.6 1.500 19.5 4.3 25.00 63.4 7.3 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Sedal,Number: 399 Sample ID: LA-3 Ref Operator. gs Client: Newflelds Northwest File: C:1... 1OFO61OF06C.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Bases law of extinction Test Number: 1 Analyzed: 1 /912009 12:52:45PM Reported: 1 /912009 1:03:57PM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Ad)) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' BaselFull Scale: 1281 77 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 4750 100.0 0.0 17.77 55.0 5.0 4750 95.0 5.0 14.78 50.0 5.0 89.92 90.0 5.0 12.03 45.0 5.0 44.37 85.0 5.0 9.490 40.0 5.0 36.87 80.0 5.0 7.113 35.0 5.0 32.19 75.0 5.0 4.806 30.0 5.0 28.18 70.0 5.0 3.130 25.0 5.0 24.51 65.0 5.0 1.786 20.0 5.0 21.07 60.0 5.0 1.069 15.0 6.0 c m m a N l6 iu c LL N a !0 E L) U Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: LA-3 Ref Operator; gs Client: NewHelds Northwest File: C*1... 1OFO61OF06C.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /9/2009 12:52:45PM Reported: 1 /9/2009 1:03:57 PM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 77 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Diameter (pm) Page 4 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 1 Sample ID: MP-10U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06D.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and'Beer's law of extinction I i Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/12/2009 1:47:47PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11:39:07AM Sample Density: 2.650 g/cm' Liquid Viso: 0.7228_cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 1281 75 kCnts/s Reynolds Number: 0.30 Report by Sieve Size s Cumulative Cumulative Sieve Aperture Mass Mass Steve Aperture Mass Mass i Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/8 in. 16000.0 100.0 0.0 No. 60 250.0 8.8 27.8 No.4 4750.0 99.2 0.8 No.120 125.0 4.0 4.8 j No.10 2000.0 96.6 2.6 No.230 63.0 2.5 1.5 No.18 1000.0 84.4 12.2 No.635 20.0 2.2 No.35 500.0 36.6 47.8 0.3 t t i i Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-10U Operator: BR Client: Newrields Northwest File: C:\...\OF06\OF06D.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 1:47:47PM Reported: 1 /13/2009 11:39:07AM Liquid Viso: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 75 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 8.8 4.1 20.00 2.1 0.1 250.0 6.6 2.2 15.00 1.8 0.2 200.0 4.7 1.9 10.00 1.5 0.3 150.0 3.4 1.3 8.000 1.0 0.5 100.0 2.8 0.6 6.000 0.9 0.1 80.00 2.5 0.3 ' 5.000 0.9 0.0 60.00 2.5 0.0 4.000 0.9 0.0 50.00 2.4 0.1 3.000 0.8 0.0 40.00 2.3 0.1 2.000 0.8 0.0 30.00 2.3 0.1 1.500 0.9 -0.1 25.00 2.2 0.1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-10U Operator: BR Client: New0elds Northwest File: C:\...\OFO6\OFO6D.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation. Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 1:47:47 P M Reported: 1/13/2009 11:39:07AM Liquid Viso: 0.7228 op Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 75 kCnts/s Reynolds Number: 0.30 Page 3 t 11 Report by Mass Percent ' Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 9500 100.0 0.0 649.8 50,b 5.0 9500 95.0 5.6 610.6 45.0 5.0 i 1606 90.0 5,0 571.5 40.0 5.0 1209 85.0 5.0 530.7 35.0 5.0 ' 1018 80.0 5.0 484.8 30.6 5.0 ' 908.3 75.0 5.0 440.3 25.0 5.0 838.4 70.0 5.0 399.2 20.0 5.0 782.5 65.0 5.0 359.5 15.0 5.0 734.3 60.0 5.0 318.6 10.0 5.0 690.6 55.0 5.0 269.1 5.0 5.0 i Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 4 Sample ID: MP-10U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06D.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 1:47:47PM Reported: 1 /13/2009 11:39:07AM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C T..+ 1 C N U N a m c U. a) a m E L) U Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 75 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Diameter (Nm) 5 J Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-10L Operator: BR Client: Newfields Northwest File: C1..1OF06\OF06E.SMP MatedaVLiquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/9/2009 4:51:53PM Reported: 1/13/200911:43:25AM Liquid Viso: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (um) (Percent) (Percent) (um) (Percent) (Percent) No.4 4750.0 100.0 0,0 No.60 250.0 89.6 7.5 No.10 2000.0 99.8 0.2 No.120 125.0 54.6 35.0 No.18 1000.0 99.2 0.6 No.230 63.0 34.5 20.1 No.35 500.0 97.1 2.1 No.635 20.0 32.6 1.9 11 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 2 Sample ID: MP-10L Operator: BR Client: Newflelds Northwest File: C:\...\OF06\OF06E.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adi) Analyzed: 1/9/2009 4:51:53PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11.43:25AM Sample Density: 2.650 g/cm' Liquid Visc: 0.7228 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Report by Size Table Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 89.6 3.3 20.00 31.6 1.0 250.0 80.7 8.9 15.00 29.8 1.8 200.0 63.6 17.1 10.00 28.3 1.5 150.0 45.8 17.9 8.000 26.4 1.9 100.0 38.2 7.6 6.000 25.1 1.3 80.00 34.5 3.7 5.000 23.4 1.7 60.00 34.3 0.2 4.000 21.1 2.2 50.00 34.0 0.3 3.000 18.4 2.7 40.00 33.5 0.5 2.000 16.6 1.8 30.00 33.0 0.4 1.500 15.0 1.6 25.00 32.6 0.5 I ' Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 3 Sample ID: MP-101- Operator: BR Client: Newflelds Northwest File: C:\...\OFO6\OF06E.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) I Analyzed: 1/9/2009 4:51:53PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11.43:25AM Sample Density: 2.650 g/cm' Liquid Viso: 0.7228 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Report by Mass Percent E Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency r (pm) (Percent) (Percent) (pm) (Percent) (Percent) 4750 100.0 0.0 126.3 50.0 5.0 4750 95.0 5.0 111.3 45.0 5.0 356.6 90.0 5.0 98.06 40.0 5.0 254.8 85.0 5.0 85.15 35.0 5.0 218.1 80.0 5.0 68.19 30.0 5.0 197.4 75.0 5.0 16,29 25.0 5.0 181.0 70.0 5.0 4.924 20.0 5:0 166.8 65.0 5.0 2.543 15.0 5.0 } 153.6 60.0 5.0 1.115 10.0 5.0 140.5 55.0 5.0 Analytical Resources, Inc. SedlGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-10L Operator: BR Client: Newflelds Northwest File: C:\...\OF06\OF06E.SMP Material/liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/9/2009 4:51:53PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11:43:25AM Sample Density: 2.650 g/Cm3 Liquid Visc: 0.7228 cp Liquid Density: 0.9941 g/cm3 Analysis Temp: 35.0 °C Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Taco4 1 Particle Diameter (pm) Page 4 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12U Operator: BR Client: Newflelds Northwest File: C:\...\OF06\OF06F.SMP Materlal/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1112/2009 1:11:12PM Reported: 1/13/200911:44:41AM Liquid Viso: 0.7229 cp Analysis Temp; 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 87 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/8In. 16000.0 100.0 0.0 No.60 250.0 43A 24.5 No.4 4750.0 95.7 4.3 No.120 125.0 16.2 27.2 No.10 2000.0 93.0 2.7 No.230 63.0 3.6 12.6 No.18 1000.0 86.1 6.9 No.635 20.0 3.5 0.1 No.35 500.0 67.9 18.2 II Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06F.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 1:11:12PM Reported: 1 /13/2009 11 A4:41 AM Liquid Visc: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 87 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 43.4 6.6 20.00 3.4 0.1 250.0 34.7 8.7 15.00 3.4 0.0 200.0 23.1 11.7 10.00 3.4 0.0 150.0 9.4 13.6 8.000 3.3 0.1 100.0 5.2 4.3 6.000 3.3 0.0 80.00 3.6 1.6 5.000 3.2 0.0 60.00 3.6 0.0 4.000 3.0 0.2 50.00 3.6 0.0 3.000 1.1 2.0 40.00 3.5 0.1 2.000 0.7 0.4 30.00 3.5 0.0 1.500 0.7 0.0 25.00 3.5 0.0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12U Operator: BR Client: Newilelds Northwest File: C:\...\OF06\OFO6F.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 1:11:12PM Reported: 1 /13/2009 11;44:41 AM Liquid Visc: 0.7229 cp Analysis Temp: 35.0'°C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941-g/cm' Base/Full Scale: 128 / 87 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (um) (Percent) (Percent) 9500 100.0 0.0 344.7 50.0 5.0 9500 95.0 5.0 299.8 45.0 5.0 4149 90.0 5.0 261.2 40.0 5.0 1327 85.0 5.0 228.4 35.0 5:0 940.5 80.0 5.0 201.3 30.0 5.0 750.7 75.0 5.0 178.0 25.0 5.0 625.7 70.0 5.0 157.4 20.0 5.0 532.8 65.0 5.0 138.5 15.0 5.0 459.0 60.0 5.0 120.8 10.0 5.0 397.1 55.0 5.0 102.2 5.0 5.0 11 ' Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 4 Sample ID: MP-12U Operator: BR Client: Newfields Northwest ' File: C:\...\OF06\OF06F.SMP Material/Liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation ' Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) '. Analyzed: 1/12/2009 1:11:12PM Run Time: 0:05 hrs:min ' Reported: 1/13/2009 11:44:41AM Sample Density: 2.650 g/cm' Liquid Viso: 0.7229 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 187 kCnts/s ' Reynolds Number: 0.30 t Cumulative Finer Mass Percent vs. Diameter t Test ' 100 90 - ' 80 j. 70 c U _ 1 a 60 y m t. f ' c 50 i LL > C E 40— U ' 30 20 ' 10 i 0 5,000 50 0.5 Particle Diameter (pm) 4" Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12L Operator: BR Client: Newfields Northwest File: C:\...\OF061OF06G.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beees law of extinction Test Number: 1 Analyzed: 1/9/2009 5:18:32PM Reported: 1 /13/2009 11:45:48AM Liquid Visc: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: HighSpeed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 73 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) No.4 4750.0 100.0 0.0 No.60 250.0 97.1 1.5 No.10 2000.0 99.4 0.6 No.120 125.0 88.7 8.4 No.18 1000.0 99.3 0.1 No.230 63.0 78A 10.3 No.35 500.0 98.6 0.7 No.635 20.0 74.9 3:5 11 '1 11 1i 11 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12L Operator: BR Client: Newfields Northwest File: C:1... 1OF061OF06G.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /912009 5:18:32PM Reported: 1 /13/2009 11:45:48AM Liquid Visc: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 73 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (Wm) (Percent) (Percent) 300.0 97.1 0.7 20.00 72.8 2.1 250.0 95.2 1.9 15.00 68.0 4.8 200.0 91.3 3.9 10.00 64.7 3.2 150.0 84.9 6.3 8.000 59.7 5.0 100.0 80.9 4.1 6.000 56.3 3.4 80.00 78.4 2.5 5.000 52.2 4.1 60.00 78.2 0.2 4.000 46.6 5.6 50.00 77.7 0.5 3.000 39.8 6.8 40.00 77.2 0.5 2.000 35.7 4.1 30.00 76.2 1.0 1.500 , 30.5 5.2 25.00 74.9 1.3 i J Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-12L Operator: BR Client: Newnelds Northwest File: Q\... \OF06\OF06G.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/9/2009 5:18:32PM Reported: 1 /13/2009 11:45:48AM Liquid Visc: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 73 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 4750 100.0 0.0 8,146 60.0 5.0 4750 95.0 5.0 6.090 55.0 5.0 196.9 90.0 5.0 4.650 50.0 5.0 137.3 85.0 5.0 3.573 45.0 5.0 100.4 80.0 5.0 2.744 46.0 5.0 75.49 75:0 5.0 2.021 35.0 5.0 20.50 70.0 5.0 1.423 30.0 5.0 11.69 65.0 5.0 11 11 I 11 1'I I I ' Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 4 Sample ID: MP-12L Operator: BR Client: Newfleids Northwest ' File: C:\...\OFO6\OF06G.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation ' Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/9/2009 5:18:32PM Run Time: 0:05 hrs:min ' Reported: 1/13/2009 11:45:48AM Sample Density: 2.650 g/cm' Liquid Visc: 0.7229 cp Liquid Density: 0.9941 g/Cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 73 kCnts/s ' Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Test 1 — ' 100 ' 90 ' 80-_ 1 ' 70 F:�\\ U 2 - - n. 60 CU � F ' 50— ii ' E 40 U ' 30— ! u ' 20 ' 10 0 !. 51000 50 0.5 Particle Diameter (pm) Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-13U Operator: BR Client: NewBelds Northwest File: C:1... 1OF061OF06H.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 3:30:40PM Reported: 1 /13/2009 11:47;33AM Liquid Viso: 0.7228 cp Analysis Temp: 35.0'C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 9/cm' Base/Full Scale: 128 / 95 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Steve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) No.10 2000.0 100.0 0.0 No.120 125.0 32.6 19.2 No.18 1000.0 98.0 2.0 No.230 63.0 12.7 19.9 No.35 500.0 79.0 19.0 No.635 20.0 11.2 1.5 No.60 250.0 51.8 27.2 Ll Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 2 Sample ID: MP-13U Operator: BR Client: Newfields Northwest ' File: C:\...\OF06\OF06H.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation ' Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) _ ' Analyzed: 1/12/2009 3:30:40PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11:47:33AM Sample Density: 2.650 g/cm' Liquid Viso: 0.7228 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 95 kCnts/s Reynolds Number: 0.30 ' Report by Size Table ' Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (Pm) (Percent) (Percent) 300.0 51.8 6.3 20.00 11.0 10.3 0.2 0.7 250.0 45.5 6.3 15.00 200.0 37.6 7.9 10.00 10.0 0.3 150.0 25.1 12.5 5.000 9.7 6.000 9.4 0.3 0.3 100.0 17.4 7.7 80.00 12.7 4.7 5.000 9.0 0.4 60.00 12.6 0.1 4.000 8.6 0.4 50.00 12.2 0.3 3.000 7.3 1.3 ' 40.00 11.9 0.4 2.000 4.3 3.0 30.00 11.6 0.3 1.500 2.6 1.7 25.00 11.2 0.4 I r i� ' f t: t Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 3 Sample ID: MP-13U Operator. BR Client: Newfields Northwest File: C:1... 1OF061OF06H.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction 11 11 Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/12/2009 3:30:40PM Run Time: 0:05 hrs:min ' Reported: 1113/200911:47:33AM Sample Density: 2.650 g/cm' Liquid Vise: 0.7228 cp Liquid Density: 0.9941 g1cm3 Analysis Temp: 35.0 °C Base/Full Scale: 128 / 95 kCnts/s Reynolds Number: 0.30 ' Report by Mass Percent High Cumulative Mass Mass Cumulative High Mass Mass ' Diameter Finer Frequency Diameter Fiber Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 3082 100.0 0.0 276.2 50.0 5.0 ' 3082 95.0 5.0 234.8 45.0 5.0 { 824.4 90.0 5.0 196.3 40.0 5.0 1 686.7 85.0 5.0 163.5 35.0 5.0 591.7 80.0 5.0 136.2 30.0 5.0 ' 514.3 75.0 5.0 114.9 25.0 5.0 449.9 70.0 5.0 99.66 20.6 5.0 398.8 65.0 5.0 86.68 15.0 5.0 355.0 60.0 5.0 73.11 10.0 5.0 315.0 55.0 5.0 7.920 5.0 5.0 i ' Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 4 Sample ID: MP-13U Operator: BR j Client: Newfields Northwest ' File: C:\...\OF06\OF06H.SMP Material/Liquid: Sediment/Water Measurement Principle: 11-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction I Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/12/2009 3:30:40PM Run Time: 0:05 hrs:min ' Reported: 1/13/2009 11:47:33AM Sample Density: 2.650 g/cm' Liquid Viso: 0.7228 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 1281 95 kCnts/s ' Reynolds Number: 0.30 it Cumulative Finer Mass Percent vs. Diameter Test ' 100 90 ' 80 (. r 70— c U , ' a 60— y 4 ' 50 iL m m 40 - E U ' 30 ' 20 I 10 i 0 1.000 100 10 1 Particle Diameter (um) Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 1 ' Sample ID: MP-13L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06l.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction S Test Number: 1 Analyzed: 1/12/2009 3:52:57PM Reported: 1 /13/2009 11:50:50AM Liquid Vise: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: '0.9941 g/cm' Base/Full Scale: 128 / 78 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/8In. 16000.0 100.0 0.0 No.60 250.0 13.5 30.2 No.4 4750.0 97.5 2.5 No.120 125.0 7.2 6.3 No.10 2000.0 93.3 4.2 No.230 63.0 3.1 4.1 No.18 1000.0 77.8 15.5 No.635 20.0 2.9 0.2 No.35 500.0 43.7 34.1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-13L Operator: BR Client: Newfieids Northwest File: C:\...\OF06\OF061.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/12/2009 3:52:57PM Run Time: 0:05 hrs:min Reported: 1/13/2009 11:50:50AM Sample Density: 2.650 g/cm' Liquid Visc: 0.7227 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 78 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 13.5 5.6 20.00 2.7 0.1 250.0 10.1 3.4 15.00 2.5 0.2 200.0 8.2 1.9 10.00 2.3 0.2 150.0 5.5 2.6 8.000 1.9 0.4 100.0 3.9 1.6 6.000 1.4 0.5 80.00 3.1 0.8 5.000 1.0 0.4 60.00 3.1 0.0 4.000 1.0 0.1 50.00 3.1 0.0 3.000 0.9 0.0 40.00 3.0 0.1 2.000 0.9 0.0 30.00 2.9 0.1 1.500 0.9 0.0 25.00 2.9 0.1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-13L Operator. BR Client: Newfieids Northwest File: C:\...\OFO6\OF061.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 3:52:57PM Reported: 1/13/2009 11:50:50AM Liquid Viso: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: HighSpeed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g1cm3 Liquid Density: 0.9941 g/cm2 Base/Full Scale: 128 / 78 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (Pm) (Percent) (Percent) 9500 100.0 0.0 628.1 50.0 5.0 9500 95.0 5.0 569.3 45.0 6.0 2730 90.6 5.0 514.0 40.0 5.0 1506 85.0 5.0 463.1 35.0 5.0 1221 80.0 5.0 419.5 30.0 5.0 1055 75.0 5.0 380.2 25.0 5.0 938.4 70.0 5.0 343.3 20.0 5.0 843.8 65.0 5.0 306.6 15.0 5.0 763.1 60.0 5.0 265.6 10.0 5.0 692.1 55.0 5.0 198.3 5.0 5.0 C U) U N 0.. N m c iL N co 7 E 7 0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-13L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF061.SMP Material/Liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 3:52:57PM Reported: 1 /13/2009 11:50:50AM Liquid Visc: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 9/cm' Base/Full Scale: 128 / 78 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Panicle Utameter tpm) Page 4 F1 Analytical Resources, Inc. ' SediGraph III V1.04 Unit 1 Serial Number: 399 Page 1 ' r Sample ID: MP-14U Operator: BR Client: Newflelds Northwest File: C:\...\OFO6\OF06J.SMP MateriallLiquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation . Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:18:05PM Reported: 1 /13/200911:51:31 AM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs;min Sample Density: 2.650 g/cm3 Liquid Density: 0.9941 g/cm3 Base/Full Scale: 128 1102 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/8 in. 16000.0 100.0 0.0 No. 60 250.0 14.1 36.4 No.4 4750.0 99.8 0.2 No.120 125.0 3.5 10.6 No.10 2000.0 97.8 2.0 No.230 '63.0 1.1 2A No.18 1000.0 83.0 14.8 No.635 20.0 1.0 0.1 No.35 500.0 60.5 32.5 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-14U Operator: BR Client: Newfiields Northwest File: C:\...\OF06\OF06J.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:18:05PM Reported: 1 /13/2009 11:51:31 AM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 14.1 8.5 20.00 1.0 0.0 250.0 7.6 6.5 15.00 1.0 0.0 200.0 4.3 3.2 10.00 0.9 0.0 150.0 2.4 1.9 8.000 0.9 0.0 100.0 1.5 0.9 6.000 0.9 0.0 80.00 1.1 0.4 5.000 0.8 0.0 60.00 1.1 0.0 4.000 0.8 0.1 50.00 1.1 0.0 3.000 0.7 0.1 40.00 1.1 0.0 2.000 0.7 0.0 30.00 1.0 0.0 1.500 0.7 0.0 25.00 1.0 0.0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number:.399 Sample ID: MP-14U Operator: BR Client: Newfields Northwest File: C:1... 1OF061OFO6J.SMP Material/Liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /12/2009 4:18:05PM Reported: 1 /13/200911:51:31 AM Liquid Visc: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Ad)) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass ,Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 9500 100.0 0.0 547.8 50.0 5.0 9500 95.0 5.0 495.0 45.0 5.0 1520 90.0 5.0 449.5 40.0 5.0 1222 85.0 5.0 410.5 35.0 5.0 1052 80.0 5.0 375.8 30.0 5.0 931.0 75.0 5.0 343.9 25.0 5.0 831.3 70.0 5.0 314.0 20.0 5.0 746.1 65.0 5.0 284.9 15.0 5.0 671.9 60.0 5.0 255.5 10.0 5.0 606.4 55.0 5.0 221.6 5.0 5.0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-14U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06J.SMP MateriallLiquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:18:05PM Reported: 1 /13/2009 11:51:31 AM Liquid Viso: 0.7228 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 glcm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 102 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter ticle Diameter (pm) Page 4 5 I Analytical Resources, Inc. SedlGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-14L Operator: BR Client: Newfields Northwest File: C:1...\OF061OFO6K.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:39:13PM Reported: 1 /13/2009 11:52:22AM Liquid Viso: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Ad)) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 88 kCnts/s Reynolds Number. 0.30 11 Page 1 , i i w'I 11 11 11 Report by Sieve Size r Sieve Aperture Cumulative Mass Mass Sieve Aperture Cumulative Mass Mass ' Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) No.4 4750.0 100.0 0.0 No.60 250.0 77.5 6.8 ' No.10 2000.0 95.5 4.5 No.120 125.0 59.6 17.9 No.18 1000.0 90.3 5.2 No.230 63.0 45.4 14.2 No.35 500.0 84.3 6.0 No.635 20.0 38.5 6.9 i , SediGraph III V1.04 Analytical Resources, Inc. Unit 1 Serial Number: 399 Page 2 Sample ID: MP-14L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06K.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:39:13PM Reported: 1 /13/2009 11:52:22AM Liquid Visc: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Report by Size Table Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 77.5 2.1 20.00 36.0 2.5 250.0 73.0 4.5 15.00 30.8 5.2 200.0 64.5 8.4 10.00 28.1 2.7 150.0 53.8 10.7 8.000 24.9 3.2 100.0 48.4 5.4 6.000 23.0 1.9 80.00 45.4 3.0 5.000 20.9 2.1 60.00 45.1 0.3 4.000 18.7 2.2 50.00 43.8 1.2 3.000 16.1 2.6 40.00 42.0 1.9 2.000 14.4 1.7 30.00 40.6 1.4 1.500 12.6 1.7 25.00 38.5 2.1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-14L Operator: BR Client: Newlields Northwest File: C:\...\OF06\OF06K.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number. 1 Analyzed: 1/12/2009 4:39:13PM Reported: 1 /13/2009 11:52:22AM Liquid Viso: 0.7227 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (um) (Percent) (Percent) 4750 100.0 0.0 104.5 50.0 5.0 4750 95.0 5.0 85.98 45.0 5.0 1864 90.0 5.0 48.94 40.0 5.0 964.5 85.0 5.0 23.51 35.0 5.0 541.6 80.0 5.0 13.74 30.0 5X 311.1 75.0 5.0 9.395 25.0 5.0 217.4 70.0 5.0 6.065 20.0 5.0 179.9 65.0 5.0 3.616 15.0 5.0 152.3 60.0 5.0 1.679 10.0 5.0 127.1 - 55.0 5.0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-14L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06K.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/12/2009 4:39:13PM Reported: 1 /13/2009 11:52:22AM Liquid Visc: 0.7227 cp Analysis Temp: 35.0 °C - Taef 9 Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 88 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Diameter (pm) Page 4 5 Analytical Resources, Inc. SedtGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15U Operator: BR Client: Newfields Northwest File: Q\... \OF06\OF06L.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/200911:30:OOAM Reported: 1 /13/200911:54:17AM Liquid Viso: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 92 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (um) (Percent) (Percent) (pm) (Percent) (Percent) No.4 4750.0 100.0 0.0 No.60 250.0 79.3 14.1 No.10 2000.0 99.4 0.6 No.120 125.0 52.2 27.1 No.18 1000.0 9&5 0.9 No.230 63.0 34.7 17.5 No.35 500.0 93.4 5.1 No.635 2d.0 30.2 4:5 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15U Operator: BR Client: New fields Northwest File: C:\...\OF06\OF06L.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/2009 11:30:OOAM Reported: 1 /13/2009 11:54:17AM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 92 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 79.3 5.0 20.00 28.4 1.8 250.0 71.3 8.0 15.00 25.6 2.9 200.0 59.1 12.2 10.00 24.1 1.5 150.0 44.5 14.6 8.000 22.1 2.0 10010 37.8 6.7 6.000 20.9 1.2 80.00 34.7 3.1 5.000 19.6 1.2 60.00 34.6 0.1 4.000 18.2 1.4 50.00 34.1 0.5 3.000 15.4 2.8 40.00 32.8 1.3 2.000 9.4 6.1 30.00 31.7 1.0 1.500 4.4 5.0 25.00 30.2 1.5 J. Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15U Operator: BR Client: Nev4ields Northwest File: Q\... \OF06\OFO6L.SMP Material/Liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/200911:30:OOAM Reported: 1 /13/2009 11:54:17AM Liquid Viso: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time; 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 92 kCnts/s Reynolds Numbee 0,30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 4750 100.0 0.0 135.2 50.0 5.0 4750 95.0 5.0 117.2 45.0 5.0 584.3 90.0 5.0 101.6 40.0 5.0 392.8 85.0 5.0 86.89 35.0 5.0 309.1 80.0 5.0 67.46 30.0 5.0 256.1 75.0 5.0 19.40 25.0 5.0 220.0 70.0 5.0 9,182 20.0 5.0 163.9 65.0 5.0 4.316 15.0 5.0 172.4 60,0 5.0 1.936 10.0 5.0 153.3 55.0 5.0 1.537 5.0 5.0 i Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06L.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/2009 11:30:OOAM Reported: 1 /13/2009 11:54:17AM Liquid Viso: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 92 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Diameter (pm) Page 4 , Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Page 1 Sample ID: MP-15L Operator: BR Client: Newfleids Northwest ; File: C:�... 1OF06\OFO6M.SMP Material/Liquid: Sediment/ Water Measurement Principle; X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/13/2009 11:52:27AM Run Time: Ot05 hrs:min Reported: 1/13/2009 12:01:07PM Sample Density: 2.650 g/cm' Liquid Viso: 0.7230 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 113 kCnts/s Reynolds Number: 0.30 Report by Steve Size Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/8 in. 16000.0 100.0 0.0 No, 60 250.0 4.8 19.4 No.4 4750.0 91.7 8.3 No.120 125.0 1.0 3.8 No.10 2000.0 74.9 16.8 No.230 63.0 0.5 0.5 No.18 1000.0 50.0 24.9 No.635 26.0 0.5 0.0 l No.35 500.0 24.2 25.8 f i e f. I i I i I Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OFO6M.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/2009 11:52:27AM Reported: 1 /13/2009 12:01:07PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 1281113 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 4.8 3.3 20.00 0.5 0.0 250.0 2.6 2.2 15.00 0.5 0.0 200.0 1.3 1.3 10.00 0.5 0.0 150.0 0.8 0.5 8.000 0.5 0.0 100.0 0.6 0.2 6.000 0.5 0.0 80.00 0.5 0.1 5.000 0.5 0.0 60.00 0.5 0.0 4.000 0.5 0.0 50.00 0.5 0.0 3.000 0.5 0.0 40.00 0.5 0.0 2.000 0.4 0.0 30.00 0.5 0.0 1.500 0.5 0.0 25.00 0.5 0.0 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number. 399 Sample ID: MP-15L Operator; BR Client; Newnelds Northwest File: C:1... \OF0610F06M.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/13/2009 11:52:27AM Reported: 1 /13/2009 12:01:07PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm3 Liquid Density: 0.9941 g1cm3 Base/Full Scale: 1281113 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 9500 100.0 0.0 1145 50.0 5.0 9500 95.0 5.0 1000 45.0 5.0 6257 90.0 5.0 873.6 40.0 5.0 4136 85.0 5.0 764.1 35.0 5.0 2978 80.0 5.0 668.6 30.0 5.0 2376 75.0 5.0 584.9 25,0 5.0 2006 70.0 5.0 511.0 20.0 5.6 1733 65.0 5.0 445.1 15.0 5.0 1506 60.0 5.0 384.0 10.0 5.0 1312 55.0 5.0 323.8 5.0 5.0 It c m U N a N fA N N C LLL N E U Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-15L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OFO6M.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/2009 11:52:27AM Reported: 1 /13/2009 12:01:07PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 113 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter vanicie uiameier tpm/ Page 4 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-16U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06N.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed; 1113/200912:15:48PM Reported: 1/13/2009 12:24:56PM Liquid Viso: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 81 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Page 1 Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (tlm) (Percent) (Percent) (Pm) (Percent) (Percent) No.4 4750.0 100.0 0.0 No.60 250.0 70.4 18.4 No.10 2000.0 99.9 0.1 No.120 125.0 31.7 38.7 No.18 1000.0 98.5 1.4 No.236 63.0 5.1 26.6 No.35 500.0 88.8 9.7 No.635 20.0 4.5 0.6 11 Inc. Analytical Resources, SediGraph III V1.04 Unit 1 Serial Number: 399 Page 2 Sample ID: MP-16U Operator: BR Client: Newiields Northwest 1 File: C:\...\OF06\OFO6N.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation 1 Calculation Method: Stokes sedimentation and Beer's law of extinction i Test Number: 1 Analysis Type: High Speed(Adj) j I i Analyzed: 1/13/2009 12:15:48PM Run Time: 0:05 hrs:min 1 Reported: 1/13/2009 12:24:56PM Sample Density: 2.650 g/cm' Liquid Visc: 0.7229 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 1281 81 kCnts/s 1 Reynolds Number: 0.30 1 Report by Size Table Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 300.0 70.4 6.4 20.00 4.4 11.1 15.00 4.1 0.1 0.3 250.0 59.3 200.0 41.8 17.6 10.00 3.9 0.2 i 150.0 20.2 21.6 8.000 3.6 6.000 3.3 0.3 0.3 100.0 9.9 10.2 80.00 5.1 4.8 5.000 2.7 0.6 60.00 5.1 0.0 4.000 1.4 3.000 1.1 1.3 0.4 50.00 5.0 0.1 40.00 4.8 0.2 2.000 1.1 0.0 30.00 4.6 0.2 1.500 1.0 0.1 25,00 4,5 0A 1 6 1 1 t 1 t 1 ' I I 1 is 1 Analytical Resources. Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample iD: MP-16U Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06N.SMP Material/Liquid: Sediment / Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Bases law of extinction Test Number: 1 Analyzed: 1 /13/2009 12:15:48P M Reported: 1/13/2009 12:24:56PM Liquid Viso: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128/ 81 kCnts/s Reynolds Number. 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (Pm) (Percent) (Percent) 4750 100.0 0.0 186.0 50.0 5.0 4750 95.0 5.0 171.5 45.0 5.0 713.2 90.0 5.0 158.2 40.0 5.0 534.7 85.0 5.0 145.7 35.0 5:0 411.2 80.0 5.0 133.3 30.0 5.0 334.8 75.0 5.0 120:8 25.0 5.0 283.9 70.0 5.0 109.7 20.0 5.0 247.5 65.0 5.0 99.69 15.0 5.0 221.9 60.0 5.0 90.16 10.0 5.0 202.4 55.0 5.0 80.15 5.0 5.0 A Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-16U Operator: BR Client: Newfields Northwest File: C:\...\OFO6\OF06N.SMP Material/Liquid: Sediment/ Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /13/2009 12:15:48 PM Reported: 1 /1312009 12:24:56 P M Liquid Visc: 0.7229 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 81 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle Ulameter tpm) Page 4 I 1 I I Analytical Resources, Inc. , SediGraph III V1.04 Unit 1 Serial Number: 399 Page 1 Sample ID: MP-16L Operator: BR Client: Newfields Northwest File: Ct\... \OF06\OF06O.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction i Test Number: 1 Analysis Type: High Speed(Adj) Analyzed: 1/9/2009 4:28:52PM Run Time: 0:05 hrs:min Reported: 1/13/2009 12:26:51PM Sample Density: 2.650 g/cm' Liquid Viso: 0.7230 cp Liquid Density: 0.9941 g/cm' Analysis Temp: 35.0 °C Base/Full Scale: 128 / 103 kCnts/s Reynolds Number: 0.30 Report by Sieve Size Cumulative Cumulative Sieve Aperture Mass Mass Sieve Aperture Mass Mass Name Size Passed Frequency Name Size Passed Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 5/81n. 16000.0 100.0 0.0 No.60 250.0 93.9 1.& No.4 4750.0 99.6 0.4 No.120 125.0 93.5 0.4 No.10 2000.0 99.3 0.2 No.230 63.0 93.3 0.2 No.18 1000.0 98.3 1.1 No.635 20.0 72.0 21.4 No.35 500.0 95.8 2.5 I �L II II Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-16L Operator: BR Client: Newfields Northwest File: C:\...\OF06\OF06O.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1 /9/2009 4:28:52PM Reported: 1 /13/2009 12:25:51 PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 103 kCnts/s Reynolds Number: 0.30 Report by Size Table Page 2 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (Pm) (Percent) (Percent) 300.0 93.9 0.3 20.00 71.5 0.5 250.0 93.7 0.2 15.00 62.0 9.5 200.0 93.6 0.2 10.00 56.8 5.2 150.0 93.5 0.1 8.000 50.1 6.7 100.0 93.4 0.1 6.000 46.1 4.0 80.00 93.3 0.1 5.000 39.9 6.2 60.00 92.3 1.0 4.000 29.9 10.0 50.00 86.2 6.1 3.000 18.2 11.7 40.00 78.7 7.5 2.000 6.6 11.6 30.00 76.8 1.9 1.500 0.0 6.6 25.00 72.0 4.8 II Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-16L Operator: SR Client: Newfields Northwest File: C:\...1OFO61OF06O.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and,Beer's law of extinction Test Number: 1 Analyzed: 1/9/2009 4:28:52PM Reported: 1 /13/2009 12:25:51 PM Liquid Vise: 0.7230 cp Analysis Temp: 35.0 "C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 g/cm' Liquid Density: 0.9941 g1cm3 Base/Full Scale: 128 / 103 kCnts/s Reynolds Number: 0.30 Report by Mass Percent Page 3 Cumulative Cumulative High Mass Mass High Mass Mass Diameter Finer Frequency Diameter Finer Frequency (pm) (Percent) (Percent) (pm) (Percent) (Percent) 9500 100.0 0.0 7.176 50.0 5.0 9500 95.0 5.0 5.983 45.0 5.0 393.4 90.0 5.0 4,720 40.0 5.0 44.61 85.0 5.6 4.011 35.0 5.0 38.82 80.0 5.0 3,486 30.0 5.0 33.35 75.0 5.0 3.012 25.0 5.0 23.15 70.d 6.0 2.552 20:0 5.0 13.37 65.0 5.0 2.096 15.0 5.0 10.94 60.0 5.0 1.861 10.0 5.0 9.381 55.0 5.0 1,660 5.0 5.0 1 Analytical Resources, Inc. SediGraph III V1.04 Unit 1 Serial Number: 399 Sample ID: MP-16L Operator: BR Client: Newrieids Northwest File: C:\...\OF06\OF060.SMP Material/Liquid: Sediment/Water Measurement Principle: X-Ray monitored gravity sedimentation Calculation Method: Stokes sedimentation and Beer's law of extinction Test Number: 1 Analyzed: 1/9/2009 4:28:52PM Reported: 1/13/2009 12:25:51 PM Liquid Visc: 0.7230 cp Analysis Temp: 35.0 °C Analysis Type: High Speed(Adj) Run Time: 0:05 hrs:min Sample Density: 2.650 9/cm' Liquid Density: 0.9941 g/cm' Base/Full Scale: 128 / 103 kCnts/s Reynolds Number: 0.30 Cumulative Finer Mass Percent vs. Diameter Particle ulamerer tpm/ Page 4 Newfields Northwest Marina Park Apparent Grain Size Distribution Summary Percent Finer Than Indicated Size Sample No. Gravel Very Coarse Sand Coarse Sand Medium Sand Fine Sand Very Fine Sand Silt Clay Phi Size .3 -2 -1 0 1 2 3 4 5 6 7 8 .9 10 Sieve Size microns 3/8" #4 4750 #10 2000 #18 WO #35 500 #60 250 #120 125 #230 63 31.00 15.60 7.80 3.90 2.00 1.00 WB-08-SS-010 100.0 100.0 - 99.8 99.1 98.0 97.3 96.8 95.2 86.7 65.0 44.6 26.7 15.1 7.6 WB-08SS-010 100.0 100.0 99.9 99.6 99.0 98.4 97.9 96.3 86.0 65.1 44.8 26.5 15.3 7.8 WB-08-SS-010 100.0 100.0 110 97.8 - 95.5 94.4 93.3 90.3 81.8 64.0 43.7 26.3 14.5 6.9 MPIOU COMP 100.0 94.6 92.9 86.8 69.5 57.2 25.5 %9 9.3- -8.5 7A 6.1 4.9 3.7 MP14U COMP 100.0 98.9 92-5 1 69.6 1 39.1 1 20.6 15.2 12.9 12.6- 12.2 10.9 9.0 7.5 5.8 MP12UCOMP 1W.0 93.9 91.8 1 83.4 1 64.8 1 45.4 23.6 13.2 13.1 12.2 10.6 8.7 6.9 5.0 Notes to the Testing: 1. Organic matter was not removed prior to testing, thus the reported values are the "apparent" grain sae distribution. See narrative for discussion of the testing. OG68 =- AIM ! so �,, I" Mf � 41W. W M I= m w � Newfields Northwest Marina Park Apparent Grain Size Distribution Summary Percent Retained in Each Size Fraction Sample No. Gravel Very Coarse Sand Coarse Sand Medium Sand Fine Sand Very Fine Sand Coarse Silt Medium Silt Fine Silt Very Fine Silt Clay Total Fines Phi Size >-1 -1 to 0to1 1to2 2to3 3to4 4to5 5to6 6to7 7to8 8to9 9to10 <10 <4 Sieve Size (microns) >#10 (2000) 10 to to (2000-1000) 18-35 (1000-500) 35-60 (500-250) 60-120 (250-125) 12a230 (125-62) 62.5.31.0 310-15.6 156-7.8 7.6-3.9 3.a2.0 2.0-1.0 <1.0 C0 (<sz) WB-08-SS-010 0.2 0.6 1.1 0.7 0.6 1.6 8.5 21.6 20.5 17.9 11.6 7.5 7.6 95.2 W13-08-SS-010 0.1 0.3 0.6 0.6 0.6 1.6 10.3L20.8 20.4 18.2 11.3 7.5 7.8 96.3 WB-08-SS-010 0.0 2.2 2.3 1.1 1.1 3.0 8.5 20.3 17.4 11.8 7.7 6.9 90.3 MP10U COMP 7.1 6.2 17.2 18.4 25.7 15.6 0.7 E 1.1 1.3 1.2 1.2 3.7 9.9 MP14U COMP 7.5 22.9 30.5 18.5 5.4 2.3 0.3 1.3 1.9 1.5 1.8 5.8 12.9 MP12U COMP 8.2 8.4 18.5 19.4 21.8 10.5 0.1 1.6 2.0 1.7 1.9 5.0 13 2 'Notes to the Testing: 1. Organic matter was not removed prior to testing, thus the reported values are the "apparent" grain size distribution. See narrative for discussion of the testing. Leith-1 OA SUMMARY Client Newfields Northwest Project No.: Marina Park ARI Trip. Sample ID: CG521 Batch No.: OG68.1 Client Trip. Sample ID: W848-SS-010 Page: 1of1 Relative Standard Deviation. Sv Phi Size Sam le ID -3 1 -2 1 4 1 4 1 2 1 3 4 5 I 6 7 8 9I 0 B-08SS-01 100.0 100.0 99.8 99.1 98.0 97.3 96.8 95.2 66.7 65.0 44.6 26.7 75.1 7.6 B-08SS-01 100.0 100.0 99.9 99.6 99.0 98.4 97.9 96.3 86.0 65.1 44.8 26.5 15.3 7.8 B408-SS01 100.0 100.0 100.0 97.8 95.5 94.4 . 93.3 90.3 81.8 64.0 43.7 263 14.5 6.9 AVE NA 100.00 99.90 98.86 97.51 96.71 95.98 93.91 84.82 64.73 44.36 26.52 14.98 7AII STOEV NA 0.00 0.13 0.92 1.82 2.09 2.38 3.16 265 0.64 0.55 0.22 0.39 0.47 %RSD NA 0.00 0.13 0.93 7.8T 216 2.48 3.36 3.13 1.00 125 0.82 2.57 6.32 Tha Trinl.' ate Annlipc TnT aGnlln nn Samnips Client ID Dale Sampled Dale Extracted Date Complete OA Ratio (95-105) Data Ouafifiers Pipette Portion (5.0- 25. WB-0O"S-010 11612009 1/14/2009 1/1612009 103.9 9.3 WB-08-SS-010 116I2009 1/1412009 1116/2009 103.7 9.9 WB-08SS-010 116/2009 1/14/2009 1/16/2009 1042 9.0 MP10U COMP 121111200E 1/1412009 1/2212009 98.7 8.8 MP14U COMP 12/11/2008 1/14/2009 1/22/20D9 99.2 7.9 MP12UCOMP 12111J2008 1114/2009 122/2009 99.5 10.3 ' ARI Internal OA limits = 95.105% totes to the Testing: . Organic matter was not removed prior to testing. thus the reported values are the "apparent" grain size distribution. See narrative for discussion of the testing. OG68 MW i' !� ! ! it � sI � wK' M � � M �m Wow i � M� MAW M M OMM WAM1111111l M W M� ww!J Im w PSEP Grain Size Distribution Triplicate Sample Plot GRAVEL SAND SILT CLAY 100 90 80 70 60 A 50 T A 40 30 20 10 0 10000 1000 100 10 1 Particle Diameter (microns) �WB-08-SS-010--FWB-08-SS-010 A WB-08-SS-010 IMIMII plommillillomillillom mmillillommillilim lommillillom 1111111mmillim1111111mmillililll man p0 � �X � M � m1 � � r �. m � M i sm ii � � SAMPLE RESULTS-CONVENTIONALS ' OF06-New£ields Northwest Matrix: Sediment 'Data Release Authorized; Reported: 01/09/09 1 E Analyte Total Solids ' Total Organic Carbon ' HEM Oil & Grease ' HEM-ST NP Oil & Grease HEM Polar Oil & Grease Project: Marina Park Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Client ID: Comp CU ARI ID: 08-34190 OF06A Date Method Units R•L ANALYTICAL RESOURCES INCORPORATED Sample 12/23/08 EPA 160.3 Percent 0.01 76.20 122308#1 01/08/09 Plumb,1981 Percent 0.020 0.685 010809#1 01/07/09 9071 B mg/kg 262 < 262 U 010709#1 01/07/09 9071 B mg/kg 262 < 262 U 01/07/09 9071 B mg/kg 262 < 262 U RL Analytical reporting limit U Undetected at reported detection limit 1 Soil Sample Report-OF06 SAMPLE RESULTS-CONVENTIONALS OF06-Newfields Northwest Matrix: Sediment Project: Marina Park Data Release Authorized Event: NA Reported: 01/09/09 Date Sampled: 12/08/08 Date Received: 12/17/08 Client ID: Comp CL ARI ID: 08-34191 OF06B Analyte Date Method Units RL Total Solids 12/23/08 EPA 160.3 Percent 0.01 122308#1 Preserved Total Solids 12/23/08 EPA 160.3 Percent 0.01 122308#1 Sulfide 12/23/08 EPA 376.2 mg/kg 1.16 122308#1 Total Organic Carbon 01/08/09 Plumb,1981 Percent 0.020 010809#1 HEM Oil & Grease 01/07/09 9071 B mg/kg 221 010709#1 HEM-ST NP Oil & Grease 01/07/09 9071 B mg/kg 221 HEM Polar Oil & Grease 01/07/09 9071 B mg/kg 221 RL Analytical reporting limit U Undetected at reported detection limit ANALYTICAL RESOURCES INCORPORATED Sample ' 87.40 85.20 ' 7.09 ' f 0.055 ' i < 221 U f < 221 U j <221 U i : t r t t t P Y t. i Soil Sample Report-OF06 SAMPLE RESULTS-CONVENTIONALS ' OF06-Newfields Northwest Matrix: Sediment ' Data Release Authorized: Reported: 01/09/09 Analyte Project: Marina Park Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Client ID: LA-3 Ref ARI ID: 08-34192 OF06C Date Method Units RL ANALYTICAL RESOURCES INCORPORATED Sample ■ Total Solids 12/23/08 EPA 160.3 Percent 0.01 43.50 '122308#1 Total Organic Carbon 01/08/09 Plumb,1981 Percent 0.020 1.82 010809#1 ' HEM Oil & Grease 01/07/09 9071 B mg/kg 450 < 450 U 010709#1 ' HEM-ST NP Oil & Grease 01/07/09 9071 B mg/kg 450 < 450 U HEM Polar Oil & Grease 01/07/09 9071 B mg/kg 450 < 450 U RL Analytical reporting limit U Undetected at reported detection limit 1 Soil Sample Report-OF06 METHOD BLANK RESULTS-CONVENTIONALS ANALYTICAL OF06-New£ields Northwest RESOURCES INCORPORATED Matrix: Sediment Project: Marina Park Data Release Authorized^ Event: NA Reported: 01/09/09 Date Sampled: NA , Date Received: NA Date Units Blank , Analyte Total Solids 12/23/08 Percent < 0.01 U Preserved Total Solids 12/23/08 Percent < 0.01 U Sulfide 12/23/08 mg/kg < 0.05 U ' Total Organic Carbon 01/08/09 Percent < 0.020 U ; HEM Oil & Grease 01/07/09 mg/kg < 200 U , t HEM-ST NP Oil & Grease 01/07/09 mg/kg < 200 U HEM Polar Oil & Grease 01/07/09 mg/kg < 200 ' I c i : f 7 .i Soil Method Blank Report-OF06 ' LAB CONTROL RESULTS-CONVENTIONALS ' OF06-Newfields Northwest Matrix: Sediment 'Data Release Authorized Reported: 01/09/09 Analyte Date ' Sulfide 12/23/08 ' Total Organic Carbon 01/08/09 1 Project: Marina Park Event: NA Date Sampled: NA Date Received: NA Spike Units LCS Added Recovery mg/kg 4.58 6.36 72.0% Percent 0.468 0.500 93.6% ANALYTICAL RESOURCES V INCORPORATED ' Soil Lab Control Report-OF06 STANDARD REFERENCE RESULTS-CONVENTIONALS OF06-Newfields Northwest Matrix: Sediment Data Release Authorized: Reported: 01/09/09 Analyte/SRM ID Total Organic Carbon NIST 88704 HEM Oil & Grease Env. Rxp. #104629 Date 01/08/09 01/07/09 ANALYTICAL O l RESOURCES INCORPORATED 1 , Pxoject: Marina Park Event: NA , Date Sampled: NA 1 Date Received: NA True 1 Units SRM Value Recovery Percent 3.36 3.35 100.3% mg/kg 8,090 8,000 101.1% Soil Standard Reference Report-OF06 REPLICATE RESULTS-CONVENTIONALS OF06-Newfields Northwest 'Matrix: Sediment Data Release Authorized: Reported: 01/09/09 Analyte Date ARI ID: OF06A Client ID: Comp CU ' Total Solids 12/23/08 Total Organic Carbon 01/08/09 ARI ID: OF06B Client ID: Comp CL ' Preserved Total Solids 12/23/08 ' Sulfide 12/23/08 HEM Oil & Grease 01/07/09 ' HEM-ST NP Oil & Grease 01/07/09 Project: Marina Park ANALYTICAL RESOURCES INCORPORATED Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Units Sample Replicates) RPD/RSD Percent 76.20 76.60 0.4% 76.80 Percent 0.685 0.684 0.2% 0.682 Percent 85.20 85.20 0.1% 85.00 mg/kg 7.09 8.56 18.8% mg/kg < 221 < 225 NA < 224 mg/kg < 221 < 225 NA < 224 ' Soil Replicate Report-OF06 MS/MSD RESULTS-CONVENTIONALS ANALYTICAL OF06-Newfields Northwest RESOURCES INCORPORATED ' Matrix: Sediment Project: Marina Park Data Release Authorized: Event: NA Reported: 01/09/09 Date Sampled: 12/08/08 Date Received: 12/17/08 Spike ' Analyte Date Units Sample Spike Added Recovery ARI ID: OF06B Client ID: Comp CL Sulfide 12/23/08 mg/kg 7.09 125 141 83.6% HEM Oil & Grease 01/07/09 mg/kg < 221 8,670 9,030 96.0% , w P r Soil MS/MSD Report-OF06 ' ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET ' TOTAL METALS Sample ID: Comp CU Page 1 of 1 SAMPLE Sample ID: OF06A QC Report No: OF06-Newfields Northwest 'Lab LIMS ID: 06-34190 Project: Marina Park Matrix: Sediment Data Release Authorize Date Sampled: 12/08/08 Reported: 01/08/09 Date Received: 12/17/08 ' Percent Total Solids: 77.9% Prep Analysis Method Analysis Date CAS Number Analyte RL mg/kg-dry Q 'Prep Math Date 3050B 12/29/08 200.8 01/02/09 7440-38-2 Arsenic 0.2 3.7 12/29/08 200,8 01/02/09 7440-43-9 Cadmium 0.2 0.4 '30508 3050B 12/29/08 200.8 01/02/09 7440-47-3 Chromium 0.6 12.4 3050B 12/29/08 200.8 01/02/09 7440-50-8 Copper 0.6 18.3 12/29/08 200.8 01/02/09 7439-92-1 Lead 1 9 '3050B CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.05 0.36 3050B 12/29/08 200.8 01/06/09 7440-02-0 Nickel 0.6 9.2 3050E 12/29/08 200.8 01/02/09 7782-49-2 Selenium 0.6 0.6 U 3050E 12/29/08 200.8 01/02/09 7440-22-4 silver 0.5 044 U 3050B 12/29/08 200.8 01/02/09 7440-66-6 Zinc U-Analyte undetected at given RL ' RL-Reporting Limit 1 i 1 FORM -I ... .:. ... .. .............. d... ... .. ..... .. a.: . .. ,.......... ...,v., _. ,. ..... ....... _ice .St.iK„e.� .. ... .. ..H' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OF06A LIMS ID: 08-34190 Matrix: Sediment Data Release Authorize Reported: 01/08/09 Analysis ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CU DUPLICATE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 MATRIX DUPLICATE QUALITY CONTROL REPORT Analyte Method Sample Control Duplicate RPD Limit Arsenic 200.8 3.7 3.6 2.7% +/- 20% ' Cadmium 200.8 0.4 0.2 U 66.7% +/- 0.2 L Chromium Copper 200.8 200.8 12.4 18.3 12.1 17.1 2.4% 6.8% +/- +/- 20% 20% Lead 200.8 9 9 0.0% +/- 20% Mercury 7471A 0.36 0.72 66.7% +/- 20% Nickel 200.8 9.2 8.9 3.3% +/- 20% ' Selenium 200.8 0.6 U 0.6 U 0.0% +/- 0.6 L Silver 200.8 0.2 U 0.2 U 0.0% +/- 0.2 L Zinc 200,8 44 40 9.5� +/- 20`b ; Reported in mg/kg-dry *-Control Limit Not Met L-RPD Invalid, Limit - Detection Limit t�. E •uCiRMV 't9 _..,....... , , , .,.................. _._.......... .. . ,.,._.,...::.. ...................... ..............._ .._......_._..., ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET METALS sample ID: Comp CU 'TOTAL Page 1 of 1 MATRIX SPIKE Lab Sample ID: OF06A QC Report No: OF06-Newfields Northwest LIMS ID: 08-34190 Project: Marina Park Matrix: Sediment Data Release Authorize Date Sampled: 12/08/08 Reported: 01/08/09 Date Received: 12/17/08 ' MATRIX SPIKE QUALITY CONTROL REPORT Analysis Spike % Analyte Method Sample Spike Added Recovery Q ' Arsenic 200.8 3.7 32.8 31.3 93.0% Cadmium 200.8 0.4 28.6 31.3 90.1% 200.8 12.4 39.4 31.3 86.3% 'Chromium Copper 200.8 18.3 45.2 31.3 31.3 65.9% 99.0% Lead 200.8 9 40 Mercury 7471A 0.36 0.94 0.510 114% Nickel 200.8 9.2 41.9 31.3 104% Selenium 200.8 0.6 U 93.7 100 93.7% Silver 200.8 0.2 U 16.2 31.3 51.8% N 'Zinc 200.8 44 142 100 98.0% Reported in mg/kg-dry Limit Not Met i 'N-Control H-% Recovery Not Applicable, Sample Concentration Too High NA -Not Applicable, Analyte Not Spiked j ' Percent Recovery Limits: 75-125% i I. FORM-V ANALYTICAL O gESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: LAB CONTROL Page 1 of 1 Lab Sample ID: OF06LCS QC Report No: OF06-Newfields Northwest LIMS ID: 08-34191 Project: Marina Park Matrix: Sediment ' Data Release Authorited: Date Sampled: NA Rdported: 01/08/69 Date Received: NA ' BLANK SPIKE QUALITY CONTROL REPORT Analysis Spike Spike ' Analyte Method Found Added Recovery Q Arsenic 200.0 24.4 25.0 97.6% Cadmium 200.8 23.5 25.0 94.0% Chromium 200.8 Copper 200.8 24.8 23.1 25.0 25.0 99.2% 92.4% Lead 200.8 26 25 104% Mercury 7471A 1.01 1.00 101% Nickel 200.8 26.8 25.0 107% Selenium 200.8 77.4 80.0 96.8% '. Silver 200.8 25.2 25.0 101s Zinc 200.8 78 80 97.5% ' Reported in mg/kg-dry i N-Control limit not met NA -Not Applicable, Analyte Not Spiked Control Limits: 80-1201 i FORM-VII INORGANICS ANALYSIS DATA SHEET 'TOTAL METALS Page 1 of 1 'Lab Sample ID: OF06B LIMS ID: 08-34191 Matrix: Sediment Data Release Authoriz 'Reported: 01/08/09 Percent Total Solids: 84.4% ' Prep Prep Analysis Analysis Math Date Method Date ANALYTICAL RESOURCES 011, INCORPORATED Sample ID: Comp CL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 CAS Number Analyte 3050E 12/29/08 200.8 01/02/09 7440-38-2 3050E 12/29/08 200.8 01/02/09 7440-43-9 305013� 12/29/08 200.8 01/02/09 7440-47-3 3050B 12/29/08 200.8 01/02/09 7440-50-8 3050B 12/29/08 200.8 01/02/09 7439-92-1 CLP 12/29/08 7471A 12/31/08 7439-97-6 3050B 12/29/08 200.8 01/06/09 7440-02-0 3050B 12/29/08 200.8 01/02/09 7782-49-2 3050E 12/29/08 200.8 01/02/09 1440-22-4 3050E 12/29/08 200.8 01/02/09 7440-66-6 U-Analyte undetected at given RL RL-Reporting Limit Arsenic Cadmium Chromium Copper Lead Mercury Nickel Selenium Silver Zinc RL 0.2 0.2 0.6 0.6 1 0.05 0.6 0.6 0.2 5 mg/kg-dry 2.1 0.2 2.8 1.2 1 0.05 1.9 0.6 0.2 6 Q U U U U U FORM -I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OF06C LIMS ID: 08-34192 Matrix: Sediment Pate Release Authoriz Reported: 01/08/09 Percent Total Solids:, 44.0% Prep Prep Analysis Analysis Meth Date Method Date ANALYTICAL RESOURCES INCORPORATED Sample ID: LA-3 Ref SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 CAS Number Analyte RL mg/kg-dry Q 3050B 12/29/08 200.8 01/02/09 7440-38-2 3050B 12/29/08 200.8 01/02/09 7440-43-9 3050B 12/29/08 200.8 01/02/09 7440-47-3 3050E 12/29/08 200.8 01/02/09 7440-50-8 3050B 12/29/08 200.8 01/02/09 7439-92-1 CLP 12/29/08 7471A 12/31/08 7439-97-6 3050B 12/29/08 200.8 01/07/09 7440-02-0 3050B 12/29/08 200.8 01/02/09 7782-49-2 3050E 12/29/08 200.8 01/02/09 7440-22-4 3050E 12/29/08 200.8 01/02/09 7440-66-6 U-Analyte undetected at given RL RL-Reporting Limit Arsenic 0.4 5.5 Cadmium 0.4 0.9 Chromium 1 40 Copper 1 22 Lead 2 13 Mercury 0.09 0.10 Nickel 1 24 Selenium 1 1 U Silver 0.4 0.4 U Zinc 8 83 FORM-1 INORGANICS ANALYSIS DATA SHEET 'TOTAL METALS Page 1 of 1 'Lab Sample ID: OF06E LIMS ID: 08-34194 Matrix: Sediment Data Release Authorize Reported: 01/08/09 Percent T< ' Prep Meth CLP U-Analytf RL-Report: ANALYTICAL RESOURCES INCORPORATED ' Sample ID: MP-10L SAMPLE QC Report No: OF06-Newfields Northwest Project! Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 ANALYTICAL © ' RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: 14P-12L Page 1 of 1 SAMPLE Lab Sample ID: OF06G QC Report No: OF06-Newfields Northwest LIMS rD: 08-34196 Project: Marina Park Matrix: Sediment Data Release Authorized Date Sampled: 12/08/08 Reported: 01/08/09 el Date Received: 12/17/08 Percent Total Solids: 59.0% , Prep Prcp Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-dry Q ' CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.06 0.07 U-Analyte undetected at given RL RL-Reporting Limit i r: FORM -I ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET ' METALS Sample ID: 14P-13V 'TOTAL Page 1 of 1 SAMPLE Lab Sample ID: 0F06H QC Report No: OF06-Newfields Northwest LIMS ID: 08-34197 Project: Marina Park Matrix: Sediment Data Release Authorize Date Sampled: 12/08/08 . Reported: 01/08/09 Date Received: 12/17/08 ' Percent Total Solids: 76.4% ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-dry Q CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.05 1.11 ' U-Analyte undetected at given RL RL-Reporting Limit i i i r { FORM -I i T........ ........ .. .... .o..n.. ................... .. .. . .... L\:S •........._. u....r n.i:J.. .'... .. ...._:.iY iC::... ... r. ....... . ...n. n. :' n� ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: MP-13L Page 1 of 1 SAMPLE Lab Sample ID: OF06I QC Report No: OF06-Newfields Northwest LIMS ID: 08-34198 Project: Marina Park Matrix: Sediment , Data Release Authorize Date Sampled: 12/08/08 Reported: 01/08/09 Date Received: 12/17/08 Percent Total Solids: 85.5% ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Anaiyte RL mg/kg-dry Q ' CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.05 0.05 U U-Analyte undetected at given RL RL-Reporting Limit i } k FORM-1 ANALYTICAL RESOURCES 1 INCORPORATED INORGANICS ANALYSIS DATA SHEET / Sample ID: MP-1� % r� s�ac�� WA TOTAL METALS 1 Page 1 of 1 SAMPLE Lab Sample ID: O106J QC Report No: OF06-New£ields Northwest 1 LIMS ID: 08-34199 Project: Marina Park Matrix: SedimentIt Data Release Authorize Date Sampled: 1?_/08/08 t d01/08/09 Date Received: 12/17/08 : 1 Repor e Percent Total Solids: 84.2E 1 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 1 U-Analyte undetected at given RL RL-Reporting Limit 1 1 1 1 1 1 1 1 • i 1 1 FORM -I i RL mg/kg-dry Q 0.06 0.06 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OF06L LIMS XD: 08-34201 Matrix: Sediment Data Release Authorize Reported: 01/08/09 Percent Total Solids: 61.1% ANALYTICAL /�` RESOURCES v INCORPORATED Sample ID: Me-15U , SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park ' Date Sampled: 12/08/08 Date Received: 12/17/08 Prep Prep Analysis Analysis ' Meth Date Method Date CAS Number Analyte RL mg/kg-dry Q CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.06 3.35 U-Analyte undetected at given RL RL-Reporting Limit I 11 FORM-1 I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET 'TOTAL METALS Sample ID: MP-15L Page 1 of 1 SAMPLE 'Lab Sample ID: OE'06M QC Report No: OF06-Newfields Northwest LIMS ID: 08-34202 Project: Marina Park Matrix: Sediment Data Release Authorize Date Sampled: 12/08/08 Reported: 01/08/01 Date Received: 12/17/08 Percent Total Solids: 90.8% . prep Prep Analysis Analysis - Meth Date Method Date CAS Number Analyte RL CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury ' U-Analyte undetected at given RL RL-Reporting Limit FORM-1 mg/kg-dry Q 0.05 0.05 U • \ `. e • ..• .. •. ..w .r.... ....w�.a •. i4'.—.—�..ir'... ..•i ... .. .... .Y.. • .. • utr .. 1. 'n •..i. r.l ...G). r••... •i.. ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: MP-16U Page 1 of 1 SAMPLE Lab Sample ID: OF06N QC Report No: OF06-Newfields Northwest LIMS ID: 08-34203 Project: Marina Park Matrix: Sediment Data Release Authorize Date Sampled: 12/08/08 Reported: 01/08/09 Date Received: 12/17/08 Percent Total Solids: 81.4% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-dry Q ' CLP 12/29/08 7471A 12/31/08 7439-97-6 Mercury 0.05 0.07 U-Analyte undetected at given RL RL�Reporting Limit i t i 'j i FOAM-1 I I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page I of I Lab Sample ID: OF060 LIMS ID: 08-34204 Matrix: Sedim, Data Release Reported: Ill Percent Total Prep P2 Math Dc CLP 12/2 U-Analyte un RL-Reporting � I � I � I II II II II II II II II ANALYTICAL RESOURCES# INCORPORATED Sample ID: 1-2-16L SAMPLE QC Report NO: OFOG-Newfields Northwest Project: Marina Park 1 INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OF06MB LIMS ID: 08-34191 Matrix: Sediment Data Release Authorized: Reported: 01/08/09 Percent Total Solids: NA Prep Prep Analysis Analysis Meth Date Method Date ANALYTICAL Q RESOURCES INCORPORATED Sample ID: METHOD BLANK QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: NA Date Received: NA CAS Number Analyte RL mg/kg-dry Q 3050E 12/29/08 200.8 01/02/09 7440-38-2 3050B 12/29/08 200.8 01/02/09 7440-43-9 3050E 12/29/08 200.8 01/02/09 7440-47-3 3050E 12/29/08 200.8 01/02/09 7440-50-8 3050E 12/29/08 200.8 01/02/09 7439-92-1 CLP 12/29/08 7471A 12/31/08 7439-97-6 3050B 12/29/08 200.8 01/06/09 7440-02-0 3050B 12/29/08 200.8 01/02/09 7782-49-2 3050E 12/29/08 200.E O1/02/09 7440-22-4 3050E 12/29/08 200.0 01/02/09 7440-66-6 U-Analyte undetected at given RL RL-Reporting Limit Arsenic 0'.2 0.2 U Cadmium 0.2 0.2 U Chromium 0.5 0.5 U Copper 0.5 0.5 U Lead 1 1 U Mercury 0.05 0.05 U Nickel 0.5 0.5 U Selenium 0.5 0.5 U Silver 0.2 0.2 U Zinc 4 4 U FORM -I ... .. . . .... a .. .. r .. • .... .. ....F ANALYTICAL /� ' RESOURCES V INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: LAB CONTROL Page 1 of 1 Sample ID: OF06LCS QC Report No: OF06-Newfields Northwest LIMS ID: 08-34191 Project: Marina Park 'Lab Matrix: Sediment Data Release Authorize Date Sampled: NA Reported: 01/08/09 Date Received: NA ' BLANK SPIKE QUALITY CONTROL REPORT ' Analysis Spike Spike & Analyte Method Found Added Recovery Q S 'Arsenic 200.8 24.4 25.0 97.6% Cadmium 200.8 23.5 25.0 94.0& Chromium 200.8 24.8 25.0 9.9.2% Copper 200.8 23.1 25.0 25 92.4% 1098 Lead 200.8 26 t Mercury 7971A 1.01 1.00 101% t Nickel 200.8 25.8 25.0 107& i Selenium 200.8 77.4 80.0 96.8% Silver 200.8 25.2 25.0 101% 200.8 78 80 97.5% 'Zinc Reported in mg/kg-dry N-Control limit not met ' NA -Not Applicable, Analyte Not Spiked I. Control Limits: 80-120% i FORM-VII ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: 14P10U COMP Page 1 of 1 SAMPLE Lab Sample ID: OG68A QC Report No: OG68-Newfields Northwest LIMS ID: 09-459 Project: MARINA PARK Matrix: Sediment Data Release Authorized: Date Sampled: 12/11/08 Reported: 01/19/09 Date Received: 01/07/09 Percent Total Solids: 78.0% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-dry CLP 01/13/09 7471A 01/16/09 7439-97-6 Mercury 0.06 0.10 U-Analyte undetected at given RL RL-Reporting Limit ©' FORM -I 1 1 INORGANICS ANALYSIS DATA SHEET TOTAL METALS 1 Page 1 of 1 Lab Sample ID: OG68A 1 LIMS ID: 09-159 Matrix: Sediment Data Release Authorized: / Reported: 01/19/09 1 ANALYTICAL RESOURCES INCORPORATED Sample ID: MP10U COMP DUPLICATE QC Report No: OG68-Newfields Northwest Project: MARINA PARK Date Sampled: 12/11/08 Date Received: 01/07/09 MATRIX DUPLICATE QUALITY CONTROL REPORT 1 Analysis Control Analyte Method Sample Duplicate RPD Limit 1 Mercury 7471A 0.10 0.11 Reported in mg/kg-dry 1 *-Control Limit Not Met L-RPD Invalid, Limit = Detection Limit 1 i 1 i i 1 1 1 1 1 1 FORM -VI 9 9.5% +/- 0.06 L INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OG68A LIMS rD: 09-459 Matrix: Sediment Data Release Authorized Reported: 01/19/09 ANALYTICAL ' RESOURCES O INCORPORATED Sample ID: 14P10U COMP MATRIX SPIKE li QC Report No: OG68-Newiields Northwest Project: MARINA PARK Date Sampled: 12/11/08 , Date Received: 01/07/09 MATRIX SPIKE QUALITY CONTROL REPORT Analysis Spike Analyte Method Sample Spike Added Mercury 7471A 0.10 0.55 0.570 Reported in mg/kg-dry N-Control Limit Not Met H-8 Recovery Not Applicable, Sample Concentration Too High NA -Not Applicable, Analyte Not Spiked Percent Recovery Limits: 75-125% Recovery Q 76.9� I i I i 1{ FORM-V ' INORGANICS ANALYSIS DATA SHEET ANALYTICAL RESOURCES INCORPORATED TOTAL METALS Sample ID: 1AP14U COMP ' Page 1 of 1 SAMPLE Lab Sample ID: OG68B QC Report No: OG68-Newfields Northwest 'LIMS ID: 09-460 Project: MARINA PARK Matrix: Sediment Data Release Authorized Date Sampled: 12/11/08 Reported: 01/19/09 & Date Received: 01/07/09 tPercent Total Solids: 78.3% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL CLP 01/13/09 7471A 01/16/09 7439-97-6 Mercury tU-Analyte undetected at given RL RL-Reporting Limit 1 1 b ' FORM -I mg/kg-dry Q 0.06 0.85 ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NP12U COMP Page 1 of 1 SAMPLE Lab Sample ID: OG68C QC Report No: OG68-Newfields Northwest LIMS ID! 09-461 Project: MARINA PARK Matrix: Sediment Data Release Authorized: Date Sampled: 12/11/08 Reported: 01/19/09 Date Received: 01/07/09 Percent Total Solids: 80.2% Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL CLP 01/13/09 7471A 01/16/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit mg/kg-dry Q 0.05 0.31 ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: METHOD BLANK 'Page 1 of 1 Lab Sample ID: OG68MB QC Report No: OG68-New£ields Northwest LIMS ID: 09-460 'Sediment / Project: MARINA PARK Matrix: Sedimenedimen t Data Release Authorized Date Sampled: NA �J�/•yJI��/// Reported: 01/19/09 Date Received: NA ' Percent Total Solids: NA Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte CLP 01/13/09 7471A 01/16/09 7439-97-6 Mercury 'U-Analyte undetected at given RL RL-Reporting Limit 1 ' FORM -I RL mg/kg-dry Q 0.05 0.05 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OG68LCS LIMS ID: 09-460 Matrix: Sediment Data Release Authorized: Reported: 01/19/09 ANALYTICAL /� RESOURCES v INCORPORATED Sample ID: LAB CONTROL QC Report No: OG68-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA BLANK SPIKE QUALITY CONTROL REPORT Analysis Spike Spike P6 Analyte Method Found Added Recovery Mercury 7471A 1.04 1.00 104% Reported in mg/kg-dry N-Control limit not met NA -Not Applicable, Analyte Not Spiked Control Limits: 80-120% FORM-VII I 'ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OG93A LIMS ID: 09-609 Matrix: Sediment Data Release Authorized: Reported: 01/12/09 Date Extracted: 01/09/09 Date Analyzed: 01/12/09 14:30 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP CU SAMPLE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 5.43 g-dry-wt Final Extract Volume: 0.50 mL Dilution 'Factor: 1.00 Alumina Cleanup: Yes Moisture: 23.5% CAS Number Analyte RL Result Q ' TBT_ION Tributyltin Ion 3.6 < 3.6 U DBT ION Dibutyltin Ion 5.3 < 5.3 U BT ION Butyltin Ion 3.8 < 3.8 U Reported in µg/kg (ppb) TBT Surrogate Recovery !_ Tripropyl Tin Chloride 67.7& 'Tripentyl Tin Chloride 71.5% FORM I ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OG93B LIMS ID: 09-610 Matrix: Sediment Data Release Authorized Reported: 01/12/09 Date Extracted: 01/09/09 Date Analyzed: 01/12/09 15:28 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No CAS Number TBT_ION DBT ION BT_ION Analyte Tributyltin Ion Dibutyltin Ion Butyltin Ion Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 8 Tripentyl Tin Chloride 8 ANALYTICAL AESOURCE3 INCORPORATED Sample IDs COMP CL SAMPLE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 5.16 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 16.8t RL Result Q 3.7 < 3.7 U 5.6 < 5.6 U 4.0 < 4.0 U 3.7& 4.6% I 1 I L FORM I 'ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OG93C LIMS ID: 09-611 Matrix: Sediment Data Release Authorized Reported: 01/12/09 Data Extracted: 01/09/09 Date Analyzed: 01/12/09 15:47 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: LA-3 REF. SAMPLE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 5.15 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 54.0 RL Result Q TBT_ION Tributyltin Ion D13T_ION Dibutyltin Ion BT ION Butyltin Ion Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride Tripentyl Tin Chloride 74.5% 81.0% 3.8 < 3.8 U 5.6 < 5.6 U 4.0 < 4.0 U FORM I ORGANICS ANALYSIS DATA SHEET Tributyl Tine by Krone 1988 SIX GC/MS Page 1 of 1 Lab Sample ID: OG93A LIMS ID: 09-609 Matrix: Sediment Data Release Authorized:x Reported: 01/12/09 Date Extracted MS: 01/09/09 Date Analyzed MS: 01/12/09 14:49 MSD: 01/12/09 15:09 Instrument/Analyst MS: NT2/YZ MSD: NT2/YZ Silica Gel Cleanup: No Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP CU MATRIX SPIKE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount MS: 5.52 g-dry-wt MSD: 5.55 g-dry-wt Final Extract Volume MS: 0.5 mL MSD: 0.5 mL Dilution Factor MS: 1.00 MSD: 1.00 Alumina Cleanup: Yes Moisture: 23.5% Spike MS Spike MSD Sample MS Added -MS Recovery MSD Added-MSD Recovery RPD Tributyltin Ion < 3.6 U 33.9 40.4 83.98 41.8 40.2 104% 20.9% Dibutyltin Ion < 5.3 U 42.0 34.8 121% 34.8 34.6 101% 18.8% Butyltin Ion < 3.8 U 22.3 28.3 78.88 18.9 28.1 67.3* 16.5% Results reported in µg/kg RPD calculated using sample concentrations .per SW846. 1'I I 11 FORM III ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIX GC/MS Page 1 of 1 Lab Sample ID: OG93A LIMS ID: 09-609 Matrix: Sediment 'Data Release Authorized Reported: 01/12/09 Date Extracted: 01/09/09 Date Analyzed: 01/12/09 14:49 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No fCAS Number Analyte TB7 DB7 BT ANALYTICAL RESOURCES INCORPORATED Sample ID: COMP CU MATRIX SPIKE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 5.52 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 23.5% RL Result Q ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: OG93A LIMS ID: 09-609 Matrix: Sediment Data Release Authorized: Reported: 01/12/09 Date Extracted: 01/09/09 Date Analyzed: 01/12/09 15:09 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No CAS Number Analyse ' ANALYTICAL ® RESOURCES INCORPORATED Sample ID: COMP CU MATRIX SPIKE DUP QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 ' Sample Amount: 5.55 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes Moisture: 23.5% RL Result Q TBT ION Tributyltin Ion 3.5 --- ' DBT_ION Dibutyltin Ion 5.2 --- BT ION Butyltin Ion 3.7 --- i Reported in µg/kg (ppb) ' TBT Surrogate Recovery f I Tripropyl Tin Chloride 74.2%- , I Tripentyl Tin Chloride 75.41d FORM I I 'ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 ' Lab Sample ID: MB-010909 LIMS ID: 09-609 'Matrix: Sediment Data Release Authorized Reported: 01/12/09 'Date Extracted: 01/09/09 Date Analyzed: 01/12/09 13:51 Instrument/Analyst: NT2/YZ Silica Gel Cleanup: No ' CAS Number Analyte TBT_ION Tributyltin Ion 3.9 ' DBT ION Dibutyltin Ion 5.8 BT_ION Butyltin Ion 4.1 Reported in µg/kg (ppb) ' TBT Surrogate Recovery Tripropyl Tin Chloride 76.2% Tripentyl Tin Chloride 81.7% FORM I ANALYTICAL RESOURCES INCORPORATED Sample ID: MB-010909 METHOD BLANK QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Date Sampled: NA Date Received: NA Sample Amount: 5.00 g-dry-wt Final Extract Volume: 0.50 mL Dilution Factor: 1.00 Alumina Cleanup: Yes RL Result Q < 3.9 U < 5.8 U < 4.1 U 11 ORGANICS ANALYSIS DATA SHEET Tributyl Tins by Krone 1988 SIM GC/MS Page 1 of 1 Lab Sample ID: LCS-010909 LIMS ID: 09-609 Matrix: Sediment Data Release Authorized Reported: 01/12/09 Date Extracted LCS: 01/09/09 Date Analyzed LCS: 01/12/09 14:11 Instrument/Analyst LCS: NT2/YZ Silica Gel Cleanup: No Analyse Tributyltin Ion Dibutyltin Ion Butyltin Ion ANALYTICAL RESOURCES V INCORPORATED Sample ID: LCS-010909 LAB CONTROL SAMPLE QC Report No: OG93-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA Sample Amount LCS: 5.00 g-dry-wt Final Extract Volume LCS: 0.50 mL Dilution Factor LCS: 1.00 Alumina Cleanup: Yes Spike LCS Added Recovery 41.5 44.6 93.09d 33.5 38.4 87.2%' 23.8 31.2 76.3%* Reported in µg/kg (ppb) TBT Surrogate Recovery Tripropyl Tin Chloride 82.71% Tripentyl Tin Chloride 96.496 11 FORM III ' Matrix: Sediment ANALYTICAL RESOURCES INCORPORATED TBT SURROGATE RECOVERY SUMMARY QC Report No: OG93-Newfields Northwest Project: MARINA PARK Event: NA Client ID TPRT TPNT TOT OUT ' MB-010909 76.2% 81.7% 0 LCS-010909 82.7% 96.4% 0 COMP CU 67.7% 71.5% 0 COMP CU MS 71.8% 74.2% 0 ' COMP CU MSD 74.2% 75.4% 0 COMP CL 83.7% 84.6% 0 LA-3 REF. 74.5% 81.0% 0 ' LCS/MB LIMITS QC LIMITS = Tripropyl Tin Chloride (30-160) (30-160) '(TPRT) (TPNT) = Tripentyl Tin Chloride (30-160) (30-160) Prep Method: SW3546 Analytical Method: TBT (Hexyl) Krone 1988 ' Log Number Range: 09-609 to 09-611 I Page 1 for OG93 FORM -II TBT ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: MB-123008 LIMS ID: 08-34190 Matrix: Sediment Data Release Authorized Reportedt 01/05/09 Date Extracted: 12/30/08 Date Analyzed: 01/02/09 12:51 Instrument/Analyst: ECDS/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample IDt MB-123008 METHOD BLANK QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: NA Date Received: NA Sample Amount: 25.0 g Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: NA CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U . 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 84.2t Tetrachlorometaxylene 87.2% FORM I I 'ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 'Lab Sample ID: OF06A LIMS ID: 08-34190 Matrix: Sediment c� ' Data Release Authorized: \ Reported: 01/05/09 Date Extracted: 12/30/08 Date Analyzed: 01/02/09 13:26 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CU SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.7 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 22.6W RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 76.5% Tetrachlorometaxylene 86.8% FORM I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OF06B LIMS ID: 08-34191 Matrix: Sediment Cy Data Release Authorized: 1%(yj Reported: 01/05/09 Date Extracted: 12/30/08 Date Analyzed: 01/02/09 13:43 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.9 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 11,0W CAS Number Analyte RL Result 12674-11�2 Aroclor 1016 19 < 19 U 53469-21-9 Aroclor 1242 19 < 19 V 12672-29-6 Aroclor 124E 19 < 19 U 11097-69-1 Aroclor 1254 19 < 19 U 11096-82-5 Aroclor 1260 19 < 19 U 11104-28-2 Aroclor 1221 19 < 19 U 11141-16-5 Aroclor 1232 19 < 19 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 86.5$ Tetrachlorometaxylene 87.81d FORM I I ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/ECD Page 1 of 1 Lab Sample ID: OF06C LIMS ID: 08-34192 Matrix: Sediment Data Release Authorized: Reported: 01/05/09 Date Extracted: 12/30/08 'Date Analyzed: 01/02/09 14:00 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes 'Acid Cleanup: Yes Florisil Cleanup: No ANALYTICAL O RESOURCES INCORPORATED Sample ID: LA-3 Ref SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: 52.5t CAS Number Analyte RL Result 12674-11-2 Aroclor 1016 20 < 20 U 53469-21-9 Aroclor 1242 20 < 20 U 12672-29-6 Aroclor 1248 20 < 20 U 11097-69-1 Aroclor 1254 20 < 20 U 11096-82-5 Aroclor 1260 20 < 20 U 11104-28-2 Aroclor 1221 20 < 20 U 11141-16-5 Aroclor 1232 20 < 20 U Reported in µg/kg (ppb) PCB Surrogate Recovery Decachlorobiphenyl 77.8%- Tetrachlorometaxylene 85.0% FORM I ANALYTICAL RESOURCES INCORPORATED SW8082/PCB SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OF06-Newfields Northwest Project: Marina Park DCBP DCBP TCMX TCMX Client ID % REC LCL-IICL % REC LCL-IICL TOT OUT MB-123008 84.2W 65-117 87.2% 63-119 0 LCS-123008 86.5% 65-117 95.0% 63-119 0 Comp CU 76.5W 43-148 86.0 48-123 0 Comp CL 86.St 43-148 87.8* 48-123 0 LA-3 Ref 77.8t 43-148 85.0% 48-123 0 PSDDA Control Limits Prep Method: SW3550B Log Number Range: 08-34190 to 08-34192 FORM -II SW8082 Page 1 for OF06 I 'ORGANICS ANALYSIS DATA SHEET PSDDA PCB by GC/BCD Page 1 of 1 'Lab Sample ID: LCS-123008 LIMS ID: 08-34190 Matrix: Sediment 'Data Release Authorized: Reported: 01/05/09 Date Extracted: 12/30/08 'Date Analyzed: 01/02/09 13:09 Instrument/Analyst: ECD5/JGR GPC Cleanup: No Sulfur Cleanup: Yes Acid Cleanup: Yes Florisil Cleanup: No ' Analyte Aroclor 1016 ' Aroclor 1260 II ANALYTICAL O RESOURCES INCORPORATED Sample ID: LCS-123008 LAB CONTROL QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: NA Date Received: NA Sample Amount: 25.0 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: No Percent Moisture: NA Lab Spike Control Added Recovery 93.1 100 93.1% 88.4 100 88.4% PCB Surrogate Recovery Decachlorobiphenyl 86.5% Tetrachlorometaxylene 95.0% ' Results reported in µg/kg (ppb) FORM III ORGANICS ANALYSIS DATA SHEET PSDDA Peaticidea/PCB by GC/ECD Page 1 of 1 Lab Sample ID: OF06A LIMS ID: 08-34190 Matrix: Sediment .� Data Release Authorized: ll r , Reported: 01/08/09 �/ Date Extracted: 12/30/08 Date Analyzed: 01/07/09 12:35 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CU SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: 22.6% CAS Number Analyte RL Result 319-84-6 alpha-BHC 0.98 < 0.98 U 319-85-7 beta-BHC 0.98 < 0.98 U 319-86-8 delta-BHC 0.98 < 0.98 U 58-89-9 gamma-BHC (Lindane) 0.98 < 0.98 U 76-44-8 Heptachlor 0.98 < 0.98 U 309-00-2 Aldrin 0.98 < 0.9B U 1024-57-3 Heptachlor Epoxide 0.98 < 0.98 U 959-98-8 Endosulfan I 6.98 < 0.98 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4--DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,4'-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.8 < 9.8 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U 5163-74-2 gamma Chlordane 0.98 < 0,98 U 5103-71-9 alpha Chlordane 0.98 < 0.98 U 8001-35-2 Toxaphene 98 < 98 U 789-02-6 2,4'-DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Peet/PCB Surrogate Recovery Decachlorobiphenyl 80.5% Tetrachlorometaxylene 68.2% LJ E E I E F FORM I I I 'ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 ' Lab Sample ID: OF06B LIMS ID: 08-34191 Matrix: Sediment Release Authorized:\J 1 'Data Reported: 01/08/09 �/ ANALYTICAL O RESOURCES INCORPORATED Sample ID: Comp CL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 'Date 'Sulfur Date Extracted: 12/30/08 Sample Amount: Analyzed: 01/07/09 12:55 Final Extract Volume: Instrument/Analyst: ECD4/AAR Dilution Factor: GPC Cleanup: No Silica Gel: Cleanup: Yes Florisil Cleanup: No Percent Moisture: Acid Cleanup: No CAS Number Analyte RL 26.6 g-dry-wt 5.0 mL 1.00 Yes 11.0% Result ' 319-84-6 alpha-BHC 0.94 0.94 < 0.94 < 0.94 U U 319-85-7 beta-BHC 0.94 < 0.94 U ' 319-86-8 58-89-9 delta-BHC gamma-BHC (Lindane) 0.94 < 0.94 U 76-44-8 Heptachlor 0.94 0.94 < 0.94 < 0.94 U U 309-00-2 1024-57-3 Aldrin Heptachlor Epoxide 0.94 < 0.94 U ' 959-98-8 Endosulfan I 0.94 1.9 < 0.94 < 1.9 U U 60-57-1 Dieldrin 1.9 < 1.9 U 72-55-9 4,4--DDE 1.9 < 1.9 U 72-20-8 Endrin 1.9 < 1.9 U t 33213-65-9 Endosulfan II 1.9 < 1.9 U 72-54-8 4,4--DDD 1.9 < 1.9 U 1031-07-8 Endosulfan Sulfate 1.4 < 1.94 U ' 50-29-3 4,4'-DDT < 4 U 72-43-5 Methoxychlor .9 1 < 19 U 7421-93-4 Endrin Aldehyde .. 0.944 < 0.944 U ' 5103-74-2 5103-71-9 gamma Chlordane alpha Chlordane 0.94 < 0.94 < 94 U U 8001-35-2 Toxaphene 94 1.9 < 1.9 U 789-02-6 2,4--DDT 1.9 < 1.9 U ' 3424-82-6 53-19-0 2,4'-DDE 2,4'-DDD 1.9 < 1.9 U Reported in µg/kg (ppb) ' Pest/PCB Surrogate Recovery Decachlorobiphenyl 78.5% ' Tetrachlorometaxylene 63.5% I I FORM I ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 Lab Sample ID: OF06C LIMS IDt 08-34192 Matrix: Sediment T Data Release Authorized: Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/07/09 13:15 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No Acid Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: LA-3 Ref SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.6 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: 52.5% CAS Number Analyte RL Result 319-84-6 alpha-BHC 0.98 < 0.98 U 319-85-7 beta-BHC 0.98 < 0.98 U 319-86-8 delta-BHC 0.98 < 0.98 U 58-89-9 gamma-BHC (Lindane) 0.98 < 0.98 U 76-44-8 Heptachlor 0.98 < 0.98 U 309-00-2 Aldrin 0.98 < 0.98 U 1024-57-3 Heptachlor Epoxide 0.98 < 0.98 U 959-98-8 Endosulfan I 0.98 < 0.98 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0 U 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4'-DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 < 2.0 U 50-29-3 4,4'-DDT 2.0 < 2.0 U 72-43-5 Methoxychlor 9.8 < 9.8 U 7421-93-4 Endrin Aldehyde 2.0 < 2.0 U 5103-74-2 gamma Chlordane 0.98 < 0.98 U 5103-71-9 alpha Chlordane 0.98 < 0.98 U 8001-35-2 Toxaphene 98 < 98 U 789-02-6 2,4--DDT 2.0 < 2.0 U 3424-82-6 2,4'-DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in µg/kg (ppb) Peat/PCB Surrogate Recovery Decachlorobiphenyl 80.0% Tetrachlorometaxylene 70.0% FORM I 1 ' SW8081 PESTICIDE SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY ' Matrix: Sediment t QC Report No: OF06-Newfields Northwest Project: Marina Park Client ID DCBP TCMX TOT OUT MB-123008 82.2% 73.5% 0 LCS-123008 83.8% 70.5% 0 Comp CU 80.5% 68.2% 0 ' Comp CL 78.5% 63.5% 0 LA-3 Ref 80.0% 70.0% 0 ' LCS/MB LIMITS QC LIMITS = Decachlorobiphenyl (65-125) (52-143) '(DCBP) (TCMX) = Tetrachlorometaxylene (53-112) (43-128) Prep Method: SW3550B Log Number Range: 08-34190 to 08-34192 FORM -II SW8081 Page 1 for OF06 1 ANALYTICAL RESOURCES INCORPORATED ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 Lab Sample ID: LCS-123008 LIMS ID: 08-34190 Matrix: Sediment Data Release Authorized; V7 5 Reported: 01/08/09 Date Extracted: 12/30/08 Date Analyzed: 01/07/09 12:14 Instrument/Analyst: ECD4/AAR GPC Cleanup: No Sulfur Cleanup: Yes Florisil Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-123008 LAB CONTROL QC Report No: OF06-New£ields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.0 g-dry-wt Final Extract Volume: 5.0 mL Dilution Factor: 1.00 Silica Gel: Yes Percent Moisture: NA Analyte Lab Control Spike Added Recovery alpha-BHC 3.12 4.00 78.0% beta-BHC 3.30 4.00 B2.58 delta-BHC 3.52 4.00 88.0% gamma-BHC (Lindane) 3.40 4.00 85.0% Heptachlor 3.24 4.00 81.0% Aldrin 3.46 4.00 86.5% Heptachlor Epoxide 4.16 4.00 104% Endosulfan I 3.74 4.00 93.5% Dieldrin 7.62 8.00 95.2% 4,4+-DbE 8.82 8.00 110% Endrin 7.34 8.00, 91.8% Endosulfan II 7.94 8.00 99.2% 4,4'-DDD 7.64 8.00 95.5% Endosulfan Sulfate 7.86 8.00 98.2% 4,4'-DDT 8.24 8.00 103% Methoxychlor 39.6 40.0 99.0% Endrin Aldehyde 5.08 8.00 63.5% gamma Chlordane 4.02 4.00 100% alpha Chlordane 4.08 4.00 102% Pest/PCB Surrogate Recovery Decachlorobiphenyl 83.8% Tetrachlorometaxylene 70.5% Reported in µg/kg (ppb) FORM III 'ORGANICS ANALYSIS DATA SHEET PSDDA Pesticides/PCB by GC/ECD Page 1 of 1 ' Lab Sample ID: MB-123008 LIMS ID: 08-34190 Matrix: Sediment Release Authorized: �� 'Data Reported: 01/08/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: MB-123008 METHOD BLANK QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: NA Date Received: NA 'Sulfur Date Extracted: 12/30/08 Sample Amount: Date Analyzed: 01/07/09 11:54 Final Extract Volume: Instrument/Analyst: ECD4/AAR Dilution Factor: GPC Cleanup: No Silica Gel: Cleanup: Yes Florisil Cleanup: No Percent Moisture: Acid Cleanup: No CAS Number Analyte RL 25.0 g-dry-wt 5.0 mL 1.00 Yes NA Result ' 319-84-6 alpha-BHC 1.0 < 1.0 U 319-85-7 beta-BHC 1.0 < 1.0 U 319-86-8 delta-BHC 1.0 < 1.0 U ' 58-89-9 gamma-BHC (Lindane) 1.0 < 1.0 U 76-44-8 Heptachlor 1.0 < 1.0 U 309-00-2 Aldrin 1.0 < 1.0 U 1024-57-3 Heptachlor Epoxide 1.0 < 1.0 U ' 959-98-8 Endosulfan I 1.0 < 1.0 U 60-57-1 Dieldrin 2.0 < 2.0 U 72-55-9 4,4'-DDE 2.0 < 2.0 U 72-20-8 Endrin 2.0 < 2.0.0 ' 33213-65-9 Endosulfan II 2.0 < 2.0 U 72-54-8 4,4--DDD 2.0 < 2.0 U 1031-07-8 Endosulfan Sulfate 2.0 <.2.0 U 50-29-3 4,4--DDT 210 <<210 ' 72-43-5 Methoxychlor U 7421-93-4 Endrin Aldehyde 2 0 < 2.0 U 5103-74-2 gamma Chlordane 1.0 < 1.0 1.0 U U ' 5103-71-9 alpha Chlordane 1.0 1.0 < < 1.0 U 8001-35-2 Toxaphene 789-02-6 2,4--DDT 2.0 < 2.0 U 3424-82-6 2,4--DDE 2.0 < 2.0 U 53-19-0 2,4'-DDD 2.0 < 2.0 U Reported in Ag/kg (ppb) ' Pest/PCB Surrogate Recovery Decachlorobiphenyl 82.2% Tetrachlorometaxylene 73.5% ' FORM I ANALYTICAL /�, RESOURCES V INCORPORATED SIX SW8270 SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OF06-Newfields Northwest Project: Marina Park Client ID 'XNP DBA TOT OUT MB-123008 67.7t 80.3W 0 LCS-123008 67.3W 82.79a 0 Comp CU 69.0t 79.7W 0 Comp CL 64.7% 81.3t 0 LA-3 Ref 71.7W 87.3% 0 LCS/MB LIMITS QC LIMITS (MNP) = d10-2-Methylnaphthalene (44-100) (37-106) (DBA) = d14-Dibenzo(a,h)anthracene (46-121) (16-118) Prep Method: SW3550B Log Number Range: 08-34190 to 08-34192 FORM -II SIX SW8270 Page 1 for OF06 I 'ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 ' Lab Sample ID: OF06A LIMS ID: 08-34190 Matrix: Sediment yf 'Data Release Authorized://x Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/03/09 18:23 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CU SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 10.3 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 22.6% CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.8 < 4.8 U 86-73-7 Fluorene 4.8 < 4.8 U 85-01-8 Phenanthrene 4.8 < 4.8 U 120-12-7 Anthracene 4.8 < 4.8 U 206-44-0 Fluoranthene 4.8 15 129-00-0 Pyrene 4.8 19 56-55-3 Benzo(a)anthracene 4.8 6.3 218-01-9 Chrysene 4.8 7.8 205-99-2 Benzo(b)fluoranthene 4.8 12 50-32-8 Benzo(a)pyrene 4.8 16 193-39-5 Indeno(1,2,3-cd)pyrene 4.8 12 53-70-3 Dibenz(a,h)anthracene 4.8 < 4.8 U 191-24-2 Benzo(g,h,i)perylene 4.8 20 Reported in µg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 69.0% d14-Dibenzo(a,h)anthracen 79.7% FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIN GC/MS Page 1 of 1 Lab Sample ID: OF06B LIMS ID: 08-34191 Matrix: Sediment Data Release Authorized: Reported: 01/06/09 � Date Extracted: 12/30/08 Date Analyzed: 01/03/09 18:48 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL /� RESOURCES * INCORPORATED Sample ID: Comp CL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 11.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 11.0% CAS Number Analyte RL Result 83-32-9 Acenaphthene 4.5 < 4.5 U 86-73-7 Fluorene 4.5 < 4.5 U 85-01-8 Phenanthrene 4.5 < 4.5 U 120-12-7 Anthracene 4.5 < 4.5 U 206-44-0 Fluoranthene 4.5 < 4.5 U 129-00-0 Pyrene 4.5 < 4.5 U 56-55-3 Benzo(a)anthracene 4.5 < 4.5 U 218-01-9 Chrysene 4.5 < 4.5 U 205-99-2 Benzo(b)fluoranthene 4.5 < 4.5 U 50-32-8 Benzo(a)pyrene 4.5 < 4.5 IT 193-39-5 Indeno(1,2,3-cd)pyrene 4.5 < 4.5 U 53-70-3 Dibenz(a,h)anthracene 4.5 < 4.5 U 191-24-2 Benzo(g,h,i)perylene 4.5 < 4.5 U Reported in jig/kg (ppb) SIX Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 64.7% dl4-Dibenzo(a,h)anthracen 81.3t FORM I ' ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 ' Lab Sample ID: OF06C LIMS ID: 08-34192 'Matrix: Sediment /� Data Release Authorized:/ Reported: 01/06/09 6'�" 'Date Extracted: 12/30/08 Date Analyzed: 01/03/09 19:13 Instrument/Analyst: NT1/YZ GPC Cleanup: No 'Silica Gel Cleanup: Yes Alumina Cleanup: No I CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: LA-3 Ref SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Event: NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 10.3 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 52.5% 83-32-9 Acenaphthene 86-73-7 Fluorene 85-01-8 Phenanthrene 120-12-7 Anthracene 206-44-0 Fluoranthene 129-00.-0 Pyrene 56-55-3 Benzo(a)anthracene 218-01-9 Chrysene 205-99-2 Benzo(b)fluoranthene 50-32-8 Benzo(a)pyrene 193-39-5 Indeno(1,2,3-cd)pyrene 53-70-3 Dibenz(a,h)anthracene 191-24-2 Benzo(g,h,i)perylene Reported in µg/kg (ppb) RL 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 4.8 SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 71.7% d14-Dibenzo(a,h)anthracen 87.3-W Result < 4.8 U < 4.8 U < 4.8 U < 4.8 U 8.7 11 4.8 U 5.8 5.3 5.3 < 4.8 U < 4.8 U 4.8 u FORM I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 Lab Sample ID: MB-123008 LIMS ID: 08-34190 Matrix: Sediment Data Release Authorized: If Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/03/09 17:34 Instrument/Analyst: NT1/YZ GPC Cleanup: No Silica Gel Cleanup: Yes Alumina Cleanup: No ANALYTICAL /� RESOURCES V INCORPORATED Sample ID: MB-123008 METHOD BLANK QC Report No: OF06-Newfields Northwest Project: Marina Park Event: NA Date Sampled: NA Date Received: NA Sample Amount: 10.0 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: NA 1 CAS Number Analyte RL Result 83-32-9 Acenaphthene 5.0 a 5.0 5.0 U U 86-73-7 Fluorene 5.0 < E 85-01-8 Phenanthrene 5.0 < 5.0 U 120-12-7 Anthracene 5.0 < 5.0 U 206-44-0 Fluoranthene 5.0 < 5.0 U 129-00-0 Pyrene 5.0 < 5.0 U 56-55-3 Benzo(a)anthracene 5.0 < 5.0 U 218-01-9 Chrysene 5.0 < 5.0 U 205-99-2 Benzo(b)fluoranthene 5.0 < 5.0 U , 50-32-8 Benzo(a)pyrene 5.0 < 5.0 U ' 193-39-5 Indeno(1,2,3-cd)pyrene 5.0 < 5.0 U 53-70-3 Dibenz(a,h)anthracene 5.0 < 5.0 U 191-24-2 Benzo(g,h,i)perylene 5.0 < 5.0 U ' Reported in µg/kg (ppb) i } SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 67.7% ! d14-Dibenzo(a,h)anthracen 80.3% , I F 11 FORM I I ORGANICS ANALYSIS DATA SHEET PNAs by SW8270D-SIM GC/MS Page 1 of 1 ' Lab Sample ID: LCS-123008 LIMS ID: 08-34190 'Matrix: Sediment Data Release Authorized Reported: 01/06/09 'Date Extracted: 12/30/08 Date Analyzed LCS: 01/03/09 17:58 Instrument/Analyst LCS: NT1/YZ I ' Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-123008 LAB CONTROL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park Event: NA Date Sampled: NA Date Received: NA Sample Amount LCS: 10.0 g-dry-wt Final Extract Volume LCS: 0.50 mL Dilution Factor LCS: 1.00 Spike LCS Added Recovery Acenaphthene 108 150 72.0% Fluorene 108 114 150 150 72.0% 76.0% Phenanthrene 115 150 76.7% Anthracene 134 150 89.3% Fluoranthene 134 150 89.3% Pyrene 132 150 88.01; Benzo(a)anthracene 132 150 88.0% Chrysene Benzo(b)fluoranthene 128 150 85.3% Benzo(a)pyrene 140 150 93.3% 82.7% Indeno(1,2,3-cd)pyrene 124 150 150 82.7% Dibenz(a,h)anthracene 124 150 78.7% Benzo(g,h,i)perylene 118 Reported in µg/kg (ppb) SIM Semivolatile Surrogate Recovery d10-2-Methylnaphthalene 67.3% d14-Dibenzo(a,h)anthracen 82.7% FORM III ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OF06A LIMS ID: 08-34190 Matrix: Sediment Data Release Authorized Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/05/09 15:59 Instrument/Analyst: NT4/LJR GPC Cleanup: No nag m ml,^r h"AZVt9 ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CD SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 26.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 22.6t RL Result Dlmetnyipntnaiate Diethylphthalate Butylbenzylphthalate bis(2-Ethylhexyl)phthalate Di-n-octyl phthalate Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 68.4% 2-Fluorobiphenyl 76.0% d14-p-Terphenyl 79.296 d4-1,2-Dichlorobenzene 64.4-W I 'ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OF06B LIMS ID: 08-34191 'Matrix: Sediment Data Release Authorized: Reported: 01/06/09 Date Extracted: 12/30/08 'Date Analyzed: 01/05/09 16:33 Instrument/Analyst: NT4/LJR GPC Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: Comp CL SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 26.3 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 11.0% RL Result 131-11-3 Dimethylphthalate 19 < 19 19 U U 84-66-2 Diethylphthalate 19 < 19 U 85-68-7 Butylberizylphthalate 19 < 117-81-7 bis(2-Ethylhexyl)phthalate 19 < 19 U 117-84-0 Di-n-Octyl phthalate 19 < 19 U Reported in µg/kg (ppb) ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: OF06C LIMS ID: 08-34192 Matrix: Sediment Data Release Authorized:/,/f Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/05/09 17:�07 Instrument/Analyst: NT4/LJR GPC Cleanup: No CAS Number Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: LA-3 Ref SAMPLE QC Report No: OF06-Newfields Northwest Project: Marina Park NA Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.2 g-dry-wt Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: 52.5% RL Result 131-11-3 Dimethylphthalate 20 < 20 U 84-66-2 Diethylphthalate 20 < 20 U 85-68-7 Butylbenzylphthalate 20 < 20 V 117-81-7 bis(2-Ethylhexyl)phthalate 20 < 20 V 117-84-0 Di-n-Octyl phthalate 20 < 20 U Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 54.8% 2-Fluorobiphenyl 62.4% d14-p-Terphenyl 66.0% d4-1,2-Dichlorobenzene 50.4% FORM I I 'ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: MB-123008 LIMS ID: 08-34190 Matrix: Sediment Data Release Authorized: Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/05/09 14:52 Instrument/Analyst: NT4/LUR GPC Cleanup: No ANALYTICAL RESOURCES INCORPORATED Sample ID: MB-123008 METHOD BLANK QC Report No: OF06-Newfields Northwest Project: Marina Park NA Date Sampled: NA Date Received: NA Sample Amount: 25.0 g Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: NA CAS Number Analyte RL Result 131-11-3 Dimethylphthalate 20 < 20 20 U U 84-66-2 Diethylphthalate 20 20 < < 20 U 85-68-7 Butylbenzylphthalate 20 U 117-81-7 bis(2-Ethylhexyl)phthalate 20 < 117-84-0 Di-n-Octyl phthalate 20 < 20 U Reported in µg/kg (ppb) Semivolatile Surrogate Recovery d5-Nitrobenzene 60.0% 2-Fluorobiphenyl 64.8% d14-p-Terphenyl 83.24; d4-1,2-Dichlorobenzene 58.096 FORM I 7' ORGANICS ANALYSIS DATA SHEET PSDDA Semivolatiles by SW8270 GC/MS Page 1 of 1 Lab Sample ID: LCS-123008 LIMS ID: 08-34190 Matrix: Sediment �f Data Release Authorized: /!al Reported: 01/06/09 Date Extracted: 12/30/08 Date Analyzed: 01/05/09 15:25 Instrument/Analyst: NT4/LJR GPC Cleanup: NO Analyte Dimethylphthalate Diethylphthalate Butylbenzylphthalate bis(2-Ethylhexyl)phthalate Di-n-Octyl phthalate Results reported in µg/kg ANALYTICAL RESOURCES INCORPORATED Sample ID: LCS-123008 LAB CONTROL QC Report No: OF06-Newfields Northwest Project: Marina Park Date Sampled: 12/08/08 Date Received: 12/17/08 Sample Amount: 25.0 g Final Extract Volume: 0.5 mL Dilution Factor: 1.00 Percent Moisture: NA Lab Spike Control Added Recovery 400 500 80.0% 427 5o0 85.4% 388 500 77.6% 397 500 79.4% 401 500 80.2% Semivolatile Surrogate Recovery d5-Nitrobenzene 57.2% 2-Fluorobiphenyl 62.8-W d14-p-Terphenyl 74.0% d4-1,2-Dichlorobenzene 50.4% FORM III SW8270 SEMIVOLATILES SOIL/SEDIMENT SURROGATE RECOVERY SUMMARY Matrix: Sediment QC Report No: OF06-Newfields Northwest Project: Marina Park Client ID NBZ PEP TPH DCB TOT OUT MB-123008 60.0% 64.8% 83.2% 58.0% 0 LCS-123008 57.2% 62.8% 74.0% 50.4% 0 Comp CU 68.4% 76.0% 79.2% 64.4% 0 Comp CL 58.4% 59.2% 68.8% 45.6% 0 LA-3 Ref 54.8% 62.4% 66.0% 50.4% 0 LCS/MB LIMITS QC LIMITS (NBZ) = d5-Nitrobenzene (37-85) (29-87) (PEP) = 2-Fluorobiphenyl (39-82) (32-88) (TPH) = d14-p-Terphenyl (38-105) (21-97) (DCB) = d4-1,2-Dichlorobenzene (33-79) (25-82) ' Prep Method: SW3550B Log Number Range: 08-34190 to 08-34192 If II II It II II II II ANALYTICAL RESOURCES INCORPORATED N ' Page 1 for OF06 FORM -II SW8270 I I I Appendix C Benthic Toxicity Tests ' Data Sheets and Supporting Information I I 1 I I I N��FIELDS ` — M 11111 IMAYMtID SSE -fir Dl! M ANN WE M WO City of Newport Beach Marina Park Ampelisca abdida Port Gamble LDS JOB NUMBER PROJECT MANAGER NEWFIELDS LABORATOR DILUTION WATER BA 1105-005-860 B. Gardiner Port Gamble I FSW121808.01 START DP: 19DecO8 TECH. USEPA/USCOE 1991 T END DATE 29Dec08 Date CLIENT/NEWFIELDS ID unr xer meter mglL o C meter ppt meter unit Control / 0 �meter 14,7 Control / 0 2 Control/ 0 3 Control / 0 4 Control / 0 5 Control/ 1 1 ?j 2� �i �°�• i - �l awl 3 Control / 2 2 3 b. 3 S R. 5 3 3 0 3 g• t I KkwAe, i a\ Control) 3 3 z, �• g 3 i�- S 3 3 a 3 9-. g�— Control / 4 4M71Control / 55Control / sControl / 7 2 7 3 3 2 3V> ' 12 � Control / 8 3 3, 5 3 I g� (P 3 30 3 $• O is t 7i/Z Control/ 9 4 3 6 g 14,1 3 30 3 S.0 `y 12%Z8 Control / 10 Control / 10 2 Control / 10 3 5 $ Control/ 10 4 37" T Control/ 10 5 D 5.� 0,0 3/ �. lcc( '✓`�J t-r� raK y„v.[� w! 5eu- wcr,-l�o/' 4✓r�,.ip ems/ Sw( C ��E `3'/a-s' �- Pagel of 4 10 DAY SOLID PHASE TEST DATA I�TEtiY/F7ELD� ` USEPA(USCOE 1991 CLIENT City of Newport Beach PROJECT Marina Park SPECIES Ampe(isce abd/da ITESTSTARTUATE I Port Gamble TEST START DATE 19Dec08 TESTEND DATE 29Dec08 NEWFIELDS JOB NUMBER 1105-005.860 PROJECT MANAGER B. Gardiner NEWFIELDS LABORATOR Port Gamble DILUTION WATER BATCH FSW121808.01 T TIME END TIME WATER QUALITY DATA D.O. (mo(L) TEMP (*Cl >4.6 20t1 SALINITY foot) 30 t 2 off (oH unitsl 7.8t0.5 TECH. Date CLIEN7/NEWFIEtASID wr D.O. TEMP SALINITY H ev meter mg/L meter o C meter ppt meter unit LA-3 Reference / 0 1 .o '� Z 3 2 42 LA-3 Reference/ 0 2 �,O 1 1.3 31 $ 1 LA-3 Reference / 0 3 LA-3 Reference / 0 4 (`f . Z 3 O LA-3 Reference / 0 5 d ?� $, Z LA-3 Reference / 1 1 '� a "Zj q g 7j 31 "Zj g, d �Ijk r a 2 0 LA-3 Reference / 2 2 3 b 3 (�► .�, 3 31 3 g• �- t�itti 8 1 2 t LA-3 Reference / 3 3 3 b. Bpi 3 I t'FI LA-3 Reference / 4 4 3 6, 0 3 I� r l, J � LA-3 Reference / 5 5 , $ t -v , / y LA-3 Reference / 6 1 1 L ,q 3 - LA-3 Reference / 7 2 G,$ 3 9.-3 3 Z 3 �-, g MPF 2% LA-3 Reference / 8 3 3 ?. 3 19.8 3 33 3 $• a � t Z/Z LA-3 Reference / 9 4 3 z, O 3 1 R• fl 3 33 3 �.cj LA-3 Reference I 10 1 / 4j 3 g /Z L• LA-3 Reference / 10 2 S $ 3 LA-3 Reference / 10 3 LA-3 Reference / 10 4 1i 3 3 LA-3 Reference/ 10 5 s Page2 of4 titititti �' � � � S r � � 1•t � t• � � � � � �+ t• M ■ '" {, NEWFIELDS f �AY4ftIDWWEK&TD*& a USEPANSCOE 1991 - CLIENT City of Newport Beach PROJECT Marina Park SPECIES Ampelisca abdida TEST START DATE Port Gamble TEST START DATE 19Dec08 TEST END DATE 29Dec08 NEWFIELDS JOB NUMBER 1105-005-860 PROJECT MANAGER B. Gardiner NEWFIELDS LABORATOR Port Gamble DILUTION WATER BATCH FSW121808 01 STARTTIME END TIME WATER QUALITY DATA D.O. (malLl TEMP ("C) >4.6 2031 SALINITY (oot) 30 t 2 off (oH units) 7.8t 0.5 TECH. Date CLIENTINEWFIELDS ID WY D.O. TEMP SALINITY _ pH nea meter mglL meter o C meter PPt meter unit Comp C-U 1 0 1 3 -( % 2 3 -3/ Camp C-U / 0 2 -7_ Comp C-U / 0 3 t .� )?j -3 ( •% Comp C-U / 0 4 Comp C-U / 0 5 /�, ( 7j p• l Comp C-U / 1 1 3 (q•9 -3 31 3 9.0 12 as Comp C-U ! 2 2 3 3 -1,, Camp C-U1 3 3 3 (o.� 3 Comp C-U / 4 4 3 6 . / ) 7,5 J 3 , Comp C-U / 6 5 33 lq3 33 pO Comp C-U / 6 1 L 3 �• b �� a� Comp C-U / 7 2 3 O �� ,3 3 31, 3 �� p Comp C-U / s 3 �j g, O 3 2, 3 33 3 2.0 11 c Z�Z Camp C-U/ 9 4 3 �.$ 3 19-0 3 32 31 z0 Comp C-U 1 10 1 3 3 Comp C-U / 10 2 CompC-U! 10 3 Comp C-U ! 10 4 Comp C-U / 10 5 Page) of 10 DAY SOLID PHASE TEST DATA "NEWIELD,S TOCOL USEPAIUSCOE 1991 CLIENT City of Newport Beach _ PROJECT Marina Park SPECIES TEST START DATE Ampeliscaa6dfda Port Gamble TEST START DATE 19Dec08 TEST END DATE 29Dec08 NEWFIEt"DS JOB NUMBER 1105-005-860 PROJECT MANAGER B. Gardiner NEWFIELDS LABORATOR DILUTION WATER BATCH Port Gamble FSW121808.01 ISTART TIME END TIME WATER QUALITY DATA D.O. (maU TEMP (*C) >4.6 20f1 SALINITY tuvO 30 t 2 off (oH units) 7.8t0.5 TECH. Date 7ENELDSID wr D.O. TEMP SALINITY H vQ meter mg1L mete o C meter ppt meter unit L/ o 1 3 �_v 9. 3 Comp -L / 0 2 C> `�, 31 p. % Comp C-L / 0 3 TO i 3r �• g, Comp C-L / 0 4 k 19. Z Camp C-L 1 0 5 7 o qf f y 2 31 $, Camp C-L / 1 1 3 Z a 3 1 T.5 3 31 3 Ij./ 11h r a as Camp C-L / 2 2 , O 3 (mil - l0 3 g ivlllrt t� { a3 l CompC-L/ 3 3 3 is.Sd2— CompC-L/ 4 4 Comp C-L / 5 5 Camp C-L / 6 1 Camp C-L / 7 2 3 4.� 3 (q,5 13 37 13 1421, Comp C-L1 8 3 3 g•D 3 18-0 3 33 3 $'D I Z1 L+ Comp C-L / 9 a 1 -3 (p. $ 3 (9-1 3 33 9 IS.O Camp C-L / 10 1 S$11W3 /2 Z Comp C-L/ 10 2 3 7 3 Camp C-L / 10 3 Comp C-L / 10 4 Comp C-L / 10 5 Ot,�c t2(141�� (L Page4 o14 Page _of ' NEwFI1 LUS Ammonia Analysis ' Total Ammonia (mg/L) ' Client/Project: Organism: NewFields Test ID: Test Duration (days): iwa• oar sG 1 H PRETEST / I V AL / OTHER (circle one) DAY of TEST: VERLXING (OV OREWATER (PW) (circle one) Calibration Standards Temperature Sample temperature should be within+l°C of standards temperature at time and date of analysis. Date: o0 Temperature: ample ID or 17esc6ptiori' ,: Conc. or Rep Date of Sampling and p g Initials Ammonia '.' :Value •': mg/i Temp oC Date of Reading and Initials Sample Preserved (YIN) pH Sal .. iPp t Sulf. mg/L �tM'f, 2 G ADS •S.S 2 N \\PspwaMprojectABIOASSAY PILES\lab Logs & Porms\Ammonia Analysis Record.doc ' Last printed 12/19/20081:37:00 PM Page _,of N•LWI�ILLDS Ammonia Analysis Total Ammonia (mg/L) Client/Project: Organism: Test ID: Test Duration (days): arl r PRETEST / NIT A / FINAL / OTHER(gitdzone) DAY of TEST: OVERLYING (OV) /C'OREWATER(MV) (circle one) Calibration Standards Temperature Sample temperature should be within ±I°C of standards temperature at time and date of analysis. Date: -Temperature: I I I I 1 Date of Ammonia' Date of Sample Sulf, Sample ID of • ' Cond: Sampling and ; ' "Value Tome -Reading and Preserved pH Snl nig/L Description or Rep Initials iti I, C Initials (Y/N) (Ppt) fro S Mt2h(4<.N L 3 �e cnw.cro ©. 6gi% C,_ < , Mrspwa0l\projects\Bl0ASSAY FILES\Lnb Logs & Forms\Ammonia Analysis Record.doe Last printed 12/19/2008 1:37:00 PM ' �10 DAY STItD WSe%Sil,TA!M0 INTEW-F-IELDS M M M M M CLIENT PROJECT NEWFIELDS JOB NO. PROJECT MAN. INEWFIELDSLAB IPROTOCOL ISPECIES City of Newport Beach Marina Park 1105-005-860 B. Gardiner Port Gamble Bath 7 1 USEPA/USCOE 19911 Ampelisca abdida Page i of 1 CETIS QC Chart Page 1 of 1 Report Date: 14 Jan-0910:23 AM Reference Toxicant 98-h Acute Survival Test NawFlelds Test Type: Survival Organism: Ampelisca abdita (Amphipod) Material: Cadmium chloride Protocol: PSEP (1995) Endpoint: Proportion Survived Source: Reference Toxicant -REF 1.2 3, 0.8 0. ............... ............................................................................................. ......................... g ii 0.2 .................. ......... ............................................ ......................................... 00 Mean: 0.37686 Count: 17 4s Warning Limit: 0.22126 -2s Action Limit: 0.12990 Stoma: CV: 70.33% +1s Warning Limit: 0.64189 +29 Action Limit: 1.09330 Quality Control Data Point Year Month Day Data Delta Sigma Warning Action Test Link Analysis 1 2006 Jan 27 0,18090 -0.19595 -1.37810 (-) 07-5436-8129 06-2014-1066 2 27 0.21846 •0.15839 -1.02383 (-) 02-3876-2955 12.1697.4541 3 Feb 23 0.63498 0,25812 0.97968 17-3687.3273 06-7672.2441 4 Sep 1 0.44694 0.07009 0.32029 11-8706.7493 01.2691-1489 5 Dec 8 0.22112 .0,16574 -1,00114 (-) 01-8163.5765 09-7294-9655 6 2007 Jan 19 0.39569 0.01873 0.09108 05-1919.0461 04-7876.6509 7 23 0.21727 -0.15958 -1.03411 (•) 13-4550.6899 02-3067.516l 8 Feb 9 0.38474 0.007e6 0.03886 04-8872-6896 02.4257.0063 9 May 25 0.26923 -0.10763 -0.63150 16.5938.6055 08.1846-1770 10 Jun 25 0.44847 0.07161 0.32669 . 02-7818.3113 07-6434.4735 11 Oct 12 0.34850 -0.02835 -0.14687 07-2723.0368 03.4167-3848 12 Nov 6 1.10809 0,73124 2.02523 (+) (+) 02-8822-100313-2266.5070 13 14 0.23515 -0,14171 -0.88567 10-0087-449311-2555.9069 14 2008 Jon 18 0,97309 0.59884 1.78244 (+) 16.7604.537313-2534.3341 16 Sep 23 0.68928 0.21243 0.83945 03-2847-788018.3138.3652 16 Oct 24 OA6182 0.08496 0.38176 14-6257-4714 01.6783.1439 17 Dec 12 0.26177 -0.11509 -0.68426 17-4134.1431 08.7847-9030 18 23 0,54803 0.17178 0.70522 21.3281.1872 04-2474.4340 000-173-102-3 CETISTM v1.1.2revG Analyst: Approval: I I' GETIS Analysis Detail Comparisons: Pagel of 1 Report Date: 14 Jan-0910:11 AM Analysis: 144952.5726 Reference Toxicant 96•h Acute Survlval Test NewFields Endpoint Analysis Type Sample Link Control Link Date Analyzed Version Proportion Survived Comparison 21-3281-1872 21-3281-1872 14 Jan-0910:11 AM CETISv1.1.2 Method Alt H Data Transform Zeta NOEL LOEL Toxic Units ChM PMSD Dunnett's Multiple Comparison C > T Angular (Corrected) 0.25 0.5 400 0.35365 39.54% Group Comparisons Control vs Conc-mg/L Statistic Critical P-Value MSD Declsion(0.06) Dilution Water 0.125 1.62492 2.46559 0.1793 0,36234 Nonsignificant Effect 0.26 1.65966 2.46659 0.1708 0.36234 Non -Significant Effect 0.5 3.0498 2.46559 0.0193 0.36234 Significant Effect 1 4.97255 2.46559 0.0010 0.36234 Significant Effect ANOVA Table Source Sum of Squares Mean Square DF F statistic P-Value Decision(0.05) Between 0.8975322 0.2243831 4 6.93 0.00613 Significant Effect Error 0.3239474 0.0323947 10 Total 1.22147965 0.2567778 14 ANOVA Assumptions Attribute Test Statistic Critical P-Value Dec(ston(0.01) Variances Bartlett 1.99337 13.27670 0.73698 Equal Variances Distribution Shapiro -Wilk W 0.94443 0.44135 Normal Distribution Data Summary Original Data Transformed Data Conc-mglL Control Typo Count Mean Minimum Maximum SD Mean Minimum Maximum SD 0 Dilution Water 3 0,80000 0,70000 1.00000 0,17321 1,13144 0.99116 1.41202 0.24298 0.125 3 0.60000 0.60000 0.80000 0.17321 0.89265 0.78540 1,10715 0.18576 0.26 3 0.60000 0.50000 0.70000 0.10000 0.88754 0.78540 0.99116 0.10289 0.5 3 0.40000 0.30000 0.50000 0.10000 0.68325 0.57964 0.78540 0.10289 1 3 0.16657 0.00000 0.30000 0.15275 0.40069 0.15878 0.57964 0.21738 Data Detail Cone-mg/L Control Type Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 Rep 6 Rep 7 Rep 8 Rep 9 Rep 10 0 Dilution Water 0.70000 0.70000 1.00000 0.125 0.50000 0.50000 0.80000 0.25 0,50000 0.60000 0.70000 0.5 0,50000 0.40000 0.30000 1 0.20000 0.30000 0.00000 000-173.102-3 CETIS%vl.1.2revG Analyst: Approval: CETIS Analysis Detail Linear Regrassiom Page 1 of 2 Report Data: 14 Jam0910:12 AM Analysis: 04.2474.4340 Reference Toxicant 96-h Acute Survival Test NewFlalds Endpoint AnalyslsType Sample Link Control Link Date Analyzed Version Proportion Survived Linear, Regression 21.3281-1872 21-3281-1872 14 Jan-0910:12 AM CETISvl.1.2 Linear Regression Options Model Function Threshold Option Threshold Threshold Opt Reweighted Pooled Groups Hat Corr Log-Normal(NED-A+B9o9(X)) Control Threshold 0.2 Yes Yes No No Regression Summary Item Log Likelihood Mu Sigma G Chi•Sq Critical P•Value Deciston(0,05) 36-76.73683 1.72745 0.29335 0.26360 10.82990 22.36203 0.62500 Non -Significant Heterogeneity Point Estimates Effect Cone-mglL 95% LCL 95% UCL 10 0.230857 0.05868554 0.379844 15 0.2724263 0.08116146 OA279859 20 0.3107803 0.1048226 0.4714451 25 0.3478742 0,1303138 0.6131632 40 OA623413 0.2229078 0.6428301 50 0.6486319 0.3036974 0.7462605 Regression Parameters Parameter Estimate Std Error 95%LCL 95%UCL tStatistic P-Value Declelon(0.05) Threshold 0.2953582 0,06229078 0.1732683 0.4174482 4.742 0,00039 Significant Slope 3.408944 0,8756865 1.092698 6.125289 3.893 0.00185 Significant Intercept 6.888776 0.2613715 5.376488 6AO1064 22.530 0.00000 Significant Residual Analysis Attrlbute Method Statlatic Critical P-Value Declslon(0.06) Variances Modified Levene 3,93714 3.47805 0.03886 Unequal Variances Distribution Shapiro -Wilk W 0.9449846 0,44916 Normal Distribution Data Summary Calculated Varlate(AIS) Cone-mg1 Control Type Count Mean Minimum Maximum SE SD A B 0 Dilution Water 3 0.80000 0.70000 1.00000 0.03636 0.17321 24 30 0.125 3 0,60000 0.50000 0.80000 0.03538 0.17321 18 30 0,25 3 0.60000 0.60000 0.70000 0.02041 0.10000 18 30 0.6 3 0,40000 0.30000 0.60000 0.02041 0.10000 12 30 1 3 0.16667 0.00000 0,30000 0.03118 0.15276 6 30 2 3 0.00000 0.00000 0.00000 0.00000 0.00000 0 30 000-173.102.3 CETISa v1.1.2revG Analyst: Approval: Linear Regression: Page 2 of 2 Report Date: 14 Jan-09 10:12 AM uetan Canc-mgIL Cana•mOIL Ills 1 i 000.173.102-3 CETISTM v1.1.2revG Analysis: 04-2474.4340 RankRa pmpprtIm Survived Analyst; Approval; 1�'Ew'FY��4DSI REFERENCE TOXICANT TEST WATER QUALITY DATASHEET CLIENT PROJECT SPECIES NEWFIELDSLABORATORY PROTOCOL City of Newport Beach Marina Park Ampelisca abdida I Port Gamble Bath 7 USEPAUSCOE 1991 NEWFIELDSJOB NUMBER PROJECTMANAGER QUANTLTYOFSTOCKTARCEr.03ML DUANTNY OF MIJENT_ MOW& tNrT 64 1105-005-860 B. Gardiner DATE PREP t2 ACTU ACTUAL: 1SfA-� L TESTID LOT* - TESTSTART DATE 7IME TESTENODATE . TIME ?P0 3� LO 761, 1 23Dec08 (?jad 27Dec08 t ava WATER QUALITY DATA DILTIN.WATMATCH TEMP REG# REFERENCE TOX. MATERIAL REFERENCE TOXXICANT LOT NO. 96-H LC,e FSW121808.01 o cadmium chloride cadmium _ 6TEMP. Wi CLIENTINEWFIELDSID CDNCQITRIITION DAY RP D.O. SALINRY pH WOTECH AMMOM YEJD4 R191L y Ta h SULFWES T"h qIW Iw is rAwL w 6tw -C Mt" PPt RIIt" - twat RMtwT : MwL. Ref.Tox. cadmium 0 mglL 0 Stock 3 7 r% . �/ 141. 1 *3 7F 77.7 Ap 4 ( 3 G4 3 111.2 3 a9 3 -4- 7 Ref.Tox-cadmium 0.125 mg/L D Stock 3 % 3 f , S 3 2$ 3 %, % pP 4 4-4 Ref.Tox-cadmium 0.25 mg/L Stock 3 7. ! 17 q 3 � 7.7 PR t 3 c0,rP g 49, 2 3 a Ref.Tox-cadmium 0.5 mg/L E04 Stock 3 ?( 9y 3 a8 3 7.7 PP 3 (-.-43 1 a.2 3 21 3-1 .4 Ref.Tox-cadmium 1 mg/L 0 Stock 3 7.0 3 I%f 3 ag 7,? AP 4 j o.s ta,2 3 a4 Ref.Tox.-cadmium 2 mg/L 0 Stock 3 7.0 3 r9,q 3 a8 3 7.7 PP 4} _ 1�08VWark_0dxj0MTWj M M _ ' JOW _ REFS, ,FNCE TOXICANT TEST SUR, MAL DATASHEET NE-'w'Fl.rLDS SPECIES �u mT Am elisca abdida CLIENT PROJECT NEWFIELDSJOB% PROJECT MANAGER NEWFIELDS LABORATORY JPROTOCO/UL SCOE City of Newport Beach Marina Park 1105-005-860 USEPA B. Gardiner Port Gamble Bath 7 1991 SURVIVAL & BEHAVIOR DATA OBSERVATION KEY N = normal DATE DATE DATE DATE LOE= loss of equilibrium (2�2+f 12I25 I GA P iaf D4 11 Q =quiescent INITIAL#OF DC= discoloration ORGANISMS................................•............... NB = no body TECHNICIAN ..... .................... TECHNICIAN ..............iAw............................ TECHNICIAN �( .......,.....,........... .................. TECHNICIAN F= Floating on Surface CLIENT/NEWFIELDS CONO. REP INITIAL #ALIVE : NDEAD : CBS #ALIVE 1 #DEAD : OBS ID Valu9 unn' nuNue %ALIV %DEAD OBS I �rO t toC 9 Ref.Tox.- 0 mg/L .....1......r...b......i.................��....o.....J........i..,./...,.....1.....,i............., 2 �• ' ......I ` ;2FoS ...I.�TVS......a......^..�....p ` 1 Eat 1 a .... �............,3............. cadmium ..r'.....!.YrCj 3 to 2rb$ ...�...................;.2........ I i y FaS ............:..................I....... ;O i I N i 1 0€ �............ ............ ............. 5 I, a�°.. Ref.Tox.- 0.125 mg/L .1.... s....:.................... [ Vj €dt 0S (a ? Z i 1 FOS �J ' I f 05 .... cadmium........... ... ,........,............. :....... ...... 1 !l Fos ............ ..>.............. >............. 9 ,..,...,.......,..,.....,........:,.................................,....;... cz ::...............................`f.......:..........................:...... A i .... Ref.Tox.- 0.25 mg/L ..............(..a.......� 2 Y € / I�fds g i Id a { 1 'IIA>�}.. �? cadmium....., .,...,.....,;.............;.,.......,................;..............;............. ....... .......... .... . .............;`d�S 1 ' $„ '• s 2 Fos •...,.•.. .. .2... 'a ,... ,,.,C.,....... • ram.. ? I FoS , ..,C....,......,,1..n....,.•.. Ref.Tox.- 0.5 mg/L ...�... ,..,.,.,.•r r.• .,.1. .,, L............. 2 ` F 1. rl �.. .... ....I................... I �i € 3 fc1S �O. .. �.. �...�.. .....'. ;. ' l..�S cadmium ....., .....r��....l 3 /p �i�o5 ...........- ................... . 3 3Fps ... :... . S 2 YFoS 3 1a i 1 /o SFo n 9„ [ i IrrDS 1 '1nt>3 ... i..nnu...... 2 ' `%......!.ED ....0..... Ref.Tox.- 1 mg/L m..uu.. ,. ..u. nG....unl•n.n.u........... 2 I 5Fe5 ...................1 .... nu ...J..nn........l.un....nn '• 1L1 Fos I .`e, r. �.. ..:2... , ... .. z €1 Fay I N . ,2......... cadmium ...... -.� ...........;..............,............. I ...... g..,............ L �3 LfioS .........................5.....:..... ' H Fa 6 i N a ....... Ref.Tox.- cadmium 2 mg/L .................. =.� 2 (o 1,O FoS ; ....... ......c.,.,.,,,,.........>,,,.........s.....,... ...............5 (� j u i�FO ............................................... (o € ..,..,.,.€.................. i.......{11;,., ..,..,.,.,p ! FO >�j i G i 12/23/2008 Marina Park Amp 10d.xls Cd RTSury Page 1 I n ORGANISM RECEIPT LOG Date; Time; NewFields Batch No. �2�6��P� Organism: Source: ' Address. Invoice Attached , II ovl Fit ls? Yes , Phone: oV, P, le. Contact: Je�.V\ No. Ordered: No. Received: Source Batch: ' Condition of Organisms: Approximate Size or Age: Shipper: B of L (Tracking No.) 1=�d Exl 86(02 & 2 ? 2 6��!?C) , Condition of Container: Received By: Confirmation of ID of Organism: Technician (Initials): Yes Notes: pH Temp. D.O. Conductivity or Technician Salinity ' (Units) (°C) (mgfL) (Initials) Include Units 7,2 `.�1•L 3�.� 3� GrZ Notes: , 0 SAY&bID WWE W D%b = M PlInTotwor— a N��vFi�ns USEPAIUSCOE 1991 CLIENT PROJECT SPECIES TEST START DATE TEST START DATE TEST END DATE City of Newport Beach Marina Park Neanthes arenaceodentata Port Gamble 19Dec08 29Dec08 ri�TANEWFtELDS JOB NUMBER PROJECT MANAGER NEWFIELDS LABORATOR DILUTION WATER BATCH R TIME END TIME 1105-005-860 1 B. Gardiner Port Gamble FSW121808.01 y (p 00 >4.6 2031 1 30 t 2 1 7.St 0.5 TECH. Date CLIENT/NEWFIELDS ID onr D.O. TEMP SALINITY H REP meter mglL meter > C meter ppt meterl unit Control / 0 1 3 7.0 3 /2, / `3 3 / 7 `6, Z Control / 0 2 7, c! F. Control / 0 3 7.0 (�j, � 1 7,7 Control / 0 4 -,7_ ( 31 ( 4,0 Ed-E� Control / 0 5 ( cj / 3 Control / 1 1 �, a 3 1q.3 3 3 / `3 9 6u to T2v Control ! 2 2 3 , ( 3 1� • kD 3 3 ( 3 $ Mm?ti l Control/ 3 3 3 e'19.. c� 3 n./q- 3 3 2L 3 a-.n Mwvlt°� j 2— Control/ 4 4 6� /, 7 /� J 3� 3 $,i% 2/61 Control/ 5 5 3 3 32 3 Control/ 6 1 Control/ 7 2 Control/ 8 3 3 a•g 3 t$'0 3 3z 3 g.Z l2fz Control/ 9 4 3 6-$ Zvi 3 1 33 Control/ 10 1 p (g—r y Control / 10 Control/ 10 3 (�.� �g'S' 33 g•z Control / 10 4 Control ! 10 5 ('p. (�(o k `3 3 $, Z I ,_ _ Pagel of 10 DAY SOLID PHASE TEST DATA I\T�IELDS PM TUGUL _.._ .. USEPA/USCOE 1991 CLIENT City of Newport Beach PROJECT Marina Park SPECIES TEST START DATE Neanthes arenaceodentata I Port Gamble TEST START DATE 19Dec08 TEST END DATE 29Dec08 NEWFIELDS JOB NUMBER 1105-005-860 PROJECT MANAGER B. Gardiner NEWFIELDS LABORATOR DILUTION WATER BATCH Port Gamble FSW121808.01 TART TIME END TIME - WATER QUALITY DATA D.O. (malL) TEMP PCl >4.6 20t1 SALINITY (oot) 30 3 2 off foH unitsl 7.8t0.5 TECH. Date CLIENTINEWFIELDS ID wr D.O. TEMP SALINITY H rrer meter mgfL meter "C meter ppt meter unit LA-3Referencel 0 1 v 33 1C� 'j -j1 �,Z7/- LA-3-Reference/ 0 2 LA-3 Reference / 0 3 LA-3 Reference / 0 4 [ l y v LA-3 Reference] 0 5 v (g 6 ?� LA-3 Reference 1 1 3 b 3 11.7 3 31 3 8,0 f3H �a b6 LA-3 Reference / 2 2 3 (P 3 l• S 3 3 3 MM �� LA-3 Reference / 3 3 3 3 [ Cl.3c?- LA-3 Reference / 4 4 LA-3 Reference / 5 513 (P t<� 2 � 33 LA-3 Reference 6 1 3 ?J 1q, &, 3 S' ( Q } as LA-3 Reference! 7 2 3 �.3 3 [9,q% 3 3 3 3 LA-3Reference l 8 3 0 3 33 3 it.Z iz/Z� LA-3 Reference] 9 4 3 3 l %.9 3 33 3 e' O LA-3 Reference / 10 1 G, f 3 tg Jr -33 3 9.0 1 Z y LA-3 Reference 1 10 2 Cd ($, s LA-3 Reference / 10 3 LA-3 Reference / 10 4 f4, S �, LA-3 Reference I 10 5 t ?> Page of \TF9 F ELD5 11- USEPAIUSCOE 1991 CLIENT Cityof NewportBeach PROJECT Marina Park SPECIES TEST START DATE Neanthes arenaceodentata Port Gamble TEST START DATE 19Dec08 TEST END DATE 29Dec08 NEWFIELDS JOB NUMBER 1105-005-860 PROJECT MANAGER B. Gardiner NEWFIELDS LABORATOR DILUTION WATER BATCH Port Gamble FSW121808.01 START TIME END TIME WATER QUALITY DATA D.O. Ima/LI TEMP (°C) >4.6 2041 SALINITY (ono 30 t 2 off (oH units) 7.830.5 TECH. Date CLIENTINEWFIELDS ID enr D.O. TEMP SALINITY pH ner meter mglL meter oC meter ppt meter Comp c-U / 0 1 � �,2 3 ) q. ( � ,Funit fir �Z / 9 Comp C-U / o z ?.2 Comp C-U / 0 3 [ Comp c-U / 0 4 7/ 101• 7' 3 ( $` I Comp C-U / 0 87.0 q, 0 Comp C-U / 1 1 3 �•� 1 q• 3 ( Comp C-U / 2 z Comp C-U / 3 3 3 `r • l nnr\n t3 L a 2— Camp C-U / 4 a 3 9,7 3 % %.E 3 �C g 0 � IZA-2:5 Comp C-U / 5 5 7 (Ct 7 ,3'L `� B, Z Comp C-U / 6 1 ;"i cL comp 7 2 7 (p.� 3 19.1 3 32- 3 77.E ► )zlz6 comp C-U / s 3 3 3 l$ 3 3 33 3 9-7- I zI comps_U/ s a 3 t�.te 3 (g.g 3 32 3 Comp C-U / 10 1 2/ G, `� 333 comp c-U / 10 2 �•�- 33 Comp C-U 1 10 3 $ (g 3 3 g, Comp C-U / 10 4 K t {933 Comp C-U / 10 5 ( 33; y. Page 3 of 4 10 DAYSOLID PHASE TEST DATA � N�W�ILLD� r USEPAIUSCOE 1991 CLIENT City of Newport Beach PROJECT Marina Park SPECIES TEST START DATE lgeanthes amnaceodentata Port Gamble TEST START DATE 19Dec08 TEST END DATE 29Dec08 NEWFIELDS JOB NUMBER 1105-005.860 PROJECT MANAGER B. Gardiner NEWFIE.DS LABORATOR DILUTION WATER BATCH Port Gamble I FSW721808.01 ISTARTTIMF END TIME WATER QUALITY DATA D.O. (mall-) TEMP (°CI >4.6 20±1 SALINITY tout) 30 t 2 DH (DH units) 7.8t0.5 TECH. Date CLIENTINEWFIELDS ID oar D.O. TEMP SALINITY pH rtv meter mg1L meter °C meter ppt meter unit Comp G-L 1 0 1 ,0 3 % Comp C-L / 0 z Comp C-L / 0 3 t<q 0 Comp C-L / 10 4 ��-31 Comp C-L / 0 5 �.O g. 2 8 Comp C-L I I1 3 7.1 3 0-7 3 31 3 g 6 / Za as Comp C-L / 2 2 a$ 3 [ q .S 3 3 l 3 Q. t MYt�Ie.d Comp C-L / 3 3 3 3 19 AV Comp C-L / 4 4 15 0.7 l %, ' '2 Comp C-L / 5 5 3 �.� 3 f .$(3 2 Comp G-L / 6 , 13, 3 t 9, 3 3 - col P 1 as Comp C-L / 7 2 3 6.3 3. R 13 3 13 1 7. mpf 121'.�V Comp C-L / 8 3 ?� 1-1 3 IFs•O 3 34 3 a-.Z -fs I21Z� Comp C-L / 9 4 3 /o.$ 3 1$.9 j 35 3 8.0 Comp C-L I 10 1 3 3 3 33 3 Elj Z 2 CompC-L/ 10 2 (e 33 � Comp C-L / 10 3$ G 3 tj 1 Comp C-L / 10 Comp C-L 1 10 5 ? 3 Page4 04 Page _of ' NI D�I1IELDS Ammonia Analysis ' Total Ammonia (mg/L) 11 Client/Project: I Organism: NewFields Test ID: I Test Duration (days): PRETEST / INAL / OTHER (circle one) DAY of TEST: 1 RLYING (O PORE WATER (PW) (circle one) Sample temperature should be within +1 eC of standards temperature at time and date of analysis. atnple ID'of " Desch tioti' P Cone." :or Re P Date of Sampling and p g •Initials Ammonia ; Value.: m' L Temp oC Date of Reading and Initials Sample Preserved" (Y�) pH", Sal " Sulf. mg/L " LA._' R � >~ L- 4 D. 5 40-s \\Pspwa01\projects\BI0ASSAY PILES\Lab Logs & Porms\ Ammonia Analysis Record,doc Last printed 12/19/2008 1:37:00 PM Page _of ' NLWNII;LDS Ammonia Analysis Total Ammonia (mg/L) Client/Project: Organism: NewFields Test ID: Test Duration (days): PRE TCST / ITI / TINAL / OTWM W cle one DAY of TEST: OVERLXING (OV) / KOREWATER (P. ) (circle one) Calibration Standards Tcm erature Sample temperature should be within ±leCof standards temperature at time and date of analysis. Date: Temperature: EuaTv— g I0 I I Date of Ammonia Date of Sample Sulf. Sample II7 or Conc. SaTemp mpling and Value - ;p Reading and Preserved pH Sal mg/L Description or Rep Initials m L C Initials (Y/N) ('pt) SDI er, tz/o/cs rA 4a s Agk0c c /v LA -3 ,c-L <©�� II Z.\Projccts\EIOASSAY PILES\Lnb Logs & Porms\Ammonla Analysis Record.doc Last printed 12/17/2008 3A6;00 PM , Page _of `• NI;A'�FIILDS Ammonia Analysis Total Ammonia (mg/L) Client/Project: Organism: NewFields Test ID: Test Duration (days): PRETEST / INITIAL /*NAi', / OTHER (circle one) DAY of TEST: OYERL ING (OV) / PORE WATER (PW) (circle one) Calibration Standards Temperature Sample temperature should be within±l°C of standards temperature at time and date of analysis. Date: Temperature: CD Sample ID or Description'' Conc.. or•Rep Date of Samplingarid Initials Ammonia Value m L) Temp Tem o C Date of Readigg and ' Initials Sample Preserved' (YIN) pil saisail"�.Sulf.. . L 3� <n.s \%rspwa0l\projects\BI0ASSAY FILES\Lab Logs & Forms\Ammonia Analysis Record.doe ' Last printed 12/29/2008 9:11:00 AM Page _of , N1:�1�11�I,DS , Ammonia Analysis Total Ammonia (mg/L) Cllient/Projecitn:I Otrganis//m: NewTields Test ID: Test Duration (days): MP,1D t Q( ll'19Jivla 2r N��t 05 PRETEST / INITIAL INAL O r ! c►rcic-Qne) DAY of TEST: OVERLYING (OV) / PjOR W(�RP )-(cirele one) Calibration Standards Temperature Sample temperature should be within ±l°C of standards temperature at time and date of analysis, Date: Temperature: 2 d I I Id I 1 N BID.. . NO®010, � '' =�=-�� zl� M '' Y ®�I OEM��010� _ O u,� , �-�INE= MI �—__--_ _--_--__==NI INEININE --__--__==E INEININEW ONE NENNE MININN \TspwaO RprojectskI310ASSAY pILES\Lab Logs & Porms\Ammonla Analysis Record.doc Last printed 120/2008 9:11:00 AM i�TE IEL-DS 10TY MID MSMOMTA= s M= M M M M CLIENT PROJECT NEWFIELDS JOB NO. PROJECT MAN. INEWFIELDS LAB IPROTOCOL ISPECIES City of Newport Beach Marina Park 1105-005-860 B. Gardiner Port Gamble Bath 7 1 USEPA7USCOE 1991 Neanttlesarenaceodentata #E=Emergence •• •• �• •• �• �• 9•T&W •• �• #M = Number of Mortality G=Growth DAT DATE - DATE DATE DATE TE DATE DATE DATE O ? (fungal. Eacteeal• malga9 De - D=No Air Flow(DO?) INITIALLOF �a ta1a, ��/y�ra-�s,(��3J/� 7vo �sg i aia ..ZORGANISMS «..._...._.............�........_ = Normal CHNICIAN 7ECHNICIAN TECHNICIAN ._...-J••................._ TECHNICIAN =J».............._..........._ TECHNICIAN CHNICIAN ..._...�......._...............».».._..............................N TECHNICIAN TECHNICIAN TECHNICIAN K Mtd 6 W191 t� iS � W2 .;LIENT/ NEWFIELDS ID REP JAR INITIAL # # OBSERVNS. OSSERVNS. OBSERVNS. OSSERVNS. OBSERVNS. OSSERVNS. OBSERVNS. OBSERVNS. OSSERVNS. OBSERVNS. 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Page 1 of 1 CETIS QC ChartOR21of 1 Report Data: 16 Jon -OR :26 PM Noanthes 10•d Survival and Growth Sediment Test NovvFlelda Test Typo: Survivai•GrovAh Organism: Noonlhes oreneceodontala (Polycha Material: Cadmium chloride Protocol: PSEP (1995) Endpoint: Proportion Survived Source: Reference Toxleanl•REF 16. 18 Sq 1"IA ............................................................. ............................ ........... .............. ........... .........� 5r..............................Z.... ............... ... . .............................. 4 2 .- p21 1'f 0 N io M p N O O N Meant 6.96264 Count: 20 -1a Warning Limit; 4A67 -2s Action Limit: 2,86508 Sigma: CV: 65.87% +1s WarningLimit: 10.8526 +2s Actlon Llmih 16.9167 Quality Control Data Point Yoar Month Day Data Delta Sigma Warning Action Test Link Analysis 1 2006 Aug 31 8.06577 1.90313 0,54443 _ 16.7169.3504 00-9849.6979 2 Dec 8 9,37176 2.40911 0.66948 10-6822.0812 10.0140.9364 3 8 9.37175 2.40911 0.66048 10.5022-0812 08-7192.3895 4 20D7 May 11 8.16263 1.19989 0.35822 03-7778.9913 06.1785.2166 5 Jun 26 0,18258 1,19994 0.35824 09-6212.3109 14.8493.4946 0 Jul 18 2.13748 4.02517 .2.66071 (-) ¢) 09-6163.063711.0760.1230 7 Sep 25 6.20193-0.76071 •0.26067 08-6354.6111 12.2113.4941 8 Oct 24 9.76006 2.79742 0,76095 05.9il3.1606 4.0319.5260 9 30 5.55412-1.40852 .0.50923 03.0327-136613.6201.6780 10 2008 Feb 17 10.12762 3.16498 0.84424 11.6936.8907 04-7495.6030 11 Jul 2 10.30107 3.33843 0,88250 07.0160.7176 03-3190.0644 12 22 2.65108 4.31166 •2.17553 (•) (•) 12-3989.8103 10-4556.3131 13 Aug 5 5.30308 .1.66956 •0,61344 12-6764.3928 00-5080.2403 14 29 4.77241 •2,19023 .0.66100 04-2088-802017-2391.7369 15 Sep 26 10.37846 3AI384 0.89893 12-2618.639115-3142-3234 16 30 5.65412 .1.40852 .0,60023 14-9906407913.4630.6299 17 Oct 9 9.26124 2.20860 0.64275 06-2717.9387 09-3671-8537 18 23 6.83792 .0.12472-0,04072 19-$732.1210 02.0490.695E 19 Nov 6 7.37067 0.41693 0.13072 15-0302-6653 14.4382.3985 20 Dec 15 10.20161 3.23007 0.80081 12.5891-147914-1600.6886 21 23 10.36175 3.38911 0.89355 17-9927-689713.4293.3697 000-173.102.3 CUISr" v1.1.2eevG Analyst._Approval: CETIS Analysis Detail Spearman-Karbor: Page 1 of 1 Report Date: 16 Jan-09 2:25 PM Analysis: 13.4293.3597 Neanthoa 10•d Survival and Growth Sediment Test NowFlolds Endpoint Analysis Type Sample Link Control Llnk - Date Analyzed Version Proportion Survived Trimmed Spearman-Karber 17-9927-6897 17-9927.6897 16 Jan-09 2:25 PM CETISv1.1.2 Spoannan-Karber Options Point Estimates Throshold Option Lower Threshold Trim Mu Sigma EC60ILC50 96%LCL 95%UCL T Control Threshold 0.1 0.00% 1.0t5014 0.0102043 10.35175 9.87655 10.84982 Data Summary Calculated Variate(A!&) Cone.pg/L Control Typo Count Mean Minimum Maximum SE SD A 0 0 Dilution Water 3 0.90000 0.80000 1.00000 0.02041 0.10000 27 30 1.875 3 1.00000 1.00000 1.00000 0.00000 0.00000 30 30 3.75 3 0.93333 0.80000 1.00000 0.02357 0.11647 28 30 7.5 3 0.93333 0.80000 1.00000 0.02357 0.11547 28 30 15 3 0.00000 0.00000 0.00000 0.00000 0.00000 0 30 30 3 0.00000 0.00000 0,00000 0.00000 0.00000 0 30 Graphlos Lo• - 0.9 0.0 07• {Rph 06 3 1}I0A 03• 02• 0.I 00'- 0 S f0 Is 10 z 30 3S 40 Cox-pi;/L I 000.173.102-3 CETIS^ v1.1.2revG Analyst: Approval: - CETIS Analysis Detail Comparisons; Pago 1 of i Report Date: 16 Jan.00 2:25 PM Analysis: 02-9071-6281 Naanthos 10-d Survival and Growth SsdlmontTost NowFielda Endpoint Analysis Type Sample Link Control Llnk Data Analyzed Version Proportion Survived Comparison 17-9927.6897 17-9927.6897 16Jan-092:25PM CETISv1.1.2 Method All H Data Transform Zota NOEL LOEL Toxic Units ChV PMSD punnetl's Multiple Comparison C > T Angular (Corroded) 7.5 15 13.3333 10.6088 24.60% Group Comparisons Control vs Conc•pglL statistic Critical P-Valuo MSD Declolon(0,06) Dilution Water 1.875 -1.3064 2.41651 0.9778 0.28802 NDn•Sig'nifieant Effect 3.76 -DA658 2,41651 0.8796 0,28802 Non -Significant Effect 7.6 -0.4658 2.41651 0.8795 0.28802 Non -Significant Effect ANOVA Table Source Sum of Squares Moon Square DF FStatistic P-Valuo Doclsion(0.05) Between 0.0381666 0.0127189 3 0,60 0.63466 Non -Significant Effect Error 0.1704716 0.021309 8 Total 0.20862617 0,0340278 11 ANOVA Assumptions Aftributo Teat Statistic Critical P•Value bacielon(0.01) Variances Modiflod Lovene 1199523 7.59099 0,19336 Equal Variances Distribution Shapiro -Wilk W 0.86248 0.05249 Normal Distribution Data Summary Original Data Transformed Data Conap911. Control Type Count Moen Minimum Maximum SD Moon Minimum Maximum SD 0 Dilution Water 3 0.90000 0.8000D 1.00000 0,10000 1.26607 1.10715 1.41202 0.16266 1.876 3 1.00000 1.00000 1.00000 0.00000 1.41202 1.41202 1.41202 0.00029 3.76 3 0.93333 0.80000 1.00000 0.11647 1.31039 1.10716 1,41202 0.17602 7.5 3 0.93333 0.80000 1.0D000 0,11547 1.31039 1.10715 IAU02 0.17602 Data Detail Cone-pgll. Control Typo Rap 1 Rap 2 Rep 3 Rep 4 Rap 5 Rap 6 Rap 7 Rap 8 Rop 9 Rep 10 0 Dilution Water 0.80000 1.00000 0.90000 1.875 1.00000 1.00000 1.000Dg 3.75 1.00000 1100000 0.80000 7.6 0.80000 1.00000 1.00000 Graphics r. • o: o.f. oas ae al � . • La7 d ...................................................... dCv<iNul" p 0.051 I; 0 EOAp .................... r. .�'.-.......................... OA � 03 030• �, -0.1S• 0.1 .0.1Pj QO 0 1./7S A79 ~- 75 -07-to' d_.s .1A 0.6 O:S 10- .$ TA C•n°•NOl4 R°pkIU I I I i 1 I ODO-173.102.3 CETISTM v1.1.2revG Analyst: Approval: CETIS Data Worksheet Page 1 of 1 Report Date: 16 Jan-09 2:25 PM Link: 17-9927-6897 Noanthes 10-d Survival and Growth SedimontTest NewFiolds Start Date: 23 Dec-08 01:00 PM Species: Neanthes arenaceodentata Sample Coda: 284325800 Ending Date: 27 Dec-0812:30 PM Protocol: PSEP (1995) Sample Source: Referonoe Toxicant Sample Data: 23 Dec-08 Material: Cadmium chloride Sample Station: P08D418.38 Cone-pg/L Code Rop Pas # Exposad N Survivod l Total Wolghl-mg I Taro Wolght•mg Pan Count_ Meen Longfh mm Notos_ 0 D l 7 14 10 a 0 � _ 0 D 2 6 7Q • 10 _ 0 ' 0 D 3_ 6 10 9 i 0 1.076 1 13 10 10 0 1.075 2 10 10 10 ,•••_ 0 _.i_�.. .. 1.075 3 11 10 10 ry ^ 0 3.75 •.,_—' 1— 3 --10 10 0 __�._ •—_- 3.76 . 2 9 10 ._ 10 .._ 3.76 3 2 10 3 0 7.6 1 17 10 e .. — �.-._.�. 0 �.... _.___ _—._... ... _.._ ..... ....._. 7.5 2 T _. 10 10 0 7.5 l 3 18 10 •.•„ 10 0 15 1 16 10 0, 0 —....____......._ _... _._ 0 1 9 10 0 — 30' 3 1 to 0 0..... 7 000.173.102-3 CETISTM v1.1.2revG Analyst: Reviewed By: 96-HOUR REFERENCE TOXICANT TEST WATER QUALITY DATASHEET CUFNT SAIC PROJECT Duwamish Liver SPECIES NEWFIELOSLABORATORY PROTOCOL NeantResaremceodentata Port Gamble Bath PSEP 1995 NEWFIELOSJOSIIUMRER 0 PROJECTMANAGER Tracy Schuh QUANTrrVOFSTOCK:4SmL Q1JANTiLYOFD1UENT.1f5WmL INIT L» ACIVAL• !S ) ACTUAL �C..n/t �JTF GATE➢REP IZ /•••'� LG TwtIO OL 4 . J9 LOT1A OG-Stom TESTSTART DATE: TIME F14D GATE TIME 23DeCW J 5�-& 1 27Dec06 I "o -50 WATER QUALITY DATA M711,1WAT.BATCH TEMPRECK REFERENCETOX MATERIAL REFERENCEToIcCANT 0 cadmium chloride cadmium -w C tTFiT ._-i'.*-v� i', xa -'•xa nm � r ' :.YG... :.;�v�'•� .. .. , .� «.. ... =R%f v _�:� �v F`.a. �.,.. �--;Yy.+'.,c<-T z CUENRNEWFIELDSID coNGENiRATIDN DAY REP D.O. TEMP. SALINITY PH WO TECH Yaivr s.iM1s mCyrL - '[C/ ./.fir, w/�w, .rc ReLToX-cadmium 0 mgil. 0 Stock i ,4. ! /.�•r 3 q 15 1 •� Qppt � 11 i- �u7rtit Z 7 7 _ 1 Rep 1 t 2 Rep 3 Rep 3 3 G •L-� 3 l�.D 3 a s a } A Rep 5 ro. 3 a 19. t 3 Iaff 3 s.y `S Ref.ToX-cadmium 1.675 m91L 0 stock 3 7.1 3 !g, 3-j 7,2 zi 9 Rep 3 6.Z 3 19 3 ZS -3 �( 2 Rep2 3 (o-S 93 1q.S ' 3 3 Rep 3 (�.3 3 0.0 3 23 3 4 Rep T JT [o. Z 3 I') e I 3 x%, 3 9-3 —� ReF.Tax. cadmium 3.7S mqn- 0 Stock 3 7, / 17.5 3 �2 T 3 7�,770 t Rep 1 �-3 . 2 Rep 2 3 te. 3 3 f ,3 3 Rep Jl 6-0 .�l /a�.5 -`.� 3 �a}} Qg 2A 3 4 Rep2 z 10.3 3 10 3 g`Z rr. 19Z:r200e Gv arrl:h NWlhes.,d,Cd RTWO Page �iEiF'ILD 96-HOUR REFERENCE TOXICANT TEST WATER QUALITY DATASHEET CLIENT SAIL PROJECT Duvramish river SPECIES NEMIELDS LABORATORY PROTOCOL Neanthes arenaceodentata Port Gamble Bath 6 PSEP 1995 NEIWIELDSJOB NUMBER O PROJECT MANAGER Tracy Schuh QUANTITY OF�SPTpOCK:4.5 mL QUANTITY OF DILUENT: 1500mL INN ACTUAL: 1 y ACTUAL- DATE PREP Teat ID LOT%: TEST START DATE: TIME ITESTENDOATE TIME 23Dec08 27DecD8 WATER QUALITY DATA OILTIN.WAT.BATCH TEMP REC# REFERENCE TOX. MATERIAL REFERENCETOXICANT o cadmium chloride cadmium • ¢' O _'A�a°e �r... •r_ti.".2a' .�° . ;.. .r, _�.c-v $' p.. .:ft �rwYa'..�s SEA-- :fslTn ff`•�+ ` y _-Ys'a^ •Y ' ...v.-a�.,T.' 11-0 ,s'" Ref.Tox: cadmium 7.5 mg1L o Stock ,3 7. 0 3 17, s 3 Q 8 3 7, i 1 Rep 1 ?j6. f 3 , 3 2 �7 7�-, 2 Rep 2 .2j 4.1 g ] y g fig' 32 �1 3 Rep .�J G.� s 1q. Iq.� 3 �S 3 -73 nTs li 0 4 Rep t Ref.Tox: cadmium 15 mg1L D Stock 3 7, 7,7 1 Rep 1 I 3 Z 0 2 Rep 2 3 (ci 3 1 q- 3 108 3 -S 3 Rep 3 3 5. 19.3 31 a.s 15 1,6 1yr/�P 4 Rep 1 : Ref.Tox.-cadmium 30 mgiL D Stock 3 7. 3 /9. 3 a 51 3 7,7 7� 1 Rep 1 �- l T• �- 3 Z �_ !' �`— 2 Rep2 $ Rep3 4 Rep 1 121232008 WwamimNennlhesr& Cd RWIQ Page 2 I NBwFII I,DS 96-KjUR. REFERENCE TOXICANT . EST OBSERVATION DATASHEET SPECIES Yeanthes arenaceodentata CLIENT PROJECT NE4IFIELDSJOSN PROJECT MANAGER 14EWFIELOS LAD PROT0004 SAIC Duwamish river 0 Tracy Schuh Post GamJ1a Both 6 Pa9P 3999 SURVIVAL, & BEHAVIOR DATA •. T:.• ; "OgyT - t, DAKT:a%; 'ie"1L 5<'f: ::'`'DAY,Y7d,:zr�: Rai:; AY 4'�<.3;T NS• Numhor on lho Surfaco :`� :•.i ;,.;}+', re r•Lf•„.:., :}p°.,1,:> ., .�;�:'i;•.r:f' '.'x:an.C.'..3i':•.idry�':a:d'_ du. 9M• Numhar of Mortality L+Anoxic Surfato DATE DATA DATE DATA F•Funpd Patahatl INITUI4NOR / 9,5- y D.NoAIr FIOW(D04) ORGANI9M3 �'� I(�%= U•Excoos food ! N.Normai...........»......•....•..»......»....•.........»»...•.....,«....,.............•..:_......»..........._...••...•.......•.»» »...... I TEd11NICIAN tECNNICIAN TECHNICIAN TLCIINICIAH•••»••••»»•• S•No Burrows OON4 INITIAL. CLIENT/NEWFIELD9ID REP volua unib LAUNDER NALIVfi NDEAD 039 LOW)Vg NO[AD cos NALIVE � NOEAO OD9 NALNE NOEgD 1 009 Ref. Tox. L i cadmium 0 mqY 2f.(O: CC t0 .T 2':fi 1 _..T. I N i f6 ; (JUCi 6 ( !E /� Qi alt 4r to I � � � jU j II N I O Rtlf .Tox . - Lgi:Ir r c4 i »...1..,».•,. • Z 1..,......•,., _........L..._......»........I.- 1.075 mg/J. •.3 I� hi` 10 �,� `` ...... »tO L cadmium ; ..��?»..•. 3!» •„»»,.•_.»..... ..�9......d•..,..f.»» • L 3.'5 4i36'r'i iii m.•tCD.$....» ...(» 10 . n.._.t. .»�_LU»»....... S � i.»N.•»» �_ .; Fr..._.N».,«..10.a.• N Ref. Tox. i.»...........jf » ».j cadmium 3.75 mq/I »2., �j,'•,4it (4 4f .; 0».,.�......_!.... .1 �,» ..I t%..»„ ..»^i (Ci ' .»..• ,.. Ref . Tox . - ..••y»,« 06 7.5 ry/l 2 :i7 r':j'"' �I•Xy�...•,Vcadmium (J .�•............... ..b,....V» ............ .•J.C«3.•.,.•.,..,dl� 1 . in' '• ( 0 D ; ! ! N F Ref. Tox.- cadmium 15 mpn. :.,.I•, ..,C .••,IJ�ra"•� ,tt .... ... .. Iv ..,..�.«.•�t l ,.�. .........II» 3.».•l,,,!....... »...,i. t Ref. Tox.- 30 ...... L, 9 cadmium I.;;,.1•.I;° �..... I........... „Y.. •..... «.• I... ». }. i•._........ �1YeYfdQ 1L� Ijl1�P I��26G0� 0 12/23/2008 Duwamish Neanthes.xis Cd Mow Page t V I I 11 F1 V t I 7 I I L ORGANISM RECEIPT LOG Date: la-j I�(og Time: I��o NewFields Batch No. b1-or Organism: Source: Address: Invoice Attached Yes No Phone: _ Contact: No. Ordered: No. Received: Source Batch: CC4t"Xg Condition Organisms: Approximate Size or Age: 3 _c", lv\M Shipper: RAP-x B of L (Tracking No.) 0099, %�(9C� Condition of Container: �5mt\ Received By: 1/iK/LiS Confirmation of ID of Organism: Yes No Technician (Initials): NW�uC, Notes: pH (Units) Temp. (°C) D.O. (mg/L) Conductivity or Salinity Include Units Technician (Initials) Notes: i 1 ' Appendix D Water -Column Toxicity Tests Data Sheets and Supporting Information 1 1 i 1 1 1 1 I I I i 1 i -- M M � 00 HCO1SPMD PAMUu4M M M M M NEDF'FIELDS PHASE TEST WATER n1 IAI iTY nATeCHFFT DENT PROJECT SPECIES DILUTION WATER BATCH TESTSTARTDATE TIME City of Newport Marina Park Menidia beryllina FSWO10609 07Jan09 i k EWF1ELDSJOBNUMSER PROJECTMANAGER NEWFIELDS LABORATORY PROTOCOL TEST END DATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPANSCOE 19981 NEWFIELDS 510067 11Jan09 1-7 0 - WATER QUALITY DATA TEST CONDITIONS ! uv > 3lmgy.7 CONCENTRATION DAY REP DO CLIENTI NEWFIELDS ID value I units meter mg Control 1. 0% 0 All Control ! . 0% 1 1 Control 1. 0% 2 2 q - _t Control /. 0% 3 3 U .1 �.._.... c 2 ......3 .._.....7.: '7 Control / . 0% 4 ... _..... ... 5 '7. Site Water 1. 0% 0 All Site Water / . 0% 1 1 L} , Site Water 1. 0% 2 2 �. Site Water / . 0% 3 3 t 1 3 Site Water/. 0% 4 ... .=� .4.........I._ 1/7/2009 Menidia SPP Test WQ Ct) WG cf IlfD!°q 0 wV C4- Yll jog r nq 20t2 31 t2 7.8±0.5 TEMP. SALINITY PH meter "C meter PPr meter uNt / 3Z 1 � 101.S 1 3� I W-MVA 33 33 3 Date I Tech I FEEDING r Page 1 96 HOUR SUSPENDED PARTICULATE \TEV7FIEIDS PHASE -TEST . WATER QUALITY DATASHEET WENT PROJECT SPECIES DILATION WATER BATCH TEST START DATE TIME City of Newport Marina Park Menidia berylfina FSW010609 •07JanO9 (600 EWFlELDSJ09NUMBER PROJECTMANAGER NEWFIELDS LABORATORY PROTOCOL TES'TENDDATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPAIIISCOE1998tNEWFIELDSB10067 11Jan09 WATER QUALITY DATA ' DO 03914 > 3.7 TEMP(C) 20±2 SAGNITY(W) 31 ±2 PH 7.8±0.5 CONCENTRATION ay �p Date Tech FEEDING D.O. TEMP. SAUNITY PH 7CUEHT1OSIDvalue units meter m9A. meta 'C meter PPt meter unit 1. 10 % 0 All 7-$ Comp GU 1. 10 % °t t 3 t �. o t $ t1N�lg /✓c;5%;// Comp C-U/. 10 % 2 2 • I 1 L4 18-S t 32 1q• $ 1 �� Comp/ . GU 10% 3 3 4 -7. tAi9. ) 3 I 7_-7 t/ta ,. . r Comp GU / . 10 % 4 3 Comp C-U / . 50 % 0 All If 17.7 Comp C-U / . 50 % 1 1 . l t;rn7 t 3 3 1 t Comp C-U / . 50 % 2 2 -j--4 33 1 4- 9 E t 644 Comp C-U /. 50 % 3 3 t t -7•7 3 �S . o2_a& � q.......-Comp GU/. 50% 4 3�. �.?5 _$ 4µ Comp C-U / - 100% 0 All (0117 9 Comp C-U /. 100% t R . g E Comp GU / . 100 % 2 2 3. Comp C-U/. 100% 3 3 7. $5 I _-i Ifto C4 CompC-U/. 100% 4 3 ZT0 2 — 'or Meni ' SPP W IM go W g* HO PHASE,`EST*jU1)&1 MIN r M W 1� NEWFIELDS wnTt:o nnet try neTncuFcr LIENT PROJECT SPECIES DILUTION WATER BATCH TESTSTARTDATE TIME City of Newport Marina Park Menidia beryllina FSWO10609 07Jan09 1600 EWFIELDSJOB NUMBER PROJECT MANAGER NEWFIELDS LABORATORY PROTOCOL TEST END DATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPA/U8COE 1998 / NEWFIELDS BI0067 11Jan09 WATER QUALITY DATA DAY CONCENTRATION REP CLIENT! NEWFIELDS ID — value units meter Comp C-L 1. 10 % 0 All Comp C-L / . 10 % 1 1 Comp C-L / . 1 E 0 2 2 Comp C-L 1. 10 % 3 3 2 Comp C-L / . 10 % 4 3 5-..... ........ Comp C-L / . 50 % 0 All Comp C-L / . 50 % 1 1 Comp C-L / . 50 % 2 2 Comp C-L / . 50 % 3 3 1 2 ..... Comp C-L / . 50 % 4 3 Comp C-L /. 100 % 0 All Comp C-L / . 100 % 1 1 Comp C-L / . 100 % 2 2 Comp C-L / . 100 % 3 3 1 Comp C-L 1. 100 % 4 3 .............. 4 mg/L r ter °C meter I. Z 9-. v rtf -7 2 t 0 32 t 1 3 7.8 a 0.5 Date Tech FEEDING meter unit Grp 1 I U Page 3 117/2009 Menidia SPP Test WQ Page _of I Ammonia Analysis Total Ammonia (mg/L) Client/Project: / Organism: 7ewFields Test ID: Test Duration (days): PRETEST / CM / FINAL / QnR rcle one) DAY of TEST: 47 OVERLYING (OV) / POREWATER (PW) (circle one) Sample temperature should be within +leC of standards temperature at time and date of analysis. I I Sample lD of Descriptioli- Cone. or ltep , Date of Sampling nand Initials Ammonia Vdlu6 m Tamp C Date of Reading and � Initials sample Preserved (YIN)' pH Sal (ppt) Sult ing/L Cc--. idl 1109 .4 O.o*G ( t # o .- A( PUP- Hh /AA S��c iJa.Fw- b•aO C-L to p.00 too O.cO Grp of oD Crt( LO 1 �•QV Z:V'rojecOB10ASSAY PII,BS\Lab Logs & PormslAmmonia Analysis Record.doe Last printed 1/7/2009 3:00:00 PM ' no Io 9MUR%%PM&DMTIdI.&TEWASIRST= DATA SHEET 3 NTtWFIELDS BPEDIES Menidia beryllina CLIENT PRQIECT NEmELOSJOBND. PROJECT MANAGER City of Newport Marina Park 1105-005-860 Bill Gardiner ON on m OBSERV=M5KEY N = ..I O< • tlsacolotaxie0 05 on be:xom DATE g 69 DATE q DATE 11.10„_•_ GATE :.OE. leas oS e5beiabiiu I ]4 Pei 0 euieaeene NB = eo botlY $DR• accfacing TECNMICIPN ^ �� ••___._._._..... 6 TECNMCIIWi".. ___._._.-..._.... ................._.........._...._._._.__._...__._._. iECNhIGIW tECHNICIAN ..............._..... CLIENONEY IFl SID va lCOW.unR1 Rat NUM R a - i 10 t O._...s._.iU 0 rJ w € € .._.._ ...lJ ' Control / - 0 % 3 1 O ..._........_._. 1 r. _..___... ........ ........ .._ 4 ?0.._._ ............... .___..._.._ .5 _. o 1 9 t €r9€ _ .. Site Hater / 0 % 2 -•-• 3 — •••--• ! __W._ _ •- -• - 1_4.__..�p ._ ._._........_._..._.. �.!? _.!R_ _ _..._._.... ...._._._...................... - "p..._c..._._._....._._..._._. .....__._. _.�(7.....__ ..........._... __..._._ _.. .......__ _.._._,........ . .............. ........_....__ l0 (�i . _.__.<_ ..._i.--._.._..._.—. ._.LU`..._....___..._..._f.._.)__..._....... __ 'l.._Q_-.E__.=�f-....._...... _ .............__..... 5 )�%•-i la LD i - E�...._._I_o .. ..........!a_.i.. ......4 ............. ._ iD = o ...... ......._�..............:_ ., ..__._.'......._ Comp C-U / - 10 % J..]3 O...... ..._.....__-_ (!7...... .Q_._.._._. .-'.. .._._...._ 10 Y% .... i{3 it ,._ ......... •iR.7. D-...._.. ............. _... .9 1 9_..._......_._.NN�_._..- ..e. .................. Comp C-U 50 ...3...�0......._.._...._.._ _.__..._._._._........ . ............_._.I...._ _..h..!..........._._._. .._._.___. . _...... 4 _�........ a...._..... .�.._'a._.._._ ........ 5 ....... ... ..>.....___....._._........._. €o to € 1 `E....._........................_...........?S�._. ......!.f6._...._.... ..SS?...__._d._......%�................ _.L..... 0 ......__.............. ...... . 2 _._ . _._.._ iD._..__._...._........... _..EQ....i._........._............_.....:... .._ N Comp C-U / 100 % .3. .... ....... _.��_._. .�.......`. ... ..._. >_0 �.:_:...._.-:.._..._.... __�,....0 ;;..__..._..._-.._...---.. Lo 1f712009 Menidia SPP Test Survival Page 1 NEWFIELDS lEM City of Newport 96 HOUR SUSPENDED PARTICULATE PHASE TEST DATA SHEET 3 beryllina marina Park 1105-005-860 1 Bill Gardiner Da3ERVAMMS KEY N - ..I w - sgtllin_Av- oo bm. Wx- Sus e! W - 0 - wi.xmt s - jasper $DR- auciacim FB rro body DATE 1 � D q was ( � Q t OATE I tO l TECNNK:UN Y• TEC/INICWI,{ TECNM�CIAM ^ TECfLYKWI /1 n l�'— CUFMINeYFIf1D5ID _ COMG R Comp C-L / 10 % 2 € O to E 0- O i 10j„�, 9 to O ` in 05 _ lb € 0t to O € € O Comp C-L / 50 .6 1 3 In€ Q to f i 9 t� 0 € b =%j O € 5 ( GO ? o A t0 € c, Comp C-L / 100 % 3 a ( i a fi€ O to = to I ice :' to @ ? JA, to i D i 5 t0! 4D t I17J2009 MenlEla SPP TwtSurvNa( Pagtr2 1— I rr-ri.(Z nr. (hart I I Pagel of 1 Report Date: 28 Jan-09 4:51 PM Reference Toxicant 96-h Acute Survival Test NewFlelds Test Type: Survival Organism: Menidia beryllina (Inland Silverside) Material: Copper sulfate Protocol: EPA/821/R-02-012 (2002) Endpoint: Proportion Survived Source: Reference Toxicant -REF 409 W 200 - _ ............................... iee.._..-__.... U o 0 0 0 0 0 o q b 4 4 c 0 o q q q G N O e� N N N O O M C'1 N � ••� N �+ Mean: 203.791 Count: 19 Sigma: CV: 49.32% Quality Control Data Point Year Month Day Data Delta Sigma Wa 1 2005 Nov -y18 231.0145 27.22398 0.31276 2 29 177.3950-26.3955-0.34600 3 2006 Jan 5 143.6334-60.1571 .0.87269 4 13 86.05408-117.736-2.15041 (-) 5 19 253.8606 60.07008 0,54799 6 25 145.0174-58.7731 .0.84867 7 Jul 14 138.7884-65.0022-0.95818 8 Sep 21 301.4977 97.70718 0.97696 9 27 400.0000 196.2094 1.68211 (+) 10 Dec 6 306,3111 102,5202 1.01646 (+) 11 2007 Jan 5 130,3407-73.4498 .1.11482 (-) 12 May 31 124.1810-79.6095-1.23558 (-) 13 31 186.8127-17.9778 .0.23036 14 Jun 21 187.8662-15.9244-0.20295 15 2008 Feb 15 298.8723 95.08178 0.95514 16 15 232.3128 28.52228 0.32674 17 May 21 277.7252 73.93468 0.77210 18 Sep 16 234.4507 30.66018 0.34969 19 Dec 16 306,7106 102.9200 1.01972 (+) 20 2009 Jan 7 227.3526 23.56208 0.27290 -1s Warning Limit: 136.481 +1s Warning Limit: 304.296 Action Test Link -2s Action Limit: 91.403 +2s Action Limit: 454.368 09.7179-4794 11.4481-7307 11.9868-2213 07-1919-5333 (.) 06-6412-0123 07-5635.3913 14-3550-5235 08-7655-3856 09-8902-4433 10.2133-1793 12-3489-2800 05.4639-7387 13-2437-4560 13-4184.0272 06-7939.8708 18-0414-2219 13-1351.8433 14-1844-9693 10.8312-3501 05-6092-7194 07-3393-4206 09.0298-1066 15-1085-6486 07-8998.8487 11.4444-5191 09-2989-1578 09-0873.1841 02-2843-3056 02-3273.3535 024632-0088 09-4275-9770 06-5552.2016 15-9104-3417 05-6930-9029 14-9978.8744 16-1416.6951 07-0376-1286 14-5736.1267 ' 000-173-102-3 CETISTm v1.1.2revG Analyst: Approval: CETIS Analvsis Detail Comparisons: Page 1 of 1 Report Date: 26 Jan-09 2:46 PM Analysis: 15-4413.4731 Reference Toxicant 96•h Acute Survival Test Newl'telds Endpoint Analysis Type Sample Link Control Link Date Analyzed Version Proportion Survived Comparison 07-0376.1286 07.0376-1286 26 Jan•09 2:46 PM CETISv1.1.2 Method Alt N Data Transform Zeta NOEL LOEL Toxic Units ChV _ PMSD Dunnetl's Multiple Comparison C > T Angulor (Corrected) 11100 200 1 141,421 21.11% Group Comparisons Control vs Conc-pglL Statistic Critical P•Value MSD Docision(0.05) Dilution Water 25 -1.1032 2.35616 0.9808 0.23853 Non -Significant Effect 50 0,28643 2.35615 0.6951 0.23863 Non•SignifcantEffect 100 .0.7528 2.35616 0.9549 0,23853 Non•Slgnificant Effect 200 2A7063 2.35616 0.0405 0.23B53 Significant Effect ANOVA Table Source Sum of Squares Mean Square DF F Statistic P-Value Decision(0.05) Between 0.3200928 0,0800232 4 3.90 0.02289 Significant Effect Error 0.3074808 0.0204987 16 Total 0.62757352 0.1006219 19 ANOVA Assumptlons Attribute Test Statistic Critical P•Valus Docision(0,01) Variances Bartlett 1,10293 13.27670 0.69381 Equal Variances Distribution Shaplro•Wilk W 0.95640 0.45657 Normal Distribulion Data Summary Original Data Transformed Data Conc•pglL Control Type Count Mean Minimum Maximum SD Moan Minimum Maximum SD 0 Dilution Water 4 0.87500 0.80000 1.00000 0.09574 1.21884 1.10715 1A1202 0.14512 25 4 0,95000 0190000 1.00000 0.05773 1.33053 1.24905 1.41202 0.09409 50 4 0.85000 0,70000 1.00000 0.12910 1.18984 0.99116 1.41202 0.18182 100 4 0.92500 0.80000 1.00000 0.09574 1.29506 1.10715 1.41202 0.14695 200 4 0.67500 0.60000 0.80000 0.12583 0.96872 0.78540 1.10715 0.13389 Data Detail COno•pglL Control Type Rep 4 Rep 2 Rep 3 Rap 4 Rep 5 Rep 6 Rep 7 Rep 8 Rep 9 Rep 10 0 Dilution Water 0.80000 0.80000 0.90000 1.00000 25 0.90000 1.00000 0.90000 1.00000 50 0.7000D 0.90000 0.80000 1.00000 100 0.80000 0.90000 1.00000 1.00000 200 0.70000 0.80000 0.70000 0.50000 Graphics 1.0 O-U 1 i os � i es o. oa ass o ......................................................... x Ol i • • Ob � 0.0T• O.S •! 0.00 .......................................................... 0.1 •005 03' •• at: -010 o.i •ais OA 0 IT 50 IOO 100 •b0 -1.S •1.0 •OS 00 OS 1.0 1.5 LO C0naY0/L R•nklU 000.173.102.3 CETISTmv1.1.2ravG Analyst: Approval: Spearman-Karber: Page 1 of 1 Report Date: 26 Jan-09 2:46 PM CETIS Analysis Detail Analysis: 14-5735-1267 Reference Toxicant 96-h Acute Survival Test NewFields Endpoint Analysis Type Sample Link Control Link Date Analyzed Version Proportion Survived Trimmed Spearman-Karber 07.0376-1286 07.0376-1286 26 Jan-09 2A6 PM CETISv1.1.2 Spearman-Karber Options Point Estimates Threshold Option Lower Threshold Trim Mu Sigma EC50/LC50 95%LCL 95%UCL Control Threshold 0.125 0.00% 2.3567 0.02359894 227.35260 203.93980 253.45320 Data Summary Calculated Variate(A/B) Control Type Count Mean Minimum Maximum SE SO A B �Conc-Ng/L 1 0 Dilution Water 4 0.87500 0.80000 1.00000 0.01954 0.09574 35 40 25 4 0.95000 0.90000 1.00000 0.01179 0.05773 38 40 50 4 0.85000 0.70000 100 4 0.92600 0.80000 1.00000 0.02635 1.00000 0.01954 0.12910 34 40 0.09574 37 40 200 4 0.67500 0.60000 0,80000 0.02569 0.12683 27 40 400 4 0.00000 0.00000 0.00000 0.00000 0.00000 0 40 ' Graphics r.o 09 • • 0.0 0.0 Qg 0.9 r 6 g oA 03 0.9 or 30l 90D 900 0 100 20D COnc-pa/L 11 I 11 I i 1 000-173-102 CFTIS Data Worksheet Page 1 of/1 Report Date: 26 Jan-09 2AS PM Link: 07-0376.1286 Reference Toxicant 96-h Acute Survival Test NewPlelds Start Date: 07 Jan-09 04:30 PM Species: Menidla beryllina Sample Code: 1329533958 Ending Date: 11 Jan-09 05:00 PM Protocol: EPA18211R-02.012 (2002) Sample Source: Reference Toxicant Sample Data: 07 Jan-09 04:30 PM Material: Copper sulfate Sample Station: P070930.99 Conc-p9tL Code Rep Pon M Exposed 8 Survived Nolen 0 D 1 12 10 8 0 D 2 11 10 8 0 D 3 7 10 9 0 D� 4 23 10 10 25 1 20 10 -_-9 25-- 2 2 10 !10 25 3 1 10 25 4 17 10 10 50 1 21 10 7 so 3 8 10 8 50 4 19 10 10 100 1 i6 10 0 100 2 24 10 9 100 3 16 10 10 _ 100 � 4 6 10 10 200 y�- 1 13 10 7 200 2 1s 10 200 3 22 10 7 200 4 9 10 5 ..� 400 1 4 10 0 400 2 1 s 1 10 0 4 4001 1 q 1 3 1 10 0 000-173.102-3 CETISI" vl.1.2revG Analyst: Reviewed By: ' I NEWFIt;LDS Reference Toxicant Test Water Quality Datasheet !pO7eO q-F)_ G4 CIJENT PROJECT SPECIES PRGTOCOL TEST START DATE TIME City of Newport Marina Park Menidia beryllina Port Gamble I Bath Wan09 VO 30 EMIELDSJOBTIUNB PRDJECTMANAGER QUANTITY OFS70CK TARGET QUANTITY OF DRUENT TARGET TESTEND,DATE TIME 1105-005-860 Bill Gardiner 1.572 mL 2000 mL 11Jan09 —VA t7oo EWFIELQS LABORATORY DILUTIONIVATERBATCN - QUANTITY OCKAMAL QUANR OFDILUEN '- INM— LAND PROTOCOL Port Gamble Bath FSWO10609 JUSEPAAISCOET89S/NEWFIELOSBIO067 !•BMI""wwML{{ { VA{/{ _ CUENTl NtWro F1ElOS DAY CONCE2ITRATKNi slue w is REP TA(mp'L) > 3.7 TEMP(C) 20 i 2 SAIYBTY(PPU 31 t 2 PH 7.8 t 0.5 n,te r«N FEEDING �� D.O. TEMP. SAUHr Y PR w4 w m41L M trt 'C IIINM ppt IIIMer uNt Ref.Tox.-copper0 mg/L 0 all 4 -Iq y t 8• o f 32 t 1,5 fi t( o `i� t OJA6 to - Ct tA- V51 •S i 32- l S t $ M"e* 2 2 1'1 b H 1$ -9 , -• S / q frrL f"'wt►S 3 3 'A (0.7 L1 11.0 f 37Z- Tf> lffo 4 4 3 tv.5 3 iq.s 33 3 -7•`6 t ct Ref.Tox.-copper25 mg/L 0 All q$.o q t8.O t 3� t g _ t(a fTx i5 tMRF� 1 1 L'r '�•. o t °(. g t 31 •t �-, $ 18 MM,b 2 2 tq, t 'rja ) 9 n)`15 3 3 y g y tij,f 4 4 3 •6 13 1 n :7 3 33 �3 �?• t%if Ref.Tox: coppe 50 mg/L 0 all ts. o t 32 11 1114co, 'CS o tk lit.'s i.8 t 8 NA Mf- 2 2 tA :7,1 Lf (q. fo 1 3 ( :7 ( 4 ell to i 3 3 6.1 tj H{ 3 Z i -I. (10, G� I� 11WI TAWRT'lln an no so Ml M r �' City of Newport = DS JOB NUMBER 1105-005-860 a.OS LABORATORY Port Gamble Bath Ref.Tox.-copped 100 Ref.Tox.-copper) 200 Ref.Tox.-coppery 400 pftfew jope bWcq*Fesj=. *a W IM pw am » W Water Quality Datasheet T SPECIES PROTOCOL TEST START DATE TIME n'l Marina Park Menidia beryllina Port Gamble / Bath 07Jan09 16 :TMANAGER QUA OFSTOCKTARGET QUARTITY OF MUENT TARGET TEST END DATE TIME Bill Gardiner 1.572 mL 2000 mL 11Jan09 )N WATERBATCH FSWO10609 QUANRTYOFSTOCK.�AtCTUAL ( 1.5?a51�,Jn( QUANTITYOFDILUENTACTUAL .1000.0� INIWUMD 99A 4S trglbe, PROTOCOL USEPAAJSC0E199SINEWFIELDSBI0067 voee ©©en ©mar, ==ME wMa■ oven a©e■ amen ao©® am© anion a©©n amen == BM Date 1 TKII FEEDING ■© • v�an�n�■■�■■� ■©�n�e - ■�®ram ■© .. om■�■■■®WN R© 177/2009 Menidia SPP Test Cu RiWQ Page 2 ORGANISM RECEIPT LOG Date: �6I0°i Time: i y30 NewFlelds Batch No. t�►�S ISY�rib Organism: Yt'e ,G ��y II; Source: ��,�� a sysl« F Address: Q �. le invoice Attached Yes No Phone: � �. Contact: No. Ordered: 775 No. Received: 1 650 Source Batch: Condition of Organisms: Itid.,41 lod«d Approximate Size or Age: )u o�r� Shipper: B of L (Tracking No.) Condition of Container: r,0o� Received By� �f Confirmation of ID of Organism: Yes Jo Technician (Initials): �!,( Notes: pH (Units) Temp. VC) D.O. (mg/L) Conductivity or Salinity Include Units Technician (Initials) ab $ r� ► �'� �3 v a a� �i� Notes: i 1 I It I I I -j';m!. am M mill M M M .L�jEWFI!`LDS 11,1 I WATER Of JALITY r)ATASHEET CLIENT PROJECT SPECIES DILUTION WATER BATCH TFSTSTARTDATE TIME City of Newport Marina Park Mysidopsis bahia, FSWO10609 07Jan09 I��Aq NEWRELDS JOB NUMBER PROJECT MANAGER NEWFIELDS LABORATORY PROTOCOL TESTENODATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPANSCOE 19981 NEWFIELDS B10067 11jan09 1 00 WATER QUALITY DATA TEST CONDITIONS . ......... ... . 1/712009 Mysid SPP Test WO Page 1 NEV�FIEIDS 96 HOUR SUSPENDED PARTICULATE PHASE TEST WeTFR f]ILAL MY neTeSHt=FT CLIENT PROJECr SPECIES DILUTION WATER BATCH TESTSTARTDATE TIME City of Newport Marina Park Mysidopsis hahia FSWO10609 07Jan09 l6t15 EWFELOSJOBNUMBER PROIECTMANAGER NEWFIELDS LABORATORY PROTOCOL TESTENODATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPA/USCOE19981NEWFIELDSBI0067 11Jan09 WATER QUALITY DATA DO(DyL) TEMP(C) SALINITY(W) PH ' >3.7 20±2 31±2 7.8±0.5 CONCENTRATION DAY REP Date Tech FEEDING D.O. TEMP SALINITY PH CLIENTINEWFIELOSIO vNts mates myL meter 'C rMttt PM meter unit Comp C-U 1. 10% 0 All :7- Cf CompC-U!. 10% t 1 CQ.� Lk tLl.�t 1 a t i.�1 l tLl*t i% Camp C-U/. 10% 1 2 2 I °L 13{ r"t)5bm Camp C-u!. 10% Comp C-U /. 10% 3 3 1 2 4 3 4 7 .2 fM Camp C-U/. 50% 0 All ,2 W I Mf C ! 71/&7 1-% Comp C-U / . 50 % 1 1 to - lv Comp C-U /- 50 % 2 2 L 1 5• K { �. i 3 t I a yj{4 HwV Y5K Comp C-U /. 50 % 3 3 14 Ig to 1 3 t4 I 7 I/TO tP-- L-9- WIT�.� Comp C-U / . 50 % 4 3' - -!� _ _ 3 _llll! !r7/ C-U / C-U C-u // Comp C-U / 100 % 0 All If I (� q ty I / -zi I I JY I f 4A,3 0 '0' 1o0% 1 1 5.% t , ;' 100 Rio 2 2 5•0 t -Is t 35 t 74 (R N �r3 100 % 3 3 y 5.9 Li l 3'`i t S t {a eel �•i_ 2 100 % 4 3 4 { •5 �? q r Page 2 NE'WFIELDS M NdH0%WsPHA WPu*916 _ PST UUAT=P nl IAI ITV nATACt4l=rT LIENT� `^�1µ PROJECT SPECIES DILUTION WATER BATCH TEST START DATE TIME City of Newport Marina Park Mysidopsis bahia FSWO10609 07Jan09 1 %4 E� S EWFIELOS JOB NUMBER PROJECT MANAGER NEWFIELDS LABORATORY PROTOCOL TEST END DATE TIME 1105-005-860 Bill Gardiner Port Gamble Bath USEPANSCOE 19981 NEWFIELDS BI0067 11Jan09 WATER QUALITY DATA TEST CONDITIONS lot . "MUA %MME/a .o///YIV .. 1 MEN MIMEN M. ROOM M�!■ V712009 Mysid SPP Test Page 3 Page _of 1 N�C�Fr>L1,pS Ammonia Anal ysis Total Ammonia (mg/L) Client/Project: Organism: NewFields Test ID: Test Duration (days): hr�4-1 PRETI'SSA IA / FINAL ! �WHERcircleone) DAY of TEST:OV YING (OV) /ATER (PW) (circle one) Calibration Standards Temperature Sample temperature should be within ±1 °C of standards temperature at time and date -of analysis. Date: Temperature: 1 0 U 1 1 1 bate of Sampling and tials BMW 'MMMMI1.M 'f owl ZAProjecIABIOASSAY FILBSIab Logs & FormAAmmonia Analysis Record.doc Last printed 1/7/2009 3:00:00 PM M M M M M M 9<RUR%%Pffl&D PRTIMTEWASMSTM M M M M M DATA SHEET 3 1rTE 141'IELI�S SPECIES Mysidopsis bahia CL�Ni moJEOT NEWFIELDSJDa M1V. PROJEGTM Gm City of Newport Marina Park 1105-005-860 Bill Gardiner DeSERvanONSKV N nomal a tliawle[a[ien w:.. loaa e: eP alinviue Da - en koccoc • DATE (� `3 I o- 1-•____._ DATE ' DATE ,('� ' DATE )1t t DAu:.... J - l'-3+c[ SVA. avrta[in9 NS - no L y •__ 6 • MON=" t�wt ....._._......_. ............_...._.__. iECNNICfAN N .__......_....._.__ -.. _ TECHNICIAN ._.._. _._.._....._._.. HNIC CIJEMINEff]ELOSID rat�NGVA RE NDWNam oss xAuvb 4 - 2 N .°5......._.........................._._.._9.....Q._._.._..........._....__.......:....._.......... A/, D... _...._...__....1_»...t).. ......._....................... . Control / 0 % 3 ice.»._ s2�,€€ !J -10_..I) _..__ . I Q.__--._.._._ _?._:i.0...::......»... ........»__....__... . o.._. _ .......... ...... __----- »-- Iv Site water / ?_ _..._...._.... _._ .».............. _.. _._....ttl.» ... ~ ....._..._.. .. .....0............... tll . 7 .......b._ __._._.i.._.__._..._....... . 10 IV Comp C-U / 10 % 3 ......_.._;_..._._ _ _._._ _ to_...o_.........»...... _._._...._._. �!� � l� _t - - ..._...._ . ...��_ �._"__..:.._ .__... _._..__ . e ... ... .. _ ... .._ .._. ___ _._..._._......�.'t%.___.._.»_......._._..._ I0 �.....-._.....» .»_..._._.. ��_...__._..._.... _..._._.. _ .... ................. (5 -_. D Comp C-U / 50 % 3 € _.t.....____ ._. �_�?............ ...._............._.._. �€— s 10 € Comp C-U / 100 1.._t. _t4 ....... ._ ..__*t_.._......t ................_.............._._..._ .._ .._Q._._ ......N-...-_._. .._...0/y....._.._._.................... _10_ ......... _..-_ __....._._..��. .1..._..... ... _..r.......)%............... _�....._.__....__......._.... ..... ..._ ._ 1I72009 Mys-Id SPP Test SDNNal Page 1 96 HOUR SUSPENDED PARTICULATE PHASE TEST DATA SHEET 3 NE'W'FIELDS SPE— - Mysidopsis bahia cuENr vAwEer e�wf=EimuoeNo. vno.merrAxAeen - City of Newport Marina Park 1105-005-860 Hill Gardiner O85ER4ATNNYSNET N . xv+i os u . au�i>:+cioo zoo- I-noof .WWbsiOn . rn b.. Dare t +� o �t t 4 QA mre /�O ! WE t fl f i O - 4vi+oc+ac 4 - j�o A1A-+cxf+cSr.4 AS-rro body TECH `, M TEOIPNmAN TECHMGIAM +{n u� O•R1K4V1 Cl]ENTINEylilF. sw COMC. a=un N) NVMBER i o t0 sir N to to O[ LO O 2 = t o° = o ;-..I T Comp C-L 1 10 % 10 4 1 to 5 `• fi Comp C-L / 50 % 3- Q { Sa' iJ td U i O N O € O 5 e tJ$ =D 1 2 a r, € Se; i " f AF6 = N O J q_ ` 3 t `- € _ '�% f � to a `- Comp C-L / 100 % Q T.E mmis U 6AY FvvA4 al;w 1/11M 60 1/7/2009 Mysid sPP Test survlW page 2 m m m M M M M M M I I' CETIS QC Chart Page 1 of 1 Report Date: 26 Jan-09 4:17 PM Reference Toxicant 96-h Acute Survival Test NewFlelds Test Type: Survival Organism: Mysidopsis bahia (Atlantic Mysid) Material: Copper sulfate Protocol: EPAI8211R-02-012 (2002) Endpoint: Proportion Survived Source: Reference Toxicant -REF 360 ......................... ......... •--� ..... .................................... ......... - 120 60 0 U' o 0 0 o q m ^ ^ ^ ^ m o 0 0 q o 0 o q o 4 {qJl c Z n 75 y IaL N n A U � 2 m 2 N N O wMi N .P-1 N 10 N Vl Yl ti 'y N O 0 O O O m H N N H rl Mean: 238.12 Count: 16 -1s Warning Limit: 182.396 -2s Action Limit: 139.713 Sigma: CV: 30.55% +1s Warning Limit: 310.868 +2s Action Limit: 405.841 Quality Control Data Point Year Month Day Data Delta Sigma Warning Action Test Link - Analysis -1- _ 2005 Nov 18 _ 270.9431 32.82316 0.48439 04-9207.2519 06-7062-9586 2 29 237.8382 -0.28174 -0,00444 13-37494170 12-0215.0194 3 29 254,1857 16.06576 0.24491 14-4179-4943 15-0893-7739 4 2006 Jan 6 216,4655 -49.6544 -0.32314 04-0317-1797 12-3195-9925 5 13 217.9948 -20.1251 -0.33123 16-1881-123712-7567-2246 6 19 248.7937 10.67376 0.16448 08-0452.0770 17-29794106 7 25 146.5691 -92.5508 -1.84597 (-) 11-3116-1669 06-2279-5163 8 Feb 6 356.1905 118.0705 1.51051 (+) 10-1630-9590 13-6331-1854 9 Jul 7 278.1486 40.02866 0.58284 02-9682-5563 11-9863-7491 10 2007 Jan 5 310.4012 72.28126 0.99437 10-8470-2803 06-4877-5470 11 May 31 137.8262 -100.294 -2.05102 (-) (-) 10-1324-7704 03-5962.2699 12 Jun 15 181.7338 -56.3861 -1.01365 (-) 08-4148-797810-6333.9348 13 21 322.6705 84.55056 1.13978 (+) 00-4869.4501 07-4507-6179 14 2008 May 21 211.1782 -26.9418 -0.45040 174827-0455 10.0698-3422 15 Sep 16 297.9535 59.83366 0.84084 07-09964754 04-2869.2915 16 Dec 16 241.8133 3.69336 0.05773 03.2797.2997 02-1235-2262 17 2009 Jan 7 233.2583 -4.86164 -0.07738 00-8997-7963 12-2358-6105 000-173.102-3 CETIST" v1.1.2revG Analyst: Approval: CETIS Analysis Detail Comparisons: Pagel of 1 Report Date: 26 Jan-09 3:57 PM Analysis: 14.7411.8771 Reference Toxicant 98-h Acute Survival Test NawFlelds Endpoint Analysis Tye Sample Link Control Link Date Analyzed Version Proportion Survived Comparison 00-8997.7963 00-8997-7963 26 Jan-09 3:57 PM CETISV1.1.2 Method Alt H Data Transform Zeta NOEL LOEL Toxic Units ChV PMSD Steel Many -One Rank C > T Rank 125 250 0.8 176,777 8.16% Group Comparisons Control va Cone-mglL Statistic Critical P•Value Ties Decision(0.05) Dilution Water 62.6 18 10 0.7500 4 Non -Significant Effect 125 14 10 0.2626 4 Non -Significant Effect 250 10 10 0.0277 0 Significant Effect ANOVA Table Source Sum of Squares Mean Square DF F Statistic P-Value Dectslon(0.05) Between 1,288702 OA296676 3 65.60 0.00000 Significant Effect Error 0.0785842 0.0065487 12 Total 1.36728660 0.4361161 15 ANOVA Assumptions Attribute Test Statistic Critical P.,Value Decislon(0.01) Variances Modified Levene 12.-99229 5.95264 0.00045 Unequal Variances Distribution Shapiro -Wilk W 0.92162 0.17909 Normal Distribution Data Summary Original Data Transformed Data Cone-mglL Control Type Count Mean Minimum Maximum SD ;can Minimum Maximum SD 0 Dllutlon Water 4 1.00000 1.00000 1.00000 0.00000 i1.6 11.5 11.5 0 62.6 4 1.00000 1.00000 1.00000 0.00000 11.5 11.5 ills 0 125 4 0.95000 0.90000 1.00000 0.05773 8.5 6.5 11.5 3.46410 250 4 0.45000 0.30000 0.60000 0.12910 2.5 1 4 1,29099 Data Detail Conc•mglL Control Type Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 Rep 6 Rep 7 Rep 8 Rep 9 Rep 10 0 Dilution Water 1.00000 1.00000 1.0000D 1.00000 82.5 1100000 1.00000 1.00000 1.00000 126 0.90000 0.90000 1.00000 1.00000 250 0.60000 0.30000 0.40000 0.50000 Graphics 09 25 2. OA 1S 0.7.1.0 a 'X/ p r,8 OA .0.5 -10z OS 0.20.100 �-'ter-----�'-1 0 GL5 125 250 • .1.0 -1.5 .1.0 4s 0.0 is 1.0 IS 2.0 cono-mp/L Wnklb 000-173.102-3 CETISTM vi.1.2revG Analyst: Approval CETIS Analysis Detail Spearman-Karber: Page 1 of 1 Report Date: 26 Jan-09 4:17 PM Analysis: 12-2358.6105 NewFlelds ' Reference Toxicant 96-h Acute Survival Test Analysis Type Sample Link Control Link Date Analyzed Version Epoint ortion Survived Trimmed Spearman-Karber 00.8997-7963 ou-8997-7963 26 Jan-09 4:11 PM CETISv1.1.2 Spearman-Karber Options Point Estimates Option Lower Threshold Trim Mu Sigma EC50/LC50 95%LCL 95016UCL 'Threshold Control Threshold 0 0.00% 2.357837 M258518 233.25830 207.07770 262.74870 Data Summary Calculated Variate(AIB) Control Type Count Mean Minimum Maximum SE SO A B 'Conc-mg/ 0 Dilution Water 4 1.00000 1.00000 1.00000 0.00000 0.00000 40 40 62.5 4 1.00000 1.00000 1.00000 0,00000 0.00000 40 40 4 0.95000 0.9000D 1.00000 0,01179 0.06773 38 40 '125 250 4 OA5000 0.3000D 0.60000 0.02635 0.12910 18 40 500 4 0,00000 0.00000 0.00000 0.00000 0.00000 0 40 1000 4 0.00000 0.00000 0,00000 0.00000 0.00000 0 40 ' Graphics 09 OR 0.7 ' 0.6 0 ' 04, 0.3• 0.2 00 000 �a00 200 400 Cont m0/L 1 000-173.102-3 CETISTm v1.1.2revG Analyst: Approval: :,ETIS Test Summary Paget of 1 Report Date: 26 Jan-09 4:17 PM Test Link: 00-8997-7963 Reference Toxicant 96-h Acute Survival Test Newplelds Test No: 09-1778.3253 Test Type: Survival Duration: 4d 1h Start Data: 07 Jan-09 05:20 PM Protocol: EPA/821/R-02.012 (2002) Species: Mysidopsts bahia Ending Date: 11 Jan-09 07:18 PM DiI Water: Laboratory Seawater Source: Aquatic Biosyslems, CO Setup Date: 07 Jan-09 0520 PM Brine: Not Applicable Comments: P070930.100 Sample No: 07-9059.4503 Code: 790694503 Client: Internal Lab Sample Date: 07 Jan-09 05:20 PM Material: Copper sulfate Project: Reference Toxicant Receive Dale: Source: Reference Toxicant Sample Ago: NIA Station: P070930.100 Point Estimate Summary Analysis Endpoint % Effect Conc-m9/L 96% LCL 96°/a UCL Method 12.2358.6105 Proportion Survived 50 233.2583 207.0777 262.7487 Trimmed Spearman -Kerber Proportion Survived Summary Cone-m9/L Control Typo Reps Mean Minimum Maximum SE SD Cv 0 Dilution Water 4 1.00000 1.00000 1.00000 0.00000 0.00000 0,00°A 62.5 4 1.0000D 1.00000 1.00000 0.00000 0.00000 0.00% 125 4 0.96000 0190000 1100000 0,02887 0.06774 8.08% 250 4 0.45000 0.30000 0.600D0 0.06455 0.12910 28.69% 500 4 0.00000 0.00000 0.00000 0,00000 0.00000 0.00% 1m 4 0.00000 0100000 0.00000 0.00000 0.00000 0.00% Proportion Survived Detail Conc-mg/L Control Type Rep 1 Rep 2 Rep 3 Rep 4 0 Dilution Water 1.00000 1.00000 1.00000 1.00000 62.5 1.00000 1.00000 1100000 1.00000 125 0.90000 0.90000 1.00000 1.00000 250 0.60000 0.30000 0.40000 0.50000 500 0.00000 0.00000 0100000 0.00000 1000 0.00000 0,00000 0.00000 0.00000 000-173.102.3 CETISTM v1.1.2revG Analyst: Approval: ' Pagel of 1 Report Date: 26 Jan-09 4:17 PM CFTIS data Worksheet Link: 00-8997-7963 ' Reference Toxicant 96-h Acute Survival Test NewFlelds tEnding Start Date: 07 Jan-09 05:20 PM Species: Mysidopsis bahia Sample Code: 790594503 Date: 11 Jan-09 07:18 PM Protocol: EPA/821/R-02-012 (2002) Sample Source: Reference Toxicant Sample Date: 07 Jan-09 05:20 PM Material: Copper sulfate Sample Station: P070930.100 Conc•mglL Code Rep Pos #Exposed #Survived ---- 0 D 1 14 10 10 '— 0 D 2 1a 10 10 _-- 0 D 3 3 10 10 62,5 62,5 1 2 7 5 10 10 70 10 62.5 3 21 10 10 4 6 10 10 ' 12s U!�. 1 2 10 9 ------- -- 125 2 23 — 10 9 ,_--___.__ _ 125 4 8 10 10 250 1 11 10 6 250 2 1 10 3 ' 250 3 22 10 4 250 4 18 �- _ � 10 _ 5 500 1 4 — 10 0 ,- --. soo _ z ..� n 10 0.-- ' 500 3 24 10 0 -._._..`------- __.— 4 20 10 ... _.._..o.__ 1000 1 9 10 0 —-1000 — 2 15 10 _..._...._...•1000 3 16 10 0 4 10 10�u v 0 000-173-102-3 REFERENCE TOXICANT TEST SURVIVAL DATASHEET Citv of Nawnort I Marina Park 6- 1 Bill Gardiner i Port Gamble Bath I u.epwteoe t.w J.t t. -•.t 0. DATA nnv I I onv P I onr I I DAY OBSERVATION KE Y LOE= loss of equilibrium DO a discoloration INITIAL# OFORGARISMS♦ • . NO = no body Fx Floating on Surface ®®®��L\•,4!lt L1aA><t•N ��LLfIQI.1y.UIt.L!!•flvPlA�l•laAltq.it•f Ot1'Ilibt aljt l.,� Ref.Tbx� copper Ref.Tox.- copper Ref.Tox.- copper Ref.Tox.- copper Ref.Tox.- copper Ref.Tox- per r • • %fir//ii////h��i?;, �/�/%�//./o s' ✓,`�„/„i✓'�%�%,�Cl/ii,!i%ii�rr % �> �i_/.'i • �i • r / I / ��i�//� .r rir/�///%i�/�%'/��.i�rr%�/'Y//j// j/� /r�r///'✓ � r°fir N .r///iir/i/,..0////�,i✓.n/r2 i/i//✓. �i//i., it/,3�Arv//ii/ A/�% /,////;a/�� r:i��% ///%/.:�z!i • i • • r �// 6r %%ir��,l�s / /'/%• %/,i�L///�� P' i /i fi/' %/%i /% / 5 /.rr/%//yr///r<l/' ��///3i/r.��%%//r/,/. ��/%r/i��i./$/�/�f.�////��/rri.•��/i/./�//.�//�/i�/e/ is'e!i�,u r2 / G r • o it � P. r r,� %!% r%%//r %r/r si%/i/ �/ %i//� •/s r�%%if S%%%i i/�i /rid%��i/%% i rf j r�r n � • A / r • r J 0+ sF-tMme 11c)[Ok ®I' C G'L- 00(ai q r 1/7/2009 Myeld SPP Test Cu RTSury Pepe 1 1 .t FEWFTEMDS City of Newport SDS JOS NUMBER .11-05-005-860 :LDS LABORATORY Port Gamble Bath mtef�cemjwicjm6Ted m M Water Quality Datasheet IECT SPEQES PROTOCOL TEST START DATE TIME Marina Park Mysidopsis Bahia Port Gamble ( Bath 07Jan09 IECTMANAGER QUANTrFYOFSTOCKTARGET QUANTITYOFDIWENTTARGET TESTENDOATE TIME Bill Gardiner a.s7-2-m1- 3 q3 2000 mL 11Jan09 19 PION WATER BATCH QUANTOY OF STOCK ACTUAL QUANTITYOFD"EUA��TCTTUAL IN ND DATE PROTOCOL FSWO10609 3"45f,q t � �QU.0 y Ar-f-j USEPAWSCOE IMINEWFIELDS 810067 - DAY CONCENTRATION CLIENT/NEWFIELDSW whm wft REP >3.( ZU�Z 0"1*L (.O S U.O Date Tech FEEDING D.O. TEMP. SALINRY PH me" Fog& may 'C met"I ppt meter unh Ref.Tox.-coppe 0 mg/L 0 All Lf S.O t4 t$.P >< M+u6 a- 2 2 �j. t( t�, 3a ( t y 6vt nrltj JSK 3 3 k 3 it t 3Z .4 G!L 4 4 3 5.18- 3 1 7.5 t%1! ele- Ref_Tox.-coppe 62.5 mg/L 0 All %.0 Lk d 1 32 t 1 1 to . rt Ll• o t 3 ?- 1 2 2 I�.fj 1-t 3a f 3 3 �l. O L, 4 4 15.t'o 3 ta.G 33 Z.-7 1 ! CR Ref.Tox.-coppe 125 mg/L 0 All 4 t �.9 _ t �(04 MM6 j.- 2 2 1A5 LA l q. I l '77'2 3 3 t 32 t,� p ii12 4 4 3 6,(o 31 15,-7 c3 1 3z. 9 -7•7 till a .......... 1/7/2L 4sid SPP Test Cu RTWQ Paget PIELDSReference Toxicant Test Water Quality Datasheet of Newport ffMPT PROJECT Marina Park SPMES Mysidopsis Bahia PROTOCOL Port Gamble/ Bath Tm5TARTDATE 07Jan09NUMBER TIME PROJECT MANAGER Bill Gardiner OUM7NYOFSTOCRTARCET 1.572 mL DUMMY OF OLLUEMT TARGET 2000 mL TEST END DATE5-005-860 11Jan09 ORATORY amble Bath DAJIDOM WATER BATCH FSWO10609 DU n" OF STOC�Kt A/CTUAL -5-`tS61;( ,[. DUANHi QFDILUENTAC W00-0 INIMLAND DATE 75 PROTOCOL USEPWUSCOE19MINEWFIELDS1310067 CLIENT/MEWFIELOSW � CONCEMM�� DAY REP ' DO(MWL) >3.7 TEMP(C) 20t2 SAUNOY("q 31 t2 PH 7.8t0.5 Dab Taeh FEEDING D.O. TEMP. SAUW" PH a .0 Da RefTox.-coppe 250 mg/L o All -..q ts.o 32 1I�IJ� iS NMt�1 1 u< In. `►q, � .1 1 3 a r17 t � M�13 NkM6 d' 2 2 rj(4 Li I M. - l -1 a l f( }�(a r-fA J3 3 '� �3 f'1 [`t 32 1110 G1t %� 4 4 tp . 4 3 l 9. (0 3 33 -7.7 } N— CAL RefTox.-copper 500 mg/L 0 A] 41 14[ .p 1 32 1 1 +. o 4- ao.o ( 3? t `i t 8 M�+� M!✓l °u 2 2 � , q vt } J,i [ ail t � •6 } a '� � rwlfi 3 3 N S.O Lf [ q, � 3Z 1 7.5 1 (O %12 � ce- 4 4 3 to•Z 3 tIP1.5 3 3$ 7•`7 VII C� Cf- RefTox.-copper1000 mg/L 0 All fi.o ►� O 1 32 �•� 1 1 a cE 3a .) t 3 t �.9 i s MM6 d� 2 2 (it - b. ( tj 1R. i' 1 �!Z 16 4 4 C5 3 ' ORGANISM RECEIPT LOG Date: Time: NewFieids Batch No. Ilblyci I30 urce: Organism: 5'S I So�th;� �' V1, i`y5'�u� ' Address: UU Invoice Attached 0,1 n F I� es No Phone: Contact: No. Ordered: No. Received: Source Batch: 6 So 1 /46`l k,;" Condition of Organisms: Approximate Size or Age: GCOA 3 44r'of Shipper:B of L (Tracking No.) ' F,� FA 6�3a og3a ls`f6 Condition of Container: e�ow� Received By: 6I r Confirmation of ID of Organism: Technician Yes (Initials): �� Notes: ' D.O. Temp. Conductivity or p Salinity Technician (Units) VC) (mg/L) (include Units)(Initials) Notes: 1 NIEwPi>r> ps $i LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST WQ DATA SHEET City of Newport Marina Park Mytilus edulis (mussel) Port Gamble Incubator WELOSJOO WM P0.0JECTNJWAOEN TESTSTNtTO11TE TINE°,,� TEST ENOOIITE TWE 1105-005-560 Bil{Gardiner 67Jan09 jwV 09Jan09 - -- -' .._.. 2q?tiu`(�)-. �. of `"iFMPF7JAtiPE1•t76. ::_dui+'ylv`iq :_..Y .akiWtn)":::: �.c-si�ij�i: _��_: ?_ ,. ___- ._-_--zaxp:>1'0:��:•'--96.3'!":':�_°:'_'3'1'£2-:"-2�"--.�0'J_'1':-''':..^^--:��'.:;_3:_>,_:_. ...._�:; :, ;.�---. ,_ CUENT/NEWFlELOSIO rANCENTMTION MY ws OXYGEN TEMPMTME 311L1NTY qr AMMDtBA SOYldes Da4 Ted vNw wks meMt mpR eiehf Y Imeer ppt mMer untl TKIm. myL TKIm. rtglL i Control/ . 0 % 2 3 4 -S 0 if 1 3 �•S 3 t6.0 3 3S 3 i lg T� Site Water Control 1 0 % 2 3 �3 g t5-tom 3 �, 3 71.9 3 q p ff— flife, .r— Page 1 \\192.168.201.29\d ddve\Projects\Madna Park\Bioassay\Larval SPP test NEWFIELD5 LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST WO DATA SHEET City of Newport I Marina Park I I Mytilus edulis (mussel) I Part Gamble Incubator I Y:v.,YssAE+�^•R�^^'�'+ 1105-005-860 I Bill Gardiner I I 07Jan09 I I 09Jan09 yN' '�"..%:J�ti.G�':n-0�]�,�.C__ .. ii7:3��2es'.GS.. �-.Y..y. rt�ISw_'kC �^'^' Yc.Fn.^•+RA �. �t `e v.,Aa.:.��fu. sxi.ix..c� .i..' u�`+n'�'Snsd it YaS..-�u`".,YY. Ir'.•.�� a'Y..=�.'-�•'a ;c ti Teat cordions g:� �, 4�^:•�... - �s`;�AQ..z_� µ -18�>>,...._,,..n.^ cam; �:8f°• i"`.::-.: ._�.z.�,�.. ' K._. ;,�' _ e+_._ a N• -P '2•r.. =.v ..�.�- �.� - �.�-,... •,:"` n_:,,..�=:.t-„-._:.ix:�su CONCENTRATION DISS.OXYGEN TEMPERATURE SALINITY pH AMMONIA SYID6¢s Date Tech CIJ IKE IEDSID ViIYO YIIUd DAY IININ Y191L RINtt I °C IY[4t ppt IIINIf VnH TGChM1 1Y9IL TK11R 11191E 1 3 a.z 3 3 32 3 .q CompC-Ui. I% 2 3 �3.3 3 ... .C� .l...l` 3 4 °. .... `�...... _1.. l4� 32 o 1 3 �.2 3 I5•q . ........!.fig._._.._ ................... Camp C-U / . 10 % 2 3 a . j 3 15. -3 33 3 & o _ .19 _�_._ 3 4 _......_'f_._. _ 'f_ rA-.5_____1........_..._._....._.� _.......... ._. ._!��1_�i..._._ _�...._. 1 4-3 3 15_�l _3 3`�.._........3 ... -4.1 _........_ . _._._._. _ �.l_�_._._... ...... ........ Comp C-U 1. 50 % 2 -- 3— - . 3.._ ...« �_....3.... _' ._._ .._3._.. 8 ° _.... . _.._......... ... ... ........ _.. �._...... ....... !............. _. 3 ' 4 (D r e.- i /.* 16 f V4- Page 2 W 92.168201.291d drive\Projects\Marina Park0oassaylLarval SPP test NEWFIELDS City of Newport Marina Park VEVIFl SJMWMMR PROJE"MANAGER 1105-005-860 Bill Gardiner LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST WO DATA SHEET Mytilus edulis (mussel) ;TWARTMM 07Jan09 0609.01 Port Gamble Incubator 09Jan09 na -arri : tea"°'• ' - _ _ z _" CLIENn NEVM1lEL0510 CONCENiRATON vLw - enls my Me6 0XY0EA ;T. rmv% TEMPMUT meftt -C SRl1MfY me'ar PK PH maYr uW A Mm _ 5_uMEn Daft Tech. ebl TZZ MK T� h S 3 Comp GU 1. 100 % z 3 1�.9 l5 3 3� 3 g• a ;" '`, 11 3 ir/-r'ia Page 3 N1192.168.201.291d driveTrojects\Marina Park0oassaylLarval SPP test M ��NFzEz D5 RVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST Ew _ WQ DATA SHEET City of Newport 1105-005-860 Marina Park Bill Gardiner Mytilus edulis (mussel) 07Jan09 Port Gamble Incubator IUSEPDNSPCEI54l. I.IRim 09Jan09 na M c:i"^ _ ^'"-...'v4,�: e.. x.. _-_ .i ^c ��A�.o i,.t�). P,uaa:,_ �.. :�.-...•�G� : - r.�-A», ac..�..-y...:.,a''.v � w..:.•..c�..�, >.c :.a:..... ..✓.,-'T., �•e-; ,y q..c.-'r""tT24t`COIIU0Ji5w. �,1 .. �,:..¢ ��. ...: .r' ,..• - �vr_n.aj,',M,T!�.:�_•�.-,yam ��.;i'>^:^{ a`r>:�.... `.^: '; "'>i'.,'s .r. 5ax 3"Eic .v+ ... {. :wr.._av r...:..r'_�•r�.nrc^_v: ^xi�•ecz�.A �Cr�..•"•;^"A�`4`�'�'7� rr "'^•"R`Obi•^ln.� ';;=?� -. c•-i.�n.:;r.. .-c ,�n. T- 01 Page 4 i1192.168.201.29\d drive\Projects\Marina Park\Bioassaylarval SPP test City of Newport 1105-005-860 Marina Park Bill Gardiner LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST WQ DATA SHEET Mytilus edulis (mussel) 07Jan09 WATER QUALITY DATA — — — — — — — - — - Port Gamble Incubator 09JanO9 CUENn NEWP1EtD510 Wm mks MY -MK M URIC Pi PH exkr mM mu Teets MOL TW. vv& 0 -�Z)q 3 16.1 3 35 3 :q-9 CompG-L1- 100% 2 3 -3 -3 3 Q,. 0 /W 4 M M M M M Page 5 11192,168.201.291d ddvekProjectsNlVlarina ParkSioassayNLarval SPP test ' �Iwt 6 Page of ample'ID or' Description Cone. or Rep Date of Sampling and Initials Ammonia Value' (m L ' ' Temp o C Date of Reading and ' Initials Sample Preserved (YIN pH' Sad (ppt) Sulf. . .mg7li IA rTK - i . (... 1 � �• owl Mwt G-o . � to L�•S 5o L0.S to 5o �0.5 co.S t1.C.1 �O.S �a. 5 5� 4- o S (cst� La. S coo I \\192.I68.201.29\D Drive\Projects\DIOASSAY FILES\Lab Logs & Forms\Ammonia Analysis Record.doc Last printed 1/2/2009 12:09:00 PM BIVALVE LARVAL DEVELOPMENTAL SUSPENDED FARTICULATE PHASE ENDPOINT DATA SHEET SPECIES -- ...._.. Mytilus edulis (mussel) USEPCLIENT PROJECT NEWYMELDS JOB NO PROJECT MANAGER NEWPIELOS LABORATORY PROTOCOL City 0f Newport Marina Park 1105-005-860 Bill Gardiner Port Gamble Incubator 098. R ISACE 10SB R IonA I 1 i i 1 J / � 1 Page 1 1 BIVALVE LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE ENDPOINT DATA SHEET 1 r NEWFII IDS SPECIES .... i Mytilus edulis (mussel) CLIENT PROJECT NEWFIELDS JOB NUA PROJECT MANAGER NEWFIELDS LABORATORY PROTOCOL USEPPNSACE City of Newport Marina Park 1105-005-860 Bill Gardiner Port Gamble Incubator 1998 Region 4 LARVAL OBSERVATIONDATA CONCENTRATION VIAL NUMBER REP NUMBER NUMBER DATE TECHNICIAN COMMENTS CLIENT/NEWFIELDS ID raluo unUs NORMAL ABNORMAL 1 Zal,� Igo ll zy(.a.......... 1... ............... 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Mytilus edulis (mussel) CLIENT 1PROJECT NEWFIUSEP M IELDS JOB NU PROJECT MANAGER NEWFIELDS LABORATORY PROTOCOL City Ol Newport Marina Park 1105-005-860 Bill Gardiner Port Gamble Incubator , RUSACE BSB R#ion4 CLIENT/NEWFIELDS ID CONCENTRATION yIALNUMBER REP NUMBER NORMAL NUMBER ABNORMAL DATE TECHNICIAN COMMENTS VAIU°, units 1,.. 2$» ».............. lP.. ....... ?..?.6... ................................ ».�J.........., ........ .................. ....... I .......... ......... Como C-L1. 1 % .................. 3 .., ......,... ,... -% ....!.......................... ..... ....... _...... I ... ......... a.. v, ..».. »I»..»..1---......., ..... «..... ........ ..»...........»..»..... » S 27� ,.S 2S.... ..,........w» .....«................. .2... ......... »t........ ................... » ... .»..........».... CompC•L /. 10 % .............,. ..... L `.... ........».......... ..... ......................... ....................«... .....» `//////� .....1. Iu.... 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Z...c. .... ....... «4»»,. .... ....... ... .».».., ....... ». ........ .... ».., .,.. »..,» ...........I.... s 710 5S Vil .........».S. »................... .2». ....�......g© ... ..«.....«. ........... .....»y.....»y .»« Como C•L1. 100 % 3 Z l �S Q ........... ................... ............... ....................... ?..�.....,� ............... ........ ...... »........... .«............. -------------- ... ------- »....,.....,........... ».................»,.. »a.. 5 1% »» ......... s .. ..... «»... ..._............. «........ cowl— W1'-1140�/r,)�,q @w(0z jakk � I4�"l W t Page 3 CETIS QC Chart Page 1 of 1 Report Date: 26 Jan-09 1:05 PM ' Mussel Shell Development Test NewFields Test Type: Development -Survival Organism: Mytilus species (Mussel) Material: Copper sulfate Protocol: EPA/600/R-95/136 (1995) Endpoint: Combined Proportion Normal Source: Reference Toxicant -REF ' 2 1 1 ....................... ... ...... ........ ...... ... ................ .... ... ................................. / ........... ........ .......... ----...-......-.-............. 5 ......................................................... ......-.........--........--......-. 04 0 0 > n ' M fn Mean: 8.05554 Count: 12 -1s Warning Limit: 5.38297 .2s Action Limit: 3.59707 Sigma: CV: 49.65% +1s Warning Limit: 12.0550 +2s Action Limit: 18.0402 ' Quality Control Data Year Month Day Data Delta Sigma Warning Action Test Link Analysis tPoint - —.--..... -— 1 2006 Jan 31-- -- --- 6.61806 -1.43748 --O-- -A8759 ---- — _ . -- _ 13-7720-1086 09-0953-9971 2 31 7.27814 -0.77740 .0.25175 07-7532-7374 03-9619.0590 3 Feb 21 15.39971 7.34417 1.60743 (+) 134991-4803 05.4083.6897 4 Mar 14 7.14387 -0.91168 .0.29794 1.40433 06.2606-4386 04-5028-3346 01-1874-9985 02-3972-6078 5 14 14.18912 6.13368 (+) 6 2007 Jan 10 4.98039 -3.07616 -1.19283 (-) 14-3905.009D 14-8759.6838 7 Jun 5 7.58039 -0.47515 -0.16081 13-7829-6492 02-0555-4940 8 26 8.51244 0.45690 0.13685 01-3435-1614 10-7297-9264 9 Jul 2 11,50108 3.44554 0.88331 054911-0140 15-1586-2946 10 Nov 14 3.68371 4.37184 -1.94096 (-) 15-3555-749315-2027-0867 11 2008 Feb 22 8.50255 0.44700 0.13397 06-6162-8975 04.4740.6893 13-1167-6043 12 Oct 22 8.57836 0.52281 0.15599 13-5164-0440 13 2009 Jan 7 9,69234 1.63680 0.45886 10-8012-7714 12-5942-1542 ' 000-173-102-3 CETIS'm v1.1.2revG Analyst: Approval: CETIS Analvsis Detail Comparisons: Pagel of 1 Report Data: 26 Jan-091:04 PM Analysis: 06.3783.7788 Mussel Shell Development Test NewFields Endpoint Analysis Type Sample Link Control Link Date Analyzed Version Combined Proportion Normal Comparison 10.8012-7714 10.8012-7714 26 Jan-091:04 PM CETISv1.1.2 Method Alt H Data Transform Zeta NOEL LOEL Toxic Units ChV PMSD Dunnell's Multiple Comparison C > T Angular (Corrected) Is 10 20 7.07107 8.11% Group Comparisons Control vs Conc-pglL Statistic Critical P-Valuo MSD Decision(0.05) Dilution Water 2.5 -2.2604 2.41651 0.9970 0,14073 Non -Significant Effect 5 -0.1888 2.41661 0.8114 0.14073 Non-SlgnificantEffect 10 10.1928 2.41651 0.0000 0.14073 Significant Effect Test Acceptability Attribute Statistic TAC Range Overlap Decision PMSD 0.08106 NL-0.25 No Passes acceptability criteria ANOVA Table Source Sum of Squares Mean Square OF F Statistic P-Value Declslon(0.05) Between 0.9569461 0,318982 3 62.70 0.00001 Significant Effect Error 0.0407007 0,0050876 8 Total 0.99764680 0,3240696 11 ANOVA Assumptions Attribute Test Statistic Critical P-Value Declelon(0.01) Variances Bartlett OA0782 11.34487 0.93862 Equal Variances Distribution Shapiro.WIIk W 0.94237 0,52940 Normal Distribution Data Summary Original Data Transformed Data Conc-pglL Control Type Count Moan Minimum Maximum SD Mean Minimum Maximum SD 0 Dilution Water 3 0.93950 0.89547 0.97879 0.04186 1.33288 1,24157 1.42463 0.09153 2.5 3 0.98811 0.97690 1.00000 0.01224 1.48452 1.41821 1.54128 0.06694 5 3 0.94733 0,91638 0,96743 0.02720 1.34387 1.27743 1.38932 0.05883 10 3 0.45412 OA0767 0.62613 0.06323 0.73927 0.69263 0.81154 0.06348 Data Detail Cone-pglL Control Type Rep 1 Rep 2 Rep 3 Rap 4 Rap 5 Rap 6 Rep 7 Rep 8 Rep 9 Rep 10 0 Dilution Water 0.89547 0.97879 0.94425 2.5 1.00000 0.98142 0.97690 5 0.96743 0.95619 0.91638 10 0.42857 OA0767 0.52613 Graphics aoe• oa "Vr o.os o.a Ob 0.03• R0. 0.00 ..........................•.................._._....... Ok os -0.04 0.2 •0.06• 0.11 •aoe OA -0,10• o is s m a.o ns 4.0 •as 00 os I,o Is ao Conc•ppJl Rankits 000-173.102.3 CETISU vl.1.2ravG Analyst: Approval: CETIS Analvsis Detail Spearman-Karber: Page 1 of 1 Report Date: 26 Jan-09 1:04 PM Analysis: 12-5942-1542 ' Mussel Shell Development Test NewFields Endpoint Analysis Type Sample Link Control Link Date Analyzed Version Combined Proportion Normal Trimmed Spearman-Karber 10-8012-7714 10-8012-7714 26 Jan-09 1:04 PM CETISV1.1.2 Spearman-Karber Options Point Estimates Option Lower Threshold Trim Mu Sigma EC601LC50 95% LCL 96% UCL 'Threshold Control Threshold 0.05862832 0.00% 0.9864286 0.005280371 9.69234 9.45950 9.93092 Data Summary Calculated Variate(AIS) Control Type Count Mean Minimum Maximum SE SO A 8 'Conc-pgfL 0 Dilution Water 3 0.93950 0.89547 0.97879 0,00854 0.04186 851 904 2.5 3 0.98611 0.97690 1.00000 0.00250 0.01224 900 913 3 0.94733 0.91638 0.96743 0.00555 0.02720 835 881 '6 10 3 0.45412 0.40767 0.52613 0.01291 0.06323 391 0 861 861 20 3 0.00000 0.00000 0.00000 0.00000 0.00000 40 3 0.00000 0.00000 0.00000 0.00000 0.00000 0 861 ' Graphics 1.07 6. 09 g O.B, £ 0.7 ' 0. g U.9 8 0.9; a ' 3 0.7• 02, ' 0. 00 0 10 20 70 40 50 C0nc40/� I I I 1 000-173-102-3 CETIS- v1.1.2revG Analyst: Approval: CETIS Data Worksheet Page 1 of 1 Report Date: 26 Jan-091:05 PM Link: 10-8012.7714 Mussel Shell Development Test NewFlelds Start Date: 07 Jan-09 06:00 PM Species: MytildS species Sample Code: 1512131168 Ending Date: 09 Jan-0906:00 PM Protocol: EPA/600/R-95/136 (1995) Sample Source: Reference Toxicant Sample Date: 07 Jan-09 06:00 PM Material: Copper adlfale Sample Station: P070930.96 Conc-pgiL Code Rep Pos I Initial Density Final Density # Counted 8 Normal Notes 0 D 1 -TS-1 287 264 _ -284_ 0 D 2 9 1 207 330 330 323 0 D 3 2 287 275 275 271 2.5 1 4 287 292 292 287 -- 2.5 i 2 13 287 T 323 323 --� 317 �2S-- 3 7 287 303 303 W� 298 5 1 16 287 T-307 307 297 T 5 _ 2 1 18 287 284 284 275 5 3 12 207 273 273 263 10 1 10 207 278 278 123 10 2 6 287 311 311 "1 10 3 11 287 285 285 161 20 1 14 287 298 298 0 20 2 17 287 265 255 0 201 3 8 287 1 295 295 40 1 1 287 25 25 _0 .� 0� 40 2 5 267 31 31 0 40 1 3 3 287 27 27 0 000-173-1023 CETIS'm vl.1.2revG Analyst: Reviewed By: NEWPIELDS gWLOWNTMUSUWECWTI%j*TEd*SE&fiT COPPER REFERENCE TOXICANT WO City of Newport Marina Park Mytilus edulis (mussel) Incubator WEP�lmg.4.4RW IM NEWFIELOS JOB NUMBER 1105-005-860 PROJECT MANAGER Port Gamble QUANTITY OF STOCK TARGET: 0.039 mt. QUANTITY OF DILUENT_ SODmL INIT ACTUAL: o-03'i 7—L( n.cL- ACTUAL: DATEPREP Test ID �07 9 LOT #. 4 tjZ TEST START DATE: 07Jan09 TIME I60D TEST END DATE 1 09Jan09 TIME 11'200 WATER QUALITY DATA ^' C• `y� S`h ffRi ;teas r�v:y3,_"y q y'xay �� r.+.yYG„T.- s� 0 0 fl`Y S`^•--'�''^ �."'�•1l�' < . xa< i ..�. wt-. ✓" ,fs `"' '��'w _. � "� . Y 'SG.... � )"�+' � is �iw� .� �a , v y,- . y-�. �`ja, e' � ^t 8 � •��Y�'�' T $ ..-. .nit ,s. _.:- ', ,.. �, z...r�,�,.c.�., r.:.: �__,^Y..n.:dz.;,.F%-��.'L.:.,.:�.'ce Pw.��.'�`.n.,,. �',"��^�..-..,:v„E,s,,,s:y.^�..,.�5� '-�..aa'.��.: •.....,�� .;;.� •--zWy,. mmffl �© - - . ...CLIENT/ NEWFIELDS ID I PV4@21168.201.29\d drive\Projects\Marina Park\Bioassay\Larval SPP test RVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST I�LD S COPPER REFERENCE TOXICANT WO CLIENT City of Newport PROJECT Marina Park SPECIES Mytilus edulis {musseq NEWFIELDS LABORATORY Incubator PROTOCOL MZPAN EIM R gb 4M IM NEWFIELDS JOB NUMBER 1105-005-860 PROJECT MANAGER Port Gamble QUANTIT'OFSTOCKTARGET:OA39mL QUANTITY OFDILUENT- SOOmL INrr ACTUAL: ACTUAL' DATE PREP Test ID LOTIP TEST START DATE 07Jan09 TIME j� 10 TEST END DATE 1 09Jan09 TIME WATER QUALITY DATA DILTIN.WAT.BATCH TEMP RECN REFERENCE TOX MATERIAL REFERENCE TOXXICANT FSW010609.01 "a CopperSuHate copper CLIENT/ NEWFIEU)StD CONCENTRATION DAY REP D.O. TEMP. SALINITY"PIWO TECHmglL mwr `C �r Ppt Ref.Tox: Copper 10 mg/L 0 Stock $ (� i . ( l ga \ $ i H 7 Stock 3 �_ 1 J9 Ito. & 3 2 J _y> 2 Stock 3 �. i v7 i� 3 32 ?J $ 3 Stock 4 Stock Reffox: Copper 20 mg/L 0 -Stock v, 6.0 2 1 Stock 2 Stock 3 S 110 •.`f 3 2 3 Stock 4 Stock Ref.Tox.-Copper 40 mg/L 0 Stock 1 Stock 3 -4-1 tt,.S 3 32 -8 2 Stock 3 Stock 4 Stock _, S �, I♦ �, )r WWa1 jW1.Wnv=jec=nna arklBiayl6WI SPP test — LARVAL DEVELOPMENTAL SUSPENDED PARTICULATE PHASE TEST COPPER REFERENCE TOXICANT ENDPOINT DATA SHEET ' NEWFIELDS �D Qg3p,�lb SPECIES Mytilus edulis (mussel) CLIENT 1PROJECT NEWFIELOS JOB NIJPROJECT MANAGER NEWFIELD3 LABORATORY PROTOCOL USEPA/USAGE City of Newport Marina Park iao5-oo5-e60 Bill Gardiner I Port Gamble Incubator 1998, Region CLIENTIMEC ID CONCENTRATION VIAL NUMBER REP NUMBER NORMAL I NUMBER ABNORMAL DATE TECHNICIAN COMMENTS value I UnIts z.fS3.........2......... Ref.TOR.-Copper 0 µg/L ....... 2 123 % ..........(4 ....................................... 3.. .�...... ..... .... ............... ........ z$7. ... .... .................... ........ . Ref.TOX.-copper 2.5 µg/L ............ ... .....ram .......... .... ........... .2 3 2 5 µg/L 2 ...Ref.TOX.-Copper I.S 3 Z63 ........... .................... ........... ............ ................................ Ref.TOX.-Copper 10 µg/L .......................1„23..........`...... 2 a.................................................. ........... ................ I ............ ... ................................. , ....... 3 ............ �sl �13N Z ..18. .... .I......... ..... ... .............. I............. Ref.Tox.-Copper 20 µg/L ..................... * ..I.... 2 ....b....... T% 3 (� Z ...... �.. Q........ .2 s..... ........ ......t ... .... ........................ Ref.TOX.-Copper 40 µg/L 2 '0 3 .... ....... ........................ ...3.. ....0..... ...D.... Z 7.. .. .... l.�Z�.....g..... ... . ..... ........ ............ .... Ref.Tox.-Copper Stocking Density .'...........................z,s..... 2 3 IPage 1 PAMarina Park\Bioassay\Larval SPP test 11 I "N ORGANISM RECEIPT LOG Date: lob Time: 1 � 3 o NewFlelds Batch No. -31a Organism: �^ !- 1 S� • Source: A Cwis ��J � r�s Address: al Invoice Attached No Phone: v� F. Contact: �dti, [/�kv[45 No. Ordered: i I),�(.� No. Received: , bJc Source Batch• r:,I� Condition of Organisms: cl Approximatee or Age: ✓ I + Shipper: r-P jrx B of L (Tracking No.) 17%? c?, % 3) a l Condition of Container, Received By: � Confirmation of ID of Organism: Year Technictn (Initials): Notes: pH (Units) Temp. (°C) D.O. (mg/L) Conductivity or Salinity include Units Technician (initials) Notes: h� it 11 11 11 J I I Appendix E Bioaccumulation Tests Data Sheets and Supporting Information I I I I I, r i I II I I . ..ems .. ...... n ..yN nn...... . .. .....� ...u. .. �` 1.... _..utti.tii.+.avuu..—..vru...v.w... ... ff.... � � s ' ANALYTICAL LIPIDS Percent ANALYSIS DATA SHEET Lipids by Method Bligh&Dyer RESOURCES( INCORPORATED Data Release Authorized: Reported: 01/22/09 1�/�Y% Date Received: 01/16/09 QC Report No: 0173-Newfields Northwest Project: Marina Park Page 1 of 2 Client/ ARI ID Date Sampled Matrix Analysis Date RL Result Mn ZERO TIME 0173A 09-1988 12/16/08 Tissue 01/20/09 0.0010 0.480 Mn ZERO TIME REP.2 12/16/08 Tissue 01/20/09 0.0010 0.449 & 0I73B 09-1989 Mn ZERO TIME REP-3 12/16/08 Tissue 01/20/09 0.0010 0.450 0173C 09-1990 NC BACKGROUND 12/19/08 Tissue 01/20/09 0.0010 0.819 0173D 09-1991 Mn LA-3 REF. REP-1 01/14/09 Tissue 01/20/09 0.0010 0.369 % 0273E 09-1992 Mn LA-3 REF. REP.2 01/14/09 Tissue 01/20/09 0.0010 0.398 0I73F 09-1993 Mn LA-3 REF. REP-3 01/14/09 Tissue 01/20/09 0.0010 0.339 % 0173G 09-1994 Mn LA-3 REF. REP-4 01/14/09 Tissue 01/20/09 0.0010 0.339 _ 0173H 09-1995 Mn LA-3 REF. REP-5 01/14/09 Tissue 01/20/09 0.0010 0.369 & 01731 09-1996 Mn COMP.C.L REP-1 0173J 09-1997 01/14/09 Tissue 01/20/09 0.0010 0.400 Mn COMP.C.L REP.2 01/14/09 Tissue 01/20/09 0.0010 0.350 & 0173K 09-1998 Mn COMP.C.L REP-3 01/14/09 Tissue 01/20/09 0.0010 0.380 0173L 09-1999 Mn COMP.C.L REP-4 01/14/09 Tissue 01/20/09 0.0010 0.429 t 0173M 09-2000 Mn COMP.C.L REP.5 01/14/09 Tissue 01/20/09 0.0010 0.459 0173N 09-2001 'Mn COMP.C.0 REP.1 01730 09-2002 , 01/14/09 Tissue 01/20/09 '0.0010 0.320 & Report for 0I73 ' ANALYTICAL LIPIDS ANALYSIS DATA SHEET Percent Lipids by Method Bligh&Dyer RESOURCES® INCORPORATED - Data Release Authorized:///+>' QC Report No: OI73-Newfields Northwest Reported: 01/22/09 j'/" Project: Date Received: 01/16/09 Marina Park Page 2 of 2 Client/ Date Analysis ARI ID Sampled Matrix Date RL Result ' , Mn COMP.C.0 REP.2 01/14/09 Tissue 01/20/09 0.0010 0.328 OI73P 09-2003 Mn COMP.C.0 REP.3 01/14/09 Tissue 01/20/09 0.0010 0.390 t 0173Q 09-2004 0.410 & , Mn COMP.C.0 REP.4 01/14/09 Tissue 01/20/09 0.0010 0I73R 09-2005 Mn COMP.C.0 REPS 01/14/09 Tissue 01/20/09 0.0010 0.408 t OI73S 09-2006 NC LA-3 REF. REP.1 01/14/09 Tissue 01/20/09 0.0010 0.759 OI73T 09-2007 Method Blank 01/20/09 0.0010 < 0.0010 W U Mn LA-3 REP. REP.4 DUP 01/24/09 Tissue 01/20/09 0.0010 0.279 % 01731IDUP 09-1995 RPD: 19.4 t Results Are On A Wet Weight Basis RL-Analytical reporting limit U-Undetected at reported detection limit ; i I 11 Report for 0173 ' ANALYTICAL LIPIDS ANALYSIS DATA SHEET RESOURCES Percent Lipids by Method Sligh&Dyer INCORPORATED Data Release Authorized: QC Report No: 0177-Newfields Northwest Reported: 01/22/09 Project: MARINA PARK Date Received: 01/16/09 Page 1 of 2 Client/ Date Analysis ARI ID Sampled Matrix Date RL Result NC LA.3 DEF REP.2 01/14/09 Tissue 01/20/09 0.0020 0.876 % 0177A 09-2015 NC LA.3 DEF REP.3 01/14/09 Tissue 01/20/09 0.0020 0.873 0177B 09-2016 0.911 NC LA.3 DEF REP.4 01/14/09 Tissue 01/20/09 0.0020 0177C 09-2017 rNC LA.3 DEF REP.5 01/14/09 Tissue 01/20/09 0.0020 0.857 % 0177D 09-2018 NC COMP.C.L REP.1 01/14/09 Tissue 01/20/09 0.0020 0.812 0I77E 09-2019 NC COMP.C.L REP.2 01/14/09 Tissue 01/20/09 0.0020 0.893 0177F 09-2020 NC COMP.C.L REP.3 01/14/09 Tissue 01/20/09 0.0020 0.940 & 0177G 09-2021 NC COMP.C.L REP.4 01/14/09 Tissue 01/20/09 0.0020 0.898 0177H 09-2022 NC COMP.C.L REP.5 01/14/09 Tissue 01/20/09 0.0020 0.871 0177I 09-2023 NC COMP.C.0 REP.1 01/14/09 Tissue 01/20/09 0.0020 0.972 0177J 09-2024 NC COMP.C.0 REP.2 01/14/09 Tissue 01/20/09 0.0020 0.812 09-2025 r0177K NC COMp.C.0 REP.3 01/14/09 Tissue 01/20/09 0.0020 0.900 W 0177L 09-2026. NC COMP.C.0 REP.4 01/14/09 Tissue 01/20/09 0.0020 0.838 W 0I77M 09-2027 r r- Report for 0I77 ANALYTICAL LIPIDS ANALYSIS DATA SHEET RESOURCES Percent Lipids by Method Bligh&Dyer INCORPORATED Data Release Authorized: .100 QC Report No: 0I77-Newfields Northwest Reported: 01/22/09 Project: MARINA PARK Date Received: 01/16/09 Page 2 of 2 Client/ Date Analysis ARI ID Sampled Matrix Date RL Result NC COMP.C.0 REP.5 01/14/09 Tissue 01/20/09 0.0020 1.08 & 0177N 09-2028 Method Blank 01/20/09 0.0020 < 0.0020 W U NC COMP.C.L REP.4 DUP 01/14/09 Tissue 01/20/09 0.0020 0.931 % 0I77HDUP 09-2022 RPD: 3.6 t Results Are On A Wet Weight Basis RL-Analytical reporting limit U-Undetected at reported detection limit Report for 0177 I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: C LIMS ID: 09-1988 Matrix: Tissue Data Release Aut Reported: 01/23/ Prep Prep Meth Date CLP-M 01/20/( U-Analyte undet RL-Reporting Lim II ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn ZERO TIME SAMPLE M, nT7'i-M.WfiP1HA Nnrthwest ANALYTICAL ' RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn ZERO TIME REP.2 Page 1 of 1 SAMPLE Lab Sample ID: OI73B QC Report No: 0I73-Newfields Northwest LIMS ID: 09-1989 Project: Marina Park Matrix: Tissue Data Release Authorized: ��_y Date Sampled: 12/16/08 Reported: 01/23/09 \III Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7939-97-6 Mercury 0.01 0.01 U U-Analyte undetected at given RL RL-Reporting Limit ° t t t 1 . i FORM -I ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn ZERO TIME REP-3 Page 1 of 1 SAMPLE Lab Sample ID: 0I73C QC Report No: 0173-Newfields Northwest LIMS ID: 09-1990 Project: Marina Park Matrix: Tissue Authorized Date Sampled: 12/16/08 Data Release Reported: 01/23/09 Date Received: 01/16/09 Analysis Analysis Prep Prep Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.009 U undetected at given RL 'U-Analyte RL-Reporting Limit I 11 I FORM -I INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: O173D LIMS ID: 09-1991 Matrix: Tissue Data Release Authorize Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: NC BACKGROUND SAMPLE QC Report No: OI73-Newfields Northwest Project: Marina Park Date Sampled: 12/19/08 Date Received: 01/16/09 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.010 U-Analyte undetected at given RL RL-Reporting Limit FORM -I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn LA-3 REF. REP.1 'Page 1 of 1 SAMPLE Lab Sample ID: 0273E QC Report No: 0I73-Newfields Northwest LIMS ID: 09-1992 Project: Marina Park Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte ' CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 'U-Analyte undetected at given RL RL-Reporting Limit 1 ' FORM -I RL mg/kg-as-rec Q 0.01 0.01 U ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn LA-3 REF. REP.2 Page 1 of 1 SAMPLE Lab Sample ID: OI73F QC Report No: 0173-Newfields Northwest LIMS ID: 09-1993 Project: Marina Park Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Math Date Method Date CAS Number Analyte CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit RL mg/kg-as-rec Q 0.009 0.009 U FORM -I ' ANALYTICAL RESOURCES O INCORPORATED ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn LA-3 REF. REP.3 1 of 1 SAMPLE 'Page Lab Sample ID: 0173G QC Report No: OI73-Newfields Northwest LIMS ID: 09-1994 Project: Marina Park 'Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte ' CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit FORM -I RL mg/kg-as-rec Q 0.009 0.009 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0173H LINS ID: 09-1995 Matrix: Tissue Data Release Authorized: / Reported: 01/23/09 �`Yp✓ ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn LA-3 REF. REP.9 SAMPLE QC Report No: OI73-Newfields Northwest Project: Marina Park Date Sampled; 01/14/09 Date Received: 01/16/09 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.01 0.01 U U-Analyte undetected at given RL RL-Reporting Limit FORM -I 1 ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS ' Page 1 of 1 Lab Sample ID: 0173I LIMS ID: 09-1996 Matrix: Tissue Data Release Authorized Reported: 01/23/09 ' Prep Prep Meth Date CLP-M 01/2C 'O-Analyte and RL-Reporting L ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn LA-3 REF. REP.5 SAMPLE QC Report No: 0I73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 Date Received: 01/16/09 Analysis Analysis Method Date CAS Number Analyte RL mg/kg-as-rec Q INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0I73J LIMS ID: 09-1997 Matrix: Tissue Data Release Authorized: Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn COMP.C.L REP.l SAMPLE QC Report No: OI73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M O1/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.009 U U-Analyte undetected at given RL RL-Reporting Limit FORM-1 ' ANALYTICAL I/�' ' RESOURCES �/ INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.L REP-2 'Page 1 of 1 SAMPLE Lab Sample ID: 0173K QC Report No: 0173-Newfields Northwest LIMS ID: 09-1998 Project: Marina Park 'Matrix: Tissue Data Release Authorize Date Sampled: 01/14/09 Reported: 01/23/09 6V Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 'U-Analyte undetected at given RL RL-Reporting Limit FORM -I RL mg/kg-as-rec Q 0.009 0.009 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0I73L LIMS ID: 09-1999 Matrix: Tissue Data Release Authorized:) W ll/ Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn COMP.C.L REP.3 SAMPLE QC Report No: 0I73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Meth Prep Date Analysis Method Analysis Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M '01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.01 0.01 U U-Analyte undetected at given RL RL-Reporting Limit FORM-1 ANALYTICAL RESOURCES O INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.L REP.4 'Page 1 of 1 SAMPLE Lab Sample ID: 0I73M QC Report No: 0I73-Newfields Northwest LIMS ID: 09-2000 Project: Marina Park Matrix: Tissue Data Release Authorized: Reported: 01/23/09 Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte ' CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0-Analyte undetected at given RL ' RL-Reporting Limit FORM -I RL mg/kg-as-rec Q 0.009 0.009 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OI73N LIMS ID: 09-2001 Matrix: Tissue Data Release Authorized: Reported: 01/23/09 61 ANALYTICAL 1 RESOURCES O 1 INCORPORATED Sample ID: Mn COMP.C.L REPS SAMPLE 1 QC Report No: OI73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 1 Date Received: 01/16/09 1 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-�97-6 Mercury 0.01 0.01 U 1 U-Analyte undetected at given RL 1 ' RL-Reporting Limit 1� i l 1 1� 1 1 1' 1 1 1 �• FORM -I 1 .. ... - .....s..___._i ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS ' Page 1 of 1 Lab Sample ID: 01730 LIMS ID: 09-2002 Matrix: Tissue (�,� Data Release AuthorizecA�*jr/ Reported: 01/23/09 �U Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte ' CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 'U-Analyte undetected at given RL RL-Reporting Limit 11 IF ANALYTICAL L RESOURCES INCORPORATED Sample ID: Mn COMP.C.0 REP-1 SAMPLE QC Report No: 0I73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 Date Received: 01/16/09 RL mg/kg-as-rec Q 0.009 0.011 FORM -I ANALYTICAL RESOURCES INCORPORATED ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.0 REP.1 Page 1 of 1 DUPLICATE , Lab Sample ID: 01730 QC Report No: OI73-Newfields Northwest LIMS ID: 09-2002 Project: Marina Park Matrix: Tissue Data Release Authorized: Date Sampled; 01/14/09 , Reported: 01/23/09 Date Received: 01/16/09 MATRIX DUPLICATE QUALITY CONTROL REPORT ' Analysis Control , Analyte Method Sample Duplicate RPD Limit Q Mercury 7471A 0.011 0.011 0.0% +/- 0.009 L Reported in mg/kg-as-rec *-Control Limit Not Met ' L-RPD Invalid, Limit Detection Limit i i t f i i j i I. FORM -VI ' I ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0I730 LIMS ID: 09-2002 'Matrix; Tissue Data Release Authorized Reported: 01/23/09 Analyte ANALYTICAL RESOURCES INCORPORATED Sample ID: Mn COMP.C.0 REP-1 MATRIX SPIKE QC Report No: 0I73-Newfields Northwest Project: Marina Park Date Sampled: 01/14/09 Date Received: 01/16/09 MATRIX SPIKE QUALITY CONTROL REPORT Analysis Method Sample Spike % Spike Added Recovery ' Mercury 7471A 0.011 0.100 0.0931 Reported in mg/kg-as-rec N-Control Limit Not Met H-% Recovery Not Applicable, Sample Concentration Too High NA -Not Applicable, Analyte Not Spiked Percent Recovery Limits: 75-125% II II Ul II II II 95.6% N ' FORM-V ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.0 REP.2 Page 1 of 1 SAMPLE Lab Sample ID: 0173P QC Report No: 0I73-Newfields Northwest LIMS ID: 09-2003 Project: Marina Park Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit RL mg/kg-as-rec Q 0.009 0.013 FORM -I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.0 REP.3 1 of 1 SAMPLE 'Page Lab Sample ID: 0173Q QC Report No: 0I73-Newfields Northwest LIMS ID: 09-2004 Project: Marina Park 'Matrix: Tissue Data Release Authorized Reported: 01/23/09 Date Sampled: 01/14/09 Date Received: 01/16/09 ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 'U-Analyte undetected at given RL RL-Reporting Limit FORM -I Mercury 0.009 0.011 , ANALYTICAL ® RESOURCES INCORPORATED , INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: Mn COMP.C.0 REP.4 Page 1 of 1 SAMPLE Lab Sample ID: OI73R QC Report NO: 0I73-Newfields Northwest LIMS ID: 09-2005 Project: Marina Park Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 , Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS' Number Analyte RL mg/kg-as-rec Q CLP-M O1/20/09 7471A O1/22/09 7439-97-6 Mercury 0.009 0.011 ' U-Analyte undetected at given RL RL-Reporting Limit 11 t 11 I 11 FORM -I ' ' ANALYTICAL RESOURCES O 'INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL. METALS Sample ID: Mn COMP.C.0 REP.5 Page 1 of 1 SAMPLE Lab Sample ID: 0173S QC Report No: 0I73-Newfields Northwest LIMS ID: 09-2006 Project: Marina Park 'Matrix: Tissue Data Release Authorized ` Date Sampled: 01/14/09 Re orted• 01/23/09 \jjlJ�/ Date Received: 01/16/09 r ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 'U-Analyte undetected at given RL RL-Reporting Limit .1 ' FORM -I Mercury 0.01 0.01 INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0173T LIMS ID: 09-2007 Matrix: Tissue Data Release Authorized: Reported: 01/23/09 ANALYTICAL ® , RESOURCES , INCORPORATED Sample ID: NC LA-3 REF. REP.1 SAMPLE QC Report No: 0173-Newfields Northwest Project! Marina Park Date Sampled: 01/14/09 t Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.01 0.01 U ' U-Analyte undetected at given RL RL-Reporting Limit i i FORM -I ' 1 ' INORGANICS ANALYSIS DATA SHEET TOTAL METALS 1 Page 1 of 1 Lab Sample ID: 0I73LCS LIMS ID: 09-1988 Matrix: Tissue Data Release Authorized�J�p/ Reported: 01/23/09 �VI ANALYTICAL RESOURCES INCORPORATED Sample ID: LAB CONTROL QC Report No: OI73-New£ields Northwest Project: Marina Park Date Sampled: NA Date Received: NA ' BLANK SPIKE QUALITY CONTROL REPORT Analysis Spike Spike % Analyte Method Found Added Recovery ' Mercury 7471A 0.21 Reported in mg/kg-wet 'N-Control limit not met NA -Not Applicable, Analyte Not Spiked Control Limits: 80-120% 1 1 ' FORM-VII 0.20 105% Q ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: METHOD BLANK Page 1 of 1 Lab Sample ID: 0I73MB QC Report No: 0173-Newfields Northwest LIMS ID: 09-1988 Project: Marina Park Matrix: Tissue Data Release Authorized:0/ Date Sampled: NA Reported: 01/23/09 Date Received; NA Percent Total Solids: NA Prep Prep Analysis Analysis Meth Date Method Data CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.01 0.01 U U-Analyte undetected at given RL RL-Reporting Limit io[►kiSo ANALYTICAL RESOURCESO ' INORGANICS ANALYSIS DATA SHEET INCORPORATED TOTAL METALS Sample ID: NC LA.3 DEF REP.2 iPage 1 of 1 SAMPLE Lab Sample ID: 0177A QC Report No: 0177-New£ields Northwest LIMS ID: 09-2015 Project: MARINA PARK Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 R orted• 01/23/09 Date Received: 01/16/09 Re ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec,Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 'U-Analyte undetected at given RL RL-Reporting Limit FORM -I Mercury 0.01 0.01 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0177A LIMS I'D: 09-2015 Matrix: Tissue Data Release Authorized: Reported: 01/23/09 Analysis ANALYTICAL RESOURCES INCORPORATED Sample ID: NC LA.3 DEF REP.2 DUPLICATE QC Report No: 0I77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 MATRIX DUPLICATE QUALITY CONTROL REPORT Analyte Method Sample Mercury 7471A 0.01 U Reported in mg/kg-as-rec *-Control Limit Not Met L-RPD Invalid, Limit = Detection Limit 0 Control Duplicate RPD Limit Q 0.01 U 0.0% t/- 0.01 L FORM -VI 1 ANALYTICAL RESOURCES INCORPORATED 1 INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC LA.3 DEF REP.2 Page 1 of 1 MATRIX SPIKE 1 Lab Sample ID: 0177A QC Report No: OI77-Newfields Northwest LIMS ID: 09-2015 Project: MARINA PARK 1 Matrix: Tissue Authorized: Date Sampled: 01/14/09 Data Release Reported: 01/23/09 Date Received: 01/16/09 1 MATRIX SPIKE QUALITY CONTROL REPORT 1 Analysis Spike % Q Analyte Method Sample Spike Added Recovery 1 Mercury 7471A 0.010 U 0.101 0.0950 106% Reported in mg/kg-as-rec 1 N-Control Limit Not Met H-% Recovery Not Applicable, Sample Concentration Too High NA -Not Applicable, Analyte Not Spiked 1 Percent Recovery Limits: 75-125% 1 i • 1 1 i 1 1 i i FORM-V INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0177B LIMS ID: 09-2016 Matrix: Tissue Data Release Authorized Reported: 01/23/09 ' ANALYTICAL O RESOURCES INCORPORATED 1 Sample ID: NC LA.3 DEF REP.3 SAMPLE QC Report No: OI77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 1 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 1439-97-6 Mercury 0.01 0.01 U U-Analyte undetected at given RL ' RL-Reporting Limit 11 1� 1j s 1 1 t{ 1 1 FORM -I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC LA.3 DEF REP.4 Page 1 of 1 SAMPLE Lab Sample ID: OI77C QC Report No: 0I77-Newfields Northwest LIMS ID: 09-2017 Project: MARINA PARK 'Matrix: Tissue Data Release Authorize q'"��yDate Sampled: 01/14/09 Reported: 01/23/09 ,( h Date Received: 01/16/09 ' Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte CLP-M 01/20/09 7471A 01/22/09 7439-97-6 U-Analyte undetected at given RL ' RL-Reporting Limit FORM -I RL mg/kg-as-rec Q Mercury 0.01 0.01 U ANALYTICAL ' RESOURCES® INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC LA.3 DEF REP.5 Page 1 of 1 SAMPLE Lab Sample ID: 0I77D QC Report No: 0I77-Newfields Northwest LIMS ID: 09-2018 Project: MARINA PARK Matrix: Tissue ' Data Release Authorized Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M O1/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.009 U ' U-Analyte undetected at given RL RL-Reporting Limit i III FORM-1 , I INORGANICS ANALYSIS DATA SHEET TOTAL METALS ' Page 1 of 1 Lab Sample ID: 0177E LIMS ID: 09-2019 / 'Matrix: Tiss�•^ ^ Data Release Reported: Oli Prep P Meth D CLP-M O1/: U-Analyte ur RL-Reporting i i ANALYTICAL RESOURCES INCORPORATED Sample ID: NC COMP.C.L REP.1 SAMPLE QC Report No: 0177-Newfields Northwest Project: MARINA PARK INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0177E LIMS TD: 09-2020 Matrix: Tissue Data Release AuthorizedjJ��/ Reported: 01/23/09 ' ANALYTICAL O RESOURCES INCORPORATED Sample ID: NC COMP.C.L REP.2 SAMPLE QC Report No: 0I77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M O1/20/09 7471A O1/22/09 7439-97-6 Mercury 0.009 0.009 U U-Analyte undetected at given RL RL-Reporting Limit i i I' FORM -I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC COMP.C.L REP.3 ' Page 1 of 1 SAMPLE Lab Sample ID: 0177G QC Report No: OI77-Newfields Northwest ID: 09-2021 Project: MARINA PARK 'LIMS Matrix: Tissue Date Sampled: 01/14/09 Data Release Authorized Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 'U-Analyte undetected at given RL RL-Reporting Limit FORM -I Mercury 0.009 0.009 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OI77H LIMS ID: 09-2022 Matrix: Tissue Data Release Authorized Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: NC COMP.C.L REP.4 SAMPLE QC Report No: OI77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.009 U ' U-Analyte undetected at given RL RL-Reporting Limit i j f 1 I I FORM -I ' ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC COMP.C.L REP.5 ' Page 1 of 1 SAMPLE Lab Sample ID: 0I77I QC Report No: 0I77-Newfields Northwest LIMS ID: 09-2023 Project: MARINA PARK Matrix: Tissue Data Release Authorize (/ Date Sampled: 01/14/09 Reported: 01/23/09 �/l//I�E�1 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte rCLP-M 01/20/09 7471A 01/22/09 7439-97-6 'U-Analyte undetected at given RL RL-Reporting Limit ' FORM -I RL mg/kg-as-rec Q Mercury 0.01 0.01 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0177J LIMS ID: 09-2024 Matrix: Tissue Data Release Authorize Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: NC COMP.C.0 REP.1 SAMPLE QC Report No: 0I77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit 0.009 0.009 FORM-1 ANALYTICAL RESOURCES INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC COMP.C.0 REP.2 rPage 1 of 1 SAMPLE Lab Sample ID: 0I77K QC Report No: 0277-Newfields Northwest LIMS ID: 09-2121 Project: MARINA PARK Matrix: Tissue Data Release Authorized: Date Sampled: 01/14/09 Reported: 01/23/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte rCLP-M 01/20/09 7471A 01/22/09 7439-97-6 U-Analyte undetected at given RL RL-Reporting Limit i r r :r .r 'r r 'r r r FORM -I RL mg/kg-as-rec Q Mercury 0.01 0.01 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: OI77L LIMS ID: 09-2026 Matrix: Tissue Data Release Authorized: Reported: 01/23/09 ANALYTICAL /�, RESOURCES V INCORPORATED Sample ID: NC COMP.C.0 REP.3 SAMPLE QC Report No: 0I71-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury U-Analyte undetected at given RL RL-Reporting Limit 0.009 0.011 46��0� ANALYTICAL RESOURCES O • INCORPORATED INORGANICS ANALYSIS DATA SHEET TOTAL METALS Sample ID: NC COMP.C.0 REP.4 Page 1 of 1 SAMPLE Lab Sample ID: 0I77M QC Report No: 0177-Newfields Northwest LIMS ID: 09-2027 Project: MARINA PARK Matrix: Tissue , Data Release Authorized / Date Sampled: 01/14/09 Re orted• 01/23/09 Date Received: 01/16/09 e Prep Prep Analysis Analysis Meth Date Method Date CAS, Number Analyte CLP-M 01/20/09 7471A O1/22/09 7439-97-6 Mercury 'U-Analyte undetected at given RL RL-Reporting Limit FORM -I RL mg/kg-as-rec Q 0.01 0.01 U INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0177N LIMS ID: 09-2028 Matrix: Tissue Data Release Authorized Reported: 01/23/09 ANALYTICAL , RESOURCES INCORPORATED ! Sample ID: NO COMP.C.0 REP.5 SAMPLE QC Report No: 0I77-Newfields Northwest Project: MARINA PARK Date Sampled: 01/14/09 Date Received: 01/16/09 Prep Prep Analysis Analysis Meth Date Method Date CAS Number Analyte RL mg/kg-as-rec Q CLP-M 01/20/09 7471A 01/22/09 7439-97-6 Mercury 0.009 0.009 U U-Analyte undetected at given RL RL-Reporting Limit , 1 FORM -I 1 I' INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Lab Sample ID: 0I77LCS LIMS ID: 09-2016 Matrix: Tissue Data Release Authorized. Reported: 01/23/09 ANALYTICAL RESOURCES INCORPORATED Sample ID: LAB CONTROL QC Report No: 0177-Newfields Northwest Project: MARINA PARK Date Sampled: NA Date Received: NA BLANK SPIKE QUALITY CONTROL REPORT 1 Analysis Analyte Method Mercury 7471A Reported in mg/kg-wet N-Control limit not met NA -Not Applicable, Analyte Not Spiked Control Limits: 80-120% M '1 i' 1 1 Spike Found 0.21 FORM-VII Spike Added 0.20 Recovery 105% 6 INORGANICS ANALYSIS DATA SHEET TOTAL METALS Page 1 of 1 Sample ID: METHOD BLANK ANALYTICAL RESOURCES INCORPORATED Lab Sample ID; 0177MB QC Report No: 0177-Newfields Northwest LIMS ID: 09-2016 Project: MARINA PARK Matrix: Tissue Data Release Authorized: Date Sampled: NA Reported: 01/23/09 Date Received: NA Percent Total Solids: NA Prep Prep Analysis Analysis Meth Date Method Date CAS Number CLP-M 01/20/09 7471A 01/22/09 7439-97-6 U-Analyte undetected at given RL RL-Reporting Limit Analyte RL mg/kg-as-rec Q Mercury 0.01 0.01 U FORM -I NVWFIELDS t - - DENT PROJECT SPECIE31 NEWMEWSrADOMTORT PROTOCOL City of Newport Beach Marina Park Macoma nasuta PDIt Gamble Bath 4 srIs rusaR SACE 199b). OTM (USEP=SACE 1991). ASTM E 1611. EPA Region 4 RIM (199J) EWFIEWSJOB NUMBER PROJECTMANAOER WATERDESCRIPTION TEST START DATE TE5TEN0 DATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16-Dec-2008 13-Jan-2009 WATER QUALITY DATA QO(mD1U >4.5 DH 7.8±0.5 D.O. W MVNEMEL051D DAY REP JARi Mier myl 9±2E PH TECHNICIPNIDATE FLOW metemeter onu min9ser 1 4 U 3 __ 45- /---- -3 _12: -- - - ?.8 ----- ...__b�...!?Ik ... _..... ............__._..._. 3�_........ _................ 2 3 pp _Q............ ................ ................ Control / 0 3 8 4 5 7,3_--- - - --'r' --- - --- --- -�l_f------ -- -- -- --- ---- ......._......._...._......._.....-..............__......... .._... _.............. -............................ .... 5 20-! G Control/ 1 1 4 C� tS. '37- Control / 2 2 3 ?l. "�•�j 3 S• 1 ; / • ff �% Control / 3 3 8 3 rj • $ 3 i5 . 3 3 ( 3 16, Gil- I -Z 3 42 Control / 4 4 5 6. ?j 15_ $ 3 �, ( 'lj �.� `{ Control/ 5 5 20 3,C'3 3 `tD-o 3 31 3 -ram MY�ItU (3 2-1 Control 6 1 4 3 �• a "3 ( r�- 3 Z 3 37 Control / 7 2 3 3 3 S 3Z -;?: i0 , I �_1 Control / 8 3 8 3- 3 Z :7-. Control/ 9 4 5 3 -4,0 sj 16.E2 3a 3 '-Y I',�,,�1tt 25 Control / 10 5 20 - 15,5 3 - j. 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Control/ 16 1 4 l 15.5 l r?!t t!1 `?q u Control / 17l 2 3 1 k� ?� Lk control 18 3 8 1�1y' 3y 2,� Control! 19 4 5 7 !f iS.� f 3Z I ]� / °Sr a 3T Control 20 -5 20 tbLO }S. 8 I 3 I :-to (IS -tog YZ Control! 21 1 4 } a N.0 S7 KM6 t 6 o`l 2 Control / 22 2 34 1 w73 'y ., 1 Control / -23 3 8 ?J- '3.13 is. 5 :3 SID- --(S t � Control! 24 4 5 42> 315-2, 3 3a 4.3 lr- 1 ft:r— Control / 25 5 20 .4 iS• z t Z � 1 control / 26 1 a 3 {-5 . 3 3Z 3 7- ! 1 Control! 27 2 3 T S [ } I `� ..S Z a 1 4 +} Fs . )o {S. 8 t 31 l 9--i-- KAUS t t3 Control / 28 3 8 �, V E�_ 31 4 5 �.� �S.It S% _ 5 20 _ .�9 o Flo. _ 3 i nf - Page _ E _ NMM DMMH� M 4MI M MM 00 RM \TEWFiELDS LIENT PROJECT SPECIESI NEWRELOSLAHORATORY City of Newport Beach Marina Park Macomanasuta Port GammeBath 4 F.,OCOL MNSEPAgr1ceism,OTMNSEWJUSACEl99t), ASTM E 1611. EPA Re91.A RDA (1993) EW IELDSJOBNUMBER PROJECTMANACER WATERDESCRIPTION TESTSTARTOATE TESTENDDATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16-Dec-2008 13-Jan-2009 WATER QUALITY DATA DO(maiLl >4.5 DO. CLIENTMEWFIELOBID meterB4 TEMP(C) 15±1 TEMP meter -C SALINJovO 32±2 SALINITY meter PPt DH 7.8±0.5 PH OAR meter..3..__.. 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LA-3 Ref / 14 4 1 1 3 t4 • 7j 5 • 3 �J �' , Ta W klg ?,,o Ly 13 1211712008 28-DAY BIOaCCUm M900M WO&SURV Page 3 28 DAY RIOACCI Toni n AMON WQ DATA SHEET _ ENT PROJECT SPROES1 NflYFlELOSI OMTORY PROTOCOL City of Newport Beach Marina Park Macomanasu(a PDRGarnbleBoth 4 ��P"A15A° 19M.° (USEP'nnACC1"n• ASTME 1511,EPAR.¢oN 4 R01(tM) ISOSA6HUMBER YROJEGTMANAGER TER DE="ON iESTSTART GATE TESTENO DATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16•Dec-2008 13Jan-2009 WATER QUALITY DATA • 1 CUENONEYlFlE w • DAY REP 00(matO >4.5 O.O. TEMP(C) 15t1 TEMP SALOUDDU 32*2 SAt1NTY ON 7.8t0.5 PH TECHNICIA1tlpATE FLOW JARa NNN( Nyt NNNf •C RIM1l PR NRgt 1dt N1YJ4s•N LA-3 Ref / 15 5 2 3 %-.mil 3 l $. to 3- 2j Z �7 -4- 9 "�S (Zl31 4Z LA-3 Ref 16 1 6 K �,a 15.5 ( 3 a t .8 al ) I D9 91 LA-3 Ref 17 2 7 Lk ?� L� ( C� t0 3 •C�j �1M�(� l 6 3� LA-3 Ref 1 18 3 11 Y� I 'S.� 3 Z 8 •� ? 3 LA3Ref / 19 4 1 `}' �. ! Is.� / 32 / ��- /� v 39 LA-3 Ref / 20 5 2 �-• ?j L� t • 7 ( - LA3Ref / 21 1 6 'T } 2 L� t�j, $ 3`� �P Mt�(� f L9 38 LA-3Ref / 22 2 7 !1 LA-3Ref / 23 3 11 3 LA-3 Ref / 24 4 1 3 LA-3 Ref 25 5 2 '� �.� �S.'j 3Z- ( �.� vF--1�(p 'Sea LA3Ref / 26 1 6 3 Q ?) [s. 3 -Z 3_ 1� 11 3c7 LA-3 Ref / 27 2 7 '7. [ S. J 1 -11 z 7 �.� lS_� LA-3 Ref 28 3 11 27 5 2 _ . t ' a28_nev mtoaG ma{��g�yjRV �• Page 4 mom S OTC DA BHM M M i M M M NEWFIELDS VENT PROJECT SPECIESt NEYIFIELDS LABORATORY PROTOCOL City of Newport Beach Marina Park Macomanasuta Part Gamble Bath mvV' FP CE1"8).OTMNSEF!NSACE1991). ASTM E 1611. EPA He&. {RIM (1993) 'EWFIELOSJ0SNUM6ER PROJECTMANAGm WATERDESCRIPM4 TEST START DATE TESTEND DATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16-Dec-2008 13-Jan-2009 WATER QUALITY Y UA) A CLIENTMEWFIELDSID DAY DO(MWL) >4.5 O.O. ftEP JARi meter m91L 7EMP(C) 15±1 TEMP SALK(Dut) 32±2 SALINITY DH 7.8t0.5 PR TECNNICLWIDATE FLOW meter °C meter PP1 meter O^a m'y� Comp C-L! 0 1....._..'°.....3... _? _ 3 5 12 13 9 ... _.. .._......3.._...�5 -!_ :.9._._._._ } _ ..........._.i.:g..._........._ .._._...3..._..3...L_._._......_3_........�7...-_3.........._...........a, .._!.S_( _.._ .. 31....._._.___......_......__...._._._..r....._._...._.._._---...._.....__ 3L,� _..._._._..__._._...._. �? ...._.........._._._......__...._.__... 2 7 ..._..fzl��...._.._._......_._.__3 ......... ......._ ...._._ ................. ... ....... .... 3 p.... 17 Comp C-L / 1 1 10 l�g 3 32 7 S Comp C-L / 2 2 12 �,?� 3 1�,�/ 32 �,� b Comp C-L / 3 3 13 3 .�j 3 IS -Ob� �j 3 7.�71 / 1 Comp C-L / 4 4 17 3 b, i 3 1S.QI 7 3 �.4' iik (.i ¢2Q Lf Comp C-L / 5 5 9 3 3 1 15 .% 3 a 3 -9°} i LMS a 21 Ikk Comp C-L / 6 1 10 G. $72- Comp C-L / 7 2 12 �i S 32 Z `� /Z 39 Comp C-L / 8 3 13 3 3 Z T U 4 cz /-2Z `f?i Comp C-L / 9 4 17 3 6. iaq -�,3 IZ�'L�j L{a Comp C-L / 10 5 9 3 6.9 3 15• 77 3 :)--i W ` 0 Comp C-L / 11 1 10 3 (P,(p —3 -4 Comp C-L / 12 2 12 3 (o.Cp 3 Comp C-L 13 3 13 `3 Z Comp C-L / 14 4 17 12/17/2008 28-DAY Bioamum MaCOM2 WO&SDRV Page 5 28 DAY RIOACCI inns 11 ATION WQ DATA SHEET _ 1�7E�VFIES.DS . LIENS PRWEPi SPEPESt NEWFAiLPS IABOMTORY PROTPCOL City of Newport Beach Marina Park Macomanasata PodrnbleBath 4 ITM(USE➢AVMEIM).MIOSEPAM1ISA INI), A E 1611. EPA Mg. 4 RIM(19M %EWiIELDSMWKUMSIM PRPJEPTMAN M WATERMSC� nNaT MTVATE TEST ENPPATE 1105-005-860 Bill -Gardiner North Hood Canal; filtered 16-Dec-2008 13-Jan-2009 WATER QUALITY DATA MIK"10111111 WENTRjejWn.MW All PAY REP JAAP DO lmcdL) >4.5 am TEMP(C) 15±1 TEMP SALIN.(PPD 32±2 9ALWITY PH 7.8t0.5 PR 1ECIEMCUWOATE FLOW Il , MWL Mthr -c meter PP, "F_ uak mom' Camp C-L 15 .5 9 4.5 J 15-5 s 32 31 s•0 -13 -\24si `4 Camp C-L 1 16 1 10 �,b b53 9i'L fli QR -J (J Camp C-L/ 17 2 12 4 �•. a lE. { C� • Cj 3 a j �'•� MMt [ 1-2-1 O" 1 3 � Camp C-L 1 18 3 13 LrI-4 K Camp C-L1 19 4 17 �,S (S 3Z f �• / o CompC-L/ 20 5 9 La S •�{ 3 a t 1, MtMaP \ 6(zF) b Comp C-L / 21 1 10 s • { '� l t �pLAM6 llkqf(ft Come C-L I 22 2 12-7.7 (3�� I c� Comp C-L / 23 3 13 P4.0 3 t r3 .3 32/ �J �-r�j �S t da Comp C-L / 24 4 17 Camp C-L / 25 5 9 L Camp C-L / 26 1 10 3 V.( 3 15• t 3�- 3 '7 • l f t t12-11 Camp C-L 1 27 2 12 12 3011 1 10 t 13 7-7 2 12 ,3 is,b 3i Y Comp C-L/ 28 3 13 (Q • [p tCj, ( �-.tD __ ,_„_ __._ ___ 4 17 (fl.� ks• 31 _ 9- AP 5 9 .lo (ram �" 3\ 4.°1 M- N! DASH M M M M M M l�T��TFTELBS . VENT PROJECT SPECIEST NEWFIELDS LABORATORY PROTOCOL City ofNe wportBeach Marina Park Macomanasuia Port Gamble Bath 4 ITMtUSEPAAISACE'"s),OTMIUSEPAA CE1"I), ABiME16I1,FPARegi¢ndRIM(199]) EWFIELDSJOa NUMBER PROJECTMANAGER WATERDESCRIPTION Mtn`STARTDATE TESTEND DATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16-Dec-2008 13-Jan-2009 WATER QUALI (Y UA I A CLIENTME JELDSID DO (mWL) >4.5 D.O. TEMP (C) 15±1 TEMP SALINA)DO 32±2 SAUNRY DH 7.8±0.5 PH TECHNICIANIOATE eter mglL meter °C meter PPt mat¢r u¢tt mv1¢uc C-u I 12715 _................._._......_.........../ 7 7j 3z rS�z .......... ...._..._3.1.........._. 7 ?� _._.._..........7 p tComp ,� rzc� o__......._.__. z- G�_ Comp C-U I 1 1 16 4 D 2 C Z 2, Comp C-U / 2 2 15 3 q , Comp C-U I 3 3 19 Qj �S 3 3 —3,, 7 CtL /ill 6) 1�t Comp C-U / 4 4 14 (rj, I ' Z> ,� � (a � t COMP C-U I 5 5 18 ?J to 5. R 3 3 t 3 �-,�- {/��1 (a-;.1 `I Comp C-U / 6 1 16 '3 • t / J 3 1.5 Comp C-U / 7 2 15 T COMP C-U / 8 3 19 3 ?j 7j [1S t I �j j i b� /Z�Z ` Y D COMP C-U / 9 4 14 `. 0 3 15. 3 3 3� 3 t zl2:5 4 Comp C-U / 10 5 18 3 (o- Z 3 I5• S µQ COMP C-U / 11 1 16 3 (p. °( 3 16.6 40 COMP C-U/ 12 2 15 �/j �,GJ 5 IS A• ,? �. 3 �'•(p � IZ�� COMP C-U / 13 3 19 ry 3 fs- /L Z 73g S� COMP C-U / 14 4 14 1 2, 3 l5 . (F 31 2, a Ia n t - `fD 12/1712008 28-DAY Bioaccum Macoma WQ&SURV Page 7 28 DAY RIOACCI IMI11 AT ON WQ DATA SHEET \TDWFIET.D� ENT PROJECT SPECIES1 NEWRELDSUBOmmw PROTOCOL City of Newport Beach Marina Park Macomanasuta Port Gamb;eBoth a 'T''' PJ'A15^`E'e'°�•°D"(cxi ""'S"E"'°• ASTM F. ISfr. EPA R691cq 4RM (IM tDSJOBADMBER PROJECTMANACEIi YGTER DESCRIPTNNI TESTSTARTDATE TMIDIDDATE 1105-005-860 Bill Gardiner North Hood Canal; filtered 16-Dec-2008 13•Jan-2009 WATER QUALITY DATA • CLIENTMEWFIEL0.4m • DAY REP JARf DO (MAIL) >4.5 D.D. 7EMP(C) 15t1 TEMP SALRUPDA 32t2 SAUNITY OH 7.8t0.5 PH TECNMpAWDATE FLOW NMff myL eMNF 'C. eMaf PPT meter YniT mVFOSee Comp C-U/ 15 5 18 3 r..-L{ 3 15.E 3 32 .��' $•?j -15 Comp C-U / 16 1 16 Iq ?-a )5.�j { 3a �•Qj do 11! �q q0 Comp C-U / 17 2 15 (•k- �.. 1 Cj . tk ( .7j `�. { �- .S mm?o l Z O ` � O- Comp C-U / 18 3 19 b� �, tf /5 3Z— g ! 5 t3 CompC-U 1 19 4 114 fr2 fS 32 �,� ! d� 3T Comp C-U / 20 5 18 .1 t S _ ( 7> 2 { .lP NJv 6 1 Comp C-U 1 21 1 16 Lk �-.'�:- (.� Comp C-U / 22 2 15 91 Comp C-U 1 23 3 19 �, 3 IrJ e 1 3 3a 3 to — 5 ( $(0q 14 zc, Comp C-U / 24 4 14 3 �- t7 CompC-U-/ 25 5 18 7. -L I� Z l 3Z { ?.? �- 1/(v �tZ Comp C-U1 26 1 16 7-c �j M.-0 �j 3�— -7. � ��(r 361 Comp C-U1 27 2 15 1 Li 3 { 3 6 Cie—1/1-1 j ( 410 1 2 16 15 L MIA6 Its Comp C-U / 3 19 4 14 M M M = = = M m. M M M M M NE��IELDS 2S-UAT pIUAt.GUMULA11V1Y mAL.vmA rGOL voocnvnnvn CLIENT CiryofNt:wportBeach PROJECT Marina Park 3B Na. 7110:-005-860 PflOJECT WNAGER Bill Gardiner NEWflELOS LABORATORY Bath4 PROTOCOL rrM (USEPAIUSACE 1998). 07M (USEPANSACE 1991),ASTM E SPECIES '�""Macomanawla=-' 1611. EPA Region 4 RIM (1993) Observation Key ENDPOINT DATA 5 OBSERVATIONS JP xumenme.s� pp NwnMer ReRary E.Arexlc6�erw hiu'�PSMJyJ �v� �y�I� va-)1q Imam (a--�a1 W einWiP o-eeNrnwr(oMr a.E.a„n� N•Hwmfl 8•HeOVrwrf OJT '_\lV �T7 IY Mrv.`� f"•""� 1/ lY oei v 1'yk&!?> NEwP1ELos Lo a LL Fo 1 2 3 4 5 6 7 8 9 10 11 12 13 14. LA-3 Ref 4 1 ` ' S N LA-3 Ref 5 - 2 Control/ 2 3 Z s 36 fps �St s (� S 5 (�5 55 45 Control, ,-.- - -- _ 4 a s s Ss _ S' �� 35 35 5S-!3— s 1 Control3 4 -_- - - 5 / 1�1 f �5` 3 5 3 - ; N LA-3 Ref 1 : 5[��\ j�5 l ` LI =- N LA-3 Ref 2 -' 7 5 L 1j � \" fS I5 ITvS \tj N Control) 3-= e �.5 �s '-Cs v S os .lfV� des (oD.ls II 3M' ` .amp GL 5 9 / 1 J 4s _I,CA' 5 s 1__— —("L �b // l ✓J'i S -Camp GL 1 ---__ t0 455 'III SS �S �'S II �� l S `c7.J �J" !� I1,t�S LA-3 Ref 3 - 11 ) : Icc N I ��94) � tv 11 Come GL 2 '.:- _ 12 V is C�/ JD L �J �OccJ Came GL 3 _ 13 5`-r �S �S �O/ 5 V/ 15 © T6AWL- G�'). �l U-v �a-ct� CT /�"6�,r-✓ (21 11 11 11 1 / I� f1/111100Ei&OAY Boettum M+coma Nac�m� EMpa'Y t-1� vi ,fj1c, Pyef NE��LELD511 28-DAY BIOACCUMULATION MACOMA TEST OBSERVATION DATA SHEET 3 PltmIECT MEY/FiElW J06 W. FpOh�1114H.�n.ER MFWFIEIDSUB011ATafY %IOimea. ITM (USEPANSACE 1996), OTM EFECE3 City of Newport Beach Marina Park 1105-OOS O Bill Gardiner Bath 4 (USEPAIUSACE 1991), ASTM E 1611. EPA Region 4 RIM(1993) McCplMAMIN Oba a6cn Key ENDPOINT DATA 3 OBSERVATIONS q.rrraerwms FIiyYll�ls 17 11 { ./ fa'EO ia(tq PW 1vrq21 rtjv2 rgl23 I�hX WLS t�ur ,ajar ,ems ,z#7 ta-I'i�o MIYI�P bWYMlemi OWtiY J' 4-- ��p CL1ENTl WWFIEEas10 vLL+ c LL LL �o 1 2 3 4 5 6 7 8 9 10 11 12 13 14 z zomp PU 4 _ 14 N J �s Cane CL 2 - 15 /gs �s 18 ; 35 i N N Carp C-L , 17 17 ��j' hs }� s `7 S s If 135 I 5 105 ta It c«mpau 5 IS s lS N ),4 \1 N Camp OU 3 19 `°ntr°" 5 20 is 35 3s 3s 3s 5 35 s SS �5 3s CP409kw� on i]JillloOIZWAYBioEca�nR4can EIrEMpen1UN P�2 28-DAY SIOACCUMULATION MACOMA TEST OBSERVATION DATA SHEET 3 1 \TET :,: IELDS CLIENT PR0.1ECr NEWFlELASJC8 N0. OJERYNN4GEA EYmEIDSLPeCRATO1tY PAOTOCaL DM(USEPANSACE 1996). OTM SPECIES City of Newport Beach Marina Park 1105-005-860 Bill Gardiner I Bath 1 (USEPANSACE 1991). ASTM E 7611, EPA Region 4 RIM(1993) .= )lfaooma no," _ Observation Key ENDPOINT DATA S OBSERVATIONS w.xi..a..nv.awrs T-wy+va+.s ��z�aq j 1 `3lei tj�t02 1�5�¢i �p(2 .a u•P�.uraee a5 I743('/'�fl� u c a� M► M MN�� G (L (,t2 �'I1— Is >3 Fntv�, m LL ou6NT1 NEWFLOS IEID 'w ¢ x a= ,.,o - 15 i 16 17 18 19 20 21 22 23 24 25 26 27 28 E Z z 2 LA-3 Ref 4 ._ t N \% . N N n I 1 V f�{` ' " A% _ LA-3 Ref 5 2 �Nj Contral - 2 3 S5 �S 35 �s �S �¢ s (35 zS 13�9-3 Control, 1 4 Control1 4 _ _:_ 5 Is as 'y (/1 �s S `� �✓ G LA3 Ref 1 1 _ - g ��\ , LA3 Ref 2 7 I S l/ 6 S /1�'' Imo'' , t tV V Z.g Contrail 3 _ 6 I^.� �7 �S �5 rJ L —s s 23 Comp C-L 5 : , 9✓OJS c� s Fss L S s &5' .3l;oc t SS,2 2G52(�( ISM (3 1 -.- 70 �_S1S LA7 �`d-`5 �wl Iv 'LFS IDS �sl o �S m3(�j��A u'(� M 4♦S QZS rELA-3 3 11 � IV i—' � 14 N f`r ly 0 rJ 0 ��P 1\) 2 12 25 'a5 FrS 1 �1S �'S I,S l� �5(2. ��5 1,�/S I ZZ 3 ...� 73 I..A 1�5. '�5 1 {2-5f l'�S s Its 1M M AS'Z IQS i't (S Comp C-U 4 ,- 14 Y� Ij N N a Comp C-U 2 15 I 11W a1A I 1L7]20082bDAY Eoacc�m Macaiu fbcoma EdK+W7538 Pape t 9R.n&v PlnACCI lMlll ATInM MACOMA TEST nRSERVATInM DATA SHEET 3 NEWFIELDS f'ROJELT NEYInF1D5.M1e Ni F110lECi YAYAOQ NflYiE1034eORATORY PROTOCOI. rrm CUSEPPAISIU:E 1996), OT.M SPE(]ES City of Newport Beach Marina Park 1105-DOS-860 Bill Gainer Bath (USEP/WSACEte6 ASTME i611, EPA Repial�RlM (19Sf) AheodRinasAa_ ObeeMUon Key ENDPOINT DATA A OBSERVATIONS aMI1�Ar�nYYMY ow.warryon ��3� ►ll ► r � ll� I �, ► ( � ► c l �( ►� [� I�� m www 4 E m LL NEWPoEI.DSD a FS 4 i6 16 17 16 19 20 21 22 23 24 26 26 27 26 E z 3 = C�m C-U 1 16 iV N lu Al 25 Comp C-L < 17 15 L�tS l�s 3 l s 3 Is, t�5 S ?,SZM ( }Nj 10� ►5 Comp6U S 16�}( N t�1 N N +'�i compCU 3 19 Iu N X G Conlmll S zM I 1)11J1N0!]bWY Km...... AYmma M�[rvw Er po`�ti]C Pp 2 oc_nAV a,nArr-I uuf n A-nnN MFRFiS TEST nRERSERVATIDN TEST DATA SHEET 3 ENDPOINT DATA & O�ERVATIONS ONE NIS ME Cwtmll Cwtfol a Comp C-L ONE mom ■OEM Comp C-U Comp C-U Comp C-L MOWN ■ ` �p cG d� L✓a �u /Z1/x1lor c� 19 IVI?r a2aoArNem6oxw.,,e*NMIs28 P�l I 14, II 1 0 F 1 1 1 U i F 1 j 1 1 1 ORGANISM RECEIPT LOG Date: ,a AR Time: s NewFields Batch No. Organism: Source: / Address: D� Invoice Attached Yes Phone: Contact: Zed 6uw34rllc No. Ordered; No. Received: Source Batch:- Condition of Organisms: / V Approximate Sizio 1 Age: Shipper: B of L (Tracking N Condition of Container: Received By: Confirmation of ID of Organism: es No Technician (initials): Notes: pH (Units) Temp. CC) D O (mg/L) Conductivity or Salinity Include Units Technician (Initials) /. Notes: i i�� r 1 . Ji ORGANISM RECEIPT LOG Date: Time: NewFlelds Batch No. is1I31v6 006 7J6 Organism: II Source: ' NerN�J-S Jo�lr7 13r C� ;�9 Address: Invoice Attached ' Un F It Yes ' Phone: Contact: No. Ordered: No. Received: Source Ba ch: l� 1 Condition of Organisms: Approximate Size or Age: Shipper: B of L (Tracking No.) rid �x 94612 6W3 sq�d i Condition of Container: Received By: Confirmation of ID of Organism: Technician (Initials): Yea COL Notes: ' Con tivity or ' PH Temp. D.O. Technician (Units) VC) (mg/L) launw Include Units (Initials) 35 �� Notes: ' ' Marina Park Draft RE1R CI GA - EVALUATION OF SURFACE SOILS MOBILE HOME PARK F 7 u I u Evaluation of Surface Soils from the Marina Park Mobile Home Park Newport Beach, California Final Report PREPARED FOR: City of Newport Beach Planning Department 3300 Newport Boulevard Newport Beach, California 92663 PREPARED BY: NewFields PO Box 216 4729 View Drive Port Gamble, Washington 98364 May 2009 I d NEWFILDS I ' May 2009 Executive Summary I� F Upland Soil Evaluation Marina Park The City of Newport Beach is in the process of preparing the Environmental Impact Report (EIR) and submitting permit applications in support of the Marina Park project, located on the Balboa Peninsula. The Marina Park project includes the expansion of existing beach areas and marina facilities, including the conversion of approximately 1.13 acres of uplands to a 28-slip marina. Approximately 62,000 cubic yards (CY) of soil/sediment is proposed for removal. Approximately 5,000 CY representing the top five feet of soil in the upland area will be excavated and used for project fill and was evaluated according to requirements in the Upland Testing Manual (USACE 2003) and California Code of Regulations (CCR) Title 22. The remaining material is proposed for nearshore or open -ocean disposal and has been characterized in a separate report (NewFields 2009). This sampling and analysis report summarizes the results of a chemical characterization of the surface soils from the mobile -home park that will be used as upland fill. Sampling and Analysis Sediment samples were collected on February 27, 2009 from three stations within the mobile home park using a stainless -steel hand -auger. Stations represented three distinct locations within the park. Samples were collected from 6" below ground surface (bgs) to 5 ft. bgs. Each of the cores was homogenized vertically and archived for possible future analysis. Subsamples from each of the three cores were then composited into one analytical sample and submitted for sediment chemistry. Analytical chemistry included sediment conventionals (grain size, organic carbon, ammonia, sulfides, Atterberg limits, total recoverable petroleum (TRPH), oil and grease, metals (arsenic, cadmium, chromium, copper, lead, mercury, nickel, selenium, silver, and zinc), organochlorine pesticides, polychlorinated biphenyls (PCBs), organotins, petroleum aromatic hydrocarbons (14 PAHs), and phthalates. The upland soils were characterized by 92% sand and gravel and 0.11% TOC. Soils appeared to be ' coarse sand with shell fragments and were not plastic, indicating that they would not hold their form. All of the metals were either undetected or detected very near the detection limits. Pesticides, PCBs, PAHs, tributyltin, TRPH, oil and grease, and phthalates were not detected in the analytical ' composite. Chemical concentrations in the test composite were below the screening threshold for Title 22 leachate testing under Title 22 Section 4.5. The upland soils collected from the top five feet in the Marina Park Mobile Home Park would not qualify as hazardous waste under California State Code and should be acceptable as fill material. J C NEWFIELDS May 2009 Upland Sol/Evaluation Marina Park 1.0 INTRODUCTION The City of Newport Beach is in the process of preparing the Environmental Impact Report (EIR) for , the CEQA process and submitting permit applications in support of the Marina Park project, located on the Balboa Peninsula. The Marina Park project includes the expansion of existing beach areas ' and marina facilities, including the conversion of approximately 1,13 acres of uplands to a 28-slip marina. Sediment and soils throughout the proposed marina complex will be excavated to accommodate the project depth of 12 ft. MLLW plus a 2 R. overdredge. Approximately 62,000 ' cubic yards (CY) of soil/sediment is proposed for removal. Approximately 5,000 CY representing the top five feet of soil in the upland area will be excavated and used for project fill on -site. Approximately 57,000 CY is proposed for aquatic disposal and has been evaluated in a separate report. Based on previous soil and sediment data collected by NewFields and Terra Costa from the , site, the surface material is expected to be eligible for use as fill material on site. The objective of this report is to characterize the top 5 ft. of upland excavation material from the mobile -home park. The material under consideration will be tested based upon criteria outlined in the UTM (USACE 2003) and California Code of Regulations Title 22. 1.1 BACKGROUND AND HISTORY , The proposed Marina Park is located in Lower Newport Bay, on the bay side of the Balboa Peninsula between 15'h and 18'h Streets immediately north of West Balboa Boulevard (Figure 1). The site currently includes some recreational areas and mobile homes. The Marina Park Master Plan includes t a 28-slip marina, a small -boat basin, and moorage for visiting vessels in the northeast comer of the site. The mobile -home park was first constructed in the early 1950s. Prior to the 1950s, the area occupied by the mobile -home park was vacant land. , I I I I NwFtELDs ell lyot fi;C► ji e4 � +2^'��^4��14`` °r7 � _- i��tl��i � I ' A _ Proposed Mahrla 144t * 4v May 2009 Upland Soil Evaluation ' Manna Park 1.1.1 EXISTING SOIL AND SEDIMENT CHARACTERISTICS The Balboa Peninsula was primarily formed from sand deposits overlying Bay sediments following a series of extreme storms in the 1860's. Subsequent dredging and construction has increased the size of the peninsula. In May 2008, the City conducted a geotechnical investigation of soils at the one location within that portion of the mobile -home park that will be excavated during marina construction (Terra Costa 2008). Terra Costa conducted soil borings (B-2) and cone penetration tests (CPT-12) at one location immediately adjacent to the footprint proposed marina. The cone penetration test (CPT) evaluated sediment type, as well as other physical features. The borings included a visual description at 5 ft intervals, as well as subsampling for grain size analysis. In addition, NewFields conducted chemical analysis of soils that included two contaminants of potential concern that have been identified in lower Newport Bay, mercury and DDT. The geotechnical survey characterized the project soils as follows: "The site is underlain by hydraulic fill, bay deposits, and older alluvial deposits beyond the depths of our deepest exploratory drilling at 50 feet. These soil and geologic units of the surface soils are described below. _Hydraulic Fill Soils: Our test borings indicate that the project site -area is generally underlain by from 5 to 6 feet of loose to medium dense, gray -brown, damp to wet, hydraulically placed sands and silty sands (SP/SM), with occasional shell fragments. It is likely that these relatively "clean" granular soils were placed as the result of dredging during one or more phases of the development of Newport Harbor. SPT blow counts within these artificially placed dry to saturated sands ranged from 7 to 25 blows per foot." The Bay Deposits extend to approximately project depth at -14 ft. MLLW. Groundwater elevations appeared to match tidal elevations in the Bay. A subsample of porewater from the borings indicated that the groundwater was at least 20%o. Samples may have been compromised by freshwater added to the sample hole used to facilitate the boring. Grain size analysis of the soil borings resulted in a similar characterization, with sand dominating throughout the area (Table 1-1). Based on the results of the geotechnical investigation, the soils underlying the mobile -home park and neighboring beach are comprised of sand with shell fragments. Soils were either hydraulically -placed from dredging events or the result of deposition following historic storm events. 1.1.2 CHEMICAL EVALUATIONS OF EXISTING SOILS AND SEDIMENTS Concentrations of contaminants of concern were evaluated for the soils collected in boring B-2. The soil borings were evaluated for metals and DDT and associated breakdown products (Table 1-1), contaminants of concern that have been found in other portions of Newport Bay. Metals were present very near or below the detection limits and DDT, DDE, and DDD were undetected in both soil borings. NEWFIELDS ' May 2009 Upland Soil Evaluation Marina Park L_ 1 ' Figure 2. Locations of recent samples collected near the proposed marina. Existing stormwater outfalls denoted by blue circles. 1 1 I Table 1-1. Data for soil/sediment samples at Marina Park, May 2008. Anal to Units ti-2 Depth below surface ft 5 11.0 10 1.0 Gravel % Sand % 84.1 98.5 Silt & Clay % 4.9 0.5 Anahrte Units Surface 4,4'-DDE /k <2.0 U 4,4'-DDD µg/kg <2.0 U 4,4'-DDT µg/kg <2.0 U 2,4'-DDT µg/kg <2.0 U 2,4'-DDE µg/kg <2.0 U 2,4'-DDD µg/kg Q.0 U Arsenic mg/kg <6 U Cadmium mg/kg <0.2 U Chromium mg/kg 1.6 Copper mg/kg 2.8 Lead mg/kg <2 U Mercury mg/kg <0.04 U Nickel mg/kg <1 U Silver mg/kg <0.3 U Zinc mg/kg 3 1 May 2009 2 METHODS Upland Soil Evaluation ' Manna Park The objective of this sampling and analysis program (SAP) was to characterize the proposed excavated materials from the upper 5 ft. of soils underlying the mobile home park and to evaluate its suitability for use as construction fill on -site based on criteria in the UTM (USACE 2003). Chemical was conducted on surface soils. If necessary, the California Title 22 Waste Extraction Toxicity (WET) test would be conducted to evaluate the potential for contaminants to leach from excavated materials. 2.1 DEFINITION OF AREAS AND SAMPLE LOCATIONS Core samples were collected from the upland areas of the site to a depth of 5 ft bgs as shown in Figure 3. Soils and sediments below 5 ft bgs were evaluated in a separate evaluation (NewFields 2009). The sampling area for this investigation included that portion of the site currently occupied by the mobile home park. Two locations were located in paved surfaces, one in a parking area (MP- 1) and one immediately adjacent to a mobile home (MP-3). An additional sampling site was located in a grass lawn between three residences (MP-2). As noted above, each core was homogenized vertically from approximately 6" bgs to 5 ft. bgs. Each of the cores was then combined into one composite sample Area composite (MP Surface Sediment). Figure 3. Area and Station Locations. Station locations denoted by red symbols. J ' May 2009 Upland Soil Evaluation Marina Park 2.2 FIELD COLLECTION PROGRAM FOR SOIL/SEDIMENT CORE SAMPLES ' Samples collected were collected on February 27, 2009 by NewFields. Upland cores were collected using a 2" stainless -steel hand auger. For locations with a paved surface, the pavement was removed ' using a cold -chisel with the top 6" of soil removed using a stainless -steel spoon. The upper 6" was not included in the analytical sample. Cores were collected to a depth of 5ft. Separate clean, solvent -rinsed stainless -steel liners were used for core section. Samples were processed in the field using clean, solvent -rinsed spoons and bowls. Coordinates for each location were recorded using a hand-held Global Positioning System (GPS) unit fitted with a WAAS antenna. Each sample was photographed and characterized for sediment ' characteristics. The core stratigraphy and other pertinent data and observations were logged. The geologic description of each core included the apparent grain size, odor, color, length, and any evident stratification of the sediment. Soils from the entire core were homogenized and a subsample placed into certified -clean I -Chem jar, labeled (project name, date, sampler ID, analysis, and preservative where applicable), logged into a ' field chain -of -custody (COC) form, and placed into a cooler for later archive. A subsample from each core was then placed in a stainless -steel bowl and homogenized to create an area composite. The composite sample was placed into a certified -clean glass jar. Samples remained on ice and in ' the dark until shipped via overnight delivery service to Analytical Resources Incorporated for chemical analysis. Prior to shipping, sample containers were placed in scalable plastic bags and securely packed inside coolers with ice packs or crushed ice. COC forms were filled out, and the original signed COC forms was placed in a sealable plastic bag and placed inside the cooler. The cooler lids were securely taped shut. 2.3 PHYSICAL AND CHEMICAL ANALYSIS Physical and chemical parameters measured in this testing program were selected to provide data on potential chemicals of concern in the surface soils from the Marina Park site. The MP -surface test composite was analyzed for all of the analytes listed in Table 2-5. The target detection limits ' (sediment — dry weight) are also presented in Table 2-5. All analytical methods used to obtain contaminant concentrations follow EPA or Standard Methods (SM; APHA/AW WA 1998). 2.3.1 PHYSICAL ANALYSES To characterize the physical properties of the soil, tests were performed, to predict the behavior of excavated soils. Physical -chemical analyses of the sediment included grain size, specific gravity, ' total organic carbon (TOC), total solids, and plasticity (Atterberg Limits). Grain size was analyzed to determine the general size classes that make up the sediment (e.g., gravel, sand, silt, and clay) and the frequency distribution of the size ranges (reported in millimeters [mm]). Grain size ' measurements were conducted using the gravimetric procedure described in Plumb (1981). The TOC, made up of volatile and nonvolatile organic compounds, was determined as recommended in the UTM (USACE 2003) or equivalent (modified SW846). This procedure involves dissolving inorganic carbon (carbonates and bicarbonates) with hydrochloric acid or sulfuric acid prior to TOC ' analysis (Plumb 1981). Total solids were also measured to convert concentrations of the chemical parameters from a wet -weight to a dry -weight basis. Percent solids was determined by USEPA Method 160.3 (USEPA 2001). Total petroleum hydrocarbons and total residual petroleum NEWFIELDS May 2009 Upland Soil Evaluation Marina Park hydrocarbons (TRPH) were analyzed using EPA Method 1664. Atterberg limits were determined using ASTM D-4318. 2.3.2 SEDIMENTCHEMISTRY The following analyses were performed as recommended by the UTM (USACE 2003). The analysis for priority pollutant metals was conducted using an inductively coupled plasma emissions spectrometer equipped with a mass detector (ICP-MS), in accordance with USEPA 6010. Mercury analysis was conducted using cold vapor atomic absorption (CVAA) using EPA 7471A (USEPA 1994). Semivolatile organics (SVOC; PAHs only) were analyzed using gas chromatography -mass spectrometry with selected ion monitoring (GUMS SIM), using USEPA Method 8270 SIM (USEPA 2001). This followed serial extraction with methylene chloride and alumina cleanup procedures. Organochlorine pesticides and PCBs were analyzed using dual column GCECD following USEPA Method 8081 and $082 respectively (USEPA 2001), with extraction modifications to reach lower detection limits. The PCBs were identified to the Aroclor level. The analytical method used to determine TBT involves methylene chloride extraction, followed by Grignard derivatization and analyzed by GUMS (Krone et al., 1989). Table 2-5. Chemical and Physical Parameters, Analytical Methods, and Target Detection Limits Parameter Method Procedure Sediment Reporting Limit Target dr wet ht Physical / Conventional Tests Grain Size Plumb 1981 Sieve/Pipette 1.0% Atterberg Limits ASTM D4318 TOC ASTM D2579 Combustion IR 0.1% Percent Solids EPA 160.3 Gmvimetric 0.1% Sulfides PSEP 1986 Colorimetric LO mg/kg Oil and Grease EPA 1664* Gmvimetric TRPH EPA 1664* Gmvimetric Ammonia SM 450ON H3F ICP-MS 0.001 mgtkg Lipids Bli hD er GmvimetricI n/a Metals Arsenic As USEPA 6010 ICP-MS 0.5 in Cadmium Cd USEPA 6010 ICP-MS 0.2 mgtkg Chromium Cr USEPA 6010 ICP-MS 0.5 mglkg Copper Cu USEPA 6010 iCP-MS 0.5 MELCE Lead(Pb)USEPA 6010 ICP-MS Mercury H USEPA 7471A CVAA 0.05 mgtkg Nickel(Ni)USEPA 6010 ICP-MS 0.5 mgtkg Selenium Se USEPA 6010 ICP-MS 0.5 m' k Silver A USEPA 6010 ICP-MS Zinc Zn USEPA 6010 ICP-MS 4 mg/kg Pesticides 4-4' DDD USEPA 8081 GCECD 2 4-4 -DDE USEPA 8081 GCECD 2 4-4'-DDT USEPA 8081 GCECD 2 2A' DDD USEPA 8081 GC/CCD 2 pgfkg 24-DDE USEPA 8081 GC/ECD 2 k 2.4'-DDT USEPA 8081 GCECD 2 Aldrin USEPA 8081 GCECD I ILgtkg a-BHC USEPA 8081 GCECD 1 BHC USEPA 8081 GC/ECD 1 µ Chlordane USEPA 8081 1 GCECD 1 2 k NEWFIELDs 11 I I I I I I I 1 LJ I I ji 17, LJI May 2009 Upland Soil Evaluation Marina Park Sediment TargetReporting Limit Parameter Method Procedure (dry weight) S-BHC USEPA 8081 GC/ECD I µg/kg ' Dieldrin USEPA Mil GC/ECD 2 pag Endosulfan i USEPA 8081 GC/ECD d Endosulfan 11 USEPA 8081 GC/ECD 2 /k Endosulfan Sulfate USEPA 8081 GC/ECD 1 k Endrin USEPA 8081 GC/ECD 1 AEVU Endrin Aldehyde USEPA 8081 GC/ECD 1 k Heptachlor USEPA 8081 GC/ECD I gglkg He tachlorE oxide USEPA 8081 GC/ECD 1 k BHC USEPA 8081 GC/ECD I pglkg Methox chlor USEPA 8081 GCBCD 10 Lindane USEPA 8081 GC/ECD t Toxa hene USEPA 8081 1 GC/ECD 100jig/kg PCBs Aroclor 1016 USEPA 8082 GC/ECD 4 ggAcg Aroclor 1221 USEPA 8082 GC/ECD 4 ' Aroclor 1232 USEPA 8082 GCBCD 4 pgtkg Aroclor 1242 USEPA 8082 GC/ECD 4 Aroclor 1248 USEPA 8082 GC/ECD 4 /k Aroclor 1254 USEPA 8082 GC/ECD 4 k ' Aroclor 1260 USEPA 8082 GC/ECD 4 Semivolatile Organics Acena hthene USEPA 8270 GC/MS SIM 7 k Fluorene USEPA 8270 GC/MS SIM 7 Phenanthrene USEPA 8270 GC/MS Sim 7 k Anthracene USEPA 8270 GC/MS SIM 7 Fluoranthene USEPA 8270 GC/MS SIM 7 ' rene USEPA 8270 GC/MS SIM 7 PJkg Ch sene 'USEPA 9270 GUMS SIM 7 Benzo a anthracene USEPA 8270 GC/MS SIM 7 Benzo b fluoranthene USEPA 8270 GC/MS Sim 7 k ' Benzo a rene USEPA 8270 GC/MS SIM 7 Indeno 1,2,3-cd rene Dibenzo a,h anthracene USEPA 8270 USEPA 8270 GC/MS SIM GC/MS SIM 7 7 Mkg 1 Benzo ,h i e iene USEPA 8270 GC/MS SIM 7 Phthalates Dieth 1 hthalate USEPA 8270 GC/MS 20 k Dimeth I hthalate USEPA 8270 GC/MS 20 pgtkjz Butylbenzylphthalate USEPA 8270 GC/MS 20 kjz bis 2-Eth lhex Iphthalate USEPA 8270 GC/MS 20 Di-n-octylphthalate USEPA 8270 GC/MS 20 Or anatins Monobutyltin Krone et al, 1989 GC/MS SIM 10 Dibutyltin Krone et al. 1989 GC/MS SIM 10 Tributy1fin Krone et al. (1989) GC/MS SIM 10 gglkg %: percent ng/kg: nanogram per kilogram µg/kg: microgram per kilogram 1 g/ec: gram per cubic centimeter n/a: not applicable GC/MS: gas chromatography/mass spectrometry SIM: selected ion monitoring ' . EPA Method 1664 is substituted for EPA 413.2 NEWFIELDS May 2009 Upland Soil Evaluation Marina Park 2.3.3 QUALITY ASSURANCE/QUALITYCONTROL The QA objectives for chemical analysis conducted by the participating analytical laboratories are detailed in their Laboratory QA Manual(s). These objectives for accuracy and precision involve all aspects of the testing process, including the following: • Methods and SOPS • Calibration methods and frequency • Data analysis, validation, and reporting • Internal QC • Preventive maintenance • Procedures to ensure data accuracy and completeness Results of all laboratory QC analyses are reported with the final data. Any QC samples that failed to meet the specified QC criteria in the methodology or QAP were identified, and the corresponding data was appropriately qualified,in the final report. All QA/QC records for the various testing programs will be kept on file for review by regulatory agency personnel. 2.4 DATA REVIEW, MANAGEMENT, AND ANALYSIS 2.4.1 DATA REviEw All data were reviewed and verified by participating team laboratories to determine whether all data quality objectives had been met, and that appropriate corrective actions had been taken, when necessary. NewFields' QA Officer or her delegate was responsible for the final review of all data generated. RESULTS Sediment cores were collected from a total of 3 stations. Information on sample location, depth (bgs), targeted core length; penetration depth and length of core recovered are included in Table 3.1. The approximate location of each sediment core is provided in Figure 3. Sediment cores were generally characterized by sand with shell fragments. The boundary layer between the overlying pavement, fill, or sod was less than 6" bgs. Sediment was dominated by clean sand, with 91.5% sand and 0.11% TOC. No oil and grease or residual petroleum hydrocarbons were detected in the composite sample. The Atterburg test indicated that sediments were not plastic and would not hold their form. Metals were either undetected or detected just above the detection limits. All values were below the screening thresholds for conducting leachate testing (CCR Title 22 Section 4.5). Leachability testing is required when the concentration in the soils exceeds 10-times the STLC (Soluble Threshold Limit Concentration). None of the organic analytes, including chlorinated pesticides, PAHs, PCBs, or phthalates were detected in the composite sample. No additional leachate testing was required for the surface soils. NEWFIELDS i H I [1 I I I I I 11 I I I May 2009 Upland Soil Evaluation Marina Park I I 11 I I I I i' d I i I I I I 7 a 3 DISCUSSION As part of the planning process for Marina Park, NewFields LLC conducted an evaluation of surface soils from area of the proposed marina that is within the existing mobile home park. The objective of this sampling and analysis program was to characterize the soils for use as construction fill on site according to guidance provided by the upland testing manual and RWQCB guidance. Surface soils to a depth of 5 R. bgs were characterized as gravelly sand with shell fragments throughout the surface depth. Metals were either undetected or detected very near the detection limits. None of the organic constituents analyzed for this evaluation were detected. None of the priority pollutants were present at concentrations exceeding the screening threshold for Title 22 WET testing. The detection limit for Endrin and Toxaphene were above the screening concentration; however, the lOxSTLC concentration is below a detection limit is typically achievable in commercial laboratories. Based on this evaluation, the upland soils collected from the top five feet in the Marina Park Mobile Home Park would not qualify as hazardous waste under California State Code and should be acceptable as fill material. Table 3-1. Sample Log Data, Marina Park 2008 Site) Coordinates Depth Target Core Length l� Actual Core Length (ft) Comments tude .�..(ftbgs)'. MP-1 r36.484 5.322 5 4.5 4.5 Cores were dominated by sand and shell fragments- surface material (pavement, fill and tuo did not extend past 6" depth MP-25.336 5 4.5 4.5 MP-2 330 36.470 11755.306 5 4.5 4.5 I NEWFIELDS May 2009 Upland Soil Evaluation Marina Park Table 3.2 Concentrations in the Test Composite and Screening Threshold for Title 22 , Ton inn Analyte I MP Surface Soil Composite Threshold for Leachate Testing Conventionals Gravel % 5.3 NA Sand % 86.3 Silt N 5.5 Clay % 2.9 Total Organic Carbon % 0.108 Total Solids % 95,6 Oil and Grease m /k <207 U TRPH <207 U Atterburg Limits Not Plastic Metals (mg/kg) Arsenic As 2.2 50 Cadmium Cd <0.2 U 10 Chromium Cr 8.6 50 Copper Cu 2.4 250 Lead Pb 2 50 Mercury H <0.05 U 2 Nickel Ni 4.9 20 Selenium Se <0.5 U 10 Silver A <0.2 U 50 Zinc Zn 12 2500 Or anotins /k Tribut Itin <3.6 Dibut Itin 14 Monobut Itin. 5.5 PAHs Acena hth lane <4.7 Acena hthene <4.7 Fluorene <4.7 Phenanthrene <4.7 Anthracene <4.7 Fluoranthene <4.7 P rene <4.7 Benz a anthracene <4.7 Chrysene <4.7 Benzo b fluoranthene <4.7 Indeno 1,2,3-c,d rene <4.7 Dibenz a,h anthracene <4.7 Benzo ,h,i a lene <4.7 Benzo a rene <4.7 Total Detected PAHs <4.7 0 NEWFiEws I LI I I i I I I I I May 2009 Upland Soil Evaluation Marina Park 1 1 1 1 1 1 1 I 1 1 LJ d 1 1 1 1 i Table 3-2 Continued. Anal a Concentration Threshold Chlorinated Pesticides /k 2,4'-DDD <1.9 U 10 2,4'-DDE <1.9 U 10 2,4'-DDT <1.9 U 10 4,4'-DDD <1.9 U 10 4,4'-DDE <1.9 U 10 4,4'-DDT <1.9 U 10 Aldrin <0.97 U 1.4 BHC-al ha <0.97 U BHC-beta <0.97 U BHC-delta <0.97 U BHC- amma <0.97 U <0.97 U -Chlordane-alpha Chlordane -gamma <0.97 U cis-Nonachlor <1.9 U trans-Nonachlor <1.9 U Ox chlordane <1.9 U Total Detectable Chlordane 0 2.5 Dieldrin <1.9 U 8 Endosulfan Sulfate <1.9 U Endosulfan-I <0.97 U Endosulfan-11 <1.9 U Endrin <1.9 U 0.2 Endrin Aldehyde <1.9 U <0.98 Endrin Ketone <0.97 U <0.98 <0.97 U 4.7 -Heptachlor Heptachlor Epoxide <0.97 U 4.7 Methox chlor <9.7 U 100 Mirex <1.9 U 21 Toxa hene <97 0.5 PCB Aroclors /k Aroclor 1016 <20 U Aroclor 1242 <20 U Aroclor 1248 <20 U Aroclor 1254 <20 U Aroclor 1260 <20 U Aroclor 1221 <20 U Aroclor 1232 1 <20 U Phthalates /k Dimeth I hthalate <20 U Dieth I hthalate <20 U Di-n-But I hthalate <20 U But Ibenz I hthalate <20 U Bis 2-Eth Ihex Iphthalate <20 U Di-n-OOct I hthalate <20 U NEWFIELDS 1 May 2009 Upland Soil Evaluation Marina Park REFERENCES APHA/AW WA (American Public Health Association/American Water Works Association). 1998. Standard Methods for the Examination of Water and Wastewater (20th Edition). Edited by Lenore S. Clesceri, Arnold E. Greenberg and Andrew D. Eaton. APHAPhildelphia PA. CCR Title 22 Division 4.5 Environmental Health Standards for the Management of Hazardous Waste Chapter I I. Identification and Listing of Hazardous Waste Article 3. Characteristics of Hazardous Waste §66261.24 Characteristics of Toxicity. Krone, C.A., D.W. Brown, D.G. Burrows, R.G. Bogar, S.L. Chan, and U. Varanasi. 1989. A method for analysis of butyltin species in measurement of butyltins in sediment and English sole livers ' from Puget Sound. Marine Environmental Research 27:1-18. Plumb, R. H., Jr. 1981, Procedure for handling and chemical analysis of sediment and water samples. Technical Report EPA/CE-81-1. U.S. Environmental Protection Agency/U.S. Army Corps of Engineers Technical Committee on criteria for dredged and fill material, U.S. Army Waterways Experimental Station, Vicksburg, MS. TerraCosta Consulting Group, Inc. 2008. Geotechnical Investigation, Marina Park Project, Newport Beach, California. Prepared for City of Newport Beach, August. USEPA. 1994. Method 7471A: Mercury in Solid or Semisolid Waste. U.S. Environmental Protection Agency, Office of Solid Waste and Emergency Response, Washington, DC, 2001. SW-846 On-line, Test Methods for Evaluating Solid Waste, Physical/Chemical ' Methods. URL: <http://www.epa.gov/epaoswer/hazwaste/test/sw846.htm>. Offife of Solid Waste. USEPA/USACE 2003. Evaluation of Dredged Material Proposed for Disposal at Island, Nearshore, or Upland Confined Disposal factilities (Testing Manual). Department of the Army, USACE Research and Development Center. Vicksberg MS. ERDC/EL TR-3-1. January 2003. I I I I NEWFIELDS 11 Marina Park Ir LJ I I I t I I I LU, I 11 I 11 H I I G.5 - CORRESPONDENCE WITH EPA AND ACOE i. NEWFIELD5 I I P, Jorine Campopiano EPA Region IX Southern California Field Office 600 Wilshire Boulevard, Suite 1460 Los Angeles, CA 90017 Dan Swenson LAD Regulatory Division U.S. Army Corps of Engineers 915 Wilshire Blvd. Los Angeles, CA 90017 Dear Dan and Jorine: April 10, 2009 Brian Ross Allan Ota EPA Region IX Dredging & Sediment Management Team 75 Hawthorne Street San Francisco, CA 94105 Thank you for your comments on the Marina Park Sampling and Analysis Program report. We will make the necessary changes to the document and resubmit. We do have several questions regarding specific comments. r1. EPA has requested that the receiver beach(es) be identified at this time and that the grain size profile be included in this report. The responses from the USACE indicate that this does not necessarily need to be part of this report. We understand the grain size requirement for determining whether this material would be suitable for a specific receiver beach; however, it was my understanding that this was required later in the permitting process. Could you please clarify whether that element is required for this SAP report? I I 1' i! 2. The USACE indicated that the approved dredging depth will not be allowed to exceed the depth of refusal. We would like to provide some additional clarity to the report that addresses this issue. a. Samples were collected from seven stations within the project area below 0 ft. MLLW. The area represented by Area C is approximately 110 ft. by 307 ft. or 3,700 sq yards. Within that area we have collected a total of seven cores, four of which attained -14 ft. MLLW (project depth plus 2 ft. of overdredge). The remaining three cores attained -11.5 to -12.0 ft. MLLW. These latter cores had evidence of coarse sand in the core catcher that while sampled was not retained in the core tube. The four cores that attained dredged depth plus 2 foot of overdredge showed a clearly defined silt -to -sand boundary layer that occurs consistently across the area at approximately -12' MLLW; continuing as Coarse sand to depths beyond -14 MLLW. This is further supported in the remaining three cores by the refusal depth at -12' MLLW and evidence of sand in the catcher. The depth of the sand layer overlying the gravel is likely due historic dredging which cut the channel to that depth. b. Analysis of both the lower Area C composite, as well as the lower portions of the individual cores that did sample and retain the overdredge depth greater than -12 ft MLLW shows that this layer is free of chemical contamination and free of toxicity or bioaccumulation. c. We believe the four cores over the relatively small area of the project footprint support the conclusion that the sand layer occurs at approximately -12 ft. MLLW throughout the marine portion of the site. This is further supported by the refusal and sand observed in the cutter head in the remaining cores. This sand layer then continues to beyond project depth as evidenced by the four cores to -14 ft. MLLW and the stratigraphy observed in the upland cores. As noted in your comments, the underlying sands, generally representing the overdredge depth, have been shown to be free of chemical contamination. Based on the consistency of the observations throughout the proposed dredging area there is little reason to believe that the material within this overdredge depth is inconsistent with the surrounding area at comparable depths and we would respectfully request that the Corps approve the dredge depth to -14 ft. MLLW across the project area. 3. Both the EPA and USACE have identified the upper sections of the offshore portion of Area C as unsuitable for ocean disposal. The reason provided is due to mercury concentrations exceeding the ERM in the isolated silt layer from individual cores. The ERM value is an estimate of the potential for adverse ecological effects and is effective at predicting an effect —50% of the time it is exceeded (Wenning et al., 2005?). The effects based testing established by USEPA and USACE under the Ocean Testing Manual (to address paragraph 227.13(c) 40 CFR Ch. 1 (7-1-88 Edition)) is designed to establish whether site specific conditions support or reject whether measureable chemical contaminants 2 I re at concentrations that produce adverse biological effects as measured by lioassays and bioaccumulation tests; predicting a potential for adverse effects due `to disposal. We would like to provide additional information for your consideration. a. The upper sections of all of the cores within Area C were tested as a composite for chemical analysis, toxicity, and bioaccumulation. As required by the Ocean Testing Manual, the toxicity testing and bioaccumulation tests were conducted to evaluate the bioavailability of any contaminants of potential concern that have been observed in the bulk sediment at concentrations that may predict biological effects. No toxicity was observed in the toxicity tests for both benthic and water -column ' species. Furthermore, Hg concentrations in the tissues exposed to this sediment were at or slightly above the detection limits, with a mean concentration of 0.011 mg/kg. This is well below any established threshold concentrations (FDA: 1.0 mg/kg; EPA Region 10 (proposed): 0.11 mg/kg for fish and shellfish; HHRA USEPA value of 0.3 mg/kg wet weight for fish consumption). Based on the Tier III analysis, while there is mercury in the sediment, it does not appear to be in a bioavailable form. In fact the uptake into tissues is at least an order of magnitude lower than the tissue guidance values that have been established for both human and ecological risk. o. While the sediment mercury concentrations exceed the ER-M M concentration, the subsequent toxicity tests and the bioaccumulation tests that evaluate the site specific availability of any contaminants of potential ecological concern indicate that this is not in a bioavailable form and does not predict a potential for eliciting adverse ecological effects in the receiving environment. The City would request that EPA and the USACE reconsider their decision to exclude the surface sediments from disposal at the LA-3 disposal site based on the lack of identified potential for adverse ecological effects. IThank you for your consideration. Sincerely, William Gardiner Partner/Senior Scientist NewFields, LLC. 1. F ' Marina Park I G.6 - SITE ASSESSSMENT SCE PARCEL I C I ' SITE ASSESSMENT REPORT MARINA PARK, 1516 WEST BALBOA BOULEVARD NEWPORT BEACH, CALIFORNIA Prepared For: 1 CITY OF NEWPORT BEACH 1 3300 Newport Boulevard ' Newport Beach, California 92663 ' Project No. 602497-003 September 22, 2009 1 Leighton Consulting, Inc. ' A LEIGHTON GROUP COMPANY ' Leighton Consulting, Inc. A LEIGHTON GROUP COMPANY ' September 22, 2009 ' Project No. 602497-003 ' To: City of Newport Beach Public Works Department 3300 Newport Boulevard Newport Beach, California 92663 Attention: Mr. Mark Reader Subject: Site Assessment Report, Marina Park, 1516 West Balboa Boulevard, Newport ' Beach, California ' INTRODUCTION ' Leighton Consulting, Inc., (Leighton Consulting) is pleased to present this Site Assessment Report summarizing environmental conditions in association with the property located at 1516 West Balboa Boulevard, in Newport Beach, California (referred to as the "Subject Property", ' Figure 1 — Site Location Map). This report is based on Leighton Consulting's "Revised Proposal to Perform Additional Site Assessment, Marina Park, 1516 West Balboa Boulevard, Newport ' Beach, California", dated July 17, 2009 (Leighton Consulting, 2009a). References are presented in Appendix A. SITE BACKGROUND ' The subject property is a rectangular parcel that is approximately 5,360 square feet in size located on the Balboa Peninsula, north of West Balboa Boulevard between 15`h and 16`h Streets in Newport Beach, California (Figure 1, Site Location Map). The subject property was formerly ' used as an electrical substation by Southern California Edison from at least 1929 to 2008 (Figure 2, Site Aerial Photograph). The control room and the transformers were removed in 2008 and ' the subject property is currently vacant. The site is proposed to be used as a parking lot for the Marina Park development. 17781 Cowan ■ Irvine, CA 92614-6009 I 949.250.1421 ■ Fax 949.250.1114 ■www.leightonconsulting.COm . r =4211M Leighton Consulting conducted a Phase I and Phase II ESA for the Subject Property to assess for potential subsurface impacts from equipment and hazardous substances, such as PCB -containing oil, associated with the former electrical substation (Leighton Consulting, 2009b). Soil sample locations were selected based on aerial photographs, a site plan provided by Southern California Edison depicting the locations of the former equipment, and a discussion with Mr. Bernard Rapan regarding the location of equipment that may have contained PCBs. On March 10, 2009, Leighton Consulting advanced five hand auger borings at the subject property to a maximum depth of 2 feet bgs and collected from each location a soil sample at a depth of approximately 0.5 feet bgs and the second between 1.3 and 2.0 feet bgs. Soil conditions were very gravelly with cobbles and refusal was encountered in boring B2, B3, and B4 at 1.5, 1.3, and 1.8 feet bgs, respectively, and soil samples were obtained from the maximum depth reached at these locations. All of the soil samples (10 total) were analyzed for total petroleum hydrocarbons — carbon chain (TPH-cc, C8-C40), by EPA 8015B and for PCBs by EPA Method 8082. Based on the initial results, the three samples with the highest TPH-cc results were also analyzed for semi -volatile organic compounds (SVOCs), and the three samples with the highest results in the C8-CIO range were also analyzed for volatile organic compounds (VOCs) and TPH as gasoline (TPH-g). TPH-cc was detected in nine of the ten samples at concentrations ranging from 16 milligrams per kilogram (mg/kg) to 110 mg/kg. TPH-g (C4-C12) was not detected above laboratory limits in the three samples analyzed. The soil screening levels established by the RWQCB are 100 mg/kg for gasoline (C4-C12) and diesel (C13-C22), and 1,000 mg/kg for heavy hydrocarbons (C23- C32) (CRWQCB,1996). Aroclor 1248, a PCB, was detected in one sample, B5-0.5 at 0.048 mg/kg. In addition, Aroclor 1254 was detected in four of the ten samples from 0.022 mg/kg to 92 mg/kg. The Industrial Regional Screening Level (RSL-I) for Aroclor 1248 and Aroclor 1254 is 0.74 mg/kg for each (USEPA,2008). No additional PCBs were detected at the subject property, No VOCs or SVOCs were detected in the samples analyzed. Based on the results of the initial Phase II ESA, Leighton Consulting recommended that additional samples should be obtained at the subject property to assess the vertical and lateral impacts to soil, and to assess potential impacts to groundwater. The boring locations and summary of the detected analytes from the initial Phase lI ESA, and this subsequent Site Assessment, are shown on Figure 3, Site Plan and Laboratory Data Summary. The laboratory report and results of the laboratory analysis are included as Appendix B and Table 1, respectively. 46 - z - Leighton 602497-003 I H 1 LJ I� SUMMARY OF WORK CONDUCTED Boring Location Mark Out and Underground Service Alert (USA) Leighton Consulting delineated the site with white paint as appropriate for USA identification. USA was then contacted at least 48 hours prior to the commencement of field activities to designate underground utility locations. Health and Safety Plan A Site Specific Health and Safety Plan (HSP) was prepared for work to be performed at the site. The HSP complied with the Occupational Safety and Health Administration (OSHA) regulation 29 CFR 1910.120. All onsite personnel signed the HSP acknowledging acceptance. The document was kept onsite at all times during the field activities. Environmental Borings On August 3, 2009, Leighton observed and directed field activities during the advancement of 8 direct -push soil borings by Millennium Environmental, Inc. (Millennium). Millennium's hydraulically -driven drilling rods were 1.5 inches in diameter and constructed of steel with a hardened drop-off steel tip. The sampling tip was decontaminated between each sample location by triple washing in water with a phosphate free detergent, water, and deionized water. Soil borings were advanced to a total depth of 8 feet bgs and groundwater was encountered between 5.5 to 7 feet bgs. Soil samples were obtained in acetate sleeves at 2 feet bgs, 5 feet bgs and/or the soil/groundwater interface. In addition, a grab groundwater sample was obtained from each location. The table below summarizes the sample location depth: Boring Depth to Groundwater (feet bgs) Sample Depth (feet bgs) B6 7 2, 5, 7, GW B7 7 2, 5, 7, GW B8 5.9 2, 5, GW, GW duplicate B9 6 2, 6, GW B 10 6 2, 6, GW 1311 5 2, 5, GW B12 6 2, 6, GW B13 5.5 2, 5, GW I 3 Leighton 602497-003 Soil sample headspace readings were recorded with a photoionization detector (PID). The soil samples retained from each boring were immediately placed in an ice -cooled chest for temporary storage, and transported to Advanced Technology Laboratories (ATL) in Signal Hill, a State of California Certified laboratory for chemical analysis. The soil boring logs are included in Appendix C. Laboratory Analyses A total of 27 soil and groundwater samples from the 8 boring locations were submitted to ATL for analysis. Samples were analyzed for one or more of the following constituents: • TPH-g by EPA Method 8015b (C4-C12) • TPH-cc by EPA Method 8015b (C8-C40) • PCBs by EPA Method 8082 • VOCs by EPA Method 8260b • SVOCs by EPA Method 8270c Standard laboratory quality control procedures were conducted and included the running of blanks, matrix -spike samples and matrix -spike duplicate samples. The laboratory report and results of the laboratory analysis are included as Appendix B and Table 1, respectively. ENVIRONMENTAL INVESTIGATION RESULTS Hvdrooeology and Geolov According to the Soil Survey of Orange County and Western Part of Riverside County, the Site is located within the soil type of "beaches." Beaches is described as sandy, gravelly, or cobbly coastal shores that are washed and rewashed by tidal and wave action (United States Department of Agriculture, 1978). Soils encountered during the subsurface investigation at the Subject Property consisted of silt, cobbly silt, silty sand, poorly graded sand, and cobbly sand to the total depth explored of 8 feet bgs. Groundwater was encountered between 5.5 to 7 feet bgs. The Pacific Ocean is located 650 feet to the southwest of the Subject Property and a marina with boat slips in the Newport Channel of Newport Bay is located approximately 180 feet to the northeast of the Subject Property; therefore, the groundwater gradient is expected to be variable. 4 Leighton 602497-003 I 1 I 1 1 L _J II i 1 Laboratory Analysis of Soil Samples Total petroleum hydrocarbons — carbon chain (TPH-cc, C8-C40), was not detected the soil samples analyzed, with the exception of B7-5' at a concentration of 41 mg/kg. TPH-cc was not detected in the deeper soil sample obtained at B7-7' or in the groundwater from Boring B7. During the previous investigation consisting of Borings 131-136, TPH-cc had been detected at a concentration from 16 mg/kg to 110 mg/kg in nine of the ten soil samples. The soil screening levels established by the RWQCB are 100 mg/kg for gasoline (C4-C12) and diesel (C13-C22), and 1,000 mg/kg for heavy hydrocarbons (C23-C32) (CRWQCB, 1996). Two of the samples contained TPH-cc over 100 mg/kg, B1-0.5' and 133-1.3' at 110 mg/kg each; however, approximately half of the TPH was in the heavy hydrocarbon range from C28-C40. The PCB Aroclor 1254 was detected in four of the samples analyzed: B7-2' at 0.36 mg/kg, B7-5' at 0.059 mg/kg, B9-2.0' at 0.35 mg/kg, and B10-2' at 0.28 mg/kg. The PCB Aroclor 1242 was detected in two samples analyzed: 137-7.0' at 0.036 mg/kg and B12-2.0' at 0.028 mg/kg. PCBs were not detected in the remaining soil samples analyzed. In the previous investigation consisting of Borings 131-136, the PCB Aroclor 1248, was detected in one sample, 135-0.5 at 0.048 mg/kg. In addition, Aroclor 1254 was detected in four of the ten samples from 0.022 mg/kg to 92 mg/kg. The Residential and Industrial Regional Screening Level (RSL-R and RSL-I) for Aroclor 1242, 1248, and 1254 is 0.22 mg/kg and 0.74 mg/kg for each, respecitvely (USEPA, 2009). TPH-g, VOCs, and SVOCs were not detected above the laboratory detection limits in the soil samples analyzed, with the exception that several SVOCs were detected in 137-5.0 feet bgs, including benzo(a)anthracene at 0.44 mg/kg, chrysene at 0.43 mg/kg, fluoranthene at 0.47 mg/kg, phenanthrene at 0.46 mg/kg, and phenanthrene at 0.76 mg/kg. All of the SVOCs were below their corresponding RSL-I, and all were below their corresponding RSL-R, with the exception of benzo(a)anthracene (the RSL-R is 0.15 mg/kg). TPH-g, TPH-cc, and PCBs were not detected in any of the groundwater samples, with the exception that TPH-cc was detected in the groundwater from B6 at the northwest corner of the Subject Property at a concentration of 0.68 milligrams per liter (mg/L). The analytical results are summarized in Table 1, located at the rear of the report text. The laboratory reports are included as Appendix B. A soil laboratory data map that summarizes the detected analytes (TPH-cc and PCBs) is included as Figure 3. 41 s Leighton 602497-003 , CONCLUSIONS AND RECOMMENDATIONS The PCB Aroclor 1254 was detected above the RSL-I of 0.78 mg/kg in two soil samples, B1-0.5' at 4.2 mg/kg and 135-2.0' at 92 mg/kg. Additionally, Aroclor 1254 was detected above the RSL- R of 0.22 mg/kg in three soil samples, B7-2,0' at 0.36 mg/kg, B9-2.0' at 0.35 mg/kg, and B 10- 2.0 mg/kg. In addition, the SVOC benzo(a)anthracene was detected above the RSL-R of 0.15 mg/kg in one soil sample, B7-5 at 0.44 mg/kg. The California Regional Water Quality Control Board (CRWQCB) has developed maximum soil screening levels for Total Petroleum Hydrocarbons (TPH) above drinking water aquifers. Since there is no adequate measure of risk or toxicity of TPH, the screening levels for TPH is based on the carbon range numbers of the TPH (CRWQCB 1996, Table 4-1). The maximum screening levels for soil located 0 to 20 feet above groundwater is as follows: C4 — C12 (gasoline range): 100 mg/kg, C13 — C22 (diesel range): 100 mg/kg, C23 - C32 (oil range): 1,000 mg/kg. These ranges reflect the mobility of the materials; the shorter carbon chain TPH moves more easily in soil than the longer carbon -chain. Soil with TPH detected below the soil screening levels with no additional hazardous constituents present generally may remain onsite without posing a threat to the groundwater or human health. Two of the samples contained TPH-cc over 100 mg/kg, B1-0.5' and B3-1.3' at 110 mg/kg each; however, approximately half of the TPH was in the heavy hydrocarbon range from C28-C40. Based on the laboratory results, the detected levels of TPH in the samples analyzed were below the maximum soil screening levels established by the CRWQCB (CRWQCB, 1996). In addition, the Subject Property is located adjacent to Newport Bay and the groundwater is expected to be brackish and not suitable for drinking water. The TPH-impacted soil is not expected to be a threat to groundwater or human health. The Subject Property is reportedly to be developed with an asphalt paved parking lot for the Marina Park project. Because the proposed development is for commercial purposes, the Site should be remediated to at least industrial standards; however, it is recommended that the Site be remediated to the more conservative residential standards. Leighton Consulting recommends that areas where soil contamination has been detected above the residential Regional Screening Level (RSL-R) be remediated by excavation and disposal to an appropriate facility. The approximate area and depth recommended for excavation is depicted on Figure 3. A depth of approximately 5 feet bgs is recommended for the area with the exception of B7, where a depth of 6 feet bgs is recommended. Confirmation soil samples should be taken to ensure that the RSL-R target goals have been met, and confirmation samples may limit or expand the area and depth required for excavation to meet these goals. u 1 CI i I t 40, Leighton ' ' 602497-003 ' It is Leighton Consulting's opinion that the low levels of TPH-cc detected in the groundwater ' from the northwest corner of the subject property appears to be from an offsite source and is not considered likely to be a threat to human health or the environment or to require mitigation. The offsite source may possibly be from the use of Newport Harbor for boating and marina purposes ' or from a former gasoline release to soil and groundwater by a Mobil gas station located at 1500 Balboa Boulevard located approximately 90 feet to the east of the Subject Property. ' If the City of Newport Beach desires a closure letter from a regulatory agency, this report should be submitted to the Orange County Health Care Agency (OCHCA) and an agreement for the voluntary oversight program should be requested. If oversight is requested, the OCHCA requires an approved Remedial Action Plan (RAP) and a Workplan prior to mitigation. i 1 1 We appreciate the opportunity to serve the City of Newport Beach. Please do not hesitate to call the undersigned at (949)-681-4208, if you have any questions regarding the findings of this report. Respectfully submitted, LEIGHTON CONSULTING, INC. Meredith Church, PG 8326 Project Geologist Senior Reviewer: Richard Williams, PG Attachments: Figure 1— Site Location Map Figure 2 — Site Aerial Photograph Figure 3 — Site Plan and Laboratory Data Summary ' (fable 1— Soil Analytical Results Summary Appendix A — References ' Appendix B — Laboratory Analytical Results Appendix C — Soil Boring Logs ' Distribution:(2 + 4 cds) Addressee !I -7- MERMTH D. CHURCH No.8326 Exp.'! J ♦# Leighton f�� Trailer t I MAVP ti J = _Park -, �✓ 1 �r L 2,000 4,000 + SJ ter SCALE FEET r C� Base Map: U5G5 Topographic Map.. Newport Beach Quadrangle, D/ California 7H series, Orange County. 1979 /� 1 a t��-� �,� ;'Tt1 I � •r ,�� ace -i�. o � �7 $ r _ y`' `j t �} marial�- ' r _t Ta�am H .... •. e ✓ {�tt Sch I .� rty Ban. Lv aao�sr .. O 4 q� Lln da i �i 'sue ' 4 are K p' y Lgl : �� ,. vr� Light, Harbor 1. 1' .- en:y \ "= 3.3 ILight Parking A A ea :'Les Arenas r _ �4 J�L,gnl Collins l Parkr w�. O J NEWPORT BEACH—_Ilr-4" p aaY1, ` I'1'Gart Park Approximate Site 8eacy Boundary Balbo B a ra 8P P any Project 1516 West Balboa Boulevard SITE LOCATION 602497-00.003 Newport Beach, California MAP Date 4 August2009 Figure 1 "GaMmieslral,onWrcGlSTem{Ye1pt1NEVJ GDT s al-ocationMal, ri II II II 10anlprolTPH-cc I PCBs 1 B6-5.0 I <10 1 <0.033 86-7.0 I <10 I NA IB6-GWI 0.68 <0.005 le Sample TPH-cc A 294r 131-0.5 110 4.2 B1-2.0 <10 70.016 Sample PCBs Sample TPH-cc Aroclor Sample ,TPH-cc Aroclor Aroclor ID TPH-cc ID 1254 ID B7-2.0 <10 1242 <16 1254 0.36 B2-0.5 55 <0.033 133-0.5 59 <0.016 B2-1.5 1 78 <0.033 63-1.3 1 110 0.022 B7-5.0* 41 <16 0.059 • B6 B7-7.0 <10 0.036 <16 67-GW <0.20 <0.0005 <0.0005 - -5' bgs - ' I 11 KV Switchrack O / 81 -CrJ /�•� �� Sample TPH-cc Aroclor 11 ID 1254 B10-2.0 I <10 1 0.28 B10-6.0 I <10 1 <16 �n B10-GW <0.20 <0.00 5 o- _ 0 S ) n mple TPH-cc Aroclor Aroclor o �. 10 OA ti ID 1254 1248 C -0.5 40 <0.016 0.04 v B5 0 m'a IZ -2.0 28 92 <0.016 ' m • / 0 t ; B9 / 0 .c a imple TPH-cc Aroclor a O Q 13 ID 1254 w 0 rp m )-2.0 <10 0.35 1-6.0 <10 <16 )-GW <0.20 0.0005 Q1 CD x w OF m B8• GE. Co. 3 - 500 KVA , 1111A KV B4 :1).111/4 No. 1 BANK A.C. Co. 4-1000 KVA I KV Limits and depth recommended for Excavation SamplelTPH-cc I PCBs ID B8-5.0 I <10 1 <0.033 1B8-Dup1 <0.22 1<0.00051 Sample TPH-cc Aroclor ID 1254 B4-0.5 62 <0.016 134-1.8 16 1 0.028 • 611 Sample TPH-cc PCBs ID B11-2.0 <10 <0.033 611-5.0 <10 1 <0.033 611-GW 70.20 <0.0005 D LEGEND C Soil Boring Location and ID a` �1 B1-85 advanced 3/10/2009 Sample Aroclor ID TPH-cc 1242 B12-2.0 <10 0.028 B12-6.0 <10 <16 B6-B13 advanced 8/3/2009 mg/kg Milligrams per Kilogram PCBs Polychlorinated Biphenyls.Aruclor 1242, 1248, and 1254 are PCBs. + RSL-I Regional Screening Levei- RSL-R Industrial (1), Residential (R) - B13 TPH-cc Total Petroleum Hydrocarbons, • Carbon Chain (C8-C40) x Semi -volatile organic compounds detected. Benzo(a)anhracene exceeded RSL-R of 0.15 mg/kg Balboa 131wd ormg/L (water) All rreported in mg/kg (soil) Red color indicates detection -above NORTH the RSL-I of 0.74 mg/kg and the RSL-R of 0.22 mg/kg forAroclor Note: All structures have been removed from the site and it is presently vacant. 1242/124811264. Modified from Southern California Edison Map, 28067-4, Master Index: M506, Newport Beach Substation Electrical Equipment Plot Plan, Revision dated July 27, 1960. Note indicated that oil in electrical equipment was mineral oil. SITE PLAN AND 4W, Project No. 602497-003 LABORATORY DATA scale 1"=15' SUMMARY Engr./BMDC Draftedd By MDC 1516 West Balboa Blvd Leighton Consulting, Inc. Date September, 2009 Newport Beach, California A LEIGHTON GROUP COMPANY Figure x i B12 Sample TPH-cc PCBs ID 613-2.0 NA <0.033 B13-5.0 NA <0.033 i I 11 TABLE 1: SUMMARY OF SOIL LABORATORY RESULTS manna eam, lo7b B41.8 03/10/09 <70 <10 16 <10 <10 16 NA <0.016 <0.033 <0.016 <0.016 <0.016 0.016 <0 016 <0.016 10.016 NA NA NA NA NA NA NAI NA NA NA NA NA NA NA NA NA NA NA NA West 13alD0a BUWeVara. Newpon DUaUlh .auw.,..o SBM to Results m /k BS-0.5 BS•ZO 86-20 B6d.0 86-7.0 H7-ZO 87-6.0 87 7.0 BS•20 BBS.O B9•ZO 89-0.0 610-ZO 810 6.0 B71-20 8715.0 812.20 " 872-6.0 B73•ZO' 67 03/10/09 03/10/09 DBl03/09 08103/09 08103109 08/03l09 08f03/09 OB/03l09 08f03/09 08/03/09 08/03l09 08103/09 08/03/09 08/03/09 08103109 08/03/09 08103f09 08/03/09 08/03/09 08/03/09 <t0 <10 < <t0 <10 <70 <10 <10 <10 <10 <10 <10 <10 <1U <10 <10 <10 <t0 <10 26 <10 <70 10 <10 <10 <10 <10 <10 <70 <70 <10 <10 <10 1U <10 <10 <10 <10 2g < <70 <7p 21 <10 <70 <10 <10 <10 a <70 70 <10 <10 10 <10 10 <10 tU ` <70 13 <10 <10 <10 <10 <70 <10 <t0 <10 <10 <10 <10 Ap <10 <10 <10 <10 10 401 28 < <70 41 <1 0 <1 0 <1 0 1•U NA NA <1.0 <7 0 NA <1.0 <7-0 NA <7.0 <0.07f < <0016 <0.016 <0.016 <0016 <0.016 <0016 <0.076 <0.016 <0.016 <p.016 NA <p.016 <0016 <p 016 <0076 c0.016 <0.016 <0.076 c0.016 0033 <0033 <0033 <0033 <0.033 <0033 <0.03< <0.033 <0 033 <p 033 <0 033 NA <0 016 <0.016 <0.016 <0 016 <p.016 <0.016 <0.016 <0 016 <0 016 <0.016 <0 016 �0 028 <0.016 <0 016 <0 till <0.016 <0.016 W.016 <0.016 <0.016 <0016 0.036 <0076 <0 Ot6 <0.016 <0.016 <0.016 <0016 <0.016 ep Ot6 <p.016 <0.016 <0016 <0.011 <0.048 <0 016 <p 016 0 016 NA <0 016 <0 016 <0 016 < <0.016 <0.016 <0-07 0.048 <0.016 <0 016 <0 016 NA <0.016 <0.016 <0.016 <0 076 <0 016 < p•Y8 <0.016 <0.016 <0 016 0.016 <0.01 <0.018 <0.076 < 92.0 <0 016 <0 016 0.36 <U 076 <0.016 <0.076 <0 016 <0 016 <0.016 <0 016 <0 016 <0.016 <0 016 <0.016 <0 016 <0 018 <0-001 <0.076 0.016 < <0.016 <0 016 <0.016 0 016 <0.016 <0 016 0- <0.0161 <0016 <0.016 <0.016 NA <0016 <0.016 <0.018 <p 076 <0.016 <0016 <0.016 <0.016 <0.016 <0.016 <0076 <0.016 <0.016 <0.016 <0016 <0016 NA <0.016 <0.016 <0016 <0.076 <0.016 � � � N I,Iq Nq <0.005 NA NA NA NA N NA NA NA <0005 NA <0.005 NA NA NA NA NA <0.005 NA NA IJA h NA NA NA <p 005 NA e0.005 NA NA NA NA NA NA NA NA NA NA NA NA <0005 NA <0.005 NA NA NA <0.005 NA NA NA NA t' NA NA NA NA NA NA NA NA NA <0.005 NA <0005 NA NA NA Nq <O.OpS NA NA NA NA NA <0005 NA <0005 NA NA NA NA NA i <033 <0.33 NA NA NA NA `D' tJA NA NA NA NA <033 NA Nq Nq <0.33 NA NA PIA NA <033 NA <0.33 <033 NA NA NA Nq <0.33 NA NA tU NA NA NA NA <033 NA <0.33 0.44 NA NA NA NA <0.33 NA NA I'1A NA NA NA <0.33 NA NA NA NA NA NA NA <033 NA <0.33 Nq <p,33 NA NA <033 NA <033 <033 NA NA NA < 33 NA NA �' NA NA NA Nq <033 NA <033 <033 NA NA NA NA NA 0. NA NA NA NA NA NA <033 NA <033 0.43 NA NA NA NA NA <0.33 NA NA NA NA NA NA NA <033 NA <0.33 <0.33 NA NA NA NA NA <0: NA tJq NA NA NA NA NA NA NA <033 NA <0.33 0.47 NA NA NA NA NA <033 NA N%r NA NA NA NA NA NA NA <0.33 NA <0.33 <033 NA NA Np NA < 33 NA NA NA NA NA NA 0 NA NA NA NA <033 NA <033 <0.33 NA NA NA NA NA <033 N/' Np NA NA NA NA NA NA <033 NA <033 NANA NA NA NA <p 33 NA <033 0.46 NA NA NA <033 Np NA NA NA NA NA <0.33 NA <0.33 0.76 NA NA t�l <033 NA t1A NA NA NA NANL <033 NA <0.33 <0.33 NA NA NA NA EPA Method 80158 Anaryte Total Petroleum H rocerhans PH C8-C70 C70.C18 C28-C361000 C36-C40 TPH as CasoiineTo H Cq.Q7p Poll chlorinated Bi hen s PCBs Are or 1016 ( Arocior 1232 Arodor 1232 AroGor 1242 A ctor 1254 A ctor 1254 AroGor 1260 Arocior1262 '4roGor 1268 SSLS mglkg) Data Sam CS-C40 100 100 1 N NL 100 NL NL NL NL NL NL NL RSL42 (mg/kg) Ie Collected NL NL NL NL NL NL 39 0.17 0.22 022 0 22 NL NL RSL4 (m NL NL NL NL NL NL 27 0.62 0.74 0.74 0.74 NL NL B1-0.5 03/10/09 18 <10 32 33 23 110 NA <0.016 <0 016 <0.016 <0 016 <0.016 <0016 <0.016 B7- . 2 0 03/10/09 <10 <10 <10 <10 <10 <10 NA <0.016 <0 016 <0.016 <0 016 <0.016 0.016 <0.016 <0.016 B2-0.5 03/10/09 55 <10 <10 <10 <10 55 <7 0 <0016 <0016 <0016 <0 016 <0 016 <0 016 <0016 <0016 B2-1.5 03110/09 52 <10 12 13 <70 78 <7.0 <0.076 <0.033 <0.016 0.016 <0.016 <0.016 <0.016 <0.016 <0016 B3-0S 03l10f09 34 <10 11 15 <59 59 NA <0.016 <0 033 <0 016 <0.016 <0.016 <0.016 <0 016 <0.016 <0016 B3-1.3 03/10/09 42 <70 16 26 20 110 <t O <0016 <0 033 <0.016 <0 016 <0.016 0.022 <0.016 <0.016 <0.016 B4-0S 03/10/09 32 <10 14 16 <62 62 NA <0016 <0.033 <0.016 100151 <0.016 <0 016 <0.016 <0.016 80158 8082 82606/ 5035 8270C Volatile O anic Com ounds OCs Benzene 0011 -Elth benzene 0.7 Toluene 0.2 Total X lenes 1.75 All Others NL Semi -Volatile O anic Com ounds SVOCs & Pol Acena hihene NL Anlhracene NL Benzoaanlhracene NL Benzo Ouoranthene NL eenzo Ouoranihene NL 1.7 5.7 5000 600 NL aromatic 3,400 17,000 0.15 0.15 1.5 0.015 15 0.015 2,300 2,300 0.15 3.9 NL 1,700 NL 5.6 29.0 46.000 2,600 NL H dmprbons 33,OOD 170,000 2.1 2.1E 21 021 210 0.213 22.0003 22,0003 2.13 203 NL3 17,0003 NL NA NA NA NA NA PAHs <0.33 <0.33 <0.33 3 NA NA NA NA NA I NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0005 <p.p05 <p.0p5 <0015 <005 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0.005 <0005 <0.005 <0015 <0.05 <033 <033 <0,33 <033 <0.33 <0.33 <0,33 <0.33 <0.33 <0.33 <0.33 <033 <0.33 <033 <0.33 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0.005 <0.005 <0.005 <0075 <0.05 <033 <0.33 e033 <033 <033 < <0.33 <033 <033 <033 <0.33 <p 33 <033 e0.33 <0.33 .-<0.0161 NA NA NA NA NA NA MAI NAI NA NA NA NA NA NA NA NA NA NA NA Benzoapyrene NL Ch ems NL Di benza,h]anlhracene NL Fluorenlhene NL Fluorene NL Intleno 1,2,3c.d ne NL Naphthalene NL Pyreno lhrena NL rene All ONers NL ' mglxg• milligrams per kilogram or parts per million - lab results for PCBs,VOCs, and SVOCs have been converted tram micrograms per kilogram ygfkg) RSL-R: Residential Regional Screening Level, United States Environmental Protection Agency (USEPA) Region 9, Apnl 2009 RSL-I: Industrial Regional Screening Level, United Stales Environmental Protection Agency (USEPA) Region 9, Apn12009 Samples depicted in red equal or exceed the corresponding RSL-R or the RSL-1 SSI-s: Soil Screening Levels. RWQCB, 1996. Table 4-1, Maximim Soil Screening Levels for TPH and BTEX above Drinking Water Aquifers <0 33: Less than laboratory detection limit NA: Not analyzed NL: Not Listed on applicable regulatory table B13-2.0 and B13-5 0 were analyzed 7 days past the 14 day hold time. This is not expected to alter the conclusions or recommendations of the report 1 11 1 1 I r � I J � APPENDIX A 1 i F1 I I I I I 602497-003 li I II APPENDIX A References California Regional Water Quality Control Board (CRWQCB), 1996, Interim Site Assessment and Cleanup Guidebook, dated May 1996. Leighton Consulting, Inc., 2009a, Revised Proposal to Perform Additional Site Assessment, Marina Park, 1516 West Balboa Boulevard, Newport Beach, California, Proposal No. P60101173, dated July 17, 2009. ' Leighton Consulting, Inc., 2009b, Phase I and Phase II Environmental Site Assessment, Marina Park, 1516 West Balboa Boulevard, Newport Beach, California, Project No. 602497-001, dated April 3, 2009. I I II I! I II United States Department of Agriculture, 1978, Soil Conservation Service and Forest Service, Soil Survey of Orange County and Western Part Riverside County, California, dated September 1978. United States Environmental Protection Agency (USEPA). Regional Screening Levels (RSL) for Chemical Contaminants at Superfund Sites. RSL Table Update. April 2009. A-1 u I �i 7 II ';� � APPENDIX B I i 1 I 1. I I I 1 't, ►ccoq D'yc0 o,�EC `W March 26, 2009 x U � Meredith Church ELAP No.:1838 iLeighton Consulting, Inc. NELAP No.:02107CA 17781 Cowan Street NEVADA.: CA-401 1 17 lJ I L✓ I7I I L� I I it J 7 L I f� IJ Irvine, CA 92614 TEL: (949)681-4208 FAX: (949) 757-7230 RE: Newport -SCE Parcel, 602497-001 Attention: Meredith Church CSDLAC No.:10196 Workorder No.: 104410 Enclosed are the results for sample(s) received on March 10, 2009 by Advanced Technology Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications. Thank you for the opportunity to service the needs of your company. Please feet free to call me at (562)989-4045 if I can be of further assistance to your company. Sincerely, Eddie F. odriguez Laborat ry Director The cover letter is an integral part of this analytical report. This Laboratory Report cannot be reproduced in part or in its entirety without written permission from the client and Advanced Technology Laboratories. ' Advanced Technology 3275 Walnut Avenue 'Stgita Hi[1, CA 90755 Tel: 562 989-4045 Fax: 562 989-4040 Laboratories ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mor-09 CLIENT: Leighton Consulting, Inc, Client Sample ID: B1-0.5 Lob Order: 104410 Collection Date: 3/10/2009 11:10:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-001 Analyses Result PQL Qua[ Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GCB 090317A OC Batch: 53868 PrepDate: 3/16/2009 Analyst: CBR TIR Hydrocarbons: CS-C110 18 10 mg/Kg 1 3/17/1909 04:19 PM T/R Hydrocarbons: CIO-C18 NO 10 mg/Kg 1 3/17/1909 04:19 PM TIR Hydrocarbons: C18-C28 32 10 mg/Kg 1 3/17/1909 04:19 PM T/R Hydrocarbons: C28-C36 33 10 mg/Kg 1 3/17/1909 04:19 PM TIR Hydrocarbons: C36-C40 23 10 mg/Kg 1 3/1711909 04:19 PM TIR Hydrocarbons: C8-C40 Total 110 10 mglKg 1 3/17/1909 04:19 PM Sum p-Terphenyl 113 57-144 %REC 1 3/17/1909 04:19 PM PCBS BY GC/ECD EPA 3550E EPA 8082 RunID: GC5 090316E OC Batch: 63874 PrepDate: 3/1612009 Analyst: HL Aroclor 1016 NO 16 pg/Kg 1 311612009 09:01 PM Aroclor 1221 NO 33 pg/Kg 1 3/16/2009 09:01 PM Aroclor 1232 NO 16 pg/Kg 1 3/16/2009 09:01 PM Aroclor 1242 ND 16 pg/Kg 1 3/1612009 09:01 PM Aroclor1248 NO 16 pg/Kg 1 3/16/2009 09:01 PM Aroclor 1254 4200 330 pglKg 20 3117/200910:25 AM Arocor 1260 NO 16 pg/Kg 1 3/10/2009 09:01 PM Aroclor 1262 NO 18 pg/Kg 1 3/16/2009 09:01 PM Aroclor 1268 NO 16 pg/Kg 1 3/1612009 09:01 PM Surn Decachlorobiphenyl 77.6 30-124 %REC 1 3/16/2009 09:01 PM SurnDecachlorobiphenyl 104 30-124 %REC 20 3/17/2009 10:25 AM Surr: Telrachloro-m-xylene 82,3 40.118 %REC 1 3/16/2009 09:01 PM Sum Tetrachloro-m-xylene 71.6 40.118 %REC 20 3/17/200910:25 AM SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunID: MS6_090320A OC Balch: 54042 PrepDate: 312012009 Analyst: DMP 1,2,4 Tdchlorobenzene NO 330 pglKg 1 31241200912AB AM 1,2-Dichlorobenzene NO 330 pglKg 1 3/24/2009 12:48 AM 1,3-Dichlorobenzene NO 330 pg/Kg 1 3/24/200912:48 AM 1,4-Dichlorobenzene NO 33D pg/Kg 1 3/24/200912:48 AM 2,4,5 Tdchlorophenol NO 33D pg/Kg 1 3/241200912A8 AM 2,4,6-Tdchlorophenol NO 330 pglKg 1 3/2412009 12:48 AM 2,4-Dichlorophenol NO 1600 pg/Kg 1 312412009 12:48 AM 2,4-Dlmethylphenot NO 330 pg1Kg 1 3/24/2009 12:48 AM 2,4-Dinilrophenol NO 1600 pg/Kg 1 3/24/2009 12:48 AM QuallRers: B Analytc detected in the associated Method Blank E Value above quantitation range H Holding times for preparation ornnalysis exceeded NO Not Detected at theRcporting Limit S Spike/Surrogatc outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out AdtatcedLabo worleologr �u/JarO(arlPs 3275 11'aGnrlAvanrre, Signal Hill, Gl 90755 Tel: 562. 939.404S /%os; 562.989.4040 2 of 43 ' ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:10:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL ' Lab ID: 104410-001 Analyses Result PQL Qual Units Dr Date Analyzed ' SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550B EPA 8270C RunID: MS6_090320A OC Batch: 54042 PrepDale: 3/20/2009 Analyst: DMP 2,4-Dinitrololuene NO 330 pg/Kg 1 3/24/2009 12.48 AM 2,6-Dinilrotoluene ND 330 pg/Kg 1 3/24/2009 12:48 AM 2-Chloronaphthalene NO 330 pg/Kg 1 3/24/2009 12:48 AM 2-Chlorophenol NO 330 pg/Kg 1 3/24/2009 12.48 AM 2-Methylnaphthalene NO 330 pg/Kg 1 3/241200912:48 AM 2-Melhylphenol ND 330 pg/Kg 1 3/24/2009 12:48 AM ' 2-Nitroaniline NO 1600 pg/Kg 1 1 31241200912:48 AM 31241200912:48 AM 2-Nitrophenol NO 330 pg/Kg 3,3'-Dichlorobenzidine NO 660 pg/Kg 1 3/241200912:48 AM 3-Nitroaniline ND 1600 pg/Kg 1 3/24/2009 12:48 AM 4,6-Dinitro-2-melhylphenol NO 1600 pg/Kg 1 31241200912:48 AM 4-Bromophenyl-phenylether NO 330 pg/Kg 1 3/24/200912,48 AM 4-C1loro-3-melhylphenol NO 660 pg/Kg 1 3124/200912:48 AM ' 4-Chloroaniline ND 660 pg/Kg 1 1 3/24/2009 12:48 AM 3/24/2009 12:48 AM 4-Chlorophenyl-phenylether NO 330 pg/Kg 4-Methylphenol NO 330 pg/Kg 1 3/24/2009 12:48 AM 4-Nitroaniline NO 1600 pg/Kg 1 3124/200912.48 AM ' 4-Nitrophenol ND 1600 pg/Kg 1 3/24/2009 12.48 AM Acenaphthene NO 330 pg/Kg 1 3/24/2009 12:48 AM Acenaphlhylene NO 330 pg/Kg 1 3/24/200912.48 AM Anthracene ND 330 pg/Kg 1 1 3/24/2009 12:48 AM 3/24/2009 12.48 AM Benzidine (M) ND 1600 pg/Kg Benzo(a)anthmcene NO 330 pg/Kg 1 3/24/2009 12:48 AM Benzo(a)pyrene NO 330 pg/Kg 1 3/24/2009 12:48 AM Benzo(b)0uoranlhene ND 330 pg/Kg 1 3/24/2009 12:48 AM Benzo(g,h,i)perylene NO 330 pg/Kg 1 3/241200912:48 AM 8enzo(k)fluoranthene NO 330 pg/Kg 1 3/2412009 12 48 AM Benzoic acid NO 1600 pg/Kg 1 1 3/24/2009 12 48 AM 3/24/2009 12:48 AM Benzyl alcohol ND 660 pg/Kg Bis(2-chloroethoxy)melhane NO 330 pg/Kg 1 3/24/2009 12.48 AM Bis(2-chloroethyl)ether NO 330 pg/Kg 1 3124/200912:48 AM Bis(2-chloroisopropyl)ether ND 330 pg/Kg 1 3/24/2009 12:48 AM Sis(2-ethylhexyl)phlhalate NO 330 pg/Kg 1 3/24/2009 12:48 AM Bulylbenzylphthalate NO 330 pg/Kg 1 3/24/2009 12:48 AM Chrysene NO 330 pg/Kg 1 1 3/24/2009 12:48 AM 3/24/2009 12:48 AM Di-n-butylphthalale NO 330 pg/Kg ' Qualifiers: D Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Lima H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ' Advanced T echnologj• 11 3275 li'aGnvtAvenrre, Signaiflill, CA 9075.5 Tel- SG2. 939A045 Fax.-562.989.4040 LnDorntories ' 3 of 43 n L ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:10:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410.001 Analyses Result PQL Qual Units DIF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunID: MS6 090320A OC Batch: 54042 PrepDate: 3/20/2009 Analyst: DMP Di-n-octylphthatate ND 330 pg/Kg 1 3/24/2009 12:48 AM Dibenz(a,h)anthracene ND 330 pg/Kg 1 3/24/2009 12:48 AM Dibenzotumn ND 330 pg/Kg 1 3/24/2009 12AB AM Diethylphlholale ND 330 pg/Kg 1 3/24/200912A8 AM Dlmethylphlhalate ND 330 pglKg 1 3/24/200912;48 AM Fluoranthene ND 330 pg/Kg 1 3/2412009 12AS AM Fluorene ND 330 pglKg 1 3124/2009 12:48 AM Hexachlorobenzene ND 330 pg/Kg 1 3I241200912:48AM' Hexachlorobuladfene ND 660 pg/Kg 1 3124/200912AB AM Hexachlorocyclopentadlene ND 660 pg/Kg 1 3/2412009 12A8 AM Hexachloroethane ND 330 pg/Kg 1 3/24/200912:48 AM Indeno(1,2,3-cd)pyrene ND 330 pg/Kg 1 3/24/200912:48 AM Isophorone ND 330 pglKg 1 3/24/2009 12:48 AM N-Nitrosodi-n-propylamine ND 330 pg/Kg 1 31241200912:48 AM N-Nitrosodiphenylamine ND 330 pg/Kg 1 3/24/2009 12A8 AM Naphthalene ND 330 pg/Kg 1 3/24/200912A8 AM Nitrobenzene ND 330 pg/Kg 1 3/24/200912A8 AM Pentachlorophenol ND 1600 pg/Kg 1 3124/200912A8 AM Phenanlhrene ND 330 pg/Kg 1 31241200912:48AM Phenol ND 330 pg/Kg 1 3/2412009 12AS AM Pyrone ND 330 pg/Kg 1 3/24/2009 12:48 AM Surc 1,2-Dichlorobenzene-d4 86.0 49-103 %REC 1 3/241200912:48 AM Surr. 2,4,6-Tribromophenol 0.490 47-129 a %REC 1 3/24/200912A8 AM Surf: 2-Chlorophenol-d4 22.9 54.109 6 %REC 1 31241200912:48 AM Surr.2-Fluorobiphenyl 108 59-108 %REC 1 3/24/200912A8 AM Sum2-Fluorophenol 15.9 50.111 a %REC 1 3124/2009 12:48 AM Burr.4-Terphenyl-d14 112 58-135 %REC 1 312412009-12:48AM Burr: Nilrobenzene-d5 106 64-115 %REC 1 3/241200912AB AM Burr: Phenol-d5 69.9 58-112 %REC 1 3/2412009 12A8 AM Qua11111M: B Analyte detected in the associated Method Blank E Value above quuntitnlion range It Holding tittles for preparation or analysis exceeded ND Not Detected at the Reporting Limit S SpiketSumagate outside of limits due to matrix interference Results are wet unless otherwise specified DO SurroguleDiluted Out Advanced 7crbttologr Laboratories 327.1 I1'alnut Avenue, Signal Hill, CA 907.1.5 Tel: 562. 989.4041 Fax. 561.989.4040 4 of 43 11 11 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI-2.0 Lab Order: 104410 Collection Date: 3/10/2009 11:20:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL ' Lab ID: 104410-002 Analyses Result PQL Qual Units OF Date Analyzed ' HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunlD: GC8_090317A QC Batch: 53868 PrepDate: 3/16/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 ND 10 mg/Kg 1 3/17/1909 10:56 AM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 3/17/1909 10:56 AM T/R Hydrocarbons: C18-1328 ND 10 mg/Kg 1 3/17/1909 10:56 AM T/R Hydrocarbons: C28-1336 NO 10 mg/Kg 1 311711909 10:56 AM T/R Hydrocarbons: C36-C40 NO 10 mglKg 1 3/17/1909 10:56 AM T/R Hydrocarbons: C8-C40 Total NO 10 mg/Kg 1 3/17/1909 10:56 AM t Surr: p-Terphenyl 115 57-144 %REC 1 311711909 10:56 AM PCBS BY GC/ECD EPA 3550E EPA $082 RunID: GC5_090316B QC Batch: 53874 PrepDate: 1 3116/2009 Analyst: HL 3116/200908:31_PM Aroclor 1016 NO 16 pg/Kg Aroclor 1221 NO 33 pg/Kg 1 3/16/2009 08:31 PM Dill Aroclor 1232 NO 16 pg/Kg 1 3/16/2009 08:31 PM , Aroclor 1242 ND 16 pg/Kg 1 3/16/2009 08:31 PM Aroclor 1248 NO 16 jig/Kg 1 3/16/2009 08:31 PM Aroclor 1254 NO 16 pg/Kg 1 3/16/2009 08:31 PM Aroclor 1260 NO 16 pg/Kg 1 3/1612009 08:31 PM Aroclor 1262 ND 16 pg/Kg 1 3116/2009 08:31 PM Aroclor 1268 NO 16 pg/Kg 1 3/16/2009 08:31 PM Surr: Decachlorobiphenyl 76.6 30-124 %REC 1 3/16/2009 08:31 PM Surr: Tetrachloro-m-xylene 84.1 40-118 %REC 1 3/16/2009 08:31 PM III I 11 ' Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Lima If holding times for preparation or analysis exceeded S Spike/Sumogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Ar/rLabo dorim/agp LnGorrrenries 32751PaInatAvenue, Signalhill, CA 90755 Tel: 562.989.4045 Fax: 562,989.4040 ' 5 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample 1D: 132-0.5 Lob Order: 104410 Collection Date: 3/10/2009 11:30:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-003 Analyses Result PQL Qua[ Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC8 090317A OC Balch: 63868 PrepDate: 3/1612009 Analyst CBR T1R Hydrocarbons: C8-C10 55 10 mg/Kg 1 3117/1909 01:38 PM T/R Hydrocarbons: C10-C18 NO 10 mg/Kg 1 3/17/1909 01:38 PM T1R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 3117/1909 01:38 PM T/R Hydrocarbons: C28-C36 NO 10 mg/Kg 1 3117/1909 01:38 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 3/17/1909 01:38 PM T/R Hydrocarbons: C8-C40 Total 55 10 mg/Kg 1 3/17/1909 01:38 PM Surr:p-Terphenyi ill 57-144 %REC 1 3/1711909 01:38 PM HYDROCARBON CHAIN IDENTIFICATION EPA 8015B RuniD: GC2_090319A QC Balch: E09VS078 PrepDate: T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg Surr: Bromonuorobenzene (FID) 90.9 59.145 %REC PCBS BY GCIECD Analyst: KHN 1 3/1912009 02:22 PM 1 311912009 02:22 PM EPA 3550B EPA 8082 RunID: G`C5 090316E QC Balch: 53874 PrepDate: Aroclor 1016 ND 16 pg/Kg 1 Aroclor 1221 NO 33 pg/Kg 1 Aroclor 1232 NO 16 pg/Kg 1 Aroclor1242 NO 16 pg/Kg 1 Aroclor 1248 NO 16 pg/Kg 1 Aroclor1264 NO 16 pg1Kg 1 Aroclor 1260 NO 16 pg/Kg 1 Aroclor 1262 NO 16 pglKg 1 Aroclor 1268 NO 16 pglKg 1 Surf: Decachloroblphenyl 72.5 30-124 %REC 1 Surr: Telmchloro-m-xylene 80.0 40.118 %REC 1 VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 8260E RunID: MS5_090319A QC Batch: T09VS076 PrepDate: 10,1,2-Tetmchloroelhane ND 5.0 pg/Kg 1 1,1,1-Tdchloroethane NO 5.0 pglKg 1 1,1,2,2-Tetrachloroethane NO 5.0 pglKg 1 1,1,2-Tdchloroethane NO 5.0 pg/Kg 1 1,1-Dichloroethane NO 5.0 plift 1 3/1612009 Analyst: HL 3/16/2009 09:30 PM 3/16/2009 09:30 PM 3116/2009 09:30 PM 3/16/2009 09:30 PM 3/16/2009 09:30 PM 3/16/2009 09:30 PM 3/16/2009 09:30 PM 3/1612009 09:30 PM 3/16/2009 09:30 PM 3/16/2009 09:30 PM 3/16/2009 09:30 PM Analyst: HH 3/19/2009 02:35 PM 3119/2009 02:35 PM 3/19/2009 02:35 PM 3119/2009 02:35 PM 311912009 02:35 PM Qualifiers: B Analyte detected in the nssocinted Method Blank E Value above quantitalion range It Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Adrvnced T echnologr Labornrorlcs 3275 I {'alnrrl Avenfm, Signal Hill, CA 907545 Tel: 562. 939.400 Pax: 562.989.4040 6 of 43 I II I( II II I I II 1 l_.l ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 132-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:30:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-003 Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunID: MS5_090319A QC Batch: T09VS076 PrepDate: Analyst: HH 1,1-Dichloroethene NO 5.0 pg/Kg 1 3119/2009 02:35 PM 1,1-Dichloropropene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2,3-Tdchoorobenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2,3-Trichloropropane NO 5.0 pg/Kg 1 3/1912009 02:35 PM 1,2,4-Trichlorobenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2,4-Tdmelhylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2-Dibromo-3-chloropropane NO 10 pg/Kg 1 3/19/2009 02:35 PM 1,2-Dibromoethane NO 5.0 pg/Kg 1 3/19/2009 0235 PM 1,2.Dichlorobenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2-Dichloroethane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,2-Dichloropropane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,3,5-Trimethylbenzene NO 5.0 pg/Kg 1 3119/2009 02:35 PM 1,3-Dichlorobenzene NO 5.0 pg/Kg 1 3119/2009 02:35 PM 1,3-Dichloropropane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 1,4-Dichlorobenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 2,2-Dichloropropane NO 5.0 jig/Kg 1 3/1912009 02.35 PM 2-Butanone NO 50 pg/Kg 1 3119/2009 02:35 PM 2-Chlorotoluene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 2-Hexanone NO 50 pg/Kg 1 3/1912009 02 35 PM 4-Chlorotoluene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 4-Isopropyltoluene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM 4-Methyl-2-pentanone NO 50 pg/Kg 1 3/19/2009 02:35 PM Acetone NO 50 pg/Kg 1 3/19/2009 02:35 PM NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Benzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Bromobenzene ND 5.0 pg/Kg 1 3/1912009 0235 PM Bromochloromethane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Bromodichloromethane NO 5.0 pg/Kg 1 3/19/20D9 02:35 PM Bromoform NO 5.0 pg/Kg 1 3/19/2009 0235 PM Bromomethene NO 5 0 pg/Kg 1 3119/2009 02:35 PM Carbon disulfide NO 5 0 pg/Kg 1 3/19/2009 02:35 PM Carbon tetrachloride NO 5.0 pg/Kg 1 3119/2009 0235 PM Chlorobenzene NO 5 0 pg/Kg 1 3/19/2009 02:35 PM Chlorcethane NO 5.0 p9/Kg 1 3/19/2009 02:35 PM Chloroform NO 5.0 pg/Kg 1 3119/2009 02:35 PM Chloromethane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM cis-1,2-Dichloroethene Qualifiers: B Analyto detected in the associated Method Blank E Value above quantitation range H holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out �i,1 Advanced nchno/ogr ud 3275 13'aGAvenxe, Signal Hill, Cal 90755 Tel: -SG2. 939.4095 Fax. 562.989.4040 Lnborn/ories 7 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 132-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:30:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: -- 104410-003--- - - - - �. -- - - --- -------- Analyses Result PQL Qual Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 8260E RunlD: MS5 090319A OC Batch: T09VS076 PrepDate: Analyst: HH cis-1,3-Dichloropropene NO 5.0 pg/Kg 1 3/1912009 02:35 PM DI -isopropyl ether NO 6.0 pglKg 1 3119/2009 02;35 PM Dibromochloromethane NO 5.0 pg/Kg 1 3/1912009 02:35 PM Dibromomelhane NO 5.0 pg/Kg 1 311912009 02:35 PM Dichlorodlnuoromelhane NO 5.0 pg/Kg 1 3/1912009 02:35 PM Ethyl Acetate NO 50 pg/Kg 1 3/1912009 02:35 PM Ethyl Ether NO 50 pg/Kg 1 3/19/2009 02:35 PM Ethyl Tert-butyl ether NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Ethylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Freon-113 NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Hexachlorobutediene NO 5.0 pg/Kg 1 311912009 02:35 PM lodomethane NO 5.0 pg/Kg 1 3/1912009 02:35 PM Isopropylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM m,p-Xylene NO 10 pg/Kg 1 311912009 02:35 PM Methylene chloride NO 5.0 pg/Kg 1 3/10/2009 02:35 PM MTBE NO 6.0 pg/Kg 1 3/19/2009 02:35 PM n-Butylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM n-Propylbenzene NO 510 pg/Kg 1 3/19/2009 02:35 PM Naphthalene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM o-Xylene NO 5.0 pg/Kg 1 3/1912009 02:35 PM sec-Butylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Styrene NO 5.0 pglKg 1 3119/2009 02:35 PM Tert-amyl methyl ether NO 6.0 pg/Kg 1 3119/2009 02:35 PM Tert-Butanol NO 100 pg/Kg 1 3/1912009 02:35 PM tert-Butylbenzene NO 5.0 pg/Kg 1 3/1912009 02:35 PM Telmchloroelhene NO 5.0 pg/Kg 1 3119/2009 02:35 PM Toluene NO 5.0 pg/Kg 1 3/1912009 02:36 PM trans-1,2-Dichloroethene NO 5.0 pg/Kg 1 3/19/2009 02:36 PM trans-1,3-Dichloropropene NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Trlchloroethene NO 5.0 pg/Kg 1 3119/2009 02:35 PM Trichloronuoromethane NO 5.0 pg/Kg 1 3/19/2009 02:35 PM Vinyl acetate NO 50 pgtKg 1 3/19/2009 02:35 PM Vinyl chloride NO 5.0 pg/Kg 1 3/1912009 02:35 PM Xylenes, Total NO 15 pglKg 1 3/1912009 02:35 PM Sum 1,2-Dichioroelhaned4 94.6 70-130 %REC 1 3/1912009 02:35 PM Surr.4-Bromonuorobanzene 100 70.130 %REC 1 311912009 02:35 PM Qualifiers: D it S DO Analyte detected in the associated Method Blank Holding tunes for preparation or analysis exceeded SpikelSumagate outside of limits due to matrix interference Surrogate Diluted Out Adrnn bo 7tories agr (sue\\ Laboratories E Value above quantitation range NO Not Detected at the Reporting Limit Results are wcl unless otherwise specified 327511'alnutAvenue, Signal Hill, CA 90755 8 of 43 Tel 561 989.4045 raw 562.989.4040 11 II I II II ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 16-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:30:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: I04410-003 Analyses Result PQL Qual Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunID: MS5_090319A QC Batch: T09VS076 PrepDate: Analyst: HH Surr: Dibromofluoromethane 54.5 70-130 s %REC 1 3/1912009 02:35 PM Sum: Toluene-d8 109 70-130 %REC 1 3119/2009 02:35 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H I lolding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out ow AdrancedTecbuologr 3175 fYaGrrelAvenrre, Signo[Ifill, CA 90755 Tel: 562. 9821045 Pas: 5G2.989.4040 LnOora[orics V-4419 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GCB 090317A QC Batch: 53868 PrepDate: 3/1612009 Analyst: CBR T/R Hydrocarbons: CB-C10 52 10 mglKg 1 3117/1909 02:05 PM T/R Hydrocarbons: C10-C18 NO 10 mg/Kg 1 3/17/1909 02:05 PM T/R Hydrocarbons: C18-C28 12 10 mg/Kg 1 3/17/1909 02:05 PM T/R Hydrocarbons: C28-C36 13 10 mglKg 1 3/17/1909 02:05 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 3/17/1909 02:05 PM T/R Hydrocarbons: C8-C40 Total 78 10 mg/Kg 1 3/17/1909 02:05 PM Surr: p-Terphenyl 114 57-144 %REC 1 3/17/1909 02:05 PM HYDROCARBON CHAIN IDENTIFICATION EPA 8015E RunID: GC2_090319A QC Balch: E09VS078 PrepDate: T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg Surr: Bromoguorobenzene (FID) 89.0 69.145 %REC PCBS BY GCIECD Analyst: KHN 1 3/1912009 02:37 PM 1 3/1912009 02:37 PM EPA 3550B EPA 8082 RunID: GCS 090316E QC Balch: 63874 PrepDate: Aroclor 1016 NO 16 pg/Kg 1 Aroclor 1221 NO 33 pg/Kg 1 Aroclor1232 NO 16 pg/Kg 1 Aroclor1242 NO 16 pg/Kg 1 Aroclor 1248 NO 16 pg/Kg 1 Aroclor 1254 NO 16 pg/Kg 1 Aroclor 1260 NO 16 pg/Kg 1 Aroclor 1262 NO 16 pg/Kg 1 Aroclor 1268 NO 16 pg/Kg 1 Surr. Decachlorobiphenyl 84.6 30.124 %REC 1 Sum Tetrachloro-m-xylene 94.3 40-118 %REC 1 VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 82608 RunID: MS5 090319A QC Batch: T09VS076 PrepDate: 1,1,1,2-Tetmchloroethane NO 5.0 pg/Kg 1 1,1,1-Tdchioroelhane ND 5.0 pg/Kg 1 1,1,2,2-Tetrachloroethane NO 5.o pg1Kg 1 1,1,2 Tdchioroethane NO 5.0 pg/Kg 1 1,1-Dichloroethene NO 5.0 pg/Kg 1 3/16/2009 Analyst: HL 3/16/2009 10:00 PM 311612009 10:00 PM 3/16/2009 10:00 PM 3/16/2009 10:00 PM 3/161200910:00 PM 3116/2009 A= PM 311612009 10:00 PM 3116/200910:00 PM 311612009 10:00 PM 3/16/2009 10:00 PM 311612009 10:00 PM Analyst: HH 3/19/2009 02:53 PM 3/19/2009 02:53 PM 3/1912009 02:53 PM 311912009 02:53 PM 3/19/2009 02:53 PM Qualifiers: ~ B Anniyto detected in the associated Method Blank E Value above quantimtion range ' H Holding times rot preparation or analysis exceeded ND Not Detected ntthe Reporting Limit S Spike/Surrogate outside of limits duo to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Adrunced Tcclrnologv Labortitorles 127.5IlrabintAvenue, Signal W11,CA 90755 Tel: 562. 989.404,1 Far.562.989.4040 10 of 43 I I I I 11 I I 11 I I I I1 L J I I II 1 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260B RunID: MS5 090319A QC Batch: T09VS076 PrepDate: Analyst: HH 1,1-Dichloroethene ND 5.0 pg/Kg 1 3/19/2009 02.53 PM 1,1-Dichloropropane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,2,3-Tdchlorobenzens ND 5.0 pg/Kg 1 3119/2009 02:53 PM 1,2,3-Tdchloropropane ND 5.0 pg/Kg 1 3119/2009 02:53 PM 1,2,4-Trichlorobenzene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,2,4-Trimelhylbenzene ND 5.0 pg/Kg 1 3/19/2009 02:63 PM 1,2-Dibromo-3-chloropropane ND 10 pg/Kg 1 3/19/2009 02:53 PM 1,2-Dibromoethane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,2-Dichlorobenzene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,2-Dichloroethane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,2-Dichloropropane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,3,5-Trimethylbenzene ND 5.0 pg/Kg 1 3119/2009 02:53 PM 1,3-Dichlorobenzene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 1,3-Dichloropropane ND 5.0 pg/Kg 1 311912009 02:53 PM 1,4-Dichlorobenzene ND 5.0 pg/Kg 1 3/1912009 02:53 PM 2,2-Dichloropropane ND 5.0 pglKg 1 3/19/2009 02:53 PM 2-Butanone ND 50 pg/Kg 1 3/1912009 02:53 PM 2-Chlorotoluene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 2-Hexanone ND 50 pg/Kg 1 3/19/2009 02:53 PM 4-Chlorotoluene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM 4-Isopropyltoluens ND 5.0 pg/Kg 1 3/19/2009 02:53 PM 4-Methyl-2-pentanone ND 50 pg/Kg 1 3/1912009 02:53 PM Acetone ND 50 pg/Kg 1 3/19/2009 02:53 PM Benzene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Bromobenzene ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Bromochloromethane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Bromodichloromethane ND 5.0 pg/Kg 1 3119/2009 02:53 PM Bromoform ND 5.0 pg/Kg 1 3119/2009 02:53 PM Bromomelhane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Carbon disulfide ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Carbon tetrachloride ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Chlorobenzene ND 5.0 pg/Kg 1 3119/2009 02:53 PM Chloroethane ND 5.0 pg/Kg 1 3/19/2009 02:53 PM Chloroform ND 5.0 pg/Kg 1 3/1912009 02:53 PM Chloromelhane ND 5.0 pg/Kg 1 3/1912009 02:53 PM cis-1,2-Dichloroethene ND 5.0 pg/Kg 1 3/19/2009 02.53 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quanutauon range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limns due to matrix interference Results are %vet unless otherwise specified DO Surrogate Diluted Out ,Adtnnced 7bc6ao/ogr , 3275Va1nntdvenre, Signalll[/, C.90755 Tel. 562. 989.4045 Fax. 5G2.>89.4040�W 11 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc, Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497.001 - ' Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 82608 RunID: MS5_090319A QC Batch: T09VS076 PrepDale: Analyst: HH cis-1,3-Dichloropropene NO 5.0 pg/Kg 1 3119/2009 02:53 PM Di -Isopropyl ether NO 5.0 pg/Kg 1 3/1912009 02:53 PM Dibromochloromelhane NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Dibremomethane NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Dichlorodifluoromethane NO 6.0 pg/Kg 1 3/1912009 02:53 PM Ethyl Acetate NO 5o pglKg 1 3119/2009 02:53 PM f Ethyl Ether NO 50 pglKg 1 3119/2009 02:53 PM Ethyl Tert-butyl ether NO 5.0 pglKg 1 3/19/2009 02:63 PM Ethylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Freon-113 NO 5.0 pg/Kg 1 3/1912009 02:53 PM Hexachlorobutediene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM ; lodomethane NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Isopropylbenzene NO 5.0 pg/Kg 1 3/1912009 02:53 PM m,p-Xylene NO 10 pg/Kg 1 3/19/2009 02:53 PM Methylene chloride NO 5.0 pg/Kg 1 3/19/2009 02:53 PM MTBE NO 5.0 pg/Kg 1 3/19/200902:53PM n-Butylbenzene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM ; n-Propylbenzene NO 6.0 pg/Kg 1 3/19/2009 02:53 PM Naphthalene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM o-Xylene NO 5.0 pg/Kg 1 3/10/2009 02:53 PM sec-Butylbenzene NO 5.0 pg/Kg 1 3/1912009 02:53 PM I� Styrene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Tort -amyl methyl ether NO 5.0 pg/Kg 1 3/19/2009 02:53 PM Tert-Butanol NO 100 pg/Kg 1 3119/2009 02:53 PM lert-Bulylbenzene NO 5.0 pg/Kg 1 3/1912009 02:53 PM q Tetrachloroelhene NO 5.0 pg/Kg 1 3/1912009 02:53 PM Toluene NO 6.0 pg/Kg 1 3/19/2009 02:63 PM j trans-1,2-Dichloroethene NO 5.0 pg/Kg 1 3/19/2009 02:53 PM trans-1,3-Dichloropropene NO 5.0 pg/Kg 1 3/1912009 02:53 PM ! ;� Trichloroethene NO 5.0 pglKg 1 3/19/2009 02:53 PM II Trichlorofluoromethans NO 5.0 pg/Kg 1 3110/2009 02:53 PM Vinyl acetate NO 50 pg/Kg 1 3/19/2009 02:63 PM Vinyl chloride NO 5.0 pg/Kg 1 311912009 02:53 PM it Xylenes, Total NO 15 pglKg 1 3/1912009 02:53 PM Surr:1,2•Dichloroelhaned4 102 70-130 %REC 1 3/1912009 02:53 PM Surr:4-Bromofluorobenzene 97.0 70-130 %REC 1 3/1912009 02:53 PM Qualifiers: B Analyle detected in the associated Method Blank E Value above quantitation range H I lolding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit 1 S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out , Adsuared 7cchnalogr. Laboratories 3175111'alnulAvearre, Signalllill, CA 90755 Tel: 562. 989,4045 Pax. 562.989.4040 12 of 43 I II II II u I_1 I I i li I I II I I II I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunlD: MS5 090319A QC Batch: T09VS076 PrepDate: Analyst: HH Surr: Dibromonuoromethane 61.4 70-130 s %REC 1 3/19/2009 02:53 PM Surr: Toluene-d8 116 70-130 %REC 1 3/19/2009 02:53 PM SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550E EPA 8270C RunID: MS6_090320A QC Batch: 54042 PrepDate: 3/20/2009 Analyst: DMP 1,2,4-Trichlorobenzene ND 330 pg/Kg 1 3/24/2009 01:16 AM 1,2.Dichlorobenzene NO 330 pg/Kg 1 3/24/2009 01:16 AM 1,3-Dichlorobenzene ND 330 pg/Kg 1 3/24/2009 01:16 AM 1,4-Dichlorobenzene ND 330 pg/Kg 1 3/24/2009 01:16 AM 2,4,5-Trtchlorophenol ND 330 pg/Kg 1 3/24/2009 01:16 AM 2,4,6-Trichlorophenol NO 330 pg/Kg 1 3/24/2009 01:16 AM 2,4-Dichlorophenol NO 1600 pg/Kg 1 3/24/2009 01:16 AM 2,4-Dimethylphenol ND 330 pg/Kg 1 3/24/2009 01:16 AM 2,4-Dinitrophenol ND 1600 pg/Kg 1 3/24/2009 01:16 AM 2,4-Dinitrololuene ND 330 pg/Kg 1 3/24/2009 01:16 AM 2,6-Dinitrololuene NO 330 pg/Kg 1 3/24/2009 01:16 AM 2-Chloronaphthalene ND 330 pg/Kg 1 3/24/2009 01:16 AM 2-Chlorophenol ND 330 pg/Kg 1 3/24/2009 01:16 AM 2-Melhylnaphthalene ND 330 pg/Kg 1 3/24/2009 01:16 AM 2-Melhylphenol NO 330 pg/Kg 1 3124/2009 01:16 AM 2-Nilroanilme NO 1600 pg/Kg 1 3/24/2009 01:16 AM 2-Ndrophenol ND 330 pg/Kg 1 3/24/2009 01:16 AM 3,3'-Dichlorobenzidine ND 660 pg/Kg 1 3124/2009 01:16 AM 3-Nitroaniline NO 1600 pg/Kg 1 3124/2009 01:16 AM 4,6-Dinilro-2-methylphenol ND 1600 pg/Kg 1 3/24/2009 01:16 AM 4-Bromophenyi-phenylether NO 330 pg/Kg 1 3/24/2009 01:16 AM 4-Chloro-3-melhylphenot ND 660 pg/Kg 1 3/2412009 01:16 AM 4-Chloroaniline NO 660 pg/Kg 1 3124/2009 01:16 AM 4-Chlorophenyl-phenylether NO 330 pg/Kg 1 3/24/2009 01:16 AM 4-Methylphenol ND 330 pg/Kg 1 3124/2009 01:16 AM 4-Nitroaniline ND 1600 pg/Kg 1 3/24/2009 01:16 AM 4-Nitrophenol NO 1600 pg/Kg 1 3/24/2009 01:16 AM Acenaphthene ND 330 pg/Kg 1 3/2412009 01:16 AM Acenaphthylene ND 330 pg/Kg 1 3/24/2009 01:16 AM Anlhracene ND 330 pg/Kg 1 3/24/2009 01:16 AM Benzidine(M) ND 1600 pg/Kg 1 3/24/2009 01:16 AM Qualifiers: B Analyle detected in the associated Method Blank E value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ,drnncedTeebnology J,ALobaratories 3275 13'alnut Avamre, Signalliill, CA 90755 TeL• 562. 989A045 Pas: 562.98R4040 13 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units Dr Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunlD: MS6_090320A QC Batch: 64042 PrepDate: 3120/2009 Analyst: DMP Benzo(a)anthracene NO 330 pg/Kg 1 3/24/2009 01:16 AM Benzo(a)pyrene NO 330 pg/Kg 1 312412009 01:16 AM Benzo(b)0uoranthene NO 330 pg/Kg 1 312412009 01:16 AM Benzo(g,h,i)perylene NO 330 pg/Kg 1 3124/2009 01:16 AM Senzo(k)Buoranlhene NO 330 pg/Kg 1 3/2412009 01:16 AM Benzoic acid NO 1600 pglKg 1 3/24/2009 01:16 AM Benzyl alcohol NO 660 pg/Kg 1 3124/2009 01:16 AM Sis(2-chloroelhoxy)methane NO 330 pglKg 1 3/24/2009 01:16 AM Bis(2-chloroethyl)ether NO 330 pg/Kg 1 3124/2009 01:16 AM Bis(2-chloroisopropyl)ether NO 330 pg/Kg 1 3124/2009 01:16 AM Bis(2-elhylhexyi)ph1hala1e NO 330 pg/Kg 1 3/24/2009 WAS AM Bulylbenzylphtholate NO 330 pg/Kg 1 3124/2009 01:16 AM Chrysene NO 330 pg/Kg 1 3/2412009 01:16 AM Di-n-butylphlhalale NO 330 pg1Kg 1 3/2412009 01:16 AM Di-n-octylphthalale NO 330 pg/Kg 1 3/2412009 01:16 AM Dibenz(a,h)anlhracene NO 330 pg/Kg 1 3124/2009 01:16 AM Dibenzofuran ND 330 pg/Kg 1 3/2412009 01:16 AM Dielhylphlhalale NO 330 pg/Kg 1 3/2412009 01:16 AM Dimethylphthalate NO 330 pg/Kg 1 312412009 01:16 AM Fluoranlhene NO 330 pg/Kg 1 3124/200901:1 SAM Fluorene NO 330 pg/Kg 1 3124/2009 01:16 AM Hexachlorobenzene NO 330 pg/Kg 1 312412009 01:16 AM Hexachlorobutadiene NO 660 pg/Kg 1 312412009 01:16 AM Hexachlorocyclopentadlene NO 660 pg/Kg 1 3/24/2009 01:16 AM Hexachloroelhane NO 330 pg/Kg 1 3/24/2009 01:16 AM Indeno(1,2,3-cd)pyrene NO 330 pg/Kg 1 3/24/2009 01:16 AM Isophorone NO 330 pg/Kg 1 3/24/2009 01:16 AM N-Nilrosodi-n-propylamine NO 330 pg/Kg 1 3124/200901:16AM N-Nitrosodiphenylemine NO 330 pg/Kg 1 3124/2009 01:16 AM Naphthalene NO 330 pg/Kg 1 3124/2009 01:16 AM Nitrobenzene NO 330 pg/Kg 1 3124/2009 01:16 AM Penlachlorophenot NO 1600 pg/Kg 1 312412009 WAS AM Phonanthrene ND 330 pg/Kg 1 3/24/2009 01:16 AM Phenol NO 330 pg/Kg 1 3/24/2009 01:16 AM Pyrene NO 330 pg1Kg 1 3/24/2009 01:16 AM Surr.1,2-Dlchlorobenzene-d4 74.0 49.103 %REG 1 3/24/2009 01:16 AM Qualifiers: B Analytedetected in theassociatcd Method Blank E Value above quantitation range H Holding times for preparation oranalysis exceeded NO Not Detected atthc Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out drfinced Laboratories 327s1i'ulnutdvurnre, SignulHill,Ci1 907.55 Tel: 562.989.4045 Fax:562.989.4040 14 of 43 I U II II it VJ I I l i I I I I! 11 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B2-1.5 Lab Order: 104410 Collection Date: 3/10/2009 11:36:00 AM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-004 Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC1MS EPA 3550B EPA 8270C RunID: MS6_090320A QC Batch: 54042 PrepDate 3/20/2009 Analyst: DMP Surr: 2,4,6-Tribromophenol 1.45 47-129 s %REC 1 3/24/2009 01:16 AM Surr: 2-Chlorophenot-d4 11.9 54-109 s %REC 1 3/24/2009 01:16 AM Surr: 2-Fluorobiphenyl 97.3 59-108 %REC 1 3/24/2009 01:16 AM Surr: 2-Fluorophenol 6.93 50-111 S %REC 1 3124/2009 01:16 AM Surr: 4-Terphenyl-d14 108 58-135 %REC 1 3/24/2009 01:16 AM Surr: Nitrobenzene-d5 92.2 54-115 %REC 1 3/24/2009 01:16 AM Surr: Phenol-d5 41.9 58-112 s %REC 1 3/24/2009 01:16 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limn S Spike/Surrogate outside of limits due to matrix interference Results am wet unless otherwise specified DO Surrogate Diluted Out Advanced Tec/mo%r ancedlorics 3275 if alnnt Averare, Signall�ill, CA 90755 Tel.SG2. 989.4045 Fax: 562.989.4040 bor15 of 43 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample IDr B3-0.5 Lab Order: 104410 Collection Date: 3/10/2009 11:43:00 AM Project: Newport -SCE Parcel, 602497-061 Matrix: SOIL Lab ID: 104410.005 ----- -- --- - - -- - - -- - - -- - -- — - - — --- - ----------------- Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC8_090317A QC Batch: 53868 PrepDate: 3116/2009 Analyst: CBR T/RHydrocarbons: CB -CIO 34 10 mg/Kg 1 3117/190901:11PM T/R Hydrocarbons: C10-CIS NO 10 mglKg 1 3/17/1909 01:11 PM T/R Hydrocarbons: C18-C28 11 10 mg/Kg 1 3/17/1909 01:11 PM T/R Hydrocarbons: C28-C36 15 10 mg/Kg 1 3/17/1909 01:11 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 3117/1909 01:11 PM T/R Hydrocarbons: CB-C40 Total 59 10 mg/Kg 1 3117/1909 01:11 PM Surr, p Terphenyl 110 57-144 %REC 1 3/17/1909 01:11 PM PCBS BY GCIECD EPA 3550B EPA 8082 RunID: GC5 090316E QC Batch: 53874 PrepDate: 3/16/2009 Analyst: HL Aroclor 1016 NO 16 pglKg 1 3/16/2009 10:30 PM Aroclor 1221 NO 33 pg/Kg 1 3/16/200910:30 PM Aroclor 1232 NO 16 pg/Kg 1 3/16/2009 10:30 PM Aroclor 1242 NO 16 pg/Kg 1 3/161200910:30 PM Aroclor 1248 NO 16 pg/Kg 1 3116/200910:30 PM Aroclor 1254 NO 16 pg/Kg 1 3116/200910:30 PM Aroclor 1260 NO 16 pg/Kg 1 3/16/2009 10:30 PM Aroclor1262 NO 16 pg/Kg 1 3116/2009 10:30 PM Aroclor 1268 NO 16 pg/Kg 1 3/161200910:30 PM Surr: Decachlorobiphenyl 80.5 30.124 %REC 1 3/161200910:30 PM Surr. Tetrachloro-m xylene 87.5 40.118 %REC 1 31161200910:30 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quanlivaion range H I lolding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Sumogatc outside of limits due to matrix interference Results are Wet unless othemisespecified DO Surrogate Diluted Out I Advanced 7agr ' LnGoratorlestodes 3275'It'alrnr+Avanae, Signu/f/ill, C.1 90753 Tc(: 562. 989.4045 Fax: 562.989.4040 16 of 43 I r, I �'I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: E3-1.3 Lab Order: 104410 Collection Date: 3/10/2009 1:12:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-006 Analyses Result PQL Qual Units DR Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC8_090317A QC Batch: 53868 PrepDate: 3116/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 42 10 mg/Kg 1 3/17/1909 02.58 PM T/R Hydrocarbons: CIO-C18 NO 10 mg/Kg 1 3/17/1909 02:58 PM T/R Hydrocarbons: C18-C28 16 10 mg/Kg 1 3117/1909 02:58 PM T/R Hydrocarbons: C28-C36 28 10 mg/Kg 1 3/17/1909 02:58 PM T/R Hydrocarbons: C36-C40 20 10 mg/Kg 1 3/17/1909 02:58 PM T/R Hydrocarbons: C8-C40 Total 110 10 mg/Kg 1 3/17/1909 02:58 PM Surr: p-Terphenyl 108 57-144 %REC 1 3/17/1909 02.58 PM HYDROCARBON CHAIN IDENTIFICATION EPA 8015E RunID: GC2 090319A QC Batch: E09VS078 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 3119/2009 02:51 PM Burr: Bromofluorobenzene (FID) 90.6 59-145 %REC 1 3/19/2009 02:51 PM PCBS BY GCIECD EPA 3550E EPA 8082 RunlD: GC5_090316B QC Batch: 53874 PrepDate: 3/16/2009 Analyst: HL Aroclor 1016 NO 16 33 pg/Kg 1 1 3/16/2009 10:59 PM 3/16/2009 10:59 PM Aroclor 1221 NO pg/Kg Aroclor 1232 NO 16 pg/Kg 1 3/16/2009 10.59 PM Aroclor 1242 NO 16 pg/Kg 1 3/16/2009 10:59 PM Aroclor 1248 NO 16 pg/Kg 1 3/16/2009 10:59 PM - Aroclor 1254 22 16 pg/Kg 1 3/16/2009 10:59 PM Aroclor 1261 NO 16 pg/Kg 1 3/16/2009 10:59 PM � Aroclor 1262 NO NO 16 16 pg/Kg 1 pg/Kg 1 3/16/2009 10:59 PM 3/16/2009 10:59 PM Aroclor 1268 Burr: Decachlorobiphenyl 75.4 30-124 %REC 1 3/16/200910:59,PM Burr: Telrachloro-m-xylene 76:9 40-118 %REC 1 3/16/2009 10:59 PM r VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 8280B RunlD. MS5_090319A QC Batch: 709VS076 PrepDate: Analyst: HH 1,1,1,2-Tetmchloroethane NO 5.0 pg/Kg 1 3/19/200903:11 PM 1,1,1-Tdchloroethane NO 5.0 pg/Kg 1 3119/200903:11 PM 1,1,2,2-Tetrachloroelhane NO 5.0 jig/Kg 1 3/19/200903:11 PM 1,1,2-Trichloroethane NO 5.0 pg/Kg 1 3/19/2009 03:11 PM 1,1-Dichloroethene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Qualifiers: B Annlyte detected in the associated Method Blank E Value above qunntitation range NO Not Detected at the Reporting Limit 11 Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Adrm+ced Technology 3275 ii'alnat Avenue, SignalHill, CA 90755 Tel: 562. 939A095 Fax. 562989.4040 LaGararorics VFW 17 of 43 I Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 104410 Project: Newport -SCE Parcel, 602497-001 ANALYTICAL RESULTS i Print Date: 26-Mar-09 j Client Sample 1D: B3-1.3 Collection Date: 3/10/2009 1:12:00 PM Matrix: SOIL Lab ID: 104410.006 Analyses Result PQL Qual Units Dr Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 8260E Run1D: MSS 090319A 1,1-Dichloroelhene 1,1.Dichloropropane 1,2,3-Tdchlorobenzene 1,2,3.Tdchloropropane 1,2,4-Tdchlorobenzene 1,2,4-Tdmethylbenzene 1,2-Dibromo-3chloropropane 1,2-Dibromoethene 1,2-Dichlorobenzene 1,2.Dichloroethane 1,2-Dichloropropane 1,3,5-T4methylbenzene 1,3-Dichlorobenzens 1,3-Dichloropropane 1,4-Dichlorobenzens 2,2.Dichloropropane 2-Bulanone 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-isopropyltoluene 4-Methyl-2-pentanone Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromelhane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroelhane Chloroform Chloromelhane cis-1,2-Dichieroelhene OC Balch: T09VS076 PrepDale: NO 5.0 p9lK9 1 NO 5.0 p91K9 1 NO 5.0 p91K9 1 NO 5.0 pg1K9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 10 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pglKg 1 NO 50 pg/Kg 1 NO 5.0 pg/Kg 1 NO 50 pglKg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 50 pg/Kg 1 NO 50 p91K9 1 NO 5.0 pglKg 1 NO 5.0 p91K9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 6.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 p91K9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pg1Kg 1 NO 5.0 pg/Kg 1 Analyst: HH 3/19/2009 03:11 PM 3/1912009 03:11 PM 311912009 03:11 PM 3119/2009 03:11 PM 3/19/2009 03:11 PM 31012009 03:11 PM 311912009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 311912009 03:11 PM 3/1912009 03:11 PM 3119/2009 03:11 PM 3/1912009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/1912009 03:11 PM 311912009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3119t2009 03:11 PM 3119/2009 03A I PM 3/1912009 03:11 PM 3119/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/19/2009 03:11 PM 3/1912009 03:11 PM 3/19/2009 03:11 PM 311912009 03:11 PM 3119/2009 03:11 PM Qualifiers: B Analyto detected in the ossooiated Method Blank E Value above qumallation range II Holding times for preparation orunnlysis exceeded NO Not Detected al the Reporting Limit S Spikc/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out Advanced 7erhaologv Laboratories 327S Il'alnntrlventie, Signal11111, CA 907.1.1 Tel: 562. 989.4045 Fax: 562.989.4040 18 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 16-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B3-1.3 Lab Order: 104410 Collection Date: 3/10/2009 1:12:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-006 Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 82608 RunlD: MS5_090319A QC Batch: T09VS076 PrepDate: Analyst: HH cis-1,3-Dichloropropene NO 5.0 jig/Kg 1 3/19/2009 03:11 PM Di -isopropyl ether NO 5.0 pg/Kg 1 3119/2009 03:11 PM Dibromochloromethane NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Dibromomethane NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Dichlorodifluoromethane NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Elhyl Acetate NO 50 pg/Kg 1 3/19/2009 03:11 PM Ethyl Ether NO 50 5.0 pg/Kg 1 1 3/19/2009 03:11 PM 3119/2009 03:11 PM Ethyl Tert-butyl ether NO pg/Kg Ethylbenzene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Freon-113 NO 5.0 pg/Kg 1 3/191200903:11 PM Hexachlorobutadiene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM lodomelhane NO 5.0 pg/Kg 1 3119/2009 03:11 PM Isopropylbenzene NO 5.0 pg/Kg 1 3/19/200903:11 PM m,p-Xylene NO 10 5.0 pg/Kg 1 1 3119/2009 03:11 PM 3/19/2009 03:11 PM Methylene chloride NO pg/Kg MTBE NO 5.0 pg/Kg 1 3119/2009 03,11 PM n-Bulylbenzene NO 5.0 pg/Kg 1 3/191200903:11 PM n-Propylbenzene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Naphthalene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM o-Xylene NO 5.0 jig/Kg 1 3/1912009 03:11 PM sec-Butylbenzene NO 5.0 pg/Kg 1 1 3119/2009 03:11 PM 3/19/2009 03:11 PM Styrene NO 5.0 pg/Kg Tert-amyl methyl ether NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Tart-Bulanol NO 100 pg/Kg 1 3/19/2009 03:11 PM ' tert-Bulylbenzene NO 5.0 pg/Kg 1 3/19/2009.03:11 PM Tetrachloroethene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Toluene NO 5.0 pg/Kg 1 3/19/2009 03:11 PM trans-1,2-Dichloroethene NO 5.0 pg/Kg 1 1 3119/2009 03:11 PM 3/19/2009 03:11 PM trans-1,3-Dichloropropene NO 5.0 pg/Kg Trichloroethene NO 5.0 pg/Kg 1 3/191200903:11 PM Trichlorofluoromethane NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Vinyl acetate NO 50 pg/Kg 1 3/19/2009 03:11 PM Vinyl chloride NO 5.0 pg/Kg 1 3/19/2009 03:11 PM Xylenes, Total NO 15 pg/Kg 1 3/19/2009 03:11 PM Surr: 12-Dichloroethane-d4 101 70-130 %REC %REC 1 1 3/19/2009 03:11 PM 3119/2009 03:11 PM Surr: 4-Bromofluorobenzene 93.8 70-130 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out anted /1 Advanced 7ec/tiro/oft 327.5 l3 aGnrt Averure, Signal Hill, CA 90755 TeG 562. 939.4045 Fax: 562.989.4040 �p 1 larles _ 19 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample to: B3-I.3 Lab Order: 104410 Collection Date: 3/10/2009 1:12:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 1044I0-006 Analyses Result PQL Quai Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GCIMS RunID: MS5 090319A QC Batch: T09VS076 Surr: Dibromo0uoromethane 60,5 70.130 Surr: Toluene-d6 112 70.130 SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550E RunID: MS6 090320A 1,2,4 Tdchlorobanzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5.Tdchlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenot 2,4-Dinilrophenol 2A.Dinihololuene 2,6-Dinilrotoluene 2-Chloronaphlhalene 2-Chiorophenol 2-Methylnaphthalene 2-Melhylphenol 2-Nilroaniline 2-Nitrephenol SX-Dichlorobenzidine 3-1,111roaniline 4,6-Dinilro-2-methylphenol 4-Bromophenyl-phenylelher 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophanyl-phenylelher 4-Methylphenol 4-Nilroaniline 4-Nilrophenol Acensphthene Acenaphthylene Anlhmcene Senzidine (M) QC Batch: 54042 EPA 8260E PrepDale: a %REC 1 %REC 1 EPA 8270C PrepDale: NO 330 p91K9 1 NO 330 pg/Kg 1 NO 330 p9IK9 1 NO 330 pO/Kg 1 ND 330 pglKg 1 ND 330 p91K9 1 ND 1600 pglkg 1 ND 330 p91K9 1 ND 160D pglKg 1 ND 330 pg/K9 1 NO 330 p9IK9 1 NO 330 p9IK9 1 NO 330 p91Kg 1 NO 330 pglKg 1 ND 330 pg/Kg 1 ND 1600 pg/Kg 1 ND 330 p9IK9 1 NO 660 pgIK9 1 NO 1600 pg/Kg 1 ND 1600 pgIK9 1 ND 330 pgIK9 1 NO 660 pgIK9 1 NO 660 pg1Kg 1 NO 330 pgIK9 1 NO 330 p9IK9 1 ND 1600 pg/Kg 1 ND 1600 pg/Kg 1 NO 330 pgIK9 1 NO 330 pg/Kg 1 NO 330 pglKg 1 NO 1600 pg/Kg 1 Qualifiers: B Analyte detected in the associated Method Blank _ E If Holding times for preparation or analysis exceeded ND S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out aAdrwaced Technology Lnborntorles Analyst: HH 3/19/200903:11 PM 3/19/200903:11 PM 3/20/2009 Analyst: DMP 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/2412009 01:43 AM 3124/2009 01:43 AM 312412009 01A3 AM 3/24/2009 WAS AM 312412009 01A3 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3124/2009 01:43 AM 312412009 01:43 AM 3/2412009 01:43 AM 3/2412009 01.43 AM 3/24/2009 01:43 AM 3124/2009 01 A3 AM 3/24/2009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01A3 AM 3/24/2009 01:43 AM 3124/2009 01:43 AM 3124/2009 01:43 AM 3/24/2009 01:43 AM 312412009 01:43 AM 3/2412009 01:43 AM 3/24/2009 01:43 AM 3/24/2009 01A3 AM Value above quantitalion range Not Detected at the Reporting Limit Results are wet unless otherwise specified .127.5 iVahntt Avenue, Signalllill, CA 907.15 20 of 43 Tch 562. 989.404S Fas: 562.989.4040 ' ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 ' CLIENT: Leighton Consulting, Inc. Client Sample ID: B3-1.3 Lab Order: 104410 Collection Date: 3/10/2009 1:12:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL ' Lab ID: 104410-006 Analyses Result PQL Qual Units DP Date Analyzed ' SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunID: MS6_090320A QC Batch: 54042 PrepDate: 3/20/2009 Analyst: DMP* Benzo(a)anthracene NO 330 pg/Kg 1 3/24/2009 01:43 AM Benzo(a)pyrene NO 330 jig/Kg 1 3/24/2009 01:43 AM Benzo(b)fluoranlhene NO 330 pg/Kg 1 3/24/2009 01:43 AM ' Benzo(g,h,i)perylene NO 330 pg/Kg 1 3/24/2009 01:43 AM Benzo(k)fluoranlhene NO 330 pg/Kg 1 3/24/2009 01:43 AM Benzoic acid NO 1600 pg/Kg 1 3/24/2009 01:43 AM ' Benzyl alcohol NO 660 330 pg/Kg 1 1 3/24/2009 01:43 AM 3/24/2009 01:43 AM Bis(2-chloroethoxy)methane NO pg/Kg Bis(2-chloroethyl)ether NO 330 pg/Kg 1 3124/2009 01:43 AM Bis(2-chloroisopropyl)ether NO 330 pg/Kg 1 3/241200901:43 AM Bis(2-ethylhexyl)phlhalate NO 330 pg/Kg 1 3/24/2009 01:43 AM Butylbenzylphthalale NO 330 pg/Kg 1 3/24/2009 01:43 AM Chrysene NO 330 pg/Kg 1 3124/2009 01:43 AM ' Di-n-bulylphthalate NO 330 pg/Kg 1 1 3/24/2009 01:43 AM 312412009 01:43 AM Dl-n-oclylphthalate NO 330 pg/Kg Dibenz(a,h)anthracene NO 330 pg/Kg 1 3/24/2009 01:43 AM Dibenzofuran NO 330 jig/Kg 1 3/24/2009 01:43 AM ' Dielhylphthalale NO 330 pg/Kg 1 3/24/2009 01:43 AM Dimethylphthalate NO 330 pg/Kg 1 3/24/2009 01:43 AM Fluoranthene NO 330 pg/Kg 1 3/24/2009 01:43 AM ' Fluorene NO 330 pg/Kg 1 1 3/24/2009 01:43 AM 3/24/2009 01:43 AM Hexachlorobenzene NO 330 jig/Kg Hexachlorobutadiene NO 660 pg/Kg 1 3/24/2009 01:43 AM Hexachlorocyclopenladiene NO 660 pg/Kg 1 3/2412009 01:43 AM Hexachloroethane NO 330 pg/Kg 1 3/24/2009 01:43 AM Indeno(1,2,3-cd)pyrene NO 330 pg/Kg 1 3/24/2009 01:43 AM Isophorone NO 330 pg/Kg 1 3124/2009 01:43 AM ' N-Nilrosodrn-propylamine NO 330 pg/Kg 1 1 3/24/2009 01:43 AM 3/24/2009 01:43 AM N-Nitrosodiphenylamine NO 330 pg/Kg Naphthalene NO 330 plift 1 31241200901:43 AM Nitrobenzene NO 330 pg/Kg 1 3/24/2009 01:43 AM ' Pentachlorophenol NO 1600 pg/Kg 1 3/24/2009 01:43 AM Phenanthrene NO 330 pg/Kg 1 3/24/2009 01:43 AM Phenol NO 330 pg/Kg 1 3/24/2009 01:43 AM Pyrene NO 330 pg/Kg 1 1 3/24/2009 01.43 AM 3/24/2009 01:43 AM Surr: 1,2-Dichlorobenzene-d4 67.4 49.103 %REC ' Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO surrogate Diluted Out Adrnnced Tcehnology 1 3275 Walaat Avenue, Signal Hill, CAI 90755 Tel:.562. 989.4045 las: 562.989.4040 ' �_ Lnhoratories 21 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 133-1.3 Lab Order: 104410 Collection Date: 3/10/2009 1:12:00 I'M Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-006 Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550E EPA 8270C RunlD: MSG 090320A QC Balch: 54042 PrepDate: 3/20/2009 Analyst: DMP Sum 2,4,6-Tribromophenol 1.21 47-129 s %REC 1 3124/2009 01:43 AM Slim,2-Chlorophenel-d4 15.9 54-109 s %REC 1 3/24/2009 01A3 AM Surr: 2-Fluorobiphenyl 90.3 59.108 %REC 1 31241200901:43 AM Surr:2-Fluorophenol 9.99 50-111 s %REC 1 3/2412009 01:43 AM Surr:4Terphenyl-dl4 97.7 58.135 %REC 1 3/2412009 01:43 AM Surr: Nitrobenzene-d5 85.9 54-115 %REC 1 3/24/2009 01:43 AM Surr:Phenol-d5 47.0 58-112 s %REC 1 3/24/2009 01A3 AM QualiOcrs: E Analyte detected in the associated Method Blank E Value above quanthation range H Holding tines for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits duo to matrix imerferenee Results arc webunless otherwise specified DO Surrogate Diluted Out AdrLabo atormologr tuGorulodes 327.51i'ulnrrtAvcune, Siguulflill, CA 90755 Tel: 562. 939.4045 lax: S62.939.4040 22 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B4-0.5 Lab Order: 104410 Collection Date: 3/10/2009 12:15:00 PM Project: Newport-SCEParcel, 602497-001 Matrix: SOIL ' Lab ID: 104410-007 I Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GCB 090317A QC Batch: 53868 PrepDate: 3/16/2009 Analyst: CBR T1R Hydrocarbons: C8-C10 32 10 mg/Kg 1 3/17/1909 12:17 PM T/R Hydrocarbons: CIO -CIO NO 10 mg/Kg 1 3/1711909 12:17 PM T/R Hydrocarbons: C18-C28 14 10 mg/Kg 1 3/17/1909 12:17 PM ' T/R Hydrocarbons: C28-C36 16 10 mg/Kg 1 3117/1909 12:17 PM T/R Hydrocarbons: C36-C40 ND 10 mg/Kg 1 3/17/1909 12:17 PM T/R Hydrocarbons: C8-C40 Total 62 10 mg/Kg 1 3/17/1909 12:17 PM ' Surr: p-Terphenyl 112 57-144 %REC 1 3/17/1909 12:17 PM PCBS BY GC/ECD EPA 3550E EPA 8082 ' RunID: GC5_090316B QC Balch: 53874 PrepDate: 3/16/2009 Analyst: HL Aroclor 1016 ND 16 pg/Kg 1 3/16/2009 11:29 PM Aroclor 1221 ND 33 pg/Kg 1 3/16/2009 11:29 PM Aroclor 1232 NO 16 pg/Kg 1 3/16/2009 11:29 PM ' Aroclor 1242 NO 16 pg/Kg 1 3/16/2009 11:29 PM Aroclor 1248 ND 16 pg/Kg 1 3/16/2009 11:29 PM Aroclor 1254 ND 16 pg/Kg 1 3/16/2009 11:29 PM ' Aroclor 1260 ND 16 pg/Kg 1 3/16/2009 11:29 PM 3/16/2009 11:29 PM Aroclor 1262 NO 16 pg/Kg 1 Aroclor 1268 ND 16 pg/Kg 1 3116/2009 11:29 PM Surr: Decachlorobiphenyl 72.9 30.124 %REC 1 3/16/2009 11:29 PM ' Surr: Tetrachloro-m-xylene 77.0 40-118 %REC 1 3/1612009 11:29 PM ' Qualifiers: B Analyte detected in the associated Method Blank E NO Value above quantimtion range Not Detected at the Reporting Limit 11 Holding times for preparation or analysis exceeded S SpiketSurregate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out �1 Advanced7ec6nologh 3275 Walnut Avenue, Signal fill, CA 907.55 Tel: SG? 989.4045 Pax: 562.989.4040 LnGarulorles ' �_ 23 of 43 I ANALYTICAL RESULTS 1 Advanced Technology Laboratories Print Date: 26-Mar-09 J CLIENT: Leighton Consulting, Inc. Client Sample ID: B4-1.8 , Lab Order: 104410 Collection Date: 3110/2009 12:30:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-008 ' Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION , LUFT EPA 8015B(M) RunID: GCB_090317A QC Balch: 53868 PrepDale: 3/16/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 10 mg/Kg 1 3/17/1909 12:45 PM ' T/R Hydrocarbons: C10-ClB NO 10 mg/Kg 1 3/17/190912A5 PM T/R Hydrocarbons: C18-C28 16 10 mg/Kg 1 3/171190912:45 PM T/R Hydrocarbons: C28-C36 ND 10 mg/Kg 1 3117/190912:45 PM , T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 31171190912:45 PM T/R Hydrocarbons: C8-C40 Total 16 10 mglKg 1 31171190912:45 PM Burr: p-Terphenyl 114 57-144 %REC 1 3/17/190912:45 PM ' PCBS BY GC/ECD EPA 3550B EPA 8082 RunlD: GC5 090316B QC Batch: 53874 PrepDale: 3/1612009 Analyst: HL ' Aroclor 1016 NO 16 pg/Kg 1 3/16/2009 11:59 PM Aroclor 1221 ND 33 pg/Kg 1 31161200911:59 PM Aroclor 1232 ND 16 pg/Kg 1 31161200911:59 PM Aroclor 1242 NO 16 pglKg 1 3116/200911:59 PM ' Aroclor1248 ND 16 pg/Kg 1 311612009 11:59 PM Aroclor 1254 Aroclor 1260 28 NO 16 16 pg/Kg pg/Kg 1 1 31161200911:59 PM 31161200911:59 PM ' Aroclor1262 NO 16 pg/Kg 1 311612009 11:59 PM Aroclor 1268 NO 16 pg/Kg 1 3/161200911:59 PM Burr: Decachlorobiphenyl 80.6 30.124 %REC 1 3116/2009 11:59 PM Surr. Tetrachloro-m-xylene 87,3 40.118 %REC 1 3/16/200911:59 PM ' I Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ' H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Sumagate outside of limits due to matrix interference Results arc wet unless other isespecificd DO Surrogate Dilutcd Out ' Adana bo Ttorles r i' Lu/iorutor/rs 327,5 IiIu6utt;;venue, S;gnulllil/, CA 907$$ Tel. 562. 939.4045 Fax: 562.989.4040 24 of 43 ' I ' ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 ' CLIENT: Leighton Consulting, Inc. Client Sample ID: E5-0.5 Lab Order: 104410 Collection Date: 3/10/2009 12:45:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL ' Lab ID: 104410-009 Analyses Result PQL Qual Units DP Date Analyzed ' HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunlD: GC8_090317A QC Batch, 53868 PrepDate: 3/16/2009 Analyst: CBR ' T/R Hydrocarbons, C8-C10 26 10 mg/Kg 1 3/17/1909 11:50 AM T/R Hydrocarbons: C10-C18 NO 10 mg/Kg 1 3/17/1909 11:50 AM T/R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 3/17/1909 11:50 AM ' T/R Hydrocarbons: C28-C36 13 10 mg/Kg 1 3117/1909 11:50 AM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 3/17/1909 11:50 AM TIR Hydrocarbons: C8-C40 Total 40 10 mg/Kg 1 3/17/1909 11:50 AM ' Burr: p-Terphenyl 113 57-144 %REC 1 3/17/1909 11:50 AM PCBS BY GC/ECD EPA 3550B EPA 8082 ' RunlD: GCS_090316B QC Batch: 53874 PrepDate: 3/16/2009 Analyst: HL Aroclor 1016 NO 16 pg/Kg 1 3/17/2009 12:29 AM Aroclor 1221 NO 33 pg/Kg 1 3/17/2009 12:29 AM Aroclor 1232 NO 16 pg/Kg 1 3/17/2009 12:29 AM ' Aroclor 1242 NO 16 pg/Kg 1 3/17/2009 12:29 AM Aroclor 1248 48 16 pg/Kg 1 3/17/2009 12:29 AM Aroclor 1254 NO 16 pg/Kg 1 3/17/2009 12:29 AM ' Aroclor 1260 NO 16 pg/Kg 1 3/17/2009 12:29 AM 3/17/2009 12:29 AM Aroclor 1262 NO 16 pglKg 1 Aroclor 1268 NO 16 pg/Kg 1 3/17/2009 12:29 AM Sort: Decachlorobiphenyl 78.7 30.124 %REC 1 3/17/2009 12:29 AM Surr: Telrachloro-m-xylene 85.2 40-118 %REC 1 3/17/2009 12:29 AM 1 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantization range I I Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Stake/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ;j AdroncedTec6nolo9r nne, Signolllill, CA90i55 TeL SGl. 939.4045 Fax: 562.939.4040 _ LnGarn[orics 32751ialnntAve 25 of 43 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B5-2.0 Lab Order: 104410 Collection Date: 3/10/2009 12:55:00 PM Project: Newport -SCE Parcel, 602497-001 Matrix: SOIL Lab ID: 104410-010 Analyses Result PQL Qual Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT RuniD: GCB 09D317A TIR Hydrocarbons: C8-C10 T/R Hydrocarbons: C10-C18 T/R Hydrocarbons: C18-C28 TIR Hydrocarbons: C28-C36 T/R Hydrocarbons: C36-C40 TIR Hydrocarbons: C8-C40 Total Surr. p-Terphenyl PCBS BY GCIECD RunlD: GC5_0903178 Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Surr: Decachlarobiphenyl Sun: Decachlorobiphenyl Surr: Tetrachloro-m-xylene Surr: Tetrachloro-m-xylene QQ Batch: EPA 3550E EPA 8015B(M) 53668 PrepDale: NO 10 mg/Kg 1 NO 10 mg/Kg 1 28 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 28 10 mg/Kg 1 107 57-144 %REC 1 QC Batch: 53914 EPA 8082 PrepDate: NO 16 pg/Kg 1 NO 33 pg/Kg 1 NO 16 pglKg 1 NO 16 pg/Kg 1 NO 16 p9/K9 1 92000 8200 pg/K9 500 NO 16 pg/Kg 1 NO 16 pg/Kg 1 NO 16 p91Kg 1 127 30.124 a %REC 1 0 30.124 soo ^/DREG 500 0 40.118 soo %REC 500 85.5 40.118 %REC 1 3/1612009 Analyst: CBR 3/17/190911:24 AM 3/17/190911:24 AM 3/17/190911:24 AM 3/17/190911:24 AM 3/17/190911:24 AM 3/17/190911:24 AM 3117/190911:24 AM 3/17/2009 Analyst: HL 3/17/2009 03:31 PM 3/1712009 03:31 PM 3/17/2009 03:31 PM 3/17/2009 03:31 PM 3/17/2009 03:31 PM 3117/2009 05:01 PM 3/17/2009 03:31 PM 3/17/2009 03:31 PM 311y/200903:31 PM 3/1712009 03:31 PM 3/1712009 05:01 PM 3/1712009 05:01 PM 3/17/2009 03:31 PM Qualifiers: D Analyte detected in the associated Method Blank E Value above quanlitntion range J� N Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside oritntitsdue tottwtrixinterference Results are wet unless otherwise specified DO Surrogate Diluted Out Adiwitecd bores rlumlogr tnborntorirs 32$5 11'alnnlAvenue, Signal/fill, C.1 90755 Tel: 562. 989.4045 Errs: 561.989.4040 26 of 43 1I M M Advanced Technology Laboratories Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8082_S iample ID MB-53874 SampType: MBLK TestCode: 8082_S Units: jig/Kg Prep Date: 3116/2009 RunNo: 106929 ;lienl ID: PBS Batch ID: 53874 TestNo: EPA 8082 EPA 3550E Analysis Date: 3/16/2009 SegNo: 1674089 \nalyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Dual Aroclor 1016 ND 16 Aroclor 1221 ND 33 Aroclor 1232 ND 16 Aroclor 1242 ND 16 Aroclor 1248 ND 16 Aroclor 1264 ND 16 Aroclor 1260 ND 16 Aroclor 1262 NO 16 Aroclor 1268 ND 16 Sum Decachlorobiphenyl 11.022 Sum Tetrachloro-m-uyiene 12.924 16.67 66.1 30 124 16.67 77.5 40 118 ;ample ID: LCS-53874 SampType: LCS TestCode: 8082_S Units: pg/Kg Prep Date: 3116/2009 RunNo: 106929 :Bent ID: LCSS Batch ID: 53874 TestNo: EPA 8082 EPA 3550E Analysis Date: 3/1612009 SegNo: 1674090 tnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 118.453 16 166.7 0 71.1 56 113 Aroclor 1260 122.869 16 166.7 0 73.7 58 111 Surr: Decachlorobiphenyl 11.462 16.67 68.8 30 124 Surr: Tetrachloro-m-xylene 12.915 16.67 77.5 40 118 iample ID: 104410-002AMS SampType: MS TestCode: 8082 S Units: pg/Kg Prep Date: 3116/2009 RunNo. 106929 ;Bent ID: B11-2.0 Balch ID: 53874 TestNo: EPA 8082 EPA 3550E Analysis Date, 3/16/2009 SegNo: 1674091 imalyte Result PQL SPK value SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val %RPD RPDLimit Dual Aroclor 1016 134.792 16 166.7 0 80.9 bi Aroclor 1260 148.574 16 166.7 0 89.1 39 Sure: Decachlorobiphenyl 13 666 16.67 82.0 30 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantization range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Adrvnttd Technology �� fslrornlnrks 3275 lf'n/nerrAvrnne, Signnf Hdf, Gl 90753 Tc% 53d 939.4045 Fae: 362.989.4040 27 of 43 ill 123 124 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Rork Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8082_S Sample ID: 104410-002AMS SampType: MS TestCodw 8082 S Units: VS/Kit Prep Date: 3/1612009 RunNo: 106929 :lienl ID: Bt-2.0 Batch ID: 53874 TestNo: EPA 8082 EPA 3550B Analysis Date: 3/1612009 SegNo: 1674091 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimd RPD Ref Val %RPD RPDLimit Qua[ Surr. Tetrachlom-m-xylene 15.112 16.67 90.7 40 I la 'ample ID: 104410-002AMSD SampType: MSD TestCode: 8082 S Units: pg/Kg Prep Date: 3/1612009 RunNo: 106929 ;Ilent ID: B7-2.0 Batch ID: 53874 TestNo: EPA 8082 EPA 3550E Analysis Date: 311612009 SegNo: 1674092 \nalyte Result PQL SPK value SPK Ref Val e/ REC LowUrnit Hfght-imit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 133.346 16 166.7 0 80.0 51 Ill 134.8 1.08 20 Aroclor 1260 146.506 16 166.7 0 87.9 39 123 148.6 1.40 20 Sun: Decachlombiphenyl 13.647 16.67 81.9 30 124 0 0 Sun: Tetrachloro-m-xylene 15.021 16:67 90.1 40 118 0 0 Qualifiers: B Anslyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogatc outsideoflimits due to matrix interference DO Surrogate Diluted Out Calculations arc based on raw values Ad�anredWchpd&MF Laborararlrs 3275 Walnur: (venue, Signal Hiff, CA 90755 Tel. 562. 939.4015 rm 5629824040 28 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8082_S Sample ID: MB-53914 SampType: MBLK TestCode: 8082_S Units: pg/Kg Prep Date: 3117/2009 RunNo: 107004 Client ID: PBS Batch ID: 53914 TestNo: EPA 8082 EPA 3550E Analysis Date: 3117/2009 SegNo: 1675401 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 ND 16 Aroclor 1221 NO 33 Aroclor 1232 NO 16 Aroclor 1242 NO 16 Aroclor 1248 NO 16 Aroclor 1254 ND 16 Aroclor 1260 NO 16 Aroclor 1262 ND 16 Aroclor 1268 NO 16 Sum. Decachlorobiphenyl 11.579 Surr: Tetrachloro-m-xylene 13.256 16.67 69.5 30 124 16.67 79.5 40 118 ;ample ID: LCS-53914 SampType: LCS TestCode: 8082_S Units: pg/Kg Prep Date: 3117/2009 RunNo: 107094 :Bent ID: LCSS Batch ID: 53914 TestNo: EPA 8082 EPA 3550B Analysis Date: 3117/2009 SegNo: 1675402 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imd RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 122 269 16 166.7 0 73.4 bb 113 Aroclor 1260 129.342 16 166.7 0 776 58 111 Surr: Decachlorobiphenyl 11.913 16.67 715 30 124 Surr. Tetrachloro-m-xylene 13275 16.67 79.6 40 118 ;ample ID: 104410-010AMS SampType: MS TestCode: 8082_S Units: pg/Kg Prep Dale: 311712009 RunNo: 107004 :Bent ID: 85-2.0 Batch ID: 53914 TestNo: EPA 8082 EPA 3550E Analysis Date: 311712009 SegNo: 1675813 lnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sum. Decachlorobiphenyl Sum Tetmchlom-m-xylene 26.298 16.67 14.625 16.67 158 30 124 87.7 40 118 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations arc based on raw values AdtartrtdTtrhno(o;,p I Labd Teches 3275 iPnlrtutdvenue Signn/Hdf, G1 90733 Tel, 562 989.4045 Fav: 36? 989.4040 29 of 43 H Holding times for preparation or analysis exceeded S SprkdSurrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Pork Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8082_S Sample 10: 104410-010AMSD SampType: MSD TestCode: 8082_S Units: pg/Kg Prep Date: 3/17/2009 RunNo: 107004 Client ID: B5-2.0 Batch ID: 53914 TestNo: EPA $082 EPA 3550E Analysis Dale: 3117/2009 SegNo: 1675814 Analyte Result POL SPK value SPK Rat Val °!DREG LowLimit Hight-imit RPD Ref Val %RPD RPDL1mit Oual Sum Decachloroblphenyl 25.862 16.67 155 30 124 0 0 S Sum Tetrechloro-m-xylene 14.722 16.67 88.3 40 118 0 0 Sample ID: 104410-010AMS SampType: MS TestCode: 8082 S Units: pg/Kg Prep Date: 3/17/2009 RunNo: 107004 ClientlD: B5-2.0 Batch ID: 53914 TestNo: EPA S082 EPA 3550B Analysis Date: 3/17/2009 SegNo: 1675815 Analyte Result POL SPKvalue SPK Ref Val %REC Lowlimit Highl-imit RPD Ref Val %RPD RPDLimit Oust Aroclor 1016 ND 8200 166.7 0 0 51 111 SDD Arocior 1260 ND 8200 166.7 0 0 39 123 SOO Sum Decachlombiphenyl 0 16.6T 0 30 124 SOO Sum Tetrachbro-m-aylene 0 16.67 0 40 118 SOO Sample ID: 104410-010AMSD SampType: MSD TestCode: 8082 S Units: pglKg Prep Date: 3/1712009 RunNo: 107004 Client ID: B5-2.0 Batch ID: 53914 TestNo: EPA 8082 EPA 3550E Analysis Date: 3117/2009 SegNo: 1675816 Analyte Result POL SPKvaiue SPK Ref Val %REC LowLimit Hight.imit RPD Ref Val %RPD RPDUmlt Quell Aroclor 1016 ND 8200 166.7 0 0 51 111 929.3 0 20 500 Aroclor 1260 ND 8200 166.7 0 0 39 123 0 0 20 SDO Sum Decachlorobiphenyl 0 16.67 0 30 124 0 0 SOO Sum Tetrachloro-m-xylene 0 16.67 0 40 118 0 0 SDO Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S SpikclSurrogate outsideof limits due to matrix interference DO Surrogate Diluted Out Calculations arc based on raw values ,Idnneed Ta6notoH Lxboratorkl 3275 Matnutdvenne, SignatHill, C4907SS Tek S62989.404S Far. 56Z989.4040 30 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8260_S Sample ID: T090319LC2 SampType: LCS TestCode: 8260_S Units: jig/Kg Prep Date: RunNo. 107234 Client ID: LCSS Batch ID: T09VS076 TestNo: EPA 8260B Analysis Date: 311912009 SegNo: 1679397 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 49.790 5.0 50.00 0 99.5 7u 19u Benzene 88.860 5.0 100.0 0 88.9 70 130 Chlorobenzene 47.350 5.0 5000 0 94.7 70 130 MTBE 47.590 5.0 50.00 0 95.2 70 130 Toluene 91.600 5.0 100.0 0 91.6 70 130 Trichloroethene 45.460 5.0 50.00 0 90.9 70 130 Surr: 1,2-Dichloroethane-d4 42.860 50.00 85.7 70 130 Surr: 4-Bromofluorobenzene 48.610 50.00 97.2 70 130 Surr: Dibromofluoromethane 49.730 50.00 99.5 70 130 Surr: Toluene-d8 50.880 50.00 102 70 130 Sample ID: T090319MB2MS Client ID: ZZ7777 Analyte SampType: MS Balch ID: T09VS076 Result TestCode: 8260_S TestNo, EPA 8260E PQL SPK value Units: pg/Kg SPK Ref Val %REC Prep Date: Analysis Date: 311912009 LowLimit HighLimit RPD Ref Val 1,1-Dichloroethene 51.820 5.0 50.00 0 104 70 130 Benzene 102.540 5.0 100.0 0 103 70 130 Chlorobenzene 52A60 5.0 50.00 0 105 70 130 MTBE 51.090 5.0 50.00 0 102 70 130 Toluene 104.980 5.0 100.0 0 105 70 130 Trichloroethene 51.030 5.0 50.00 0 102 70 130 Surr: 1,2-Dichloroethane-d4 44.530 5000 89.1 70 130 Surr: 4-Bromofluorobenzene 51.740 50.00 103 70 130 Surr: Dibromofluoromethane 50.690 50.00 101 70 130 Surr: Toluene-d8 54.990 50.00 110 70 130 RunNo: 107234 SegNo: 1679398 %RPD RPDLimit Qual Sample ID. T090319MB2MSD SampType: MSD TestCode: 8260_S Units: pg/Kg Prep Date' RunNo: 107234 Client ID: ZZ7777 Batch ID. T09VS076 TestNo: EPA 8260E Analysis Date: 311912009 SegNo: 1679399 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imil HighLimtt RPD Ref Val %RPD RPDLimit Qual Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limn R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations am based on raw values A .tdrmnc rr no zahn tnricr oy 3275 'alnntAvenrce, Signn(Xil Rn: CA 90755 Tel. 562. 939.404i i62.989.4040 31 of 43 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of hmits due to matrix interrercnce CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8260 S Sample ID: T090319MB2MSD SampType: MSD TestCode: 8260_S Units: pglKg Prep Date: RunNo: 107234 Client ID., 77 Batch ID: T09VS076 TesWo: EPA 8260B Analysis Date: 3/19/2009 SegNo: 1679399 Analyte Result PQL SPKvalue SPKRef Val %REC LowLimit HighLimit RPD Ref Va1 %RPD RPDLimit Qual 1,1-Dichloroethene 51.330 5.0 50.00 0 103 70 130 5L82 0.95D 20 Benzene 102.480 5.0 100.0 0 102 70 130 102.5 0.0585 20 Chlorobenzene 51.590 5.0 50.00 0 103 70 130 52A6 1.67 20 MTBE 52.560 5.0 50.00 0 105 70 130 51.09 2.84 20 Toluene 103.000 5.0 100.0 0 103 70 130 105.0 1.90 20 Trichiorcethene 50.040 6.0 50.00 0 100 70 130 51.03 1.96 20 Sum 1,2-Dichlorcethane-d4 44.350 50.00 88.7 70 130 0 20 Sum. 4-Bmmofluorobenzene 51.240 50.00 102 70 130 0 20 Surr: Dibromoffuommethane 52.140 60.00 104 70 130 0 20 Surr. Toluene-d8 54.910 50.00 110 70 130 0 20 iample ID: T090319MB2 SampType: MBLK TeslCode: 8260 S Units: pg1Kg Prep Date: RunNo: 107234 Nent ID: PBS Batch ID: T09VS076 TesWo: EPA 8260E Analysis Date: 3/1912009 SegNo: 1679400 4nalyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 1,1,1,2-Tetrachloroethans NO 5.0 1,1,1-Trichloroethane NO 5.0 1,1,2,2 Tetrachlomethane NO 5.0 1,1,2 Trichloroethane NO 5.0 1,1-Dichloroethane NO 5.0 1,1-Dichlomethene ND 5.0 1,1-Dichlompropene ND 5.0 . 1,2,3-Trichlorobenzene ND 5.0 1,2,3-Trichloropropane ND 5.0 1,2,4-Trichlorobenzene NO 5.0 1,2,4-Trimethylbenzene NO 5.0 1,2-Dbromo-3-chloropropane NO 10 T,ZDibromoethane ND 5,0 1,2-Dichlombenzene NO 5.0 1,2-Dichloroethane ND 5.0 QuaiiBees: B Analyte detected in theassociated Method Blank E Value above quantization range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted rccoverylimiLs S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on mw values AdrnncedTeeAwo/ay lyyo+yrom 3217+ Il'a/nurdvenne, Signal Hi/l, C•1 90755 Tel: 562 939.4045 Pac 50.989.4040 32 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8260_S Sample ID: T090319MB2 Client ID: PBS Analyte 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropylloluene 4-Methyl-2-pentenone Acetone Benzene Bromobenzene Bromochloromethane Bromod ichloromethane Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Di -isopropyl ether Dibromochloromethane Dibromomethane SampType: MBLK TestCode: 8260_S Units: pglKg Batch ID: T09VS076 TestNo: EPA 8260E Result PQL NO 5.0 ND 5.0 NO 5.0 NO 5.0 NO 50 NO 5.0 NO 50 NO 5.0 ND 50 NO 50 NO 5.0 NO 50 NO 50 ND 5.0 NO 5.0 ND 5.0 NO 5.0 ND 5.0 NO 5.0 NO 5.0 NO 5.0 NO 5.0 ND 5.0 NO 5.0 NO 5.0 NO 5.0 NO 5.0 NO 5.0 NO 5.0 NO 5.0 SPK value SPK Ref Val Prep Date: Analysis Date: 3/19/2009 %REC LowLimit Highl-imit RPD Ref Val Qualifiers: B Analytc detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Ad MTh o! rvnr n n o,,,t I' , laboromrhk 3275 flnlnutdvertng StgurtlHill, CA 90755 Tel. 562. 939.4045 Fat. 562.9324040 33 of 43 RunNo: 107234 SegNo: 1679400 %RPD RPDUmit Qual H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8260_S RunNo: 107234 Sample ID: T090319MB2 SampType: MBLK TestCode: 8260 S Units: Ng/Kg Prep Date. Client ID: PBS Batch ID: T09VS076 TestNo: EPA 8260E Analysis Date: 311912009 SegNo: 1679400 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RP.D Ref -Val yoRPD RPDLimit Qual Dichlorodifluommelhane NO 5.0 Ethyl Acetate NO 50 Ethyl Ether NO 50 Ethyl Tert-butyl ether NO 5.0 Etylbenzene NO 5.0 Freon-113 NO 5.0 Hexachlorobutadiene NO 5.0 lodomethane NO 5.0 Isopropylbenzene NO 5.0 m,p-Xylene NO 10 Methylene chloride- NO 5.0 MTBE NO 5.0 n=Butylbenzene NO 5.0 n-Propyibenzene NO 5.0 Naphthalene NO 5.0 o-Xylene NO 5.0 sec-Butylbenzene NO 5:0 Styrene NO 5.0 Tert-amyl methyl ether NO 5.0 Tert-Butanol NO 100 tert-Butylbenzene NO 5.0 Tetrachloroethene NO 5.0 Toluene NO 5.0 trans-1,2-Dichloroethene NO 5.0 trans-1,3-Dichloropropene NO 5.0 Tdchlomethene NO 5.0 Trichloronuommethane NO 5.0 Vinyl acetate NO 50 Vinyl chloride NO 5.0 Xylenes, Total NO 15 Qualifiers: B Analyte detected in the associated Method Blank E Value aboverquantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arc baud on raw values AdrgnrMTecAaa/oar Lafrnnlarms 327571 rs1nnlAvemn; Signallfill, C4 90755 Tel: 562939.4045 Far: 50?.984.J040 34 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8260_S 'ample ID: T090319MB2 SampType: MBLK TestCode: 8260_S Units: pglKg Prep Date, RunNo: 107234 :lien( ID: PBS Batch ID: T09VS076 TestNo: EPA 8260E Analysis Date: 3119/2009 SegNo: 1679400 4nalyte Result PQL SPK value SPK Ref Val %REC LowUrmt Highl-imit RPD Ref Val %RPD RPDLimit Qua] Sum. 1,2-Dichloroelhane-d4 45950 50.00 91.9 /u 13u Surr: 4-Bmmofluorobenzene 48.740 50.00 97.5 70 130 Sur. Dibromolluoromethane 52.540 50.00 105 70 130 Sum, Toluene-d8 53290 50.00 107 70 130 Qualifiers: B Analytc detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Dtlutcd Out Calculations am based on raw values gl' G� Adtvnred Tocbnolalvlrorn/a ev 3275 /nn/dvertne Signs/Hi C4 90735 Tel. 562.939.40{5 rim. 561.989.{0{0 35 of 43 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8270 S FULL RunNo: 107270 Sample ID: MB-54042 SampType: MBLK TestCode: 8270 S FUL Units: pg/Kg Prep Date: 3/20/2009 Client ID: PBS Batch ID: 54042 TestNo: EPA 8270C EPA 3550E Analysis Date: 312312009 SegNo: 1680777 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighUmit RPD Ref Val %RPD RPDLimit Qua[ 1,2,4-Trichlorobenzene NO 330 1,2-Dichlorobenzene NO 330 1,3-Dichlorobenzene NO 330 1,4-Dichlorobenzene NO 330 2,4,5-Trichlorophenol NO 330 2,4,6-Trichlorophenol NO 330 2,4-Dichlorophenol ND 1600 2,4-Dimethylphenol ND 330 2,4-Dinitmphenol NO 1600 2,4-Dinitrotoluene NO 330 2,6-Dinitmtoluene NO 330 2-Chlaronaphthalene NO 330 2-Chlorophenol NO 330 2-Methylnaphthalene NO 330 2-Methylphenol NO 330 2-Nitroaniline NO 1600 2-Nitrophenol NO 330 3,3'-Dichlorobenzidine NO 660 3-Nitroaniline NO 1600 4,6-Dinitro-2-methylphenol NO 1600 4-Bmmophenyl-phenylether NO 330 4-Chloro-3-methylphenol NO 660 4-Chloreaniline NO 660 4-Chlomphenyl-phenylether NO 330 4-Methylphenoi NO 330 4-Nitroaniline NO 1600 4-Nitrophenol NO 1600 Acenaphlhene NO 330 Acenaphthylene NO 330 Anlhracene ND 330 Qualifiers: B Analyte detected in the associated Method Blank E Value above quant[mtion range H Holding times for pmpamtion or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spikc/Suaogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations am based on raw values AdWaced Trebnolu_� j. LyDorNcda 3275 Watnrt0.brnm; Signal Hill, C4 90755 Tel: 56A 939.4045 raw 561989.4040 36 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8270_S_FULL Sample ID: MB-54042 SampType: MBLK TestCode: 8270_S_FUL Units: pg1Kg Prep Date: 3/2012009 RunNo: 107270 Client ID. PBS Balch ID: 54042 TestNo: EPA 8270C EPA 3550B Analysis Date: 312312009 SegNo: 1680777 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Senzidine (M) NO 1600 Benzo(a)anthracene NO 330 Benzo(a)pyrene NO 330 Benzo(b)0uomnthene NO 330 Benzo(g,hd)perylene NO 330 Benzo(k)0uoranthene NO 330 Benzoic acid NO 1600 Benzyl alcohol NO 660 Bis(2-chloroethoxy)methane NO 330 Bis(2-chloroethyl)ether NO 330 Bis(2-chloroisopropyl)ether NO 330 Bis(2-ethylhexyl)phthalate NO 330 Bulylbenzylphthalate NO 330 Chrysene NO 330 Di-n-butylphthalate NO 330 Di-n-oclylphthalale NO 330 Dibenz(a,h)anthracene NO 330 Dibenzofuran NO 330 Diethylphthalate NO 330 Dimelhylphthalate NO 330 Fluoranthene NO 330 Fluorene NO 330 Hexachlorobenzene NO 330 Hexachlorobutadiene NO 660 Hexachlorocyclopentadiene NO 660 Hexachloroethane NO 330 Indeno(1,2,3-cd)pyrene NO 330 ]sophorone NO 330 N-Nitrosodi-n-propylamine NO 330 N-Nitrosodiphenylamme NO 330 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S SpikedSurrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arc based on rawvalues Adr'arsrcdTirhrsalo� j, 1 Labo 7'mhll 3275 A'nlnn4lveime, Signa/Xil; CA 90755 Tel: 562. 939.4045 Fm: i62.989.4040 37 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 TestCode: 8270 S_FULL Sample ID: MB-54042 SampType: MBLK TestCode: 8270_S_FUL Units: pg/Kg Prep Date: 312012009 RunNo: 107270 'lient ID: PBS Batch ID: 54042 TestNo: EPA 8270C EPA 3550B Analysis Date: 3/23/2009 SegNo: 1680777 knalyte Result PQL SPKvalue SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %,RPO RPDLimit Quai Naphthalene ND 330 Nitrobenzene NO 330 Pentachlorophenot NO 1600 Phenanthrene NO 330 Phenol NO 330 Pyrene NO 330 Sun: 1,2-Dlchiorobenzene-d4 3005.000 Sun. 2,4,6-Tribromophenol 3380.333 Sum. 2-Chlorophenol-d4 3199.000 Sum 2-Fluorobtphenyl 3513.000 Sun: 2-Fiuorophenol 3104.333 Sure 4-TerphenyW14 3693.000 Sum.Nitrobenzene-d5 3581.000 Surr. PhenoW5 3308.333 3330 90.2 49 103 3330 102 47 129 3330 96.1 54 109 3330 105 59 108 3330 93.2 50 111 3330 111 58 135 3330 108 54 115 3330 99.3 58 112 Sample ID: LCS.54042 SampType: LCS TestCode: 8270 S FUL Units: pg/Kg Prep Date: 3120/2009 RunNo: 107270 Client ID: LCSS Batch ID: 54042 TestNo: EPA 8270C EPA 3550E Analysis Dale: 3123/2009 SegNo: 1680778 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HlghLimit RPD Ref Val %RPD RPDUmit Qual 1,2.4 Trichlorobenzene 3050.000 330 3330 0 91.6 61 107 1,4-Dichlorobenzene 2890.667 330 3330 0 86.8 56 100 2,4-Dinitrotoluene 3327.667 330 3330 0 99.9 72 130 2-Chlorophenol 3008.667 330 3330 0 90A 64 105 4-Chloro-3-methylphenol 3560.000 660 3330 0 107 74 125 4-Nitrophenol 4197.000 1600 3330 0 126 77 137 Acenaphthene 3419.333 330 3330 0 103 63 117 N-Nttmsodi-n-propylamine 3594.000 330 3330 0 108 71 121 Pentachlorophenol 3133.667 1600 3330 0 94.1 69 125 Phenol 3342.000 330 3330 0 100 67 111 Pyrene 3164.333 330 3330 0 95.0 60 122 Qualifiers: B Analytc detected in the associated Method Blank E Value above quandtation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S SpikdSurrogate outside oflimits due to matrix interference DO Surrogate Diluted Out Calculationsarc based onraw values Adranred TirAno 31751f ulnnldvrnnr, SignalMill, C4 90755 Tck 562 989.4045 Fur::6-'.989.4040 LnDarslaries 00 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8270_S_FULL Sample ID: LCS-54042 SampType: LCS TestCode: 8270_S_FUL Units: pglKg Prep Date: 3120/2009 RunNo: 107270 Client ID: LCSS Batch ID: 54042 TestNo: EPA 8270C EPA 3550E Analysis Date: 3/2312009 SegNo: 1680778 Analyle Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imn RPD Ref Val %RPD RPDLimd Qual Surr: 1,2-Dichlorobenzene-d4 2811.000 3330 84.4 49 103 Surr. 2,4,6-Tribromophenol 3668 000 3330 110 47 129 Surf: 2-Chlorophenol-d4 2943.333 3330 88.4 54 109 Sum 2-Fluorobiphenyl 3525.667 3330 106 59 108 Sum 2-Fluorophenol 2836.000 3330 85.2 50 ill Sum 4-Terphenyl-dl4 3115.333 3330 93.6 58 135 Sum: Nitrobenzene-d5 3325.667 3330 99.9 54 115 Suff: Phenol-d5 3112.000 3330 93.5 58 112 Sample ID: 10451M02AMS SampType: MS TestCode: 8270_S FUL Units: pglKg Prep Date: 3/2012009 RunNo: 107270 Client ID: ZZZZZZ Batch ID: 54042 TestNo: EPA 8270C EPA 3550B Analysis Date, 3123/2009 SegNo: 1680779 Analyte Result PQL SPK value SPK Ref Val %REC LowLtmit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trmhlorobenzene 3014.667 330 3330 0 90.5 60 105 1,4-Dichlorobenzene 2830.667 330 3330 0 850 50 99 2,4-Dinitrotoluene 3313.667 330 3330 0 99.5 70 130 2-Chlorophenol 3153.333 330 3330 0 947 58 107 4-Chloro-3-methylphenol 3626 667 660 3330 0 109 72 124 4-Nitrophenoi 4299.000 1600 3330 0 129 69 139 Acenaphlhene 3496.333 330 3330 0 105 59 118 N-Ndrosodi-n-propylamine 3697.667 330 3330 0 ill 61 125 Pentachlorophenol 3311.667 1600 3330 0 99A 56 131 Phenol 3493.000 330 3330 0 105 60 113 Pyrene 3089.667 330 3330 0 928 51 130 Surr: 1,2-Dichlorobenzene-d4 2772.667 3330 833 49 103 Surr: 2,4,6-Tribromophenol 3732.667 3330 112 47 129 Surr: 2-Chlorophenol-d4 3081.000 3330 92.5 54 109 Surr: 2-Fluorobiphenyl 3534.667 3330 106 59 108 Sun: 2-Fluorophenol 2949.667 3330 886 50 i l l Surr: 4-Terphenyl-dl4 3223.333 3330 96.8 58 135 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogatc outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arc based on raw values 1 Adrmnred Terhaalo,�• La60n1011tes 3275 {I0/mrbl venue, Signal Hill, Cif 90755 Tel. 562 939.4045 Pm: 562.989.4040 39 of 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: 8270_S_FULL RunNo., 107270 Sample ID: 104519-002AMS SampType: MS TestCode: 8270 S FUL Units: pg/Kg Prep Date: 312012009 client ID: 777777 Batch ID: 54042 TestNo: EPA 8270C EPA 3550B Analysis Date: 3/2312009 SegNo: 1680779 Malyte Result POL SPK value SPK Ref Val %REC LowUmit HighLfmit RPO Ref Val %RPD RPDLimit Qual Sun: Nitmbenzened5 3338.667 3330 100 54 115 Surr. Phenotd5 3219,000 3330 96.7 58 112 Sample ID: 104519-002AMSD SampType: MSD TestCode: 8270 S_FUL Units: pg/Kg Prep Date: 3/20/2009 RunNo: 107270 client ID: 2Z2ZZZ Batch ID: 54042 TestNo: EPA 8270C EPA 3550B Analysis Date: 3/2312009 SegNo: 1680780 4nalyte Result PQL SPK Value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene 3272.333 330 3330 0 98.3 60 105 3015 8.20 20 1,4-Dichlombenzene 3069.000 330 3330 0 92.2 50 99 2831 - 8.08 20 2,4-Dirdhotoluene 3606.333 330 3330 0 108 70 130 3314 8A6 20 2-Chlorophenol 3368.333 330 3330 0 101 58 107 3153 6.59 20 4-Chloro3-melhyiphenol 3870.667 660 3330 0 116 72 124 3627 6.51 20 4-Nitrophenol 4482.000 1600 3330 0 135 69 139 4299 4.17 20 Acenaphthene 3845.333 330 3330 0 115 59 118 3496 9.51 20 N-Nitrosodi-n-propylamine 3928.333 330 3330 0 118 61 125 3698 6.05 20 Pentachlorephenol 3613.000 1600 3330 0 108 56 131 3312 8.70 20 Phenol 3744.333 330 3330 0 112 60 113 3493 6.95 20 Pyrene 3367.000 330 3330 0 101 51 130 3090 8.59 20 Sun: 1,2-Dichlombenzened4 2990.000 3330 89.8 49 103 0 0 Sum 2.4,6 Tribmmophenol 3932.667 3330 118 47 129 0 0 Sum 2-Chiomphenol-d4 3271.000 3330 98.2 54 109 0 0 Sun: 2-Flucrobipheoyl 3877.333 3330 116 59 108 0 0 S Sum 2-Fluomphenol 3172.667 3330 95.3 50 111 0 0 Sum 4-Terphenyid14 3450.667 3330 104 58 135 0 0 Sum Nitrebenzened5 3580.333 3330 108 54 115 0 0 Sum Phenol-d5 3431.000 3330 103 58 112 0 0 Qualifiers: 8 Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits ,DO Surrogate Dilutcd Oul Calculations are based on raw values Adtwncrd rorAaafe-r• LAQW.rirt 31"3 n'almrtfirnn , Signnllfi/1, C4 90755 TtL• 562 989.4045 Frcv: s6E989.4040 H Holding times forprepamtion ormalysis exceeded S Spike/Surrogate outside of limits due to matrix interference 40 Ul 43 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: HC_S_ATL Sample ID: MB-53868 SampType: MBLK TestCode: HC_S_ATL Units: mg/Kg Prep Date: 3/16/2009 RunNo: 107003 client ID: PBS Batch ID: 53868 TeslNo: EPA 8015B(M LUFT Analysis Date: 311711909 SegNo: 1675387 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-mut RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: C8-C10 ND 10 T/R Hydrocarbons: C10-C18 ND 10 T/R Hydrocarbons: C18-C28 NO 10 T/R Hydrocarbons: C28-C36 NO 10 TIR Hydrocarbons: C36-C40 NO 10 T/R Hydrocarbons: C8-C40 Total NO 10 Surr: p-Terphenyl 78.681 80.00 98.4 57 144 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations arc based on raw values tdtmared Terhaofo^v Gj' , ' LaBontraries n 3275 WalmnAvenue, Stgnal Hill, CA 90755 Telr 562. 939.4045 rhw 562.989.4040 ��PW 41 of 43 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel, 602497-001 TestCode: HC_S_V0AC4C12 Sample ID: E090319MBI SampType: MBLK TestCode: HC S_VOAC Units: mg/Kg Prep Date: RunNo: 107164 Client ID: PBS Batch ID: E09VS078 TestNo: EPA 8015E Analysis Date: 3/1912009 SegNo: 1678173 Analyte Result POL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: C4-C12 NO 1.0 Surr.-Bromofluorobenzene (FID) 86207 100.0 862 59 145 Sample ID: 104410-0O6AMS SampType: MS TestCode: HC S VOAC Units: mg/Kg Prep Date: RunNo: 107164 Client ID: B34.3 Batch ID: E09VS078 TeslNo: EPA 8015E Analysis Date: 3/19/2009 SegNo: 1678177 Analyte Result PQL SPKvalue SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Hydrocarbons: C4-C12 4.481 1.0 5.000 0 89.6 39 135 ;um Bromofluombenzene (FID) 104.104 100.0 104 59 145 triple ID: 104410-0O6AMSD SampType: MSD TestCode: HC S VOAC Units: mg1Kg Prep Date: RunNo: 107164 ent ID: B34.3 Batch ID: E09VS078 TesWo: EPA 8015B Analysis Date: 3/1912009 SegNo: 1678178 alyte Result PQL SPKvalue SPKRef Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: C4-C12 4.455 1.0 5.000 0 89.1 39 135 4.481 0.582 20 Sum Bromofluorobenzene (FID) 104.796 100.0 105 59 145 0 0 Sample ID: E090319LCSI SampType: LCS TestCode: HC_S VOAC Units: mg/Kg Prep Date. RunNo: 107164 Client ID: LCSS Batch ID: E09VS078 TesWo: EPA 8015E Analysis Date: 311912009 SegNo: 1678179 Analyte Result PQL SPK-value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] TIR Hydrocarbons: C4-C12 4.784 1.0 6.000 0 95.7 73 120 Sum Bromofluorobenzene (FID) 90.156 100.0 90.2 59 145 - QuAlrrers: B Analytc detected- in the associated Method Blank E Value above quantization range H Holding times fortimpamtion or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside orlimits due to matrix interference ,DO Lv Surrogate Diluted Out Calculations arc based on raw values AlftnZ dTnDr/nrirsro(w�r ban 32>S 1l'alnrrt.4venrre, Sigua(Hi(l, C4 90'55 T<Y. 562 989.4645 Far. 562.98R4P40 42 of 43 M " = M = = M r= r"= M M= M Advanced Technology Laboratories Date: 26-Mar-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 104410 Project: Newport -SCE Parcel,602497-001 BatchID: 53868 ,ample ID: LCS-53868 SampType: LCS TestCode: 8015_S_DM Units: mg/Kg Prep Date: 311612009 RunNo: 107003 ;lien[ ID: LCSS Balch ID: 53868 TestNo: EPA 8015B(M LUFT Analysis Date: 3/17/1909 SegNo: 1675383 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 1021.900 10 1000 0 102 81 128 Surf: p-Terphenyl 89.756 80.00 112 57 144 ;ample ID: 104410-009AMS SampType: MS Testcode: 8015_S_DM Units: mg/Kg Prep Date: 311612009 RunNo: 107003 :lien ID: B5-0.5 Batch ID: 53868 TestNo: EPA 8015B(M LUFT Analysis Date: 3/17/1909 SegNo• 1675385 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Vat %RPD RPDLimit Dual DRO 1089.485 10 1000 11.74 lob b8 140 Surr: p-Terphenyl 97.132 80.00 121 57 144 ;ample ID: 104410-009AMSD SampType: MSD TeslCode: 8015_S_DM Units: mg/Kg Prep Dale. 3/1612009 RunNo: 107003 :lien[ ID: B5-0.5 Batch ID: 53868 TestNo: EPA 8015B(M LUFT Analysis Date: 3117/1909 SegNo: 1675386 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimd Qual DRO Sum p-Terphenyl 1057.622 10 1000 11.74 lob 91.527 80.00 114 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits w DO Surrogate Diluted Out Calculations arc based on raw values am• .lduincrdrr no ,„f lalm/nmw, 3275 ll'almndrenue, Signal Hill, CA 90755 Tel: 56Z 989.4045 Fax: 562.989.4040 43 of 43 0-1 7 h ln b8 140 lubu Z a/ zu 57 144 0 0 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference M = I r I I 11 I I I I LJ j 1 I August 12, 2009 Meredith Church Leighton Consulting, Inc. 17781 Cowan Street Irvine, CA 92614 TEL: (949) 681-4208 FAX: (949) 757-7230 RE: SCE Newport, 602497-003 Attention: Meredith Church ACCC9poy s= n S� U [ S ELAP No.:1838 NELAP No.: 02107CA NEVADA.: CA-401 CSDLAC No.:10196 Workorder No.: 106685 Enclosed' are the results for sample(s) received on August 03, 2009 by Advanced' Technology Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications. Thank you for the opportunity to service the needs of your company. Please feel free to call me at (562)989-4045 if'I can be of further assistance to your company. Sincerely, ' The cover letter and the case narrative, are an integral part of this analytical report and cannot be reproduced in part or ' in its entirety without written permission from the client and Advanced Technology Laboratories. Advanced Technology 3275 Walnut Avenue Signal Hill, CA 90755 Tel: 562 989-4045 Fax: 562 989-4040 Laboratories 1 of 68 I Advanced Technoloev Laboratories - CLIENT: Leighton Consulting, Inc. Project: SCE Newport, 602497-003 Lab Order: 106685 Analytical Comments for EPA 8015B(M) (C8-C40) -Date: 11-A❑ -09 _- - — - CASE NARRATIVE Samples 106654-OOIAMS and 106654-001AMSD. Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are outside recovery criteria; however, the analytical batch was validated by the Laboratory Control Sample (LCS). Sample 106654-001AMSD, RPD for Matrix Spike Duplicate (MSD) is outside criteria; however, the analytical batch was validated by the Laboratory Control Sample (LCS). Analytical Comments for EPA 8260B Sample 106685-006A, surrogate recovery biased low possibly due to matrix interferences. Samples 106685-006AMS and 106685-006AMSD, Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are outside recovery criteria; however, the analytical batch was validated by the Laboratory Control Sample (LCS). Analytical Comments for EPA 8270C Sample 106685-006A, surrogate recovery biased low possibly due to matrix interferences. Page Iof 65 Ad�maccdfechna/oar ^�-- --- - ` - --� -� - - --_ -- -- ' /�\\ 3275 (yrdnittAvemra, Signal HIH, CA 907.15 7a1: 562, 989.4045 fax. 562.989.4040 Laborararlcs 2 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-GW Lab Order: 106685 Collection Date: 8/3/2009 10:03:00 AM Project: SCE Newport,602497-003 Matrix: GROUNDWATER Lab ID: 106685-001A Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 8015B ' RunID: GC6_090804A QC Batch: 109VW0134 C4-C12 NO 0.20 PrepDate: Analyst: BD mg/L 1 8/4/2009 07:23 PM T/R Hydrocarbons: Surr: Bromofluorobenzene (FID) 85.4 71-130 %REC 1 8/4/200907:23 PM 1 Qualifiers: B Analyte detected in the associated Metbod Blank E Value above quantitation range H Holding limes for preparation or analysis exceeded ND Not Detected at (lie Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO surrogate Diluted Out wAdtuaced-Technology 11 Laboratories3275 Nalarr(Aveaue, Signal Hill, CA 90755 Tel: 562. 989.4045 Pas: 5(2.989.4040 3 of 68 ANALYTICAL It>;SULTS Advanced TechnologyLaboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-GW Lab Order: 106685 Collection Date: 8/3/2009 10:03:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-001B Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RunID: GC16 090806F QC Batch: T/R Hydrocarbons: C8-C10 57067 NO 0.20 PrepDale: mg/L 8/4/2009 Analyst: CBR 1 8/6/2009 06:40 PM T/R Hydrocarbons: CIO-C18 0.23 0.20 mg/L 1 8/6/2009 06:40 PM T/R Hydrocarbons: C18-C28 0.45 0.20 mg/L 1 8/6/2009 06:40 PM T/R Hydrocarbons: C28-C36 NO 0.20 mg/L 1 8/612009 06:40 PM T/R Hydrocarbons: C36-C40 ND 0.20 mglL 1 8/8/2009 06:40 PM TIR Hydrocarbons: CB-C40 Total 0.68 0.20 mg/L 1 8/612009 06AO PM Surr: p-Terphenyl 78.5 36.131 %REC 1 816/2009 06:40 PM r I I I I 1 I Qualifiers: B Analyte defected in the associated Method Blank E Value above quantilation range H Holding times for preparation or analysis exceeded NO Not Defected at the Rcponing Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out 14, Advanced Technology Laborulorles 327S Malurrl Avenue, Signal KCill. CA 9075S M. 56Z 989.4045 Fasr S62.989.4040 4 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample 1D: B6-GW Lab Order: 106685 Collection Date: 8/3/2009 10:03:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-001C Analyses Result PQL Qual Units DF Date Analyzed PCBS BY GC/ECD EPA 3510C EPA 8082 Run1D: GC4_090807A QC Batch: 57126 PrepDate: 8/6/2009 Analyst: BB Aroclor 1016 NO 0.50 pg/L 1 8/7/200911:01 AM Aroclor1221 ND 1.0 pg/L 1 8/7/2009 11:01 AM Aroclor 1232 ND 0.50 pg/L 1 817/200911:01 AM Aroclor1242 NO 0.50 pg/L 1 8/7/200911:01AM Aroclor 1248 NO 0.50 pg/L 1 8/7/2009 11:01 AM ' Aroclor 1211 NO 0.50 pg/L 1 8/7/2009 11:01 AM Aroclor 1260 ND 0.50 pg/L 1 8/7/200911:01 AM Aroclor 1262 NO 0.50 pg/L 1 817/200911:01 AM Aroclor1268 NO 0.50 pg/L 1 SI7/200911:01AM Surr: Decachlorobiphenyl 83.4 29-130 %REC 1 8l7/2009 11:01 AM Surr: Tetrachloro-m-xylene 85.2 48-126 %REC 1 8/7/2009 11.01 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out , Advanced Ter y 1Laboratories 3275 Va/td Avenue, Sigin[Hil1, CA 90755 7e[: 562. 939.4045 Fax: 562.989.4040�_ 5of68 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. _ Client Sample ID: B6-2 — Lab Order: 106685 Collection Date: 8/3/2009 9:47:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-002A Analyses Result PQL Qua] Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC16 0908060 T/R Hydrocarbons: C8-C10 QC Batch: 57087 NO 10 PrepDate: mglKg 8/5/2009 Analyst: CBR 1 8/612009 02:20 PM T/R Hydrocarbons: CIO-C18 NO 10 mg/Kg 1 816/2009'02:20 PM T/R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 8/6/2009 02:20 PM T/R Hydrocarbons: C28-C36 NO 10 mg/Kg 1 8/6/2009 02:20 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 8/6/2009 02:20 PM T/R Hydrocarbons: CB-C40 Total NO 10 mg/Kg 1 8/612009 02:20 PM Surr. p-Terphenyl 98.4 57.144 %REC 1 816/2009 02:20 PM , HYDROCARBON CHAIN IDENTIFICATION EPA 8015B RunID: GC2 090804E QC Batch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 8/4/2009 09:40 PM Surr. Bromolluorobenzene (FID) 95.5 59-145 %REC 1 8/4/2009 09:40 PM PCBS BY GC/ECD EPA 3550E EPA 8082 RunID: GC5 090806B QC Batch: 57129 PrepDate: 8/612009 Analyst: BB Aroclor1016 NO 16 pg/Kg 1 8171200912:12AM Aroclor1221 NO 33 pg/Kg 1 8f7/2009 12:12 AM Aroclor1232 NO 16 pg1Kg 1 8f7/200912:12AM Aroclor1242 ND 16 pg/Kg 1 W/2009 12:12 AM Aroclor1248 NO 16 pg/Kg 1 8/712009 12:12 AM Aroclor1264 NO 16 pg/Kg 1 8f7/200912:12AM Aroclor1260 NO 16 pg/Kg 1 81712009 12:12 AM Aroclor1262 NO 16 pg/Kg 1 8/7/2009 12:12 AM Aroclor1268 NO 16 pg/Kg 1 Bf7/200912:12AM Surr. Decachloroblphenyl 97.6 30.124 %REC 1 8f7/200912:12AM Surr: Tetrachloro-m-xylene 86.7 40.118 %REC 1 8f7/2009 12:12 AM I _1 Qualifiers: B Analyte detected in the associated Method Blank _ B Value above quantitation range H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside or limits due to matrix interfercnec Results arc wet unless otherwise specified DO Surrogate Diluted Out ' Advanced Tochnofogv LnGorAlorfes 3275 IVaGurlAverura, Sigurd Hill, C.I 90755 Tat: 562. 939.9045 !'ax: S62.989.4040 , 6 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-5 Lab Order: 106685 Collection Date: 8/3/2009 9:52:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL ' Lab ID: 106685-003A _ Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 801513(M) RunID: GC16 090806C QC Balch: 57087 PrepDate: 8/5/2009 Analyst: CBR ' T/R Hydrocarbons: C8-C10 ND 10 mg/Kg 1 8/612009 02:29 PM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 8/6/2009 02:29 PM T/R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 8/6/2009 02:29 PM T/R Hydrocarbons: C28-C36 ND 10 mg/Kg 1 8/6/2009 02:29 PM T/R Hydrocarbons: C36-C40 ND 10 mg/Kg 1 8/612009 02:29 PM T/R Hydrocarbons: CI-C40 Total ND 10 mg/Kg 1 8/6/2009 02:29 PM ' Surr: p-Terphenyl 95.6 57-144 %REC 1 8/6/2009 02:29 PM HYDROCARBON CHAIN IDENTIFICATION EPA 8015B RunID: GC2 090804B QC Batch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 ND 1.0 mg/Kg 1 814/2009 09:55 PM Burr: Bromofluorobenzene (FID) 94.4 59-145 %REC 1 8/4/2009 09:55 PM PCBS BY GC/ECD EPA 35506 EPA 8082 RunlD: G05 090806E QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB Aroclor 1016 ND 16 pg/Kg 1 8/7/2009 12:42 AM 8171200912:42 AM Aroclor 1221 ND 33 pg/Kg 1 Aroclor1232 ND 16 pg/Kg 1 817/2009 12:42 AM Aroclor 1242 ND 16 pg/Kg 1 8M200912:42 AM Aroclor1248 No 16 pg/Kg 1 8/712009 12:42 AM Aroclor 1254 ND 16 pg/Kg 1 8l7/200912:42 AM Aroclor 1260 ND 16 pg/Kg 1 817/200912:42 AM Aroclor 1262 ND 16 pg/Kg 1 8/7/2009 12:42 AM Aroclor 1268 ND 16 pg/Kg 1 8f7/200912:42 AM Surr. Decachlorobiphenyl 91.9 30-124 %REC 1 8/7/200912:42AM Surr: Tetrachloro-m-xylene 72.8 40-118 %REC 1 8/7/200912:42 AM VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunID: MS4 090805A QC Batch: K09VS145 PrepDate: Analyst: HH 1,1,1,2-Tetrachloroethane ND 50 pg/Kg 1 8/5/2009 12:33 PM 1,1,1-Trichloroethane ND 5.0 pg/Kg 1 8/5/200912:33 PM 1,1,2,2-Tetrachloroethane ND 5.0 pg/Kg 1 8/512009 12:33 PM 8/5/2009 12:33 PM 1,1,2-Trlchloroelhane ND 5.0 pg/Kg 1 B Analyle detected in the associated Method Blank E Value above quantitation range ' Qualifiers: H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out 11 AdtancedTechnolow 3275 TVrdnn[Avennq Signa[Hi[4 CA LuLorntorirs 9U755 %'eL 562. 989.4045 Pas: 562.989.4040 7 of 68 J Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-003A ANALYTICAL RESULTS Print Date: /2-Aug-09 Client Sample 1D: B6-5 - - - -- _- - Collection Date: 8/3/2009 9:52:00 AM Matrix: SOIL Analyses Result PQL Qual Units DF I Il ' Date Analyzed VOLATILE ORGANIC COMPOUNDS BY'GC/MS EPA 8260E RunlD: MS4 090805A QC Batch: K09VS145 PrepDate: Analyst: HR 1,1-Dichloroethane ND 5.0 pg/Kg 1 8/5/200912:33 PM 1,1-Dichloroethene No 5.0 pg/Kg 1 8/51200912:33 PM 1,1-Dichloropropene NO 5.0 pg/Kg 1 8/51200912:33 PM 1,2,3-Tdchlorobenzens NO 5.0 pg/Kg 1 8/512009 12:33 PM 1,2,3-Tdchloropropone ND 5.0 pg/Kg 1 8151200912:33 PM 1,2,4-Trichlorobenzene NO 5.0 pg/Kg 1 815/200912:33 PM 1,2,4-Trimelhylbenzene ND 5.0 plift 1 815/2009 12:33 PM 1,2-Dibromo-3-chloropropane ND 10 pg/Kg 1 815/200912:33 PM 1,2-Dibromoethane ND 5.0 pg/Kg 1 8/5/200912:33 PM 1,2-Dichlorobenzene ND 5.0 pg/Kg 1 8151200912:33 PM 1,2-Dichloroethane NO 5.0 pg/Kg 1 8/5/200912:33 PM 1,2-Dichloropropane NO 5.0 pg/Kg 1 8/5120091233 PM 1,3,5-Tdmelhylbenzene NO 5.0 pg/Kg 1 8151200912:33 PM 1,3-Dichlorobenzene ND 5.0 pg/Kg 1 8/51200912:33 PM 1,3-Dichloropropane ND 5.0 pg/Kg 1 815/200912:33 PM 1,4-Dichiorobenzene ND 5.0 pg/Kg 1 815/200912:33 PM 2,2-Dichlaropropane ND 5.0 pg/Kg 1 815/200912:33 PM 2-Chlorotoluene ND 5.0 pglKg 1 815/200912:33 PM 4-Chlorotoluene ND 510 pg/Kg 1 8/5/200912:33 PM 4-Isopropylloluene ND 5.0 pg/Kg 1 8/5/200912:33 PM Benzene ND 5.0 pg/Kg 1 815/200912:33 PM Bromobenzene NO 5.0 pg1Kg 1 8/5/200912:33 PM Bromodichloromethane NO 5.0 pg1Kg 11 8/51200912:33 PM Bromoform NO 5.0 pg/Kg 1 8/51200912:33 PM Bromomethane ND 5.0 pg/Kg 1 8/51200912:33 PM Carbon tetrachloride ND 5.0 pglKg 1 815/2009 12:33 PM Chlorobenzene NO 5.0 pg/Kg 1 815/200912:33 PM Chloroethane ND 5.0 pg/Kg 1 815/200912:33 PM Chloroform ND 5.0 pglKg 1 8/5/200912:33 PM Chloromelhane NO 5.0 pg/Kg 1 815/200912:33 PM cis-1,2-Dichloroethane ND 5.0 pg/Kg 1 8l5/200912:33 PM cis-1,3-Dichloropropene NO 5.0 pg/Kg 1 8/5/200912:33 PM DI -Isopropyl ether NO 5.0 pg/Kg 1 8/51200912:33 PM Dibromechloromelhane NO 5.0 pg/Kg 1 815/200912:33 PM Dibromomethene ND 5.0 pg/Kg 1 8/51200912:33 PM �I u 1 1..1 �J I A I I�I !I Qualifiers: �B Analyle detected in the associated Method Blank - ^ v 5 Value above quantitation range -�- - H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out 44Adrnnced Tccbnologr , LuborntarJcs 3275 tFttlntdApcunq Sigurt!!li!/, CA 90755 7i1: 562. 939.4045 Fa.-C.-SG2.989.4040 ' 8 of 68 I I I I I I I I I II I I I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-5 Lab Order: 106685 Collection Date: 8/3/2009 9:52:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-003A Analyses Result PQL Qual Units DP Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunID: MS4_090805A QC Batch: K09VS145 PrepDate: Analyst: HH Dlchlorodl0uoromethane ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Ethyl Tert-butyl ether ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Ethylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Hexachlorobutadiene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Isopropylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM m,p-Xylene ND 10 pg/Kg 1 8/5/2009 12:33 PM Methylene chloride ND 5.0 pg/Kg 1 8/5/2009 12:33 PM MTBE ND 5.0 pg/Kg 1 8/5/2009 12:33 PM n-Butylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:33 PM n-Propylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:33 PM Naphthalene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM o-Xylene ND 5.0 pg/Kg 1 8/51200912:33 PM sec-Butylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Styrene NO 5.0 pg/Kg 1 815/200912:33 PM Tert-amyl methyl ether ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Tert-Butanol ND 100 pg/Kg 1 8/5/2009 12:33 PM lert-Butylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Tetrachloroethene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Toluene NO 5.0 pg/Kg 1 8/5/2009 12:33 PM trans-1,2-Dlchloroelhene ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Trichloroelhepe ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Trichlorofluoromethane ND 5.0 pg/Kg 1 8/5/2009 12:33 PM Vinyl chloride NO 5.0 pg/Kg 1 815/200912:33 PM Burr:1,2-Dichloroethane-d4 109 70-130 %REC 1 8/5/2009 12:33 PM Surr:4-Bromofluorobenzene 99.6 70-130 %REC 1 8/5/2009 12:33 PM Surr: Dlbromo0uoromethane 113 70-130 %REC 1 8/5/2009 12:33 PM Surr: Toluene-d8 109 70-130 %REC 1 815/200912:33 PM SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550E EPA 8270C RuniD: MS 13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP 1,2,4-Tiichlorobenzene ND 330 pg/Kg 1 8/5/2009 04:02 PM 1,2-Dichlorobenzene ND 330 pg/Kg 1 8/5/2009 04:02 PM 1,3-Dichlorobenzene ND 330 pg/Kg 1 8/5/2009 04:02 PM 1,4-Dichlorobenzene ND 330 pg/Kg 1 8/5/2009 04:02 PM 2,4,5-Trichlorophenol NO 330 pg/Kg 1 8/5/2009 04:02 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ow AdvnncedTechnalogy �111 Lnhernfarles 3275 NrdnrrlAverrue, SigualNi7/, Cal 90955 Tel: 562. 939.4045 Fax: S(2.989.4090 ,_ 9 of 68 Advanced TechnologyLaboratories ANALYTICAL RESULTS Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: E6-5 Lob Order: 106685 Collection Date: 8/3/2009 9:52:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-003A Analyses Result PQL Qual Units DP Date Analyzed SEMIVOIATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550B EPA 8270C RunlD: MS13_09D805A QC Batch: 57085 PrepDate: 8/512009 Analyst: DMP 2,4,6-Tdchlorophenol NO 330 pg/Kg 1 81512009 04:02 PM 2,4-Dichiorophenol NO 1600 pg/Kg 1 815/2009 04:02 PM 2,4-Dimethylphenol NO 33D pg/Kg 1 815/200904:02PM 2,4-Dinihophenol NO 1600 pg/Kg 1 8/512009 04:02 PM 2,4-Dinilrotoluene NO 330 pg/Kg 1 8I5/200904:02PM 2,6.Drnitrotoluene NO 330 pg/Kg 1 8/512009 04:02 PM 2-Chloronaphlholene NO 330 pg/Kg 1 8/5I2009 04:02 PM 2-Chlorophenol NO 330 pg/Kg 1 8/512009 04:02 PM 2-Melhylnaphthelene NO 330 pg/Kg 1 815/2009 04:02 PM 2-Methylphenol ND 330 pg/Kg 1 815/200904:02PM 2-Nitroaniline ND 1600 pg/Kg 1 815/2009 04:02 PM 2-Nitrophenol ND 330 pg/Kg 1 8/5/2009 04:02 PM 3,3'-Dlchlorobenzidlne NO 660 pg/Kg 1 8/512009 04:02 PM 3-Nitroaniline NO 1600 pg/Kg 1 81512009 04:02 PM 4,6-Dinitro-2-methylphenol NO 1600 pglKg 1 815/2009 04:02 PM 4-Bromophenyl-phenylether NO 330 pglKg 1 815/2009 04:02 PM 4-Chloro-3-methylphenol ND 660 pg/Kg 1 8/5/2009 04:02 PM 4-Chloroaniline NO 660 pg/Kg 1 8l5/200904:02PM 4-Chlorophenyl-phenylether NO 330 pg/Kg 1 8/5/2009 04:02 PM 4-Methylphenol NO 330 pg/Kg 1 81512009 04:02 PM 4-Nitroaniline NO 1600 pglKg 1 815/2009 04:02 PM 4-Nitrophenol NO 160D pg/Kg 1 815/2009 04:02 PM Acensphthene NO 330 pgft 1 815/200904:02PM Acenaphthylene ND 330 pg/Kg 1 8/5/2009 04:02 PM Anthracene No 330 pg/Kg 1 815/2009 04:02 PM Benzidine (M) NO 1600 pg/Kg 1 8/5/2009 04:02 PM Benzo(a)anthrecene NO 330 pg/Kg 1 81512009 04:02 PM Benzo(a)pyrens NO 330 pg/Kg 1 81512009 04:02 PM Benzo(b)8uoranthene NO 330 pg/Kg 1 81512009 04:02 PM Benzo(g,h,l)perylene ND 330 pg/Kg 1 815/2009 04:02 PM Benzo(k)8uoranthene NO 330 pg/Kg 1 815/2009 04:02 PM Benzoic acid NO 1600 pg/Kg 1 8l5/2009 04:02 PM Benzyl alcohol NO 660 pg/Kg 1 8/5/2009 04:02 PM Bis(2-chloroethoxy)methane NO 330 pg/Kg 1 8/512009 04:02 PM Bis(2-chloroethyl)elher NO 330 pg/Kg 1 8/612009 04:02 PM Qualifiers: B Analytc detected in the associated Method Blank E Value above quantitation range H Holding times ror preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogale outside or limits due to matrix interference Results arewel unless otherwise specified DO Surrogate Diluted Out 1124 Advanced Techn010911 LuhOrnlOr/es 3275 Walnut Avenue, Signal Hill, CA 90755 Tel.,5G2. 939.9045 Fas: SG2.939.�1040 10 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Azig-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-5 Lab Order: 106685 Collection Date: 8/3/2009 9:52:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-003A Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550E EPA 8270C RunlD: MS 13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP Bis(2-chlorolsopropyl)elher NO 330 pg/Kg 1 1 8/5/2009 04:02 PM 8/5/2009 04:02 PM - Bis(2-ethylhexyl)phthalate NO 330 pg/Kg Bulylbenzylphthalate NO 330 pg/Kg 1 8/5/2009 04:02 PM Chrysene NO 330 pg/Kg 1 8/5/2009 04:02 PM Di-n-butylphthalate ND 330 pg/Kg 1 8/5/2009 04:02 PM Di-n-octylphthelale NO 330 pg/Kg 1 8/5/2009 04:02 PM Dibenz(a,h)anthracene ND 330 pg/Kg 1 8/5/2009 04:02 PM Dibenzofuran ND 330 pg/Kg 1 8/5/2009 04:02 PM Diethylphthalate NO 330 pg/Kg 1 8/5/2009 04:02 PM Dlmelhylphthalate ND 330 pg/Kg 1 8/5/2009 04:02 PM Fluoranthene ND 330 pg/Kg 1 1 8/5/2009 04:02 PM 8l5/200904:02PM Fluorene ND 330 pg/Kg Hexachlorobenzene ND 330 pg1Kg 1 8/5I2009 04:02 PM Hexachlorobutadiene ND 660 pg/Kg 1 8/5/2009 04:02 PM Hexachlorocyclopentadiene NO 660 pg/Kg 1 815/2009 04:02 PM Hexachloroethane NO 330 pg/Kg 1 8/5I2009 04:02 PM indeno(1,2,3-od)pyrene ND 330 pg/Kg 1 8/5/2009 04:02 PM �i isophorone NO 330 pg/Kg 1 8/5/2009 04:02 PM N-Nitrosodl-n-propylamine NO 330 pg/Kg 1 8/5/2009 04:02 PM N-Nitrosodiphenylamine NO 330 pg/Kg 1 815/2009 04:02 PM Naphthalene ND 330 pg/Kg 1 1 815/200904:02 8/5/2009 04:02 PM Nitrobenzene ND 330 pg/Kg Pentachlorophenol ND 1600 pg/Kg 1 8/5/2009 04:02 PM Phenanthrene NO 330 pg/Kg 1 8/5/2009 04:02 PM � Phenol NO 330 pg/Kg 1 8/5/2009 04:02 PM Pyrene NO 330 pg/Kg 1 8/5/2009 04:02 PM Surr:1,2-Dichlorobenzene-d4 59.3 49-103 %REC 1 8l5/2009 04:02 PM Sun:2,4,6-Tribromophenol 82.0 47-129 %REC 1 8/5/2009 04:02 PM Surr:2-Chlorophenol-d4 67.1 54-109 %REC 1 8/5/2009 04:02 PM Surr:2-Fluorobiphenyl 68.6 59-108 %REC 1 8/5/2009 04:02 PM Surr:2-Fluorophenol 66.9 50-111 %REC 1 8l5/2009 04:02 PM Surr:4-Terphenyl-d14 82.7 58-135 %REC 1 8/5/2009 04:02 PM Surr:Nitrobenzene-d5 63.9 54-115 %REC 1 81512009 04:02 PM Star: Phenol-d5 68.9 58-112 %REC 1 8/5/2009 04:02 PM B Analyze detected in the associated Method Blank E Value above quantitation range Qualifiers: H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out AdrvnrcedTechua/ogV inced cchn 3275 Widnrrt Avenue, Signal flit!, CA 90755 Tel: 562. 989.4045 I ax: SG2.989.d040 �r,, �l Labo_ 11 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories - ---- ------ -- Print Date: /1 ang-09 ---- - - - -- - ------------- --- -- -- - - - CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-GW Lab Order: 106685 Collection Date: 8/3/2009 10:55:00 AM Project: SCE Newport,602497-003 Matrix: GROUNDWATER Lab ID: 106685-005A v Analyses Result PQL Qual Units DF Date Analyzed '!'I HYDROCARBON CHAIN IDENTIFICATION EPA 8015B RunlD: GC6 090804A OC Batch: 109VW0134 PrepDate: Analyst: BD T/RHydrocarbons.C4-C12 NO 0.20 mg/L 1 8/4/200905:58PM Surr. Bromolluorobenzene (FID) 90.4 71-130 %REC 1 8/4/2009 05:58 PM QualiRers: _ B Analytc detected in the associated Method Blank H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out A AdvancedTechnologv Laboratories E Value above quantitation range NO Not Detected at the Reporting Limit Results am vecl unless othenvise specified 32751Yalnut Avenue, Signal Hill, CA 90955 Tel., 562. 989.4045 ram 562.989.4040 12 of 68 M' n [- 1'I 1'.il ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-GW Lab Order: 106685 Collection Date: 8/3/2009 10:55:00 AM Project: SCE Newport,602497-003 Matrix: GROUNDWATER Lab ID: 106685-005B Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 351 OC EPA 8015B(M) RunlD: GC16_090806F QC Batch: 57067 PrepDale: 8/4/2009 Analyst: CBR T/R Hydrocarbons: CB-Cl 0 NO 0.20 mg/L 1 8/6/2009 06:49 PM PM T/R Hydrocarbons: CIO-C18 NO 0.20 mg/L 1 8/6/2009 06:49 T/R Hydrocarbons: C18-C28 NO 0.20 mg/L 1 8/6/2009 06:49 PM T/R Hydrocarbons: C28-C36 NO 0.20 mg/L 1 8/6/2009 06:49 PM 1 8/6/2009 06:49 PM T/R Hydrocarbons: C36-C40 NO 0.20 mglL T/R Hydrocarbons: C8-C40 Total NO 0.20 mg/L 1 8/6/2009 06:49 PM Surr: p-Terphenyl 80.2 35-131 %REC 1 8/6/2009 06:49 PM r� �1 B Analyte detected in the associated Method Blank E Value above quantitation range Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ' r L Laboratories 3275 Nalrrnt Avenue, Signal Hill, CA �n,1 ftdvnn ed Laboratories 90755 Tel: 562. 959.4045 Tax: 5(2.9824040 _ 13 of 68 ANALYTICAL RESULTS Advanced TechnologyLaboratories Print Date: 12-Aug-09 ; CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-GW Lab Order: 106685 Collection Date: 8/3/2009 10:55:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-005C ----------------------------- - - - ---------- -------------- - ------ ------ Analyses Result - PQL - Qual Units DP Date Analyzed PCBS BY GC/ECD EPA 3510C EPA 8082 RunID: GC4_090807A QC Batch: 57126 PrepOate: 8/612009 Analyst: BB Aroclor 1016 ND 0.50 pg/L 1 8/7/200911:30 AM ' Aroclor1221 NO 1.0 pg/L 1 8171200911:30AM Aroclor1232 ND 0150 pg/L 1 817/200911:30AM Aroclor1242 ND 0.50 pg/L 1 8l7/200911:30AM Aroclor 1248 ND 0.60 pg/L 1 8/71200911:30 AM Aroclor1264 ND 0.50 pg/L 1 817/200911:30AM Aroclor 1260 ND 0.50 pg/L 1 817/200911:30 AM Aroclor 1262 ND 0.80 pg/L 1 817/200911:30 AM Aroclor1268 ND 0.50 pg/L 1 817/200911:30AM Surr:Decachlorobiphonyl 81.7 29-130 %REC 1 817/200911:30AM Surr:Tetrachloro-m-xylene 92.2 48.126 %REC 1 8/7/2009 11:30 AM 11 I I 1 Qualifiers: B Analyte detected In the associated Method Blank E Value above quantitationrange H Holding limes for preparation or analysis exceeded NO Not Detected at the Repotting Limit S SpikelSurrogate outside orlimits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out 1 A dranced aeluralogy Laborubarutarles 3275 NulrtrrlAvenue, Sigurr{Hil1, CA 90755 Tel: 562. 939.4045 Fnx: S61.989.4040 , 14 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 11-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-2 Lab Order: 106685 Collection Date: 8/3/2009 10:33:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-006A Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunlD: GC16 090806C QC Batch: 57087 PrepDate: 8/5/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 ND 10 mg/Kg 1 8/6/2009 03:43 PM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 8/6/2009 03:43 PM T/R Hydrocarbons: C18-C28 ND 10 mg/Kg 1 8/6/2009 03:43 PM T/R Hydrocarbons: C28-C36 NO 10 mg/Kg 1 1 8/6/2009 03:43 PM 8/6/2009 03:43 PM T/R Hydrocarbons: C36-C40 ND 10 mg/Kg T/R Hydrocarbons: C8-C40 Total NO 10 mg/Kg 1 8/6/2009 03:43 PM Surr: p-Terphenyl 92.7 57-144 %REC 1 8/6/2009 03:43 PM HYDROCARBON CHAIN IDENTIFICATION EPA 801513 RunID: GC2 090804B QC Batch: E09VS246 PrepDate: Analyst: KHN '. T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 8/4/200910:09 PM Surr: Bromofluorobenzene (FID) 97.3 59.145 %REC 1 814/200910:09 PM PCBS BY GC/ECD EPA 3550E EPA 8082 RunID: GCS_0908063 QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB Aroclor 1016 NO 16 pg/Kg 1 8/712009 01:11 AM 8/7/2009 01:11 AM Aroclor 1221 ND 33 pg/Kg 1 Aroclor 1232 NO 16 pg/Kg 1 817/2009 01:11 AM Aroclor 1242 NO 16 pg/Kg 1 817/200901:11 AM Aroclor 1248 ND 16 pg/Kg 1 8/7/2009 01:11 AM Aroclor 1254 360 33 pg/Kg 2 8/7/2009 07:38 AM Aroclor 1260 ND 16 pg/Kg 1 817/2009 01:11 AM Aroclor 1262 NO 16 pg/Kg 1 8l7/2009 01:11 AM Aroclor 1268 NO 16 pg/Kg 1 8/7/2009 01:11 AM Surr: Decachlorobiphenyl 95.9 30-124 %REC 1 8/7/2009 01:11 AM Surr: Decachlorobiphenyl 102 30-124 %REC 2 %REC 1 8/7/2009 07:38 AM 8f7/200901:11AM Surr:Tetrachloro-m.xylene 97.3 40-118 Surr: Tetrachloro-m-xylene 89.6 40-118 %REC 2 8/7/2009 07:38 AM VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260B RunID: MS4 090805A QC Batch: K09VS145 PrepDate: Analyst: HH 1,1,1,2-Tetmchloroethane ND 5.0 pg/K9 1 1 8151200912:17 PM 8/5/200912:17 PM _ 1,1,1-Tdchloroethane NO 5.0 pg/Kg B Analyte detected in the associated Method Blank E Value above quantitation range Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at tite Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified � DO Surrogate Diluted Out ,Adtwnced Teelmologi 5TVa1nrrtAvenuc, SigualHill,CA 90755 Tel. 562.939.4045 Fax:5G2.9$9.4040 04317Laboratories 15 of 68 ora Advanced TechnologyLaboratories - ------------ -- - -- - ----------- --- CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-006A Analyses Result ANALYTICAL RESULTS Print Date: 12-Avg-09 ------ - --- -- ------- --- - --- - ------------- Client Stunple ID: 137-2 Collection Date: 8/3/2009 10:33:00 AM Matrix: SOIL PQL Qual Units DF Date Analyzed 1 VOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 82608 RunID: MS4_090805A QC Batch: K09VS145 PrepDate: Analyst: HH 1,1,2,2-Tetrachloroelhane NO 5.0 pg/Kg 1 8/51200912:17 PM 1,1,2Trichloroethene NO 5.0 pg/Kg 1 8/512009 12:17 PM 1,1-Dichloroelhone ND 5.0 pg/Kg 1 8/5/200912:17 PM 1,1-Dichloroethene NO 5.0 pglKg 1 815/200912:17 PM 1,1-Dichloropropene ND 5.0 pg/Kg 1 8/512009 12A7 PM 1,2,3-Tdchlorobenzene ND 5.0 pg/Kg 1 8/51200912:17 PM 1,2,3-Tdchloropropane NO 5.0 pg/Kg 1 8/51200912:17 PM 1,2,4-Tdchlorobenzene NO 5.0 pg/Kg 1 8/51200912:17 PM 1,2,4-Tdmethylbenzene ND 5.0 pg/Kg 1 815/200912:17 PM 1,2-Dibromo-3-chloropropene NO 10 pg/Kg 1 815/200912:17 PM 1,2-Dibromoethane NO 5.0 pglKg 1 8151200912:17 PM 1,2-0ichlorobenzene ND 5.0 pglKg 1 815/200912:17PM 1,2-Dichloroalhane ND 5.0 pglKg 1 8/51200912:17 PM 1,2-Dichloropropane NO 5.0 pg/Kg 1 8/51200912:17 PM 1,3,5-Tdmethylbenzene NO 5.0 pgll<g 1 815/2009 12:17 PM 1,3.Dichlorobenzene NO 6.0 pg/Kg 1 815/200912:17 PM 1,3.Dichloropropane ND 5.0 pg/Kg 1 815/200912:17 PM 1,4.Olchlorobenzene NO 5.0 pg1Kg 1 815/200912:17 PM 2,2-Dichloropropane NO 5.0 pg/Kg 1 815/200912:17 PM 2-Chlorololuene ND 5.0 pg/Kg 1 8/51200912:17 PM 4-Chlorotoluene ND 5.0 pg/Kg 1 8/5/200912:17 PM 4-1sopropyltoluene No 5.0 pg/Kg 1 815/200912:17 PM Benzene ND 5.0 pg/Kg 1 815/200912:17 PM Bromobenzene NO 5.0 pg/Kg 1 815/200912:17 PM Bromodichloromelhane NO 5.0 pg/Kg 1 816/200912:17 PM Bromoform ND 5.0 pg/Kg 1 8/5/200912:17 PM Bromomelhane Carbon tetrachloride NO ND 5.0 5.0 pglKg pglKg 1 1 815/200912:17 PM 815/200912:17 PM Chlorobenzene ND 5.0 pglKg 1 8/5/200912:17 PM Chloroethane ND 5.0 pg/Kg 1 8/51200912:17 PM Chloroform No 5.0 pg/Kg 1 8151200912:17 PM Chloromelhane ND 5.0 pg/Kg 1 815/200912:17 PM cis-1,2-Dichloroethene NO 5.0 pg/Kg 1 815/200912:17 PM cis-1,3-Dichloropropene NO 5.0 pg/Kg 1 815/200912:17 PM Di -Isopropyl ether ND 5.0 pgNq 1 815/200912:17 PM Qualifiers: D Analyte detected in the associated Method Blank f G Value above quantilation range - H Holding times for preparation or analysis exceeded NO Not Detected at die Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwisespccificd DO Surrogate Diluted Out ��* AoftnacodTerlarology L* , LnGara(orles 3275 {Valnn(Aveaurr, Signal Hill, Cr! 90755 16114 Tel. 562. 939.4045 Far. S62.939.4040 16 of 68 11 I t O I I I I! I� I , I I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 Client Sample ID: 137-2 CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Collection Date: 8/3/2009 10:33:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-006A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunID: MS4_090805A QC Batch: K09VS145 PrepDate: Analyst: HH Dibromochloromethane ND 5.0 pg/Kg 1 8151200912:17 PM Dibromomethane NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Dtchlorodifluoromelhane NO 5.0 pg/Kg 1 8/51200912:17 PM Ethyl Tert-butyl ether NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Ethylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Hexachlorobutadiene ND 5.0 pg/Kg 1 815/200912:17 PM Isopropylbenzene ND 5.0 pg/Kg 1 8/51200912:17 PM m,p-Xylene NO 10 pg/Kg 1 8/5/2009 12:17 PM Methylene chloride NO 5.0 pg/Kg 1 8/5/2009 12:17 PM MTBE NO 5.0 pg/Kg 1 8/5/2009 12:17 PM n-Butylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:17 PM n-Propylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Naphthalene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM o-Xylene NO 5.0 pg/Kg 1 815/200912:17 PM sec-Butylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:17 PM Styrene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Tert-amyl methyl ether NO 5.0 pg/Kg 1 815/200912:17 PM Tert-Butanol ND 100 pg/Kg 1 8/5/2009 12:17 PM tert-Butylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Tetrachloroethene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Toluene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM trans-1,2-Dichloroethene NO 5.0 pg/Kg 1 8l5/2009 12:17 PM Trichloroethene NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Trichlorofluoromethane NO 5.0 pg/Kg 1 8/5/2009 12:17 PM Vinyl chloride ND 5.0 pg/Kg 1 8/51200912:17 PM Surr:1,2-Dichloroethane-d4 109 70-130 %REC 1 8/5/2009 12:17 PM Surr:4-Bromofluorobenzene 98.8 70-130 %REC 1 8/5/2009 12:17 PM Surr: Dibromoflucromethane 53.7 70-130 s %REC 1 815/200912:17 PM Surr: Toluene-d8 105 70-130 %REC 1 815/200912:17 PM SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunlD: MS 13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP 1,2,4-Trcchoorobenzene NO 330 pg/Kg 1 8/5/2009 08:38 PM 1,2-Dichlorobenzene NO 330 pg/Kg 1 8/5/2009 08:38 PM 1,3-Dichlorobenzene ND 330 pg/Kg 1 8/512009 08:38 PM B Analyte detected in the associated Method Blank E Value above quantitation range Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out WAINAdncedTocbrrolow, rwLuboratories 3275 iYa/nutAvenne, Signa[Hi((. CA 90755 Tel: 562. 989.9045 Tax: SG2.989.4040 17 of 68 1 Advanced TechnologyLaboratories ANALYTICAL RESULTS Print Date: 12 Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 117-2 Lab Order: 106685 Collection Date: 8/3/2009 10:33:00 AM Project SCE Newport602497-003 Matrix: SOIL i II Lab ID: 106685-006A Analyses Result PQL Quad Units Df Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550B EPA 8270C RunID: MS 13 090805A OC Belch: 57085 PrepDale: 8/612009 Analyst: DMP 1,4-Dichlorobenzene NO 330 pgfKg 1 81512009 08:38 PM 2,4,5-Tdchiorophenol NO 330 pgfKg 1 8/5/2009 08:38 PM 2,4,6-Tdchlorophenol NO 330 pg/Kg 1 8/6/2009 08:38 PM 2,4-Dichiorophenol ND 1600 pgfKg 1 8/5/2009 08:38 PM 2,4-Dlmethylphenol ND 330 pg/Kg 1 8/5/2009 08:38 PM 2,4-Dinitrophenol ND 1600 pgfKg 1 8/5/2009 08:38 PM 2,4-Dinilrotoluene ND 330 pg/Kg 1 8/512009 08:38 PM 2,6-Dlnilrotoluene ND 330 pgfKg 1 816/2009 08:38 PM 2-Chloronaphtholene ND 330 pg/Kg 1 815/200908:38PM 2-Chlorophenol ND 330 pg/Kg 1 815/2009 08:38 PM 2-Methylnaphthalene ND 330 pg/Kg 1 815/2009 08:38 PM 2-Methylphenol ND 330 pg/Kg 1 8/5/2009 08:38 PM 2-Niuoanlline ND 1600 pg/Kg 1 8/5/200908:38PM 2-Nitrophenol NO 330 pg/Kg 1 8/5/200908:38PM ' 3,3'-Dichlorobenzidine NO 660 pg/Kg 1 81512009 08:38 PM 3-141troanlline No 1600 pgfKg 1 8/5/2009 08:38 PM 4,6-Dinitro-2-methylphenol ND 1600 pg/Kg 1 81512009 08:38 PM 4-Bromophenyl-phenylether ND 330 pgfKg 1 815/2009 08:38 PM 4-Chloro-3-methylphenol ND 660 pgfKg 1 8/5/2009 08:38 PM 4-Chlorooniline NO 660 pgfKg 1 8/512009 08:38 PM 4-Chlorophenyl-phenylether NO 330 pgfKg 1 8151200908:38PM 4-Methylphenol ND 330 pg/Kg 1 8/512009 08:38 PM 4-Nitroanlline ND 1600 pg/Kg 1 8/5/2009 08:38 PM 4-Nitrophenol No 1600 pg/Kg 1 815/2009 08:38 PM Acenaphthene NO 330 pg/Kg 1 815/2009 08:38 PM Acenaphthylene No 330 pg/Kg 1 81512009 08:38 PM Anthracene ND 330 pg/Kg 1 8/5/2009 08:38 PM Benzidine (M) NO 1600 pgfKg 1 8/512009 08:38 PM Benzo(a)anthracene NO 330 pg/Kg 1 8/5/200908:38PIA Benzo(a)pyrene ND 330 pgfKg 1 8/51200908:38PM Benzo(b)8uorenthene ND 330 pg/Kg 1 8/5/2009 08:38 PM Benza(g,h,i)perylene ND 330 pgfKg 1 81512009 08:38 PM Benzo(k)fluoranthene ND 330 pg/Kg 1 8/5/2009 08:38 PM Benzoic acid ND 1600 pgfKg 1 8/5/2009 08:38 PM Benzyl alcohol NO 660 pgfKg 1 815/2009 08:38 PM Qualifiers: B Analyle detected in the associated Methad➢lank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S SpikeJSurrogale outside of limits due to matrix interference Results are Wet unless otherwise specified DO Surrogate Diluted Out !� Advanced reclmologr' Laboratories 3275 IPalnuldvererre, Sigunl Hill, CA 907S5 TaL• 562, 939.4r745 1'ae: SG2.939.4040 � I, 18 of 68 I iJ II I I I 91 I G 1 H I U 11 I 1 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-006A Client Sample ID: 137-2 Collection Date: 8/3/2009 10:33:00 AM Matrix: SOIL Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550E EPA 8270C RunIO: MS 13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP Bis(2-chloroelhoxy)methane NO 330 pg/Kg 1 8/5/2009 08:38 PM Bis(2-chloroelhyl)ether NO 330 pg/Kg 1 8/5/2009 08:38 PM Bis(2-chloroisopropyl)ether NO 330 pg/Kg 1 8/5/2009 08:38 PM Bis(2-ethylhexyl)phthalate NO 330 pg/Kg 1 8/5/2009 08:38 PM Butylbenzylphthalate NO 330 pg/Kg 1 8/5/2009 08:38 PM Chrysene NO 330 pg/Kg 1 8/512009 08:38 PM Di-n-butylphthalate NO 330 pg/Kg 1 8/512009 08:38 PM Di-n-octylphthalate NO 330 pg/Kg 1 815/2009 08:38 PM Dibenz(a,h)anthracene NO 330 pg/Kg 1 8/5/2009 08:38 PM Dibenzofuran ND 330 pg/Kg 1 815/200908:38PM Diethylphlhelate NO 330 pg/Kg 1 815/2009 08:38 PM Dimelhylphthalete NO 330 pg/Kg 1 815/2009 08:38 PM Fluoranthene NO 330 pg/Kg 1 8/5/2009 08:38 PM Fluorene NO 330 pg/Kg 1 8/5/2009 08:38 PM Hexachlorobenzene ND 330 pg/Kg 1 8/5/2009 08:38 PM Hexachlorobutadiene NO 660 pg/Kg 1 8/5/2009 08:38 PM Hexachlorocyclopentadlene NO 660 pg/Kg 1 8/5/2009 08:38 PM Hexachloroelhane ND 330 pg/Kg 1 8/5/2009 08:38 PM indeno(1,2,3-od)pyrene NO 330 pg/Kg 1 8/5/2009 08:38 PM Isophorone NO 330 pg/Kg 1 815/2009 08:38 PM N-Nitrosodi-n-propylamine NO 330 pg/Kg 1 8/5/2009 08:38 PM N-Nitmsodiphenylamine ND 330 pg/Kg 1 8/5/2009 08:38 PM Naphthalene NO 330 pg/Kg 1 815/2009 08:38 PM Nitrobenzene NO 330 pg/Kg 1 815/2009 08:38 PM Pentachlorophenol NO 1600 pg1Kg 1 8/5/2009 08:38 PM Phenanlhrene NO 330 pg/Kg 1 8/512009 08:38 PM Phenol NO 330 pg/Kg 1 8/5/2009 08:38 PM Pyrene NO 330 pg/Kg 1 8/5/2009 08:38 PM Surr:1,2-Dichlorobenzene-d4 67.6 49-103 %REC 1 8/5/2009 08:38 PM Surr:2,4,6-Tribromophenol 9.32 47-129 s %REC 1 8/5/2009 08:38 PM Surr:2-Chlorophenol-d4 37.2 54-109 s %REC 1 8/5/2009 08:38 PM Surr:2-Fluorobiphenyl 75.1 59-108 %REC 1 8/5/2009 08:38 PM Surr:2-Fluorophenol 25.8 50-111 S %REC 1 8/5/2009 08:38 PM Surr:4-Terphenyl-d14 86.7 58-135 %REC 1 8/5/2009 08:38 PM Surr: Nitrobenzene-d5 71.4 54-115 %REC 1 8/5/2009 08:38 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limn S Spike/Suriogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out OWW,, AdrancedTechaolo8!V 3275 1ValnrrtAverure, Signal URI, CA 90755 Tel: 562. 989.4045 Fax: 562,989.4040 Laboratories r _ 19 of 68 11 Advanced TechnologyLaboratories ANALYTICAL RESULTS Print Date: 12-Aug-09 ---------- - ------ - -- -- -- - --- --- -- - ---- - - - - - CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-2 Lab Order: 106685 Collection Date: 8/3/2009 10:33:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-006A Analyses Result PQL Qual Units DP Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS EPA 3550E RuniD: MS 13 090805A QC Balch: 57085 Surn Phenol-d5 68.1 58.112 EPA 8270C PrepDale: %REC 8/5/2009 Analyst: DMP 1 8/512009 08:38 PM Quallfiers: B Amd;te detected in the associated Method Blank E Value above quantization range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside or limits due to matdx.interfercnce Results arc wet unless otherwise specified DO Surrogate Diluted Out & Advanced Technologr Laboratories 3275 Walnut Avenue, Signal Hill. CA 90755 20 of 68 11 11 11 II I 1 11 Tel: 562. 989.4045 Fam 562.989.4040 ' RESULTS 'ANALYTICAL Advanced Technology Laboratories Print Date: 12-Arig-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 137-5 ' Lab Order: 106685 Collection Date: 8/3/2009 10:48:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL ' Lab ID: 106685007A Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC16_090806C QC Batch: 57087 PrepDate: 8/5/2009 Analyst: CBR ' T/R Hydrocarbons: C8-C10 NO 10 mg/Kg 1 8/6/2009 04:15 PM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 8/6/2009 04:15 PM T/R Hydrocarbons: C18-C28 21 10 mg/Kg 1 8/6/2009 04:15 PM ' T/R Hydrocarbons: C28-C36 20 10 mg/Kg 1 1 8/6/2009 04:15 PM 8/612009 04:15 PM T/R Hydrocarbons: C36-C40 ND 10 mglKg T/R Hydrocarbons: C8-C40 Total 41 10 mg/Kg 1 8/6/2009 04:15 PM Surr: p-Terphenyl 100 57-144 %REC 1 8/612009 04:15 PM HYDROCARBON CHAIN IDENTIFICATION EPA 80158 RunID: GC2 090804B QC Batch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 ND 1.0 mg/Kg 1 8/4/200910:24 PM Surr: Bromofluorobenzene (Flo) 94.6 59-145 %REC 1 8/4/2009 10:24 PM PCBS BY GC/ECD EPA 35508 EPA 8082 RunID: GC5_090806B QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB ' Aroclor 1016 NO 16 pg/Kg 1 1 8l7/2009 01:41 AM 817/200901:41 AM Aroclor 1221 NO 33 pg/Kg Aroclor 1232 ND 16 pg/Kg 1 8/7/2009 01:41 AM Aroclor 1242 NO 16 pg/Kg 1 8/7/2009 01:41 AM Aroclor1248 ND 16 pg/Kg 1 8/7/2009 01:41 AM Aroclor 1254 59 16 pg/Kg 1 8/7/2009 01:41 AM Aroclor 1260 ND 16 pg/Kg 1 8/7/2009 01:41 AM ' Aroclor 1262 NO 16 pg/Kg 1 8/7/2009 01:41 AM Aroclor 1268 ND 16 pg/Kg 1 8/7/2009 01:41 AM Surr: Decachlorobiphenyl 96.2 30-124 %REC 1 8/7/2009 01:41 AM ' Surr: Tetrachloro-m-xylene 103 40-118 %REC 1 8/7/2009 01:41 AM B Analyte detected in the associated Method Blank E Value above quantuation range ' Qualifiers: H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified ' DO Surrogate Diluted Out ' AIL AdvancedTechaalogp Lnboralories 32751ValnxlAvenae, SignnlHill, CAI 90755 Tel. 562. 959.4045 Fax: 562.989.4040 21 of 68 ANALYTICAL RESULTS Advanced TechnologyLaboratories Print Date: 12-A:rg-09 ' CLIENT: Leighton Consulting, Inc. Client Sample ID: B8-GW Lab Order: 106685 Collection Date: 8/3/2009 11:27:00 AM , Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-009A Analyses Result PQL Qual Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 8015E ' RunID: GC6 090804A OC Batch: 109VW0134 Prepbate: Analyst: BD T/R Hydrocarbons: C4-C12 ND 0.20 mg1L 1 8/412009 07:02 PM Surr: Bromofluorobenzene (Flo) 90.7 71-130 %REC 1 8/412009 07:02 PM ' I I -1 Qualifiers: B Analym detected in the associated Method Blank E Value above quantilation range} H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit ' S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out 1001 Advanced Technolow ' Laboratories 3175'IVnlnnlAvcune, Signal ffill, CA 90755 Tel: 562. 939.4045 Pax: 562.939.4040 22 of 68 , J I I 'rl I n L 1 1 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 138-GW Lab Order: 106685 Collection Date: 8/3/2009 11:27:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-009B Analyses Result PQL Qual Units DP Date Analyzed PCBS BY GC/ECD EPA 3510C EPA 8082 RunlD: GC4 090807A QC Batch: 57126 PrepDate: Aroclor 1016 ND 0.50 pg/L 1 Aroclor 1221 ND 1.0 pg/L 1 Aroclor1232 ND 0.50 pg/L 1 Aroclor 1242 ND 0.50 pg/L 1 Aroclor 1248 NO 0.50 pg/L 1 Aroclor 1254 ND 0.50 pg/L 1 Aroclor 1260 ND 0.50 pg/L 1 Aroclor 1262 ND 0.50 pg/L 1 Aroclor1268 ND 0.50 pg/L 1 Burr: Decachlorobiphenyl 84.2 29-130 %REC 1 Surr:Tetrachloro-m-xylene 87.2 48-126 %REC 1 8/6/2009 Analyst: BB 8/7/2009 12:00 PM 8l7/200912:00 PM 8/7/2009 12:00 PM 8/7/200912:00 PM 817/200912:00 PM 8171200912:00 PM 817/200912:00 PM 8/7/2009 12:00 PM 817/200912:00 PM 8171200912:00 PM 8/7/2009 12:00 PM ' Qualifiers: B Analyse detected in the associated Method Blank E Value above quantilation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out /, Advanced Technology ' V Lnhoratorles 3275TVulnnlAvenue, Signal Hill, CA 90755 23 of 68 Tel. 562. 989.4045 Fax.502.989.4040 Advanced TechnologyLaboratories ANALYTICAL RESULTS Print Date: 11 plug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B8-GW Lab Order: 106685 Collection Date: 8/3/2009 11:27:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-009C Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RunID: GC16_090806F T/R Hydrocarbons: CB-Cl 0 T/R Hydrocarbons: C10-C18 T/R Hydrocarbons: C18-C28 T/R Hydrocarbons: C28-C36 T/R Hydrocarbons: C36-C40 T/R Hydrocarbons: CB-C40 Total Surr: p-Terphanyl OC Batch: 57067 PrepDale: NO 0.22 mg/L 1 NO 0.22 mg/L 1 NO 0.22 mglL 1 ND 0.22 mglL 1 ND 0.22 mg/L 1 ND 0.22 mg/L 1 74.2 35.131 %REC 1 8/4/2009 Analyst: CBR 8/6/2009 06:58 PM 8/612009 06:58 PM 81612009 06:58 PM 81612009 06:58 PM 8/6/2009 06:58 PM 8/6/2009 06:58 PM 8/6/2009 06:58 PM Qualifiers: D Analylc detected In the associated Method BlankE Value above timmitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogatcoutside of limits due to matrixinterfarcnee Results are wet unless otherwise specified DO Surrogate Diluted Out Adrmp huolog} LnboratoGorumrlrs 3175 iVtdirrrfslvrrrrre, SrgnalHilL GI 90755 TeL 562. 989.4045 Fax: SG2.939.4040 24 of 68 I RESULTS 'ANALYTICAL Advanced Technology Laboratories Print Date: 12-Aug-09 ' CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Client Sample ID: 138-2 Collection Date: 8/3/2009 11:20:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL ' Lab ID: 106685-OIOA Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RurdD. GC16_090806C QC Batch: 57087 PrepDate: 815/2009 Analyst: CBR ' T/R Hydrocarbons: C8-C10 ND 10 mg/Kg 1 8/612009 04:04 PM 8/6/2009 04:04 PM T/R Hydrocarbons: C10-Cl B ND 10 mg/Kg 1 T/R Hydrocarbons: C18-C28 ND 10 mg/Kg 1 8/6/2009 04:04 PM T/R Hydrocarbons: C28-C36 NO 10 mg/Kg 1 8/6/2009 04:04 PM ' T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 8/6/2009 04:04 PM T/R Hydrocarbons: C8-C40 Total ND 10 mg/Kg 1 8/612009 04:04 PM Surr: p-Terphenyl 99.0 57-144 %REC 1 8/6/2009 04:04 PM ' HYDROCARBON CHAIN IDENTIFICATION EPA 8015E RunlD: GC2_090804B QC Balch: E09VS246 PrepDate: Analyst: KHN ' T/R Hydrocarbons: C4-C12 ND 1.0 mg/Kg 1 8/4/200910:38 PM Surr: Bromofluorobenzene (FID) 98.4 59-145 %REC 1 8/4/200910:38 PM ' PCBS BY GC/ECD EPA 3550B EPA 8082 RunlD: GC5_090806B QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB Aroclor 1016 ND 16 pg/Kg 1 8/7/2009 02:11 AM ' Aroclor 1221 ND 33 pg/Kg 1 8/7/2009 02:11 AM Aroclor 1232 NO 16 pg/Kg 1 8/7/2009 02:11 AM Aroclor 1242 ND 16 pg/Kg 1 8/7/2009 02:11 AM ' Aroclor1248 ND 16 pg/Kg 1 8/7/200902:11AM Aroclor1254 ND 16 pg/Kg 1 817/2009 02:11 AM Aroclor 1260 NO 16 pg/Kg 1 8/7/2009 02:11 AM ' Aroclor 1262 NO 16 pg/Kg 1 1 8M2009 02:11 AM 8/7/2009 02:11 AM Aroclor 1268 NO 16 pg/Kg Surr: Decachlorobiphenyl 95.9 30-124 %REC 1 8/7/2009 02:11 AM ' Surr: Tetrachloro-m-xylene 106 40.118 %REC 1 8/7/2009 02:11 AM B Analyte detected in the associated Method Blank E Value above quantitation range ' Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ' / t AdrancedTechaolow, �= 562.989.4090 GnGoralorics 3275 1{ irinrd Avemre, Signal Hill, CA 90755 Teh 562. 989.4045 Par: 25 of 68 Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-011A Analyses Result HYDROCARBON CHAIN IDENTIFICATION LUFT RunlD: GC16 090806C QC Balch: T/R Hydrocarbons: C8-C10 TIR Hydrocarbons: C10-C18 TIR Hydrocarbons: C1B-C28 TIR Hydrocarbons: C28-C36 TIR Hydrocarbons: C36-C40 TIR Hydrocarbons: C8-C40 Total Star. p-Terphenyl HYDROCARBON CHAIN IDENTIFICATION ANALYTICAL RESULTS ' Print Date: 12 Arrg-09 Client Surnple ID: E8-5 Collection Date: 8/3/2009 11:24:00 AM Matrix: SOIL PQL Qual Units DF Date Analyzed EPA 8015B(M) 57087 PrepDate: NO 10 mglKg 1 ND 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mglKg 1 NO 10 mg/Kg 1 100 57-144 %REC 1 RunID: GC2 090804E QC Batch: TIR Hydrocarbons: C4-C12 NO Surr. Bromofluorobenzens (FID) 94.7 PCBS BY GCIECD EPA 3550E RunIO: GC5_090806B Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Sum., Decachlorobiphenyl Sun: Tetrachloro-m-xylene E09VS246 OC Balch: $7129 ND ND NO NO NO NO NO ND ND 95.3 58.6 EPA 8015E PrepDate: 1.0 mg/Kg 1 59.145 %REC 1 EPA'8082 PrepDate: 16 pg/Kg 1 33 pg/Kg 1 16 pg/Kg 1 16 pg/Kg 1 16 pglKg 1 16 pg/Kg 1 16 pg/Kg 1 16 pglKg 1 16 pg/Kg 1 30-124 %REC 1 40.118 %REC 1 8/512009 Analyst: CBR 816/2009 02:39 PM 8/612009 02:39 PM 816/2009 02:39 PM 8/6/2009 02:39 PM 8/612009 02:39 PM 8/6/2009 02:39 PM 8/612009 02:39 PM Analyst: KHN 814/200910:53 PM 8/41200910:53 PM 8/6/2009 Analyst: BB 81712009 02:41 AM 8/7/2009 02:41 AM 8/7/2009 02:41 AM 8f7/2009 02:41 AM 817/2009 02:41 AM 817/2009 02:41 AM 81712009 021.41 AM 8/7/2009 02:41 AM 8/712009 02:41 AM 8/7/2009 02:41 AM Br1/2009 02:41 AM Qualifiers: B Analyte detected in the associated Method Blank E Vatue above quantitation range H Holding limes for preparation or analysis exceeded NO Not Deucled of the Reporting Limit S Spike/Surrogate outside of limits due to matrix imerfereace Results are wet unless otherwise specified DO Surrogate Diluted Out A Advanced 7echnologr Laboratories 3175 RaInaf Avenna, Signal Hill, CA 90755 %dl: 562. 989.4045 Fas: 542,989.4040 t 26 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B8 Dup Lab Order: 106685 Collection Date: 8/3/2009 11:27:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-012A Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 8015E RunID: GC6_090804A ' T/R Hydrocarbons: C4-C12 Burr: Bromofluorobenzene (FID) CI CI QC Batch: 109VW0134 NO 0.20 mg/L 89.1 71-130 %REC PrepDate: Analyst: BD 1 8/4/2009 05:36 PM 1 8/4/2009 05:36 PM ' Qualifiers: B Analyte detected in the associated Method Blank E H Holding times for preparation or analysis exceeded NO S Spike/Surrogate outside or limits due to matrix interference Value above quanlitation range Not Detected at the Reporting Limit Results are wet unless otherwise specified ' ' 11 � DO Surrogate Diluted Out lldwincedTechnologr Laboratories 3275 iVa[nrrlAvenne, SignnllJi71, CA 90755 Tel: 562. 939.4045 Fax: 562.989.4040 _ 27 of 68 ANALYTICAL RESULTS Advanced TechnologyLaboratories Print Date: 12-A1rg-09 ' CLIENT: Leighton Consulting, Inc. Client Sample ID: B8 Dup Lab Order: 106685 Collection Date: 8/3/200911:27:00 AM ' Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-012B ' Analyses Result PQL Qual Units DC Date Analyzed PCBS BY GCIECD EPA 3510C EPA 8082 ' RurdD: GC4 090807A QC Balch: 57126 PrepDale: 8/612009 Analyst: BE Aroclor1016 NO 0.50 pg/L 1 81712009 12:30 PM Aroclor1221 ND 1.0 pg/L 1 817/200912:30PM Aroclor 1232 NO 0.50 pglL 1 8/7/200912:30 PM Aroclor 1242 ND 0.50 NgIL 1 817/200912:30 PM Aroclor1248 NO 0.50 pg/L 1 8/71200912:30PM ' Aroclor 1254 NO 0.50 pg/L 1 8M200912:30 PM Aroclor 1260 NO 0.50 pg/L 1 817/200912:30 PM Aroclor1262 NO 0.50 pglL 1 8/71200912:30PM ' Aroclor1268 NO 0.50 pglL 1 817/2009 12:30 PM Surr. Decachloroblphenyl 82.8 29-130 %REC 1 817/200912:30 PM Surr.Tetrachlom-m-xylene 88.5 48-120 %REC 1 817/2009 12:30 PM ' 1 1 I I.■ i QuollRers: B Anolyte detected in the associated Method Blank B Value above quantitation range ' H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are Nvct unless otherwise speeirred DO Surrogate Diluted Out Advanced Tedeuolow ' Laboratories 327S IVaInitl Avenue, Signalllill, CA 90755 Tel. S62. 989.4045 Fax: S62.989.4040 28 of 68 ' I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B8 Dup Lab Order: 106685 Collection Date: 8/3/2009 11:27:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-012C Analyses Result PQL Qual Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RunID: GC16 090806F QC Batch: 57067 PrepDate: 8/4/2009 Analyst: CBR ' T/R Hydrocarbons: C8-C10 NO 0.22 mg/L 1 8/6/2009 07:06 PM 1 8/6/2009 07:06 PM T/R Hydrocarbons: C10-Cl8 ND 0.22 mg/L T/R Hydrocarbons: C18-C28 NO 0.22 mg/L 1 8/6/2009 07:06 PM T/R Hydrocarbons: C28-1336 NO 0.22 mg/L 1 8/612009 07:06 PM ' T/R Hydrocarbons: C36-C40 ND 0.22 mg/L 1 8/612009 07:06 PM T/R Hydrocarbons: C8-C40 Total NO 0.22 mg/L 1 8/6/2009 07:06 PM ' Burr: p-Terphenyl 71.7 35-131 %REC 1 8/6/2009 07:06 PM B Analyte detected in the associated Method Blank E Value above quantilalion range ' Qualifiers: H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO surrogate Diluted Out ' ' / Advanced7echnologr ��11 LnGorutaries 3275 IValnntAvefure, Signalflill, CA 90755 Tel: 562. 939.4045 Fax: 502.939.4040 1 29 of 68 1 Advanced TechnologyLaboratories ANALYTICAL RESULTS ' Print Date: 12 Arrg-09 CLIENT: Lcigbton Consulting, Inc. Client Sample iD: B10-GW ' Lab Order: 106685 Collection Date: 8/3/2009 11:58:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-013A ' Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION ' EPA 80158 RunID: GC6 090B04A T/R Hydrocarbons: C4-C12 Star, BromoBuorobenzone (FID) QC Belch: 109VW0134 NO 0.20 91.4 71-130 Prepoale: Analyst: BD mg/L 1 8/412009 06:40 PM %REC 1 81412009 06.40 PM II 1 11 Quallners: B Analyle detected in the associated Method Blank B Value above quantitation range ' H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside orlimitsdue tomatrix hucrfcrcnce Results arc wet unless otherwise specified DO Surrogate Diluted Out 44 Adownced Teebno/ogr Laboratories 3275 {VrilnrrlAvenrta, Signal /Gill, Gil 907.55 Tel: 562. 939.4045 Pax: 562.939.4040 ' 30 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Arrg-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B10-GW Lab Order: 106685 Collection Date: 8/3/2009 11:58:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-013B Analyses Result PQL Qual Units DR Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RUnlD: GC16_090806F QC Batch: 57067 PrepDate: 8A/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 0.20 mg/L 1 8/6/2009 07:15 PM T/R Hydrocarbons: CIO-C18 ND 0.20 mg/L 1 8/612009 07:15 PM T/R Hydrocarbons: C18-C28 NO 0.20 mg/L 1 8/6/2009 07:15 PM T/R Hydrocarbons: C28-C36 NO 0.20 mg/L 1 8/6/2009 07:15 PM T/R Hydrocarbons: C36-C40 NO 0.20 mg/L 1 8/612009 07:15 PM T/R Hydrocarbons: C8-C40 Total NO 0.20 mg/L 1 8/6/2009 07:15 PM Sort: p-Terphenyl 73.0 35-131 %REC 1 8/6/2009 07:15 PM I ' Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitahon range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ' /, AdvancedTedarology ' C= LuGorufaries 3275 Widnul Avenue, Signal Hill, CA 90755 31 of 68 Tel, 562. 989.4045 Tax: 562.989.4040 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12 Aag-09 ' CLIENT: Leighton Consulting, Inc. Client Sample ID: B10-GW Lab Order: 106685 Collection Date: 8/3/2009 11:58:00 AM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-013C Analyses Result PQL Quo Units DP Date Analyzed PCBS BY GCIECD EPA 3510C EPA 8082 ' 'RunID: GC4_090807A QC Batch: 57126 PrepDate: 816/2009 Analyst: BB Aroclor 1016 NO 0.50 pg/L 1 8/7/2009 01:00 PM Aroclor 1221 NO 1.0 pg/L 1 81712009 01:00 PM ' Aroclor 1232 NO 0.60 pg/L 1 8/7/2009 01:00 PM Aroclor1242 ND 0.50 pg/L 1 817/200901:00PM Aroclor1248 NO 0.50 pg/L 1 8771200901:00PM , Aroclor 1254 NO 0.60 pg/L 1 8/7/2009 01:00 PM Aroclor1260 NO 0.50 pg/L 1 817/2009 01:00 PM Aroclor 1262 NO 0.50 pg/L 1 8/7/2009 01:00 PM ' Aroclor 1268 ND 0.50 pg/L 1 8t7/2009 01:00 PM Surr: Decachloroblphenyl 80.0 29.130 %REC 1 8/712009 01:00 PM Surr:Tetmchloro-m-xylene 88.9 48.126 %REC 1 817/2009 01:00 PM ' 7 I Qualifiers: B Analytc detected in the associated Method Blank i J E Value above quantilalion range H Holding times rorprepamtion or analysis exceeded NO Not Detected at the Reporting Limit ' S Spike/Surrogate outside of limits due to matrix interference Results are wet unless olitcnvise specified DO Surrogate Diluted Out ' / Adiwaced nchn0/0911 989.404S Par: 962.989.4040 Luboratorles 327S IN(bi rt Avenue, Signal Hill, CA 90755 Tel: 562. 32 of 68 , ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B 10-2 Lab Order: 106685 Collection Date: 8/3/2009 11:53:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-014A Analyses Result PQL Qual Units DT Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: G016_090806C QC Batch: T/R Hydrocarbons: C8-C10 TIR Hydrocarbons: C10-C18 T/R Hydrocarbons: C18-C28 T/R Hydrocarbons: C28-C36 TIR Hydrocarbons: C36-C40 T/R Hydrocarbons: CB-C40 Total Burr: p-Terphenyl HYDROCARBON CHAIN IDENTIFICATION 57087 PrepDate: NO 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 83.8 57-144 %REC 1 EPA 8015B 8/5/2009 Analyst: CBR 8/6/2009 02:48 PM 8/6/2009 02:48 PM 8/6/2009 02:48 PM 8/6/2009 02:48 PM 8/6/2009 02:48 PM 8/612009 02:48 PM 8/6/2009 02:48 PM RunID: GC2 090804E QC Batch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 ND 1.0 mg/Kg 1 8/4/200911:07 PM Burr: Bromofluorobenzene (FID) 96.6 59.145 %REC 1 8/41200911:07 PM ' PCBS BY GC/ECD EPA 3550E EPA 8082 RunlD: GC5_0908065 QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB Aroclor 1016 ND 16 jig/Kg 1 8/7/2009 03:10 AM Aroclor 1221 ND 33 pg/Kg 1 8/7/2009 03:10 AM Aroclor 1232 ND 16 pg/Kg 1 8/7/2009 03:10 AM ' Aroclor 1242 NO 16 pg/Kg 1 8/712009 03:10 AM Aroclor 1248 ND 16 pg/Kg 1 6/7/2009 03:10 AM Aroclor 1254 280 33 pg/Kg 2 8I7/2009 08:08 AM Aroclor 1211 ND 16 pg/Kg 1 8/7/2009 03:10 AM ' Aroclor 1262 NO 16 pg/Kg 1 8/7/2009 03:10 AM Aroclor 1268 ND 16 pg/Kg 1 8/7/2009 03:10 AM Burr: Decachloroblphenyl 107 30-124 %REC 1 8/7/2009 03:10 AM ' Surr: Decachlorobiphenyl 103 30-124 %REC 2 8/7/2009 08:08 AM Burr: Tetrachloro-m-xylene 113 40-118 %REC 1 8/7/2009 03:10 AM SurnTetrachloro-m-xylene 103 40-118 %REC 2 8/7/2009 08:08 AM ' VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 82606 RunID: MS4_090805A QC Batch: K09VS145 PrepDate: Analyst: HH ' 1,1,1,2-Tetrachloroethane NO 5.0 pg/Kg 1 8/5/200912:48 PM 1,1,1-Tnchloroethane ND 5.0 pg/Kg 1 8/5/200912:48 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out eikk idtwucedTecbnotogy ' 11 Lnbd T ec n 3275 Nalnut Aveuue, Signal Hill. CA 90755 Tel: 562. 939.4045 Fax: 562.989.4040 _ 33 of 68 Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-014A ANALYTICAL RESULTS Print Date: 11 Aug-09 CllentSamplelD: 1310-2 Collection Date: 8/3/2009 11:53:00 AM Matrix: SOIL Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC• COMPOUNDS BY GCIMS EPA 8260B RuniD: MS4 090805A 1,1,2,2-Teirachloroethane 1,1,2-Tdchloroethane 1,1.Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trlchlorobenzen e 1,2,3-Tdchloropropane 1,2,4.Tdchlorobenzene 1,2,4-Trimethylbenzene 1,2.Dlbromo-3-chloropropane 1,2-Dibromoethane 1,2-Dichiorobenzene 1,2-Dichioroethane 1,2-Dichloropropane 1,3,5-Tdmethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chiorotoluene 4-Chiorotoluene 4-isopropylloluene Benzene Bromobanzene Bromadichioromethene Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chiomelhone Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Di -Isopropyl ether OC Balch: K09VS145 PrepDale: NO 5.0 pgIK9 1 NO 5.0 pg1Kg 1 NO 5.0 pg/Kg 1 ND 5.0 p91K9 1 ND 5.0 pg/Kg 1 ND 5.0 p9/K9 1 ND 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pgIK9 1 No 10 pg/Kg 1 ND 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 NO 5.0 p9/K9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 p9IK9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 ND 5.0 pg/Kg 1 NO 5.0 p91K9 1 NO 5.0 pgIK9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 ND 5.0 pgIK9 1 NO 5.0 p9IK9 1 NO 5.0 pg/Kg 1 NO 5.0 pg/Kg 1 NO 5.0 pgIK9 1 NO 5.0 pg/Kg 1 NO 6.0 pg/Kg 1 ND 5.0 pg/Kg 1 NO 5.0 p9IK9 1 Analyst: HH 815/200912:48 PM 8/5/200912:48 PM 8151200912:48 PM 8/51200912:48 PM 815/200912:48 PM 815/200912:48 PM 81512009 12:48 PM 81512009 12:48 PM 815/200912'.48 PM 8/51200912:48 PM 8/51200912.48 PM 8151200912:48 PM 8/51200912:48 PM 815/200912:48 PM 81512009 12:48 PM 815/200912:48 PM 8/5/200912:48 PM 815/200912:48 PM 8/51200912:48 PM 8/61200912:48 PM 815/200912:48 PM 8/51200912:48 PM 815/200912:48 PM 8/5/200912:48 PM 8/5/200912:48 PM 8/5/200912:48 PM 815/200912:48 PM 815/200912:48 PM 8/5/200912:48 PM 8l5/200912:48 PM 8/5/200912:48 PM 815/200912:48 PM 8151200912AS PM 8151200912:48 PM' 815/200912:48 PM Qualiners: E Analyte delceled in the associated Method Blank E `Value above quanlitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Itepoding Limit S Spike/Surrogate outside orlimits due to matrix interferonce Results ale wet unless otherwise specified DO Surrogate Diluted Out AdpnncedTer/urology LuLorulorlrs 3275 IVaGrn(dvcrurc, Signu[fli[G CA 90755 %u[: 562.989.4045 1%a,Y: 562.939.4090 ' 34 of 68 id 11 11 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B10-2 Lab Order: 106685 Collection Date: 8/3/2009 11:53:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-014A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 8260E RunlD: MS4_090805A QC Balch: K09VS145 PrepDate: Analyst: HH Dibromochloromethane NO 5.0 pg/Kg 1 8/512009 12:48 PM Dibromomethane ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Dichloroddluoromethane NO 5.0 pg/Kg 1 815/200912:48 PM Ethyl Tert-butyl ether ND 5.0 pg/Kg 1 815/200912:48 PM Ethylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Hexachlorobutadiene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM Isopropylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM m,p-Xylene NO 10 pg/Kg 1 815/200912:48 PM Methylene chloride NO 5.0 pg/Kg 1 8/5/200912:48PM MTBE NO 5.0 pg/Kg 1 815/200912:48 PM n-Butylbenzene ND 5.0 pg/Kg 1 8151200912:48 PM n-Propylbenzene ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Naphthalene ND 6.0 pg/Kg 1 8/5/2009 12:48 PM o-Xylene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM sec-Butylbenzene ND 5.0 pg/Kg 1 815/200912:48 PM Styrene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM Tert-amyl methyl ether NO 5.0 pg/Kg 1 8/5/2009 12:48 PM Tert-Butanol NO 100 pg/Kg 1 81512009 12:48 PM tert-Butylbenzene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM Tetrachloroethene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM Toluene NO 5.0 pg/Kg 1 8/5/2009 12:48 PM trans-1,2-Dichloroethene ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Trichloroethene NO 5.0 pg/Kg 1 8/512009 12:48 PM Tdchlorotluoromethane ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Vinyl chloride ND 5.0 pg/Kg 1 8/5/2009 12:48 PM Surr:1,2-Dichloroethane-d4 118 70-130 %REC 1 8/5/2009 12:48 PM Surr:4-Bromotluorobenzene 102 70-130 %REC 1 8/5/2009 12:48 PM Surr: Dibromo0uoromethane 117 70-130 %REC 1 8151200912:48 PM Surr: Toluene-d8 108 70-130 %REC 1 8/512009 12:48 PM SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550B EPA 8270C RunID: MS 13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP 1,2,4-Tiichoorobenzene ND 330 pg/Kg 1 8/5/2009 04:30 PM 1,2.Dichlorobenzene ND 330 pg/Kg 1 8/5/200904:30PM 1,3-Dichlorobenzene NO 330 pg/Kg 1 8/512009 04:30 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out OjENLaboratories AdvancedTechnolow 11 3275 N�dnulflvenne, SignalHiTl, CA 90755 Tel: 562. 959.4045 Fax: 562.959.4040 1 35 of 68 Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order., 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-014A Analyses Result �I ANALYTICAL RESULTS Print Date: 12-Aug-09 Client Sample ID: B10-2 Collection Date: 8/3/2009 11;53:00 AM Matrix: SOIL PQL Qual Units DG Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550B EPA 8270C RunIO: MS13_090805A QC Batch: 57086 PrepDate: 8/5/2009 Analyst: DMP 1,4-Dichlorobenzene NO 330 pg/Kg 1 8/51200904:30.PM 2,4,5-Tdchlorophenol NO 330 pg/Kg 1 815/2009 04:30 PM 2,4,6-Trichiorophenol NO 330 pg/Kg 1 815/2009 04:30 PM 2,4-Dichlorophenot ND 1600 pg/Kg 1 815/2009 04:30 PM 2,4-Dimethylphenol ND 330 pg1Kg 1 815/2009 04:30 PM 2,4-Dinllrophenoi NO 1600 pg/Kg 1 8/5/2009 04:30 PM 2,4-Dinilrololuene ND 330 pg/Kg 1 8/5/200904:30FM 2,6-Dinitrololuene ND 330 pg/Kg 1 815/2009 04:30 PM 2-Chloronaphthalene ND 330 pg/Kg 1 8/5/2009 04:30 PM 2-Chlorophenol ND 330 pg/Kg 1 8l5/2009 04:30 PM 2-Melhy1naphthalene ND 330 pg/Kg 1 8/5/2009 04:30 PM 2-Methylphenol ND 330 pg/Kg 1 815/2009 04:30 PM 2-Nitrcanlline NO 1600 pg/Kg 1 8/5/200904:30'PM 2-Nitrophenol NO 330 pg/Kg 1 81512009 04:30 PM 3,3'-Dichlorobenzidine ND 660 pg/Kg 1 81512009 04:30 PM 3-Niuoanlline NO 1600 pg/Kg 1 815/2009 04:30 PM 4,6-Dinitro-2-methylphenol NO 1600 pg/Kg 1 8/512009 04:30 PM 4-Bromophenyl-phenylether NO 330 pglKg 1 815/2009 04:30 PM 4-Chloro-3-methylphenol NO 660 pg/Kg 1 8/5/2009 04:30 PM 4-Chloroaniline ND 660 pg/Kg 1 8/5/2009 04:30 PM 4-Chlorophenyl-phenylether ND 330 pg/Kg 1 8/51200904:30PM 4-Melhylphenoi ND 330 pg/Kg 1 8/5/2009 04:30 PM 4-Nitroanlllne ND 1600 pg/Kg 1 815/2009 04:30 PM 4-Nitrophenol No 1600 pg/Kg 1 81512009 04:30 PM Acenaphlhene NO 330 pg/Kg 1 8/5/2009 04:30 PM Acenaphlhylene ND 330 pg/Kg 1 815/2009 04:30 PM Anthracene ND 330 pg/Kg 1 8/51200904:30PM Benzidine (M) ND 1600 pg/Kg 1 815/2009 04:30 PM Benzo(a)anlhracene ND 330 pg/Kg 1 815/2009 04:30 PM Benzo(a)pyrene No 330 pg/Kg 1 815/2009 04:30 PM Benzo(b)0uoranthene ND 330 pg/Kg 1 8/5/2009 04:30 PM Benzo(g,h,i)perylene NO 330 poft 1 8/5/200904:30PM Benzo(k)8uoranthene NO 330 pg/Kg 1 8/5/2009 04:30 PM Senzolcacid ND 1600 pg1Kg 1 8/51200904:30PM Benzyl alcohol ND 660 pg/Kg 1 815/2009 04:30 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range !� ' H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc teat unless othenvise specified DO Surrogate Diluted Out , ZAdvmrced Teclrnologr ' Laboratories 3275 Walnut Avenue, SigrlalHilb CA 90755 Tel: 562. 989.4045 kax: 562.939.4040 36 of 68 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12 Aug-09 Client Sample ID: B10-2 CLIENT: Leighton Consulting, Inc. ' Lab Order: 106685 Collection Date: 8/3/2009 11:53:00 AM Project: SCE Newport,602497-003 Matrix: SOIL Lab ID: 106685-014A ' Analyses Result PQL Qual Units DP Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS 1 EPA 3550B EPA 8270C RunlD: MS 13 090805A QC Batch. 57085 PrepDale: 8/5/2009 Analyst: DMP Bis(2-chloroethoxy)methane ND 330 pg/Kg 1 1 8/5/2009 04:30 PM 8/512009 04:30 PM Bis(2-chloroethyl)ether ND 330 pg/Kg Bis(2-chloroisopropyl)ether ND 330 pg/Kg 1 8/512009 04:30 PM Bis(2-ethylhexyl)phthaiate ND 330 pg/Kg 1 8/5/2009 04:30 PM ' Bulylbenzyiphthalate ND 330 pg/Kg 1 8/5/200904:30PM Chrysene ND 330 pg/Kg 1 8/5/2009 04:30 PM Di-n-butylphthelate ND 330 pg/Kg 1 8/5/2009 04:30 PM Di-n-octylphthalate ND 330 pg/Kg 1 8/5/2009 04:30 PM Dibenz(a,h)anthracene ND 330 pg/Kg 1 8/5/2009 04:30 PM Dibenzofuran ND 330 pg/Kg 1 815/2009 04:30 PM t Dlethyiphthalate ND 330 pg/Kg 1 1 815/2009 04:30 PM 815/2009 04:30 PM Dimelhylphthaiate ND 330 pg/Kg Fluoranthene ND 330 pg/Kg 1 8/5/2009 04:30 PM Fiuorene ND 330 pg/Kg 1 8/5/2009 04:30 PM ' Hexachlorobenzene ND 330 pg/Kg 1 8/5/2009 04:30 PM Hexachiorobutadiene NO 660 pg/Kg 1 8/5/2009 04:30 PM Hexachlorocyclopentadiene NO 660 pg/Kg 1 8l5/2009 04:30 PM ' Hexachloroethane NO 330 pg/Kg 1 8/5I2009 04:30 PM Indeno(1,2,3-cd)pyrene ND 330 pg/Kg 1 8l5/2009 04:30 PM Isophorone ND 330 pg/Kg 1 8/5/2009 04:30 PM N-Nilrosodi-n-propylamine ND 330 pg/Kg 1 8/5/2009 04:30 PM N-Nitrosodiphenylamine ND 330 pg/Kg 1 8/5/2009 04:30 PM Naphthalene ND 330 pg/Kg 1 8/5/2009 04:30 PM Nitrobenzene ND 330 pg/Kg 1 8/512009 04:30 PM ' Pentachlorophenol ND 1600 pg/Kg 1 815/2009 04:30 PM Phenanthrene ND 330 pg/Kg 1 8l5/2009 04:30 PM Phenol ND 330 pg/Kg 1 8/512009 04:30 PM ' Pyrene ND 330 pg/Kg 1 8/5/2009 04:30 PM Surr:1,2-Dichlorobenzene-d4 68.4 49-103 %REC 1 8/5/2009 04:30 PM Surr:2,4,6-Tribromophenol 83.1 47-129 %REC 1 8/51200904:30PM Surr:2-Chlorophenol-d4 76.4 54-109 %REC 1 8/5I2009 04:30 PM ' Surr:2-Fiuorobiphenyl 75.3 59-108 %REC 1 815/2009 04:30 PM Surr:2-Fluorophenol 75.8 50-111 %REC 1 8/5/2009 04:30 PM SurrA-Terphenyl-d14 89.9 58-135 %REC 1 8/5/2009 04:30 PM ' Surr: Nitrobenzene-d5 70.2 54-115 %REC 1 8/5/2009 04:30 PM B Analyte detected in the associated Method Blank E Value above quantilation range ' Qualifiers: H Holding times for preparation or analysts exceeded ND Not Detected at the Reporting Litnit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out A dranced Technologx �= 3275Wa1nrrlAvenuy Signal Hill, CA 90755 Laboratories Ta1:562.959.4045 1%ax:5(2.989.4040 37 of 68 ,64 �r,_ AdviuleedTechnolow Laboratories Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lob Order: 106685 Project: SCE Newport, 602497.003 Lob ID: 106685-014A Analyses Result ANALYTICAL RESULTS Print Date: 12-Aug-09 =-- -- -- - -- ------ - --- -------- ---- --- -- Client Sample lD: E10-2 Collection Date: 8/3/2009 11:53:00 AM Matrix: SOIL PQL Qual Units _ DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550E EPA 8270C RunlD: MS13_090805A QC Batch: 57085 PrepDate: 8/5/2009 Analyst: DMP Sutr: Phenol-d5 78.5 58-112 %REC 1 8/5/2009 04:30 PM Quallflers: B Analyte detected in the associated Method Blank 0 Value above quantization range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out I 3275 WainntAvenue. Signal Hill, CA 90755 Tel. • 562. 989.4045 Fax. 96Z989.4040 38 of 68 I I F— L ANALYTICAL RESULTS Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab ID: 106685-015A Print Date: 12-A:rg-09 Client Sample ID: B10-6 Collection Date: 8/3/2009 11:56:00 AM Matrix: SOIL _ Analyses Result PQL Qual Units DF ' Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunlD: GC16_090806C QC Batch: 57087 PrepDate: 8/5/2009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 10 mg/Kg 1 816/2009 02:58 PM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 8/6/2009 02:58 PM T/R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 8/6/2009 02:58 PM TIR Hydrocarbons: C28-C36 NO 10 mg/Kg 1 8/6/2009 02:58 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 8/612009 02:58 PM T/R Hydrocarbons: C8-C40 Total NO 10 mg/Kg 1 8/6/2009 02:58 PM Surr: p-Terphenyl 93.5 57-144 %REC 1 8/6/2009 02:58 PM HYDROCARBON CHAIN IDENTIFICATION EPA 8015E RunID: GC2_090804B QC Batch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 814/200911:22 PM Surr: Bromolluorobenzene (FID) 92.4 59-146 %REC 1 814/200911:22 PM PCBS BY GC/ECD EPA 3550E EPA 8082 RunlD: GC5 090806E QC Batch: 57129 PrepDate: 8/612009 Analyst: BB Aroclor 1016 NO 16 pg/Kg 1 8I7/2009 03:40 AM Aroclor 1221 NO 33 pg/Kg 1 8/7/2009 03:40 AM Aroclor 1232 NO 16 pg/Kg 1 8/7/2009 03:40 AM Aroclor 1242 NO 16 pg/Kg 1 877/2009 03:40 AM Aroclor 1248 NO 16 pg/Kg 1 817/2009 03:40 AM Aroclor 1254 NO 16 pg/Kg 1 8/7/2009 03:40 AM Aroclor 1260 NO 16 pg/Kg 1 8/7/2009 03:40 AM Aroclor 1262 NO 16 pg/Kg 1 8/7/2009 03:40 AM Aroclor 1268 NO 16 pg/Kg 1 8/7I2609 03:40 AM Surr: Decachlorobiphenyl 93.4 30-124 %REC 1 8f7/2009 03:40 AM Surr: Tetrachloro-m-xylene 102 40-118 %REC 1 817/2009 03:40 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitauon range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out OWN Advanced Adramced7eelchmology ' 11 LnGd ncs 3275 NalnrdAvennu, SignalAill, CA 90755 7e1: 562. 939.4045 Tax: 501.989.4040 _ 39 of 68 I ANALYTICAL R)✓SULTS ' Advanced TechnologyLaboratories Print Date: I2-Atrg-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B9-GW� Lab Order: 106685 Collection Date: 8/3/2009 12:20:00 PM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-016A ' Analyses Result PQL Qual Units DR Date Analyzed HYDROCARBON CHAIN IDENTIFICATION ' EPA 80156 RunID: GCE 090804A QC Batch: IGOVW0134 TIR Hydrocarbons:,C4-C12 NO 0,20 PrepDate: Analyst: BD mg/L 1 8/4I2009 05:15 PM Burr: Bromolluorobenzene (FID) 91.2 71-130 %REC 1 8/4/2009 05:15 PM I 1 I Quallflers•. B Analyte deteetcd in the associated Method Blank 8 Value above quantitation range H Holding times forpreparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogale outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out a Advanced Techuo/og.r LnhorulorJcs 32'1S Wal nut Avennc, Signs/ Hill, CA 907i5 Tel:SG2. 939.4045 lax: 562.939.4090 , 40 of 68 I I 1 1 1 i 1 I 1 1 I C 1 r, F 1 7 u II 1 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B9-GW Lab Order: 106685 Collection Date: 8/3/2009 12:20:00 PM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-016B Analyses Result PQL Qual Units DT Date Analyzed PCBS BY GC/ECD EPA 3510C EPA 8082 RunID: GC4_090807A QC Batch: 57126 PrepDate: Aroclor 1016 NO 0.50 pg/L 1 Aroclor 1221 NO 1.0 pg/L 1 Aroclor 1232 NO 0.50 pg/L 1 Aroclor 1242 ND 0.50 pg/L 1 Aroclor 1248 NO 0.50 pg/L 1 Aroclor 1254 NO 0.50 pg/L 1 Aroclor1260 NO 0.50 pg1L 1 Aroclor 1262 NO 0.50 pg/L 1 Aroclor 1268 ND 0.80 pg/L 1 Burr: Decachlorobiphenyl 79.6 29-130 %REC 1 Burr: Tetrachloro-m-xylene 92.4 48-126 %REC 1 8/6/2009 Analyst: BB 8/7/2009 01.30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 817/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM 8/7/2009 01:30 PM Qualifiers: B Analyse detected in the associated Method Blank E Value above quantilation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out n t AdroLaboratoruo/oS , teedT r Laboratories 275 Walnut Aventie, Sigi:afHill, CA 90755 7e1: 562. 959.4045 Fax: 562.989.4040 _ 41 of 68 Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 ANALYTICAL RESULTS Print Date: 12-Arrg-09 CllentSomplelD: B9-GW Collection Date: 8/3/2009 12:20:00 PM Project: SCE Newport,602497-003 Matrix: GROUNDWATER Lab ID: 106685-016C Analyses Result P L Qual Units DI' Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RunID: GCIU90806F QC Batch: 57067 PrepDate: 81412009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 0.20 mg1L 1 816/2009 07:24 PM TIRHydrocarbons; C10-C18 NO 0.20 mg/L 1 816/2009 07:24 PM TIR Hydrocarbons: C18-C28 NO 0.20 mg/L 1 8/6/2009 07:24 PM T/RHydrocarbons: C28-C36 ND 0.20 mg/L 1 816/2009 07:24 PM T/R Hydrocarbons: C36-C40 No 0.20 mg/L 1 8/6/2009 07:24 PM T/R Hydrocarbons: C8-C40 Total NO 0.20 mg1L 1 8/6/2009 07:24 PM Surr: p Terphanyi 74.8 35.131 %REC 1 8/6/2009 07:24 PM Quulltlers: B Analyte detected in the associated Method Blank _ E Value above quantitalion range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Sutrognle outside or limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out !� Ad Lfibo worleYeelinologp LvGoratorles 32751Vrrinat Averrrra, Signal fli!!, CA 90755 Til: 562. 939.4045 Fae: 562.939.4040 42 of 68 11 I 11 L' I I IJ I lit J I'I I 1 i I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B9-2 Lab Order: 106685 Collection Date: 8/3/2009 12:12:00 PM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-017A Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC16_090806C QC Batch: T/R Hydrocarbons: C8-C10 T/R Hydrocarbons: C10-C18 T/R Hydrocarbons: C18-C28 T/R Hydrocarbons: C28-C36 T/R Hydrocarbons: C36-C40 TIR Hydrocarbons: CB-C40 Total Surr: p-Terphenyl HYDROCARBON CHAIN IDENTIFICATION RunID: G02_090804B T/R Hydrocarbons: C4-C12 Surr: Bromofluorobenzene (FID) PCBS BY GC/ECD RunID: GC5_090806B Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Burr: Decachloroblphenyl Surr: Decachloroblphenyl Burr: Tetrachloro-m-xylene Surr. Tetrachloro-m-xylene 57087 PrepDate: NO 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 NO 10 mg/Kg 1 86.2 57-144 %REC 1 8/5/2009 Analyst: CBR 8/6/2009 03:54 PM 8/6/2009 03:54 PM 8/6/2009 03:54 PM 8/612009 03:54 PM 8/6/2009 03:54 PM 8/6/2009 03:54 PM 8/6/2009 03:54 PM EPA 801513 QC Batch: E09VS246 PrepDate: Analyst: KHN NO 1.0 mg/Kg 1 814/2009 11:37 PM 94.0 59-145 %REC 1 814/200911:37 PM EPA 3550E EPA 8082 QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB NO 16 pg/Kg 1 8/7/2009 04:10 AM ND 33 pg/Kg 1 817/2009 04:10 AM NO 16 pg/Kg 1 8/7/2009 04:10 AM ND 16 pg/Kg 1 8/7/2009 04:10 AM NO 16 pg/Kg 1 8/7/2009 04:10 AM 350 33 pg/Kg 2 8/7/2009 08:38 AM NO 16 pg/Kg 1 8/7/2009 04:10 AM NO 16 pg/Kg 1 8/7/200904:10AM ND 16 pg/Kg 1 8/7/2009 04:10 AM 99.9 30.124 %REC 1 8/7/2009 04:10 AM 99.8 30-124 %REC 2 8/7/2009 08:38 AM 98.2 40-118 %REC 2 8/7/2009 08:38 AM 108 40-118 %REC 1 8/7/2009 04:10 AM ' Qualifiers: - Analyte detected in the associated Method Blank E Value above quamitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reponing1imit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ' /, AdrancedYechnology ' C� Labornlorics 3275 IValnut Avenue, SignallJill, CA 90755 43 of 68 Tel. 562. 989.4045 Fax. 502.989.4040 ' Advanced Technology Laboratories CLIENT: Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 LabIM 106685-018A ANALYTICAL RESULTS Print Date: 12-Arrg-09 Cliau Sample ID: 139.6 --- - --- _-- Collection Date: 8/3/2009 12:17:00 PM Matrix: SOIL Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC16 090806C QC Batch: 67087 T/R Hydrocarbons: C8-C10 T/R Hydrocarbons: CIO-C18 TIR Hydrocarbons: C18-C28 TIR Hydrocarbons: C28-C36 TIR Hydrocarbons: C36-C40 TIR Hydrocarbons: C8•C40 Total Surr. p-Terphenyl HYDROCARBON CHAIN IDENTIFICATION RunID: GC2 090804B TIR Hydrocarbons: C4-Cl2 Surr; Bromofluorobenzene (FID) PCBS BY GCIECD RunIO: GC5.090806B Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Surr. Decochloroblphenyi Surr. Tetrachloro-m-xylene PrepDate; NO 10 mg/Kg 1 NO 10 mglKg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mglKg 1 NO 10 mglKg 1 93.6 57-144 %REC 1 8l5/2009 Analyst: CBR 8/6/2009 03:07 PM 81612009 03:07 PM 8/612009 03:07 PM 81612009 03:07 PM 816/2009 03:07 PM 8/6/2009 03:07 PM 8/6/2009 03:07 PM EPA 8015E QC Batch: E09VS246 PrepDate: Analyst: KHN NO 1.0 mg/Kg 1 814/200911:51 PM 93.5 59-145 %REC 1 8141200911:51 PM EPA 3550E EPA 8082 QC Balch: 57129 PrepDate: $1612009 Analyst: BB NO 16 pg/Kg 1 817/2009 04:40 AM NO 33 pg/Kg 1 8/7/2009 04:40 AM NO 16 pg/Kg 1 8/7/2009 04:40 AM NO 16 pg*9 1 8f7/200904:40AM NO 16 pg/Kg 1 8f71200904:40AM NO 16 pg1Kg 1 81712009 04:40 AM ND 16 pg/Kg 1 8M2009 04:40 AM ND 16 pg/Kg 1 8012009 04:40 AM NO 16 pg/Kg 1 8/7I200904:40AM 100 30-124 %REC 1 8/7/2009 04:40 AM 109 40-118 %REC 1 8012009 04:40 AM J LJ rI7' LJI l� I� I I I QnnllOcra: B Anatyte detected in the associated Method Blank 6 Value above quantitation range �~ , H Holding limes for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Sutrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out , Adl Hared Tec/rrro/aa1' LuGoralar/cs 3275 {4'a/rrn/Avertne, SignalAilG CA 90755 Tel. • 562. 939.40.15 tar: SG2.989.404U' 44 of 68 L li U ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI 1-GW Lab Order: 106685 Collection Date: 8/3/2009 12:57:00 PM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-019A Analyses Result PQL Qual Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 8015B ' RunID: GC6_090814A T/R Hydrocarbons:C4-C12 Surr: Bromofluorobenzene (FID) I I QC Balch: 109VW0134 ND 0.20 mg/L 92.5 71-130 %REG PrepDate: Analyst: BD 1 814/2009 06:19 PM 1 8/4/2009 06:19 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantilahon range H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified LDO Surrogate Diluted Out ' A dvanced Technologf, 11 3275 iVelnntAvenue, Signal Flill, CA Laboratories 90755 7e1: 562. 989.4015 Far:.S(2.989.4040 45 of 68 ANALYTICAL RESULTS , Advanced TechnologyLaboratories Print Date: 12 -Ang-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI I-GW Lab Order: 106685 Collection Date: 8/3/2009 12:57:00 PM ' Project: SCE Newport, 602497-003 Matrix: GROUNDWATER Lab ID: 106685-019B ' Analyses Result PQL Qual Units DG Date Analyzed PCBS BY GCIECD ` EPA 3610C EPA 8082 RunlD: GC4 090807A QC Batch: Aroclor 1016 57126 ND 0.50 PrepDale: pg1L 1 8/612009 Analyst: BB 8/7/2009 02:00 PM ' Aroclor 1221 NO 1.0 pg/L 1 817/2009 02:00 PM Aroclor 1232 NO 0.50 pg/L 1 817/2009 02:00 PM Aroclor 1242 NO 0.50 pgn- 1 8/7/2009 02:00 PM Aroclor 1248 NO 0.50 pg/L 1 8/712009 02:00 PM Aroclor 1264 'ND 0.50 pglL 1 8/712009 02:00 PM Aroclor1260 NO 0.50 pg/L 1 81712009 02:00 PM Aroclor 1262 NO 0.50 pg1L 1 8f7/2009 02:00 PM ' Aroclor1268 ND 0.50 pg1L 1 8R/200902:00PM Surr. Decachlorobiphenyl 84.0 29-130 %REC 1 8/7/2009 02:00 PM Surr:Telrachloro-m-xylene 92.2 48-126 %REC 1 8/7/2009 02:00 PM , Qualiners: ➢ Analyte detected in the associated Method Blank E Value above quanlitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogatcoutside ortimitsdue tomatrix interrerence Results are wet unless othenvisespecified DO Surrogate Diluted Out LuGoru(or/es 3275 IVrdnwAvenee, Signalf ill, CA 90755 46 of 68 Tclr 562. 989,4045 Far: 562.989.4040 i I ANALYTICAL RESULTS 1 Advanced Technology Laboratories Print Date: 12-Aug-09 1 CLIENT: Leighton Consulting, Inc. Client Sample ID: BI I-GW Lab Order: 106695 Collection Date: 8/3/2009 12:57:00 PM Project: SCE Newport, 602497-003 Matrix: GROUNDWATER 1 Lab ID: 106685-019C Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION EPA 3510C EPA 8015B(M) RuniD: GC16_090806F QC Batch: 57067 PrepDate: 8/4/2009 Analyst: CBR 1 T/R Hydrocarbons: C8-C10 NO 0.20 mg/L 1 8/6/2009 07:33 PM 8/6/2009 07:33 PM T/R Hydrocarbons: C10-CIB NO 0.20 mg/L 1 T/R Hydrocarbons: C18-C28 NO 0.20 mg/L 1 816/2009 07:33 PM T/R Hydrocarbons: C28-C36 NO 0.20 mglL 1 8l6/2009 07.33 PM 1 T/R Hydrocarbons: C36-C40 NO 0.20 mg/L 1 8/6/2009 07:33 PM T/R Hydrocarbons: C8-C40 Total NO 0.20 mg/L 1 8/6/2009 07:33 PM 1 Surr: p-Terphenyl 77.8 35-131 %REC 1 8/612009 07:33 PM 1 1 1 i 1 1 1 B Analyte detected to the associated Method Blank E Value above quantitation range 1 Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out 1 1 Adraa bo Technoatories P �1 Laboratories 3275 Wttftttrt Avett:re, Signal Hill, CA 90755 7e1: 562. 989.4045 17ax: 562.989.4040 _ � 47 of 68 I ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample 1D: B 11-2 Lob Order: 106685 Collection Date: 8/3/2009 12:51:00 PM Project: SCE Newport,602497-003 Matrix. SOIL Lab ID: 106685-020A , Analyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LOFT EPA 8015B(M) , RunID: GC16 090806C QC Balch: 57087 PrepDate: 8/512009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 10 mg/Kg 1 816/2009 03:16 PM ' T/R Hydrocarbons: CIO-C18 NO 10 mg1Kg 1 8/612009 03A6 PM T/R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 816/2009 03:16 PM T/RHydrocarbons,.C28-C36 NO 10 mg/Kg 1 816/2009 03:16 PM T/R Hydrocarbons: C36-C40 NO 10 mglKg 1 8/6/2009 03:16 PM T/R Hydrocarbons: C8-C40 Total NO 10 mg/Kg 1 8/612009 03:16 PM Surr. p-Terphenyl 96.7 57-144 %REC 1 8/612009 03:16 PM HYDROCARBON CHAIN IDENTIFICATION ' EPA 80158 RumID: GC2 090804B QC Balch: E09VS246 PrepDate: Analyst: KHN T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 8/5/200912:06 AM Surr. BroMo8uorobenzene (FID) 96.4 59.145 %REC 1 8/5/200912:06 AM PCBS BY GC/ECD EPA 3550E EPA 8082 ' RunlD: GCS 090806E QC Batch: 57129 PrepDate: 81612009 Analyst: BB Aroclor 1016 NO 16 pg/Kg 1 8/712009 05:10 AM Aroclor1221 NO 33 pglKg 1 8/71200905:10AM , Aroclor1232 NO 16 pg/Kg 1 8/7/200905:10AM Aroclor1242 Aroclor1248 NO NO 16 16 pg/Kg pg/Kg 1 1 817/2009 05:10 AM 817/2009 05:10 AM ' Aroclor 1254 NO 16 pg/Kg 1 8/7/2009 05:10 AM Aroclor 1260 NO 16 pg/Kg 1 8/7/2009 05:10 AM Aroclor 1262 ND 16 pg/Kg 1 8/7/2009 05:10 AM Aroclor 1268 NO 16 pg/Kg 1 8/7/2009 05:10 AM , Surr. Decachloroblphenyl 98.0 30-124 %REC 1 8/7/2009 05:10 AM Surr: Tetrachloro-m-xylene 108 40.118 %REC 1 8/7I2009 05:10 AM I Qualifiers: B Analyte detected in the associated Method Blank B Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out 00 Adranced Techno/09.11 Luhornl0rles 3275 IValrrrrlAvenne, Signulflill. CA 90755 TOI: 562. 939.4045 Fax: 562.939.4040 48 of 68 RESULTS 'ANALYTICAL Advanced Technology Laboratories Print Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B11-5 Lab Order: 106685 Collection Date: 8/3/2009 12:56:00 PM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-021A Analyses Result PQL Qual Units DR Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunlO: GC16_090806C QC Batch: 57087 PrepDate: 8/5/2009 Analyst: CBR ' T/R Hydrocarbons: CB-010 NO 10 mg/Kg 1 8/6/2009 03:27 PM T/R Hydrocarbons: C10-C18 ND 10 mg/Kg 1 8/612009 03:27 PM T/R Hydrocarbons: C18-C28 ND 10 mg/Kg 1 8/6/2009 03:27 PM ' T/R Hydrocarbons: C28-C36 ND 10 mg/Kg 1 1 8/6/2009 03:27 PM 8/6/2009 03:27 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg T/R Hydrocarbons: C8-C40 Total NO 10 mg/Kg 1 8/6/2009 03:27 PM Surr: p-Terphenyl 101 57-144 %REC 1 8/6/2009 03:27 PM ' HYDROCARBON CHAIN IDENTIFICATION EPA 801513 RunID: GC2 090804E QC Batch: E09VS246 PrepDate: Analyst: KHN ' T/R Hydrocarbons: C4-C12 NO 1.0 mg/Kg 1 8/51200912:21 AM Surr: Bromofluorobenzene (FID) 92.9 59-145 %REC 1 8/51200912:21 AM PCBS BY GC/ECD EPA 35508 EPA 8082 RunlD: GC5 090806E QC Batch: 57129 PrepDate: 8/6/2009 Analyst: BB ' Aroclor 1016 ND 16 pg/Kg 1 1 8/712009 05:39 AM 8/7/2009 05:39 AM Aroclor 1221 ND 33 pg/Kg Aroclor1232 No 16 pg/Kg 1 8/7/200905:39AM Aroclor 1242 ND 16 pg/Kg 1 8/7/2009 05:39 AM �- Aroclor 1248 NO 16 pg/Kg 1 8/712009 05:39 AM Aroclor 1264 ND 16 pg/Kg 1 8/7I2009 05:39 AM Aroclor 1260 ND 16 pg/Kg 1 8/7/2009 05:39 AM Aroclor 1262 NO 16 pg/Kg 1 817/2009 05:39 AM Aroclor 1268 NO 16 pg/Kg 1 8/7/2009 05:39 AM Surr: Decachlorobiphenyl 96.3 30-124 %REC 1 8/7/2009 05:39 AM Surr: Tetrachloro-m-xylene 106 40.118 %REC 1 8/7/2009 05:39 AM Ul Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified ' DO Surrogate Diluted Out �y,, 11 _ inced Technology Adrnn boratohrmlogr 3275 Walnut Avenue, Signal Hill, CA 90755 Tr : 562. 939.4045 Far: 502.989.4040 49 of 68 Advanced Technology Laboratories Date: 12 Aug-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8082_S Sample ID: MS-57129 SampType: MBLK TestCode: 8082 S Units: pg1Kg Prep Date: 81612009 RunNo: 111484 ;lient ID: PBS Batch ID: 57129 TestNo: EPA 8082 EPA 3550E Analysis Date: 8/6/2009 SegNo: 1757122 4nalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroctor 1016 NO 16 Arodor 1221 ND 33 Arodor 1232 ND 16 Arodor 1242 NO 16 Arodor 1248 NO 16 Arodor 1254 NO 16 Arodor 1260 ND 16 Amclor 1262 ND 16 Arodor 1268 ND 16 Surr. Decachlorobiphenyl 12.911 Surr. Tetrachlonrm-xylene 14.894 16.67 77.5 30 124 16.67 89.3 40 118 RunNo: 111484 'ample ID: LCS-57129 SampType: LCS TestCode: 8082 S Units: pglKg Prep Date: 81612009 :lient ID: LCSS Batch ID: 57129 TestNo: EPA 8082 EPA 3550E Analysis Date: 8/6/2009 SegNo: 1757123 lnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua) Aroctor 1016 142.917 16 166.7 0 85.7 56 113 Amclor 1260 157.177 16 166.7 0 94.3 58 111 Surr. Decachiombiphenyl 15.036 16.67 90.2 30 124 Surr. Tetrachloro-m-xylene 17.191 16.67 103 40 118 Sample ID: 106727-OOSAMS SampType: MS TestCode: 8082 S Units: pg1Kg Prep Date: 816/2009 RunNo: 111484 client ID: 777777 Batch ID: 57129 TestNo: EPA 8082 EPA 3550B Analysis Date: 8/6/2009 SegNo: 1767124 knalyte Result POL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroctor 1016 131.355 16 166.7 0 78.8 S1 111 Aroctor 1260 152.117 16 166.7 0 91.3 39 123 Surr. Decachiorobipheny) 15.189 16.67 91.1 30 124 Qualifiers: B Analyte detected in the associntedMethodBlank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Adron<MTer�rro I LalrontorRs loRr. 3275 )I ofnrrtiL•cune, Signnf Hill, 07 90755 Tel.562. 949.40J5 Fay: 562.9S9.J0{0 50 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference M M � an i CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8082_S Sample ID: 106727-OOSAMS SampType: MS TestCode: 8082_S Units: pg/Kg Prep Date: 8/612009 RunNo: 111484 Client ID: ZZ777 Batch ID: 57129 TestNo: EPA 8082 EPA 3550B Analysis Date: 81612009 SegNo: 1757124 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighL[mit RPD Ref Val %RPD RPDLimit Qua[ Surr. Tetrachloro-m-xylene 14.991 16.67 89.9 40 118 '>ample ID: 106727-005AMSD SampType: MSD TestCode: 8082_S Units: pglKg Prep Date: 816/2009 RunNo: 111484 client ID: ZZ7777 Batch ID: 57129 TestNo: EPA 8082 EPA 3550B Analysis Date: 8/6/2009 SegNo: 1757125 4nalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 133.900 16 166.7 0 80.3 51 ill 131.4 1.92 zu Aroclor 1260 154.630 16 166.7 0 92.8 39 123 152.1 1.64 20 Surr: Decachlorobiphenyl 14.807 16.67 88.8 30 124 0 0 Surr. Tetrachloro-m-xylene 15.266 16.67 91.6 40 118 0 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantrtation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values / I , Adrnnrcd Tethnolo�l' need T chna 3275 R'aLmrA•cnne, Signnl Hill, CA 90755 Tick 562. 989.4045 Fax: 562.989.4040 51 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8082 W Sample ID: MB-57126 SampType: MBLK TestCode: 8082 W Units: pg[L Prep Dale: 8/612009 RunNo. 111503 Client ID: PEW Batch ID: 57126 TestNo: EPA-8082 EPA 3510C Analysis Date: 8/7/2009 SegNo: 1767548 I Analvte Result PQL SPK value SPK Ref Val %REC Lowltmit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Sum Decachlorobiphenyl Sample ID: LCSA-57126 SampType: LCS TestCode: 8082 W Units: pg/L Prep Dale: 816/2009 RunNo: 111503 Client ID: LCSW Batch ID: 57126 TestNo: EPA 8082 EPA 3510C Analysis Date: W12009 SegNo: 1757549 I Anatvtp Result POL SPK value SPK Ref Val %REC LOWUmit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1260 Sum Decachlorobiphenyl Sample ID: MB-57126MSA SampType: MS TestCode: 8082LW Units: pg1L Prep Date: 8/6/2009 RunNo: 111503 Client ID: 772777 Batch ID: 57126 TestNo: EPA 8082 EPA 3510C Analysis Date: 8/7/2009 SegNo: 1757550 AnaMe Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] Aroclor 1260 Sum Decachlorobiphenyl Sum Tebachloro-m-xylene tluanuers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Adranred TerAnohyr I LaAaralodn 3275 8'alnnrArenue. Signal Hill, 01 90755 Tel: 562 989.4045 Far 562.989.4040 M 1&0, H Holding times for preparation or analysis exceeded S Spike/Surregate outside of Limits due to matrix interference M 1-ft CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8082_W ample ID: MS-57126MSDA SampType: MSD TestCode: 8082 W Units: pg1L Prep Date: 8/6/2009 RunNo: 111503 lient ID: 727777 Batch ID: 57126 TestNo: EPA 8082 EPA 3510C Analysis Date: 817/2009 SegNo: 1757551 nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imrt Highl-imit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 3.778 0.50 5.000 0 75.6 59 113 3.736 1.u5 zu Aroclor 1260 3.901 0.50 5.000 0 78.0 60 114 3.856 1.15 20 Surr: Decachlorobiphenyl 0.386 0.5000 77.2 29 130 0 0 Surr: Tetrachloro-m-xylene 0.437 0.5000 87.4 48 126 0 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations am based on raw values �= "inured Teehnotanr 7.aGarJtaries 327511'aGmtdrenne, Signal Hill, CA 9t7735 Tet: 562. 989.JOJ5 Fax: 561.989.1040 53 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 TestCode: 826O_S Sample ID: K090805LCl SampType: LCS TestCode: 8260 S Units: pglKg Prep Date: RunNo: 111443 Client ID: LCSS Batch ID: K09VS145 TestNo: EPA 8260E Analysis Date: 8/512009 SegNo: 1756323 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1.Dichloroethene 51.920 5.0 50.00 0 104 70 130 Benzene 99.490 5.0 100.0 0 99.5 70 130 Chlorobenzene 53.930 5.0 50.OD 0 108 70 130 MTBE 51.210 5.0 50.00 0 102 70 130 Toluene 101.540 5.0 100.0 0 102 70 130 Trichloroethene 48,900 5.0 50.00 0 97.8 70 130 Sum 1,2-Dichloroethanetl4 53,840 50.00 108 70 130 Sum 4-Bromofluorobenzene 51.610 50.00 103 70 130 Sum Dibromo0ucromethane 54.170 50.00 108 70 130 Sum. Toluene-d8 53.390 50.00 107 70 130 Sample ID: 106685-OOSAMS SampType: MS TestCode: 8260 S Units: pglKg Prep Date: RunNo: 111443 ,lient ID: B7-2 Batch ID. K09VS145 TestNo: EPA 8260E Analysis Date: 8/512009 SegNo: 1756324 knalyte Result PQL SPKvalue SPK Ref Val %REC LowLimit Hight -limit RPD Ref Val %RPD RPDLimit Quai 1,1-Dichloroethene 56.990 5.0 50.00 0 114 70 130 Benzene 91.510 5.0 100.0 0 91.5 70 130 Chlorobenzene 48.190 5.0 50.00 0 96.4 70 130 MTBE 51.730 5.0 50.00 0 103 70 130 Toluene 92AOO 5.0 100.0 0 92.4 70 130 Trichloroethene 80.810 5.0 50.00 0 162 70 130 S Sum 1,2-Dichloroethan"4 51.910 50.00 104 70 130 Sum 4-Bromofluorobenzene 49.560 50.00 99.1 70 130 Sum Dibromo0uoromethane 26.130 50.00 52.3 70 130 S Sum Toluene-d8 51.360 50.00 103 70 130 'ample ID: 106685-OOSAMSD SampType: MSO TestCode: 826C S Units: pg/Kg Prep Date: RunNo: 111443 :lient ID: B7-2' Batch ID: K09VS145 TestNo: EPA 8260E Analysis Date: 81512009 SegNo: 1756325 \nalyte Result PQL SPK value SPK Ref Val %REC Lowt.imit HighLimit RPD Ref Val °SRPD RPDLimit Qual Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected arthe Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations arc based on mw values rldraacedTirAnofa�m �' labnruforin i='S flirinut Arcrurr, Slgna[Hilf, C.1 907,55 Tel: 562. 939.4015 Facf562.9S9.JOJ0 5 4O �68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8260_S Sample ID: 106685-006AMSD SampType: MSD TestCode: 8260_S Units: pg/Kg Prep Date: RunNo: 111443 Client ID: B7-2 Batch ID: K09VS145 TestNo: EPA 8260E Analysis Date: 8/5/2009 SegNo: 1756325 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 63.950 5.0 50.00 0 128 70 130 55.99 11.5 LU Benzene 95.260 5.0 100.0 0 95.3 70 130 91.51 4.02 20 Chlorobenzene 48.570 5.0 50.00 0 97.1 70 130 48.19 0.785 20 MTBE 49.000 5.0 50.00 0 98.0 70 130 51.73 5.42 20 Toluene 97.560 5.0 100.0 0 97.6 70 130 92.40 5.43 20 Trichloroethene 85.840 5.0 50.00 0 172 70 130 80.81 6.04 20 S Surr: 1,2-Dichloroethane-d4 49.480 50.00 99.0 70 130 0 20 Surr: 4-Bromofluorobenzene 50.870 50.00 102 70 130 0 20 Surr: Dibromolluoromethane, 22.300 50.00 44.6 70 130 0 20 S Surr. Toluene-d8 53.610 50.00 107 70 130 0 20 Sample ID: K09OB05MBI SampType: MBLK TestCode: 8260_S Units: pglKg Prep Date: RunNo: 111443 Client ID: PBS Batch ID: K09VS145 TestNo: EPA 8260B Analysis Date: 8/512009 SegNo. 1756326 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit oust 1,1,1,2-Tetrachloroethane ND 5.0 1, 1, 1 -Trichloroethane NO 5.0 1,1,2,2-Tetmchloroethane ND 5.0 1,1,2-Trichloroethane ND 5.0 1,1-Dichloroethane NO 5.0 1,1-Dichloroethene ND 5.0 1,1-Dichloropropene NO 5.0 1,2,3-Tdchlorobenzene ND 5.0 1,2,3-Trichloropropane NO 5.0 1,2,4-Trichlorobenzene ND 5.0 1,2,4-Trimethylbenzene NO 5.0 1,2-Dibromo-3-chloropropane NO 10 1,2-Dibromoethane ND 5.0 1,2-Dichlorobenzene NO 5.0 1,2-Dichloroethane ND 5.0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Dduted Out Calculations are based on raw values .tdrshred Tirhno&�,r 3275 WalnutAvenue, Signal HGI ill, 90755 Tel: 562. 989.4045 F¢r. 562.959.1040 LaDurs+roria �= 55 of 68 CLIENT-- Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 TestCode: 8260_S Sample ID: K090805MBI SampType. MBLK TestCode: 8260_S Units: pg1Kg Prep Date: RunNo: 111443 Client ID: PBS Batch ID: K09VS145 TestNo: EPA 8260E Analysis Date: 8/5/2009 SegNo: 1756326 Analyte Result POL SPK value SPK Ref Val %REC LowUmit HighUmit RPD Ref Val %RPD RPDUmit Qual 1,2-Dichloropropane NO 5.0 1,3,5-Trimethylbenzene NO 5.0 1,3-Dichlorobenzene NO 5.0 1,3-Dichloropropane NO 5.0 1,4-Dichlorobenzene ND 5.0 2,2-Dichloropropane ND 5.0 2-Chlorotoluene ND 5.0 4-Chlorotoluene ND 5.0 4-Isopropyltoluene ND 5.0 Benzene NO 5.0 Bromobenzene ND 5.0 Bromodichlommethane NO 5.0 Bromofonn ND 5.0 Bromomethane ND 5.0 Carbon tetrachloride NO 5.0 Chlorobenzene ND 5.0 Chloroethane ND 5.0 Chloroform ND 5.0 Chloromethane ND 5.0 cis-1,2-Dichloroethene NO 5.0 cis-1,3-Dichloropropene NO 5.0 Di -isopropyl ether ND 5.0 Dibromochloromethane ND 5.0 Dibromomethane ND 5.0 Dichlorodifluoromethane NO 5.0 Ethyl Tert-butyl ether NO 5.0 Ethylbenzene NO 5.0 Hexachlorobutadiene NO 6.0 Isopropylbenzene ND 5.0 m,p-Xylene ND 10 Qualirlers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outsideaccepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values i dr �uax d Terhrrolop�, I La(wnrorirs 3'7= )rulrrurdrnme. SigualHi!!, Cif 90733 Trl: Sti1 939.J4J5 Far. 36A939.4OaO ' M 5U668 M M M M M M M M M Work Order: 106685 Project: SCE Newport, 602497-003 A�CTFMAMYM0" TestCode: 8260 S iample to: K090805MB1 SampType: MBLK TestCode: 8260_S Units: pglKg Prep Date: RunNo: 111443 :lien[ ID: PBS Batch ID: K09VS145 TestNo: EPA 8260E Analysis Date: 8/512009 SegNo: 1756326 lnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Methylene chloride ND 5.0 MTBE ND 5.0 n-Butylbenzene ND 5.0 n-Propylbenzene ND 5.0 Naphthalene NO 5.0 o-Xylene ND 5.0 sec-Butylbenzene ND 5.0 Styrene NO 5.0 Tert-amyl methyl ether ND 5.0 Tert-Butanol NO 100 tert-Butylbenzene NO 5.0 Tetrachloroethene ND 5.0 Toluene ND 5.0 trans-1,2-Dichloroethene NO 5.0 Trichloroethene NO 5.0 Trichlorofluoromethane ND 5.0 Vinyl chloride NO 5.0 Surr: 1,2-Dichloroethane-d4 54.310 50.00 109 70 130 Surr. 4-Bromofluorobenzene 50.580 50.00 101 70 130 Sum: Dibromofluoromethane 56.260 50.00 113 70 130 Surr: Toluene-d8 53.050 50.00 106 70 130 Qualifiers: B Analyte detected in the associated Method Blank 'E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values rtd,T-"7'0 ' bu0un+torirs 32751Vubuttdrenue Signal Hill, CA 90755 Tel. 562. 989.4045 Far.561.989.4040 57 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8270 S FULL Sample ID: MB-57085 SampType: MBLK TestCode: 8270_S_FUL Units: pglKg Prep Date: 8/5/2009 RunNo: 111444 Client ID: PBS Batch ID; 57085 TestNo: EPA 8270C EPA 3550B Analysis Date: 815/2009 SegNo: 1756266 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Hight-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene NO 330 1,2.Dichlorobenzene NO 330 1,3-Dichlorobenzene NO 330 1,4-Dichlorobenzene NO 330 2,4,5-Trichlorophenol NO 330 2,4,6-Trichlorophenol NO 330 2,4-Dichlorophenol NO 1600 2,4-Dimethylphenol NO 330 2,4-Dinitrophenot NO 1600 2,4-Dinitrotoluene NO 330 2,6-Dinitrotoluene NO 330 2-Chloronaphthalene NO 330 2-Chlorophenol NO 330 2-Methylnaphthalene NO 330 2-Methylphenol NO 330 2-Nitroaniline NO 1600 2-Nitrophenol NO 330 3,3'-Dichlorobenzidine NO 660 3-Nitroaniline NO 1600 4,6'Dinitro-2-methylphenol NO 1600 4-Bromophenyl-phenylether NO 330 4-Chloro-3-methylphenol NO 660 4-Chloroanitine NO 660 4-Chtorophenyl-phenylether NO 330 4-Methylphenol NO 330 4-Nitroaniline NO 1600 4-Nitrophenol No 1600 Acenaphthene NO 330 Acenaphthylene NO 330 Anthracene NO 330 Qualifiers: B Analyte detected in the associated Method Blank E Value abovequantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values AdrnnredTetAnalogrr Ladorarndce 3?'S 6'aLnn.b'eimr, Signal Hill, C1 90755 rel. 56Z 989.4045 Fax 562.989.4040 �� 58 of 68 M M M M M M Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8270 S FULL Sample ID: MS-57085 SampType: MBLK TestCode: 8270 S FUL Units: pg/Kg Prep Date: 8/5/2009 RunNo: 111444 Client ID: PBS Batch ID: 57085 TestNo: EPA 8270C EPA 3550E Analysis Date: 81512009 SegNo: 1756266 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qua] Benz]dine (M) NO 1600 Benzo(a)anthracene ND 330 Benzo(a)pyrene NO 330 Benzo(b)fluoranthene NO 330 Benzo(g,h,])perylene NO 330 Senzo(k)fluoranthene NO 330 Benzoic acid NO 1600 Benzyl alcohol NO 660 Bis(2-chloroethoxy)methane NO 330 Bis(2-chloroethyl)ether NO 330 Bis(2-chloroisopropyl)ether ND 330 Bis(2-ethylhexyl)phthalate NO 330 Butylbenzylphlhalate NO 330 Chrysene ND 330 Di-n-butylphthalate NO 330 Di-n-octylphthalate ND 330 Dibenz(a,h)anthracene NO 330 Dibenzofuran NO 330 Diethylphthalate ND 330 Dimethylphthalate NO 330 Fluoranthene NO 330 Fluorene ND 330 Hexachlorobenzene NO 330 Hexachlorobutadiene NO 660 Hexachlorocyclopentadiene NO 660 Hexachloroethane NO 330 Indeno(1,2,3-cd)pyrene ND 330 Isophorone NO 330 N-Nilrosodi-n-propylamine NO 330 N-Nitrosodiphenylamine - NO 330 Qualifiers: B Analyte detected in the associated Method Blank NO Not Detected at the Reporting Limit /, DO Surrogate Diluted Out Idranced Teehnulo•• E Value above quantitation range R RPD outside accepted recovery limits Calculations are based on raw values I, ♦= ahorJraries 3275 Walnut drmure, Signal Hill, Gl 90755 TeL•562. 989.4045 Far.562.989.J010 59 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCENewport, 602497-003 TestCode: 8270_S_FULL RunNo: 111444 Sample ID: MB-57085 SampType: MBLK TestCode: 8270 S FUL Units: pg1Kg Prep Date: 81512009 3rient ID: PBS Batch ID: 57085 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/512009 SegNo: 1756266 4nalyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual Naphthalene NO 330 Nitrobenzene NO 330 Pentachlorophenol NO 1600 Phenanthrene NO 330 Phenol NO 330 Pyrene NO 330 Sum. 1,2-Dichlorobenzene-d4 2841.000 Sun: 2,4,6-Tribromophenol 3180.333 Sun: 2-Chlorophenol-d4 3021.000 Surr. 2-Fluorobiphenyl 2881.000 Surr. 2-Fluorophenol 2991.000 Sum. 4-Terphenyl-d14 3005.333 Sun- Nitrobenzene-d5 2887.333 Sun: Phenol-d5 3085.667 3330 85.3 49 103 3330 95.5 47 129 3330 90.7 54 109 3330 86.5 59 108 3330 89.8 50 III 3330 90.3 58 135 3330 86.7 54 115 3330 92.7 58 112 RunNo. 111444 Sample ID: LCS-57085 SampType: LCS TestCode: 8270_S_FUL Units: pglKg Prep Date: 8/5/2009 Client ID: LCSS Balch ID: 57085 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/5/2009 SegNo: 1756267 Analyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene 2838.667 330 3330 0 85.2 61 107 1,4-Dichlorobenzene 2875.667 330 3330 0 86.4 56 100 2,4-Dinitmtoluene 3180.333 330 3330 0 95.5 72 130 2-Chlorophenol 2733.667 330 3330 0 82.1 64 105 4-Chloro-3-methylphenol 2955.667 660 3330 0 88.8 74 125 4-Nitrophenol 2887.000 1600 3330 0 86.7 77 137 Acenaphthene 2885.333 330 3330 0 86.9 63 117 N-Nitrosodi-n-propylamine 3055.667 330 3330 0 91.8 71 121 Pentachlorophenol 289T 667 1600 3330 0 87.0 69 125 Phenol 2795.000 330 3330 0 83.9 67 111 Pyrene 3107.333 330 3330 0 93.3 60 122 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Sunogate outside of limits due to matrix interference DO SunogateDiluted Out Calculations am based on rawvalues lid, sacMTirhwotol- 7y ynyrories 921-5 Walnut Arenae, Signal Hill, CA 90755 Tel.• $62. 989.4045 Fac 562.989.4040 M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8270_S_FULL Sample ID: LCS-57085 SampType: LCS TestCode: 8270_S_FUL Units: pg/Kg Prep Date: 8/5/2009 RunNo: 111444 Client ID: LCSS Batch ID: 57085 TestNo: EPA 8270C EPA 3550B Analysis Date: 8/5/2009 SegNo: 1756267 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual Surr: 1,2-Dichlorobenzene-d4 2793.333 3330 83.9 49 1u3 Surr. 2,4,6-Tnbromophenol 3216.667 3330 96.6 47 129 Surr: 2-Chlorophenol-d4 2931.333 3330 88.0 54 109 Surr: 2-Fluorobiphenyl 2832.000 3330 85.0 59 108 Surr. 2-Fluorophenol 2849.667 3330 85.6 50 111 Surr: 4-Terphenyl-dl4 2954.667 3330 88.7 58 135 Surr: Nitrobenzene-d5 2759.667 3330 82.9 54 115 Surr: Phenol-d5 2931.000 3330 88.0 58 112 Sample ID: 106650-014AMS SampType: MS TestCode: 8270_S_FUL Units: pg/Kg Prep Date: 8/5/2009 RunNo: 111444 Client ID: ZZ7777 Batch ID: 57085 TestNo: EPA 8270C EPA 3550B Analysis Date: 8/512009 SegNo: 1756268 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Tnchlorobenzene 2592.000 330 3330 0 77.8 60 105 1,4-Dichlorobenzene 2460.000 330 3330 0 73.9 50 99 2,4-Dinitrotoluene 3379.000 330 3330 0 101 70 130 2-Chlorophenol 2516.333 330 3330 0 75.6 58 107 4-Chloro-3-methylphenol 2980.333 660 3330 0 89.5 72 124 4-Nitrophenol 3025.333 1600 3330 0 90.9 69 139 Acenaphthene 2905.333 330 3330 0 87.2 59 118 N-Nitrosodi-n-propylamine 2901.000 330 3330 0 87.1 61 125 Pentachlorophenol 3106.667 1600 3330 0 93.3 56 131 Phenol 2657.333 330 3330 0 79.8 60 113 Pyrene 3263.667 330 3330 0 98.0 51 130 Surr. 1,2-Dichlorobenzene-d4 2413.667 3330 72.5 49 103 Surr: 2,4,6-Tnbromophenol 3194.667 3330 95.9 47 129 ' Surr: 2-Chlorophenol-d4 2649.000 3330 79.5 54 109 Surr: 2-Fluorobiphenyl 2738.333 3330 82.2 59 108 Surr. 2-Fluorophenol 2593.667 3330 77.9 50 ill Surr. 4-Terphenyl-dl4 3115.000 3330 93.5 58 135 Qualifiers: B Analyte ddiected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Sunogateoutside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values .dinned Technology 3?751fuluru Abcuue, Signal Hill, C.19t7i55 �= Tel.i62. 989.dOJi Tar: 562.989.tOJd Lnhorolorler 61 of 68 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: 8270 S FULL Sample ID: 106650-014AMS SampType: MS TestCode: 8270 S PUL Units: pglKg Prep Date: 8/5/2009 RunNo: 111444 Client ID: 277722 Batch ID: 57085 TestNo: EPA 8270C EPA 3550E Analysis Date: 81512009 SegNo: 1756268 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sum Nitrobenzene-d5 2525.333 3330 75.8 54 115 Surr. Phenol-d5 2743.667 3330 82.4 58 112 Sample ID: 106650-014AMSD SampType: MSD TestCode: 8270 S FUL Units: pg[Kg Prep Date: 815/2009 RunNo: 111444 Client ID: 2271ZZ Balch ID: 57085 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/5/2009 SegNo: 1756269 Analyte Result POL SPK value SPK Ref Val %REC Lowl-imil HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,2,4-Trichlorobenzene 2521.333 330 3330 0 75.7 60 105 2592 2.76 20 1,4-Dichlorobenzene 2391.667 330 3330 0 71.8 50 99 2460 2.82 20 2,4-Dinitrotoluene 3298.333 330 3330 0 99.0 70 130 3379 2.42 20 2-Chlorophenol 2446.667 330 3330 0 73.5 58 107 2516 2.81 20 4-Chloro-3-methylphenol 2952.667 660 3330 0 88.7 72 124 2980 0.933 20 4-Nitropheno] 2977.000 1600 3330 0 89.4 69 139 3025 1.61 20 Acenaphthene 2864:000 330 3330 0 8&0 59 118 2905 1.43 20 N-Nitrosodi-n-propylamine 2831.667 330 3330 0 85.0 61 125 2901 2.42 20 Pentachlorophenol 3041.333 1600 3330 0 91.3 56 131 3107 213 20 Phenol 2564.000 330 3330 0 77.0 60 113 2657 3.58 20 Pyrene 3215.667 330 3330 0 96.6 51 130 3264 1.48 20 Sun: 1,2-Dichlorobenzene-d4 2383.333 3330 71.6 49 103 0 0 Sum 2,4,6-Tribromophenol 3176.667 3330 95.4 47 129 0 0 Surr.2-Chlorophenol-d4 2587.667 3330 77.7 54 109 0 0 Surr.2-Fluombiphenyl 2732.667 3330 82A 59 108 0 0 Sun: 2-Fluorophenoi 2552.333 3330 76.6 50 111 0 0 Surr. 4-Terphenyl-d14 2997.667 3330 90.0 58 135 0 0 Surr. Nitrobenzene-d5 2658.000 3330 79.8 54 115 0 0 Surr. Phenol-d5 2679.333 3330 80.5 58 112 0 0 Qualifiers: B Analytcdetectedin theassociatedMobod Blank E NO Not Detected at the Reporting Limit R DO Surrogate Diluted Out Idivamd Ter4nolo� 1 Labor:raries 3275 lruLmrihraae. Sigaa1H111, C1907,5 Value above quantitation range H Holding times for preparation or analysis exceeded RPD outside accepted recovery limits S Spike/Surmgate outside of limits due to matrix interference Calculations arebased on raw values 5 TM 562. 939.4045 Far 562-939.4040 M M 6Jfi68 _ M M M M M M M M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: HC_S_ATL Sample ID: MB-57087 SampType: MBLK TestCode: HC_S_ATL Units: mg/Kg Prep Date: 8/5/2009 RunNo: 111474 711ent ID: PBS Batch ID: 57087 TestNo: EPA 8015B(M LUFT Analysis Date: 8/612009 SegNo: 1756826 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual T/R Hydrocarbons: C8-C10 ND 10 T/R Hydrocarbons: CIO-C18 NO 10 T/R Hydrocarbons: C18-C28 ND 10 T/R Hydrocarbons: C28-C36 ND 10 T/R Hydrocarbons: C36-C40 NO 10 T/R Hydrocarbons: C8-C40 Total ND 10 Surr: p-Terphenyl 79A60 80.00 99.3 57 144 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantttation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on mw values �= eId,uneed T"hnalaV• 3275 S'nlnutAtenue, Signal Hill, GI 90755 Tel: 562.989.4045 Far: 562.989.4040 Lnhur�tories 63 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: HC_S_VOAC4C12 ;ample ID: E0908041-CS3 SampType: LCS TestCode: HC 8 VOAC Units: mg1Kg Prep Dale: RunNo: 111447 :lient ID: LCSS Batch ID. E09VS246 TestNo: EPA 8015E Analysis Dale: 8/4/2009 SegNo: 1756412 lnalyte Result PQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: 04-C12 4.210 1.0 5.000 0 84.2 73 120 Sun: Bromoiluorobenzene (FID) 90.520 100.0 90.5 59 145 Sample ID: 106685-002AMS SampType: MS TestCode: HC S VOAC Units: mg1Kg Prep Data. RunNo: 111447 Client ID: B6-2 Batch ID: E09VS246 TestNo: EPA 8015B Analysis Date: 8/412009 SegNo: 1756413 Analyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Rer Val %RPD RPDLimit Dual TIR Hydrocarbons: C4-C12 4.118 1.0 5.000 0 82.4 39 135 Sun: Bromonuorobenzene (FID) 94.864 100.0 94.9 59 145 Sample ID: 106685-002AMSD SampType: MSD TestCode: HC S VOAC Units: mglKg Prep Date: RunNo: 111447 Client ID: B6-2 Batch ID: E09VS246 TestNo: EPA 8015E Analysis Date: $1412009 SegNo: 1756414 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: C4-C12 4.088 1.0 5.000 0 81.8 39 135 4.118 0.731 20 Surr. Bmmonuorobenzene (FID) 92.606 100.0 92.6 59 145 0 0 Sample ID: E090804MB4 SampType: MBLK TestCode: HC S VOAC Units: mg1Kg Prep Date: RunNo: 111447 Client ID: PBS Batch ID: E09VS246 TestNo: EPA 8015E Analysis Date: 8/4/2009 SegNo: 1756415 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TIR Hydrocarbons: C4-C12 NO 1.0 Sum Bromonuorobenzene (FID) 90.669 100.0 90.7 59 145 Qualireers: B Analyte detected in the associated Method -Blank E Value above quantitation range H Holding times rorprepamtionoronalysis exceeded NO Not Detected at the ReponingLimit R RPD outside accepted recovery limits S SpikelSumagate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values IId' eL dTecknoloyr I Labarylndu 32%51ralmdAvcnnr. SignalNill, CA 90755 TO: 562. 939.404 Far: 56d9.9.40J0 64 of 68 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: HC_W_ATL Sample ID: MS-57067 SampType: MBLK TestCode: HC W_ATL Units: mg/L Prep Date: 814/2009 RunNo: 111496 31lent ID. PBW Batch ID: 57067 TestNo: EPA 8015B(M EPA 3510C Analysis Date: 8/6/2009 SegNo: 1757447 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual T/R Hydrocarbons: C8-C10 NO 0.20 T/R Hydrocarbons: C10-C18 NO 0.20 T/R Hydrocarbons: C18-C28 NO 0.20 T/R Hydrocarbons: C28-C36 NO 0.20 T/R Hydrocarbons: C36-C40 NO 0.20 T/R Hydrocarbons: CB-C40 Total NO 0.20 Sun. p-Terphenyl 0.040 0.08000 50.6 35 131 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values td• dT h 7 ♦=nonce rr no ag) Lnbornfarirs 3275 B ulnutArenue, Signal Hill, CA 90755 Tel. 989.4045 Far. 562.989.4040 65 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 TestCode: HC W VOAC4Ci2 Sample ID: 090804LCS2 SampType: LCS TestCode: HC_W VOAC Units: mg/L Prep Date: RunNo: 111429 Client ID: LCSW Batch ID: 109VW0134 TestNo: EPA 8015E Analysis Date: 8/4/2009 SegNo: 1755962 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Qua] T/R Hydrocarbons: C4-C12 0.815 0.20 1.000 0 81.5 69 125 Surr. Bromofluorobenzene (FID) 91.838 100.0 91.8 71 130 Sample ID: 090804MB1 SampType: MBLK TestCode: HC W VOAC Units: mg/L Prep Date: RunNo: 111429 Client ID: PBW Batch ID: 109VW0134 TestNo: EPA 8015E Analysis Date: 8/4/2009 SegNo: 1755963 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit Hight -milt RPD Ref Val %RPD RPDLimit Qua] T/R Hydrocarbons: C4-C12 NO 0.20 Surr. Bromofluorobenzene (FID) 90205 100.0 90.2 71 130 Sample ID: 106685-001AMS SampType: MS TestCode: HC W VOAC Units: mg/L Prep Date: RunNo: 111429 Client ID: B6-GW Batch ID: 109VW0134 TestNo: EPA 8015E Analysis Date: 8/4/2009 SegNo: 1755971 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Dust T/R Hydrocarbons: C4-C12 0.909 0.20 1.000 0 90.9 69 125 Surr. Bromofluorobenzene (FID) 89.181 100.0 89.2 71 130 Sample ID: 10668"01AMSD SampType: MSD TestCode: HC W VOAC Units: mg/L Prep Date: RunNo: 111429 Client ID: B6-GW Batch ID: f09VW0134 TestNo: EPA 8015E Analysis Date: 81412009 SegNo: 1755972 Analyse Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual r/R Hydrocarbons: C4-C12 0.912 0.20 1.000 0 91.2 69 125 0.9090 0.329 20 Surr: Bromofluorobenzene (FID) 89.026 100.0 89.0 71 130 0 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted mcoverylimits S Spike/Sumagate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arc based on raw values 1d.snmiTxrArrolo�r• 1, 4aDararnrirs 327S f!"alnurdrti•nnw Signa1Hi11, G! 90755 Tel. 562. 939.4045 Fax: 562.989.4040 Hof (an M i 'Ad v d '1 MnofoMff La oratonf M M M = DJ=z-ArPM M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 BatchID: 57087 Prep Date: 81512009 RunNo: 111474 Sample ID: LCS-57087 SampType: LCS TestCode: 8015_S_DM Units: mglKg Client ID: LCSS Batch ID: 57087 TestNo: EPA 8015B(M LUFT Analysis Date: 81612009 SegNo: 1756809 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual ORO 1212.490 10 1000 0 121 81 128 Surr: p-Terphenyl 108.220 80.00 135 57 144 Sample ID: 106654-001AMS SampType: MS TestCode: 8015_S_DM Units: mglKg Prep Date: 815/2009 RunNo: 111474 ;Bent ID: 77ZZZZ Batch ID: 57087 TestNo: EPA 8015B(M LUFT Analysis Date: 8/612009 SegNo: 1756823 lnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual DRO Surr: p-Terphenyl 18729.500 500 1000 25280 -858 58 140 J 0 80.00 0 57 144 SOO ;ample ID: 106654-001AMSD SampType: MSD TestCode: 8015_S DM Units: mglKg Prep Date: 815/2009 RunNo: 111474 :Bent ID. ZZ7772 Batch ID: 57087 TestNo. EPA 8015B(M LUFT Analysis Date: 8/612009 SegNo: 1756824 tnalyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qual DRO Surr: p-Terphenyl 11541.500 500 1000 25280 -1370 58 145 18730 47.5 20 SR 0 80.00 0 57 144 0 0 SDO Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Lidrsnced TmImolagr -= butiurururies 3275 Ifalnatibe+nre, Signal Hill, CA907SS TeL 562. 98240d5 Fuv: 562.9fi9.a010 67 of 68 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Advanced Technology Laboratories Date: 12-Aug-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatehID: 57067 Sample ID: LCS-57067 SampType: LCS TeslCode: 8015 W_DM Units: mglL Prep Date: 8/4/2009 RunNo: 111496 Client ID: LCSW Batch ID: 57067 TestNo: EPA 8015B(M EPA 3510C Analysis Date: 816/2009 SegNo: 1757437 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD-Ref Val %RPD RPDLimit Qual DRO 0.917 0.20 1.000 0 91.7 42 118 Surr. p-Terphenyl 0.041 0.08000 50.8 35 131 ;ample ID: MB-57067MS SampType: MS TestCode: 8015 W DM Units: mg/L Prep Date: 814/2009 RunNo: 111496 Bent ID: 777777 Batch ID: 57067 TestNo: EPA 8015B(M EPA 3510C Analysis Date: 816/2009 SegNo: 1757438 inalyte Result PQL SPK value SPK Ref Val %REC LowLirnit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 0.866 0.20 1.000 0 86.6 42 118 Surr, p-Terphenyi 0.042 0.08000 53.1 35 131 ;ample ID: MB-57067MSD SampType: MSD TestCode. 8015 W_DM Units: mg/L Prep Date: 81412009 RunNo: 111496 :lient to: ZZ2227 Batch ID: 57067 TestNo: EPA 8015B(M EPA 3510C Analysis Date: 81612009 SegNo: 1757439 inalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 0.887 0.20 1.000 6 88.7 42 118 0.8663 2.39 20 Surr, p-Terphenyi 0.040 0.08000 50.1 35 131 0 0 Qualifiers: B Anal)le detected in theassaciated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on mwwlues .idrsneedTeednoMi*- Lxfrurarorlel 31:5 H ulnnl Arenne. Signal Hill, GI 90755 Tel• 562. 98RJ0d5 F= 5629S9.4940 M M M r M M M CMN 6PCIUMOMPREMIRI! M M M =Wg—iWf AW FOR LABORATORY USE ONLY: Sampl_eX CCoor�dion Upon Receipt } Method of Transport Advanced Technology P•0•R Client ❑ / 1. CHILLED � • 7, G � Yj3 N ❑ 4. SEALED Y ❑ N - �- Laboratories ATL j� �! 3275 Walnut Avenue b b CAOverN ❑ 2.HEADSPACE(VOA) Y❑ NO 5.#OFSPISMATCHCOC Ye N❑ Signal Hill, CA 90755 (562) 989-4045 • Fax (562) 989-4040 Logged y Date: O FEDEX ❑ Other: 3. CONTAINER INTACT Y fd N NO 6. PRESERVED Y ( N ❑ Address: %SS •tLl I ) ?5'eNlLClient: } e1Z6)L} Attn: .•"vl tiv d:>(n (�✓•'ti J City 1—Yvi•'tL State (:� ZPCode FAX:("i Y=r )ZS C.. r//L( Project r Project#: Sampler. (Pdnled Name) (sg umre) $0E_ j\Div t� *17OL)_ rt�r�s1� iHf-rt: � ed by. vane (, ,rJ Date: �..SrC Time: Isib Rece' P- - Time: lRorru}YIs Rellnqulshed by. N•m•) Date:&J3 Jtl Time: lG?SO Receivedbyts,auw•uda➢t•dN l TRW/O Dale, y Time; / Relinquishedby., l Date (/ Time: y Recelved by: tsmww•.mnwwa ) Dale. ( e y Time: / Y-w I hereby authorize ATL to perform the work - Send epos To: sm To: Special Imtru ions/Comments: Indicated below: Attn: Attn: met+a' tt •-, Projeict Mgr/Submitter. fer VL6g 1;g60 SVOCs �7v 'v�Ltt•k. �1,1t)}+fSI- �' L5`T Co: W S - Co. 4C PPM1 Name Date Address tl 60r"L Address ��}M(yL+ S �� kka4,�kt, s atura city -state-ZIP_ city State -Zip- & Disposal Circle or Add SPECIFY APPROPR(A7E O A / Q C amplelRecords-Archival Unless otherwise requested by client, all samples will be disposed 45 days after Anatysis(es) \ MATRIX Z RTNE ❑ O receipt and records will be disposed 1 year after submittal of final report. Requested ap CT ❑ Storage Fees (applies when storage is requested):1 0 SWRCS ❑ • Sample : $2.00 / sample / mo (after 45 days) c a 1 • Records: $1.00 / ATL workorder / mo (after year) a•» �" TnD m� \m�� i e tea, to Logcode S' Q Containers) s i LAB USE ONLY• «r' m. o o` o �` ri O T Batch #: Sample Description e0 m 0' ¢ O7HER_ ; '0 a°�mQ �� v ��e ono M Lab No. Sample I.D. / Location Date Time g� $ m^ e^ IC yo �� ¢ �� TAT # Type a REMARKS m� 00� 1xi I IlIKIX I I I►- V:, ooy t3E' 2 riy'7 x t LLn iC, x t 1 e' -Z(' 4; 3 �iS Z X X n i; 1 t ao 3b-7 �G-3 tip$ 9.X X �! iklo 33 7-1,iJ 3 IiiSS IA `x 1= V;t ts"r ets t� �,7-2 - ql'3 1�33 X y; i� 1 T S •3 a5 - i q X T, TAT starts 8 a.m. followingday ti y' TAT.. A— - — Overnight <24 hr B Emergency Next workda C_ — Crifcal 2 WDrkda s D= Urgent E_ 3 Workda s = Routine 7 Workda s Preservatives: Preservatives: Nives: S=H:SO. C=4'C samples received after3 p.m. Z=Zn(AC)x O=NaOH T=Na:S:Qa Container T pes: T=Tube V=VOA L=Liter P=Pint J=Jar B=Tedlar t G=Glass P=Plastic M=Metal DISTRIBUTION: White with report, Yellow t0 Maier. Pink to_suommer. CHAIN OF CUSTODY Pg Z of y ��?4ha Advanced Technology t , �'• Laboratories 3275 Walnut Avenue Signal Hill, CA 90755 (562) 989-4045 - Fax (562) 989-4040 FOR LABORATORY USE ONLY: P•o• : Method Of Transport Client o ' ATL CX CA OverN ❑ FEDEX ❑ Other: Sample Condition Upon Recelp[ 7. CHILLED Y��afN ❑ 4. SEALED Y ❑ ❑ 2 HEADSPACE(VOA) Y❑ NQ 5.#OFSPLSMATCHCOC Y ZN ❑ 3. CONTAINER INTACT Y15 N ❑ & PRESERVED Y ❑ N ❑ Logged By. Date: Client (<; t v C��s�l ^ j Attn: fLfE2" 1Ctivrcln Address 1770St Cxwx . >�1 (rru4 > 2 • iK4 J city rrvdTe State C, Zip Code f�, FAX:('�i�f4) Z5i)'1//� Project Napm�e: �jC i� 111 ✓. s., t Project #: 2 r{� 7r7a L Sampler. `, a v- e> e' R IJ' - rvl) E' C •j'(�ry ✓✓ Date:.,-; �> ` Tkne: f-!�Z Received n�aa ) te: TimJ Reg Date:v 3 c1 Timei[t 3 U pecei erg. Da me)G� Relmquishedby:ta,w..e Pd cw l Date • U TimWgCJ Received Dat• I herebyaulhorize ATL to perform the We 'mdicatedbelow. Project Mtg'r/fSubmitter. � + f� cjr4 L Ir�.i{.EUW' 46 �'SS end ReponTo: Art, Sat.nt q5 Bill To: Aan: .3 le-t Special lrsiru ns/Commmits: tc{Z bIQ ; mot. szeo SvG � �% 5 � �27� CM u �`� R Co: 5 Address cl state_zp_ Address C(6` dZ Chy state=ap_ Prim ''�y%ttune ti0d Date Sample/Records-Archival&Disposal Unless otherwise requested by went, all samples will be disposed 45 days after receipt and recordswiil be disposed T year after submittal of final report. StorageFees(applies when storage is requested): •Sample :$200/sample/ me (after 45 days) •Records:St.00/ATLworkordarInto (afterT year) GrdearAdd SPECIFYAPPROpRiATE Avmysistes) y MATRIX Requested ^�� ,., y o� u & • � � Q ti4Q ` \�a o. `Ate¢- `�`�@ za* tit' `pc oe mtiv9" �� ,` D �� =oti F ConWner(s) �4 a�_�&$m�1"ma eory+ �� i� yo Q oQo�ey TAT # Type z O > w w a. QA/QC RTNE ❑ CT ❑ SWRCB ❑ Logcode— 1 I LAB USE ONLY: Batch #: Sample Description OTHER_ M Lab No. Samplel.D•/Location Date Time REMARKS os— LIT D VVZA -Z 3 Ili2c oil 16`3 \a'k x X1 I X- t? 1 r; (91� X X rz 4I :v yflL gsri of nt�-�- �s-� tt5$ AXN K Kr 1 ; trlr 60- 115G x 4K, 1Aov r, ec 8 7> tizu X X r S v:✓ X X - 1 • TAT starts B am. following day if samples received after 3 pm. TAT: A= Ov� nh h' 2 B NBMrworl ad C= 2 Workda s D= 3 Workda s 7Wolrkda s Preservatives: H=Hcl N=HNO, S=H:SO. C=4'C Z=Zn(AC): O=NaOH T=Na.S:O, ContamerT pes: T=Tube V=VOA L=Liter P=Pint J=Jar B=Teclarr G=Glass P=Plastic M=Metal PI _ M, M M M �TRIW1. V�rth rr_YeIIc*Ideq*.o SUVW M r M /t}�} Advanced Technology i, Laboratories 3275 Walnut Avenue Signal Hill, CA 90755 (562) 989-4045 • Fax (562) 989-4040 FOR LABORATORY USE ONLY: _.D.,, ,T _� P,O.a: MethodofTransport ATL CA OverN ❑ FEDF-X ❑ Other: Sample Con d"wn Upon Receipt I. CHILLED Y NO 4.SEALEO Y ❑ N � 2. HEADSPACE(VOA) Y❑ NO S.00FSPLSMATCH000 Y t9 N ❑ 3, CONTAINER INTACT Y N ❑ 6. PRESERVED Y ❑ N ❑ Logged By: Date: Client: L"e'j'\Or �D �S �iin� Attn: Address: 07g\ eWnh TEL:(zi4'( ) 2Sr J4Z) I City -trv;wL State C,4 Zip Code q%i(r{ FAX:(c+HS ) 'ZS&p /l/I-1 Project Name: Pro ect #: Sampler. (Pnr1 Namay (SvMIure) ) rjLG APW o"-T ) �,ALL1i7t^a2 pk �^ ,�(. rD)J 47Y�3r✓/� Relinquis t N•) Date: {S. -�,r Time: 5�U Received Dy .vd _ 17ue cT"`'Or Relinqulshedb . �.. awbn.e Date: $•(�,lD`I Time:),y S'O Received try: tsvPunre¢M PnaedNvrt Dat v d>/ Tim (ar0 Relinquis ed by, tsh..u+•ena P�.mn.ms) Date: Q Time: Received by; (syww.oa.a Anean.ma) Dat i(�N') Time: (Si" I hereby authorize ATL to perform the work indicated below: Project Mgr /Submitter. tMA\,./; �'o'u 6"3.O+A d -- Send Report To: Alm; Bit To: Attn:-/NLtt�i:�I� �1wrL11 Special lnsiru lions/Comments. co: CA S Co: stiwtiZ Address Q6J,1.1- CI stale — Zip— Address �5 city G-)✓OV-' State ZIP— Pmt Name Dale tinature Sample/Records - Archival&Disposal Unless otherwise requested by client, all samples well be disposed 45 days after receipt and records will be disposed 1 year after submittal of final report. Storage Fees (applies when storage is requested): • Sample : $2.00 / sample / mo (after 45 days) • Records: $1.00 / ATL workorder / mo (after 1 year) ClrcleorAdd SPECIFYAPPRDPRIATE Analysis(es) l MATRIX Requested og „ A� o�^ ` ry0 ^@� ' • �2- m �v ; L% �rvQ• op o e'' e°� e°1 3� °P G 0 3� container(s) gm `0 2 m o m ryM1 ` �¢ J2 ti� 00: 00� mn^ g m^�mmmo^ yo �� ¢°mac TAT # Type Z O < > w In w a QA/DC RTNE ❑ CT ❑ SWRCB ❑ Logcode _ I T LAB USE ONLY: Batch #: Sam le Description P P OTHER _ E M Lab No. Sample I.D. Location Date Time REMARKS v 019 �-3 )IS7 6,2,b S 3 12,$ t X X t T; o 131i' S t 3 12Sk X X oZ t2-6v1 3 �335 E 5 L i v DLO o 13 a- Z ovi-3 X 5 ; v 3� �Z 46-3 13)7 x ,_ Ti � 13)6 x 1 r a� �41 —XI I TAT starts S a.m. following day if TAT• A= Ov right 2 B Nextrworkda C= 2 Wo kda 0=11 3 Workda s E= 7Workda s Preservatives: H=HcI N=HNO, S=H:SO. C=4'C samples received after 3 p.m. Container Types: T=Tube V=VOA L=Liter P=Pint J=Jar B=Tedlar i G=Glass P=Plastic M=Metal Z=Zn(AC)z O=NaOH T=Nar&O� DISTRIBUTION: White with report, Yellow to folder. Pink to suomlaer. Page 1 of 1 1 1 Rachelle Arada From: Meredith Church [mchurch@le!ghtongroup.comj 1 Sent: Tuesday, August 04, 2009 11:07 AM To: Rachelle Arada ' Subject: PN Hi Rachelle, 1 We submitted samples for a project yesterday, the PN was listed as 602597-002. The PN should be 602597-003, please list this number on the invoice. Also, we've had problems receiving some of the invoices within 30 days of the work. Could you please check with whoever send the invoices in your office and let them we know that we need the invoices either mailed or smelled to our accounting department within in 30 days of the work. Thanks!! 1 1 1 1 1 11 i i 1 1 1 1 1 Meredith Church, PG Project Geologist LEIGHTON Solutions You Can Build On 17781 Cowan Irvine, CA 92614 (949) 681-4208 (Direct) (949) 293-2519 (Cell) (949) 477-4040 (Office) (949)250-1114 (Fax) 1 8/4/2009 Page 1 of 1 1 Rachelle Arada From: Meredith Church [mchurch@leightongroup.coml ' Sent: Tuesday, August 11, 2009 6:35 PM To: ' Rachelle Arada Subject: additional analysis Hi Rachelle, ' For the Newport Beach Project (submitted on 8/3), we need some additional analysis. In addition, I made a typo on the project number, it should be 602497-003 (not 602597). ' Please Analyze 136-7' for TPH-cc (we don't need TPHg, C10 on up will be fine for all these requests) B7-5' for SVOCs B7-7' for PCBs and TPH-cc B12-2' for PCBs and TPH-cc B12-6' for PCBs and TPH-cc I will probably be out of the office tomorrow, so if you have any questions, please call me on my cell phone. Thanks! Meredith Church, PG Project Geologist LEIGHTON ' Solutions You Can Build Oil 17781 Cowan Irvine, CA 92614 (949) 681-4208 (Direct) ' (949) 293-2519 (Cell) (949) 477-4040 (Office) (949)250-1114 (Fax) C I IJ 8/12/2009 ".4,4 August 18,2009 1 Meredith Church ELAP No.:1838 Leighton Consulting, Inc. NELAP No.: 02107CA 17781 Cowan Street NEVADA.: CA-401 ' Irvine, CA 92614 CSDLAC No.:10196 TEL: (949) 681-4208 rPAX: (949) 757-7230 Workorder No.: 106685 rRE: SCE Newport,602497-003 Attention: Meredith Church Enclosed are the results for sample(s) received,on August 03, 2009 by Advanced Technology Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications. rThis is an addendum report. Please incorporate with documentation previously submitted. Thank you for the opportunity to service the needs of your company. Please feel free to call me at (562)989-4045 if I can be of further assistance to your company. r • Sincerely, ' vv Eddie F. R driguez rLaborato Directox r The cover letter is an integral part of this analytical report. This Laboratory Report cannot be reproduced in part or in ' its entirety without written permission from theclient and Advanced Technology Laboratories. A Advanced 7cchnoatones g mtwies Lubn3275 Walnut Avenue Signal Hill, CA90755 Tel: 562 989-4045 Fax:562 989-4040 1 of 19 1 ANALYTICAL RESULTS Advanced Teclinolo Laboratories gy Print Date: I8-Atlg•09 1 CLIENT: Leighton Consulting, Inc. Client Sample ID: B6-7 Lab Order: 106685 Collection Date: 8/3/2009 9:55:00 AM 1 Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-004A ' Ann lyses Result PQL Qual Units DF Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LOFT EPA 8015B(M) 1 RunID: GC16_090817C QC Batch: 57378 PrepDale: 8/1712009 Analyst: CBR T/R Hydrocarbons: C8-C10 NO 10 mg/Kg 1 8/17/2009 04:00 PM 1 T/R Hydrocarbons: CIO-C18 NO 10 mg/Kg 1 8/1712009 04:00 PM T1R Hydrocarbons: C18-C28 NO 10 mg/Kg 1 8117/2009 04:00 PM TIR Hydrocarbons: C28-C36 ND 10 mg/Kg 1 8/17/2009 04:00 PM TIR Hydrocarbons: C36-C40 ND 10 mg/Kg 1 8/17/2009 04:00 PM 1 T/R Hydrocarbons: C8-C40 Total ND 10 mg/Kg 1 8/17/2009 04:00 PM Burr: p-Terphenyl 118 57.144 %REC 1 8/17/2009 04:00 PM 0 i t 1 i Ll 'i Qualifiers: B Analyte detected in the associated Method Blank E Value above qu rntilalion range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit 1 S Spike/Surrogn(c outside or limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Adranced ncGnolo69 Laboratories 317.5 i4•alnnt Avcluru. Signal Hi11, Cr! 90755 Tel: 562. 939.4045 Far: 562.989.4040 2of19 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 18-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: 137-5 ' Lab Order: 106685 Collection Date: 8/3/2009 10:48:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID_ 106685-007A ' -- Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550B EPA 8270C RunlD: MS6_0908120 QC Batch: 57271 PrepDate: 8/12/2009 Analyst: DMP 1,2,4-Tdchoorobenzene ND 330 jig/Kg 1 1 8/14/2009 06:56 PM 8/14/2009 06:56 PM 1,2-Dichlorobenzene NO 330 pg/Kg 1,3-Dichlorobenzene ND 330 pg/K9 1 8/14/2009 06:56 PM 1,4-Dichlorobenzene ND 330 pg/Kg 1 8/14/2009 06:56 PM 1 2,4,5-Trichlorophenol NO 330 pg/Kg 1 8/14/2009 06:56 PM 2,4,6-Trichlorophenol ND 330 pg/Kg 1 8/1412009 06:56 PM 2,4-Dichlorophenol NO 1600 pg/Kg 1 8/14/2009 06:56 PM 2,4-Dimethylphenol NO 330 pg/Kg 1 8/14/2009 06:56 PM 2,4-Dinilrophenol No 1600 pg/Kg 1 8/14/2009 06:56 PM 2,4-111nitrotoluene ND 330 pg/Kg 1 8/14/2009 06:56 PM 2,6-Dinitrotoluene ND 330 pg/Kg 1 1 8/14/2009 06:56 PM 8114/2009 06:56 PM 2-Chloronaphlhalene ND 330 pg/Kg 2-Chlorophenol ND 330 pg/Kg 1 8/14/2009 06:56 PM 2-Methylnaphlhelene ND 330 pg/Kg 1 8/14/2009 06:56 PM 2-Methylphenol ND 330 pg/Kg 1 8/14/2009 06:56 PM 2-Nitroaniline No 1600 pg/Kg 1 8114/2009 06:56 PM 2-Nilrophenol ND 330 pg/Kg 1 8/14/2009 06:56 PM 3,3'-Dichiorobenzidine ND 660 pg/Kg 1 8/14/2009 06:56 PM 3-Nitroaniline ND 1600 pg/Kg 1 8/14/2009 06:56 PM 4,6-Dinitro-2-melhylphenol ND 1600 pg/Kg 1 8/14/2009 06:56 PM 4-Bromophenyl-phenylelher ND 330 pg/Kg 1 8/14/2009 06:56 PM 4-Chloro-3-methylphenol ND 660 pg/Kg 1 8/14/2009 06:56 PM 4-Chloroaniline ND 660 pg/Kg 1 8/14/2009 06:56 PM 4-Chlorophenyl-phenylether ND 330 pg/Kg 1 8/14/2009 06:56 PM 4-Methylphenol NO 330 pg/Kg 1 8/14/2009 06:56 PM 4-Nitroaniline NO 1600 pglKg 1 8/14/2009 06:56 PM 4-Nitrophenol ND 1600 pg/Kg 1 8/14/2009 06:56 PM Acenaphthene ND 330 pg/Kg 1 1 8/14/2009 06:56 PM 8/14/2009 06:56 PM Acenaphthylene No 330 pg/Kg Anthracene NO 330 pg/Kg 1 8/14/2009 06:56 PM Benzidine(M) ND 1600 pg/Kg 1 8/1412009 06:56 PM ' Benzo(a)anthracene 440 330 pg/Kg 1 8/14/2009 06:56 PM Benzo(a)pyrene NO 330 pg/K9 1 8/14/2009 06:56 PM Benzo(b)8uoranlhene ND 330 pg/Kg 1 8/14/2009 06:56 PM Benzo(g,h,i)perylene ND 330 pg/Kg 1 8/14/2009 06:56 PM Qualifiers: B Analyte detected in the associated Method Blank E H Holding times for preparation or analysis exceeded ND S Spike/Surrogate outside of limits due to matrix interference Value above quantitation range Not Detected at the Reporting Limit Results are wet unless otherwise specified DO Surrogate Diluted Out Advanced!'echnologr AINLaboratories 3275 Walnut Avwsre, Signal Hill. CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040 3of19 Advanced Technology Laboratories Leighton Consulting, Inc. 106685 SCE Newport, 602497-003 106685-007A ANALYTICAL RESULTS Print Date: I8-Au&09 Client Sample ID: B7-5 Collection Date: 8/3/2009 10:48:00 AM Matrix: SOIL Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS EPA 3550E EPA 8270C Rung): MS6 090812D OC Batch: 57271 PrepDate: 8/12/2009 Analyst: DMP Benzo(k)0uoranlhene NO 330 pg/Kg 1 8/1412009 06:56 PM Benzoic acid NO 1600 pg/Kg 1 8/1412009 06:56 PM Benzyi alcohol NO 660 pg/Kg 1 8/1412009 06:56 PM Bis(2-chloroethoxy)melhene NO 330 pg/Kg 1 8/14/2009 06:56 PM Sis(2-chioroethyl)ether NO 330 pg/Kg 1 8114/2009 06:56 PM Bis(2-chlorotsopropyl)ether NO 330 pg/Kg 1 8/14/2009 06:56 PM Bis(2-ethylhexyl)phthalale NO 330 pg/Kg 1 8/14/2009 06:56 PM Butylbenzylphthatate NO 330 pg/Kg 1 8/14/2009 06:56 PM Chrysene 430 330 pg/Kg 1 8114/2009 06:56 PM Di-n-butylphlhelate 'ND 330 pg/Kg 1 8114/2009 06:56 PM Di-n-octylphthalale NO 330 pg/Kg 1 8114/2009 06:56 PM Dibenz(a,h)anthmcene NO 330 pg/Kg 1 8114/2009 06:56 PM Dibenzofuran NO 330 pg1Kg 1 8/14/2009 06:56 PM Dlelhylphthalale NO 330 pg/Kg 1 8/1412009 06:56 PM Dlmethyiphlhalale NO 330 pglKg 1 8/14/2009 06:56 PM Fiucranthene 470 330 pglKg 1 8/14/2009 06:56 PM Fluorene NO 330 pg/Kg 1 8/1412009 06:56 PM Hexachlorobenzene NO 330 pglKg 1 8/14/2009 06:56 PM Hexachlorobutodlene NO 660 pg/Kg 1 8114/2009 06:56 PM Hexachlorocyclopentedlene ND 660 pg/Kg 1 8114/2009 06:56 PM Hexachloroelhane ND 330 plift 1 8114/2009 06:56 PM Indeno(1,2,3-cd)pyrene ND 330 pg/Kg 1 8114/2009 06:56 PM Isophorone NO 330 pg/Kg 1 8/14/2009 06:56 PM N-Nitrosodi-n-propylemine NO 330 pg/Kg 1 8114/2009 06:56 PM N-Nitrosodiphenyiamine NO 330 pg/Kg 1 811412009 06:66 PM Naphthalene NO 330 pg/Kg 1 811412009 06:66 PM Nitrobenzene NO 330 pg/Kg 1 811412009 06:56 PM Pentachlorophenol NO 1600 pg/Kg 1 8/1412009 06:66 PM Phenanthrene 460 330 pglKg 1 8/14/2009 06:56 PM Phenol NO 330 pglKg 1 8/14/2009 06:56 PM Pyrene 760 330 pg/Kg 1 8/14/2009 06:56 PM Surr:1,2-Dlchlorobenzene-d4 64.6 49-103 %REC 1 8/14/2009 06:56 PM Surr:2,4,6-Tribromophenol 61.7 47-129 %REC 1 811412009 06:66 PM Surr:2-Chlorophenot-d4 69.7 54.109 %REC 1 811412009 06:56 PM Surr:2-Fluorobiphenyl 76.2 59.108 %REC 1 8/1412009 06:56 PM - ---- -- ------ - --- -- ---- - - - ---- ---- -- - . Anaiyte— detected— -in-I-heassocioted- Meth-od Blank C Vnluc above quanlitation range Holding limes for preparation or analysts exceeded ND Not Detected atthe Reporting Limit Spike/Surrogatc outside of limits due to matrix interference Results arc wct unless olhcnvise specified Surrogate Diluted Out aAdwinced Tec6nolagv Laboratarlcx 3275 IVUlenl Avenim Signal Hlll. CA 90755 Tel: 56Z 989.4045 Pax: 562.989.4040 1 RESULTS 'ANALYTICAL Advanced Technology Laboratories Print Date: 18-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B7-5 Lab Order: 106685 Collection Date: 8/3/2009 10:48:00 AM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID:- 106685-007A ' — Analyses Result PQL Qual Units DF Date Analyzed SEMIVOLATILE ORGANIC COMPOUNDS BY GCIMS ' EPA 3550B EPA 8270C RunlD: MS6_090812D QC Balch: 57271 PrepDate: 8/1212009 Analyst: DMP ' Burr: 2-Fluorophenol 67.3 50-111 %REC 1 8/14/2009 06:56 PM %REC 1 8/14/2009 06:56 PM Surr:4-Terphenyl-d14 83.6 58-135 Sort: Nitrobenzene-d5 80.1 54-115 %REC 1 8/14/2009 06:56 PM Star: Phenol-d5 71.6 58-112 %REC 1 8/14/2009 06:56 PM I I r 1, B Analyte detected in the associated Method Blank E Value above quantitation range Qualifiers: H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit specified S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise DO Surrogate Diluted Out / I dwinced Technology Laboratories 3275 iValnntAvenue, Sigua[Hi1l, CA 90755 Tel: 562. 989.4045 Pas: Sfi2.989.4040 _ 5of19 i Advanced Technology Laboratories CLICN7': Leighton Consulting, Inc. Lab Order: 106685 Project: SCE Newport, 602497-003 Lab -ID: 106685-COSA Analyses Result HYDROCARBON CHAIN IDENTIFICATION LUFT RunID: GC16_090816A QC Batch: T/R Hydrocarbons: C8-C10 T/R Hydrocarbons: CIO-C18 T/R Hydrocarbons: C18-C28 T/R Hydrocarbohs:-C28-C36 T/R Hydrocarbons: C36-C40 T1R Hydrocarbons: C8-C40 Total Surr: p-Terphenyl PCBS BY GCIECD EPA 3550B RunID: GC4 090814A Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260 Aroclor 1262 Aroclor 1268 Surr: Decachlorobiphenyl Sum Telrachloro-m.xylene ANALYTICAL RESULTS ' Print Date: 18 Avg-09 Client Sample JIM E7.7 ~ Collection Date: 8/3/2009 10:51:00 AM ' Matrix: SOIL PQL Qual Units DF EPA 80158(M) 57376 PrepDate: NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 119 57-144 %REC 1 EPA 8082 QC Batch: 57365 NO NO NO 36 NO NO NO NO NO 82.0 87.8 PrepDate: 16 pg/Kg 1 33 pg/Kg 1 16 pg/Kg 1 16 pg/Kg 1 16 pg/Kg 1 16 pg/Kg 1 16 pglKg 1 16 pg1Kg 1 16 pg1Kg 1 30-124 %REC 1 40.118 %REC 1 Date Analyzed , 8114/2009 Analyst: CBR 8/16/2009 01:59 PM 8/1612009 01:59 PM 8/16/2009 01:59 PM 8/16/2009 01:59 PM 8/16/2009 01:59 PM 8/16/2009 01:59 PM 8116/2009 01:59 PM 8/14/2009 Analyst: BB 8114/2009 07:24 PM 8/14/2009 07:24 PM 8/14/2009 07:24 PM 8/14/2009 07:24 PM 8/14/2009 07:24 PM 8/14/2009 07:24 PM 8114/2009 07:24 PM 8/14/2009 07:24 PM 8/14/2009 07:24 PM 8114/2009 07:24 PM 8/14/2009 07:24 PM Qualifiers: B Analyie detected in the associated Melhod Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogate outside of limits due to matrix interference Results arc wet unless otherwise specified DO Surrogate Diluted Out Adtmnred l'eebnologv Lriboratories 3275 l6'rrintrt Avenue. Signal Kill. CA 90755 Tel: 562. 989.4045 Fax: 561.989.4040 6of19 I I I I 1 ANALYTICAL RESULTS Advanced Technology Laboratories Print Date: 18-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B12-2 Lab Order: 106685 Collection Date: 8/3/2009 1:29:00 PM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-023A Analyses Result PQL Qual Units DP Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 8015B(M) RunID: GC16 090816A T/R Hydrocarbons: C8-C10 T/R Hydrocarbons: CIO-C18 T/R Hydrocarbons: C18-C28 T/R Hydrocarbons: C28-C36 T/R Hydrocarbons: C36-C40 T/R Hydrocarbons: C8-C40 Total Surr: p-Terphenyl PCBS BY GC/ECD QC Batch: 57376 PrepDate: NO 10 mg/Kg 1 ND 10 mg/Kg 1 NO 10 mg/Kg 1 NO 10 mg/Kg 1 ND 10 mg/Kg 1 ND 10 mg/Kg 1 118 57-144 %REC 1 EPA 3550E EPA 8082 RunID: GC4_090814A QC Batch: 57365 PrepDate: Aroclor 1016 ND 16 pg/Kg 1 Aroclor 1221 ND 33 pg/Kg 1 Aroclor 1232 NO 16 pg/Kg 1 Aroclor 1242 28 16 pg/Kg 1 Aroclor 1248 ND 16 pg/Kg 1 Aroclor 1254 NO 16 pg/Kg 1 Aroclor 1260 ND 16 pg/Kg 1 Aroclor 1262 NO 16 pg/Kg 1 Aroclor 126E NO 16 pg/Kg 1 Surr: Decachlorobiphenyl 74.1 30-124 %REC 1 Surr: Tetrachloro-m-xylene 81.8 40-118 %REC 1 I 1- 8114/2009 Analyst: CBR 8/16/2009 04:24 PM 8/1612009 04:24 PM 8/16/2009 04:24 PM 8/16/2009 04:24 PM 8/16/2009 04:24 PM 8/16/2009 04:24 PM 8/16/2009 0424 PM 8/14/2009 Analyst: BB 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM 8/14/2009 07:54 PM Qualifiers: 6 Analyte detected in the associated Method Blank E H Holding times for preparation or analysis exceeded NO Value above quantitauon range Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Il Advanced nchnalogp 3275 Na/nulAvernre, SigrurlHill, CA 90755 7eL 562. 959.9015 Tax: 502.989.4040 Laboratories _ 7of19 ANALYTICAL RESULTS Advanced TechnologyLaboratories Print Date: 18-Ar1g-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B12-6 Lob Order: 106685 Collection Date: 8/3/2009 1:32:00 PM Project: SCE Newport, 602497-003 Matrix: SOIL Lab ID: 106685-024A Analyses Result PQL Qual Units Dr Date Analyzed HYDROCARBON CHAIN IDENTIFICATION LUFT EPA 80158(M) RunlD: GC16 090816A QC Batch: 57376 PrepDate: 8/1412009 Analyst: CBR TIR Hydrocarbons: CB-C10 NO 10 mglKg 1 8116/2009 02:08 PM ' TIR Hydrocarbons: CIO-C18 NO 10 mg/Kg 1 6/1612009 02:08 PM TIR Hydrocarbons: C18-C28 NO 10 mglKg 1 8/1612009 02:08 PM T/R Hydrocarbons: C28-C36 ND 10 mg/Kg 1 8/16/2009 02:08 PM T/R Hydrocarbons: C36-C40 NO 10 mg/Kg 1 8/1612009 02:08 PM ' T/R Hydrocarbons: CB-C40 Total NO 10 mg/Kg 1 8/16/2009 02:08 PM Surr. p-Terphonyl 118 57-144 %REC 1 8/16/2009 02:08 PM PCBS BY GCIECD EPA 35506 EPA 8082 RunID: GC4 090814A QC Batch: 57365 PrepDate: 8114/2009 Analyst: 88 Aroclor 1016 NO 16 pg/Kg 1 8/1412009 08:24 PM , Aroclor 1221 NO 33 pg1Kg 1 8/14/2009 08:24 PM Aroclor 1232 ND 16 pg/Kg 1 8/14/2009 08:24 PM Aroclor 1242 NO 16 pg1Kg 1 8/14/2009 08:24 PM Aroclor1248 ND 16 pg/Kg 1 8114/2009 08:24 PM Aroclor1254 NO 16 pglKg 1 8114/2009 08:24 PM Aroclor1260 NO 16 pg/Kg 1 8/14/2009 08:24 PM Aroclor 1262 NO 16 pg1Kg 1 8/1412009 08:24 PM Aroclor 1268 NO 16 pg/Kg 1 8/1412009 08:24 PM Sum. Decachloroblphenyl 82.1 30.124 %REC 1 8/14/2009 08:24 PM Burr: Tetrachloro-m-xylene 86.0 40-118 %REC 1 8/14/2009 08:24 PM Quallners: B Anulyte detected in the associated Method plank E Value above quantitation range H Holding times ror preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spikc/Surrogute outside of limits due to matrix interference Results arc wct unless otherwise specified DO Surrogate Diluted Out AdwincedTechnoIaSV '_' LuOaralarles 3275 1Vidntit /1venite, Signal Hill, C.1 90755 Tel: 562. 989.4045 Fax: 562.989.4040 8of19 ' Advanced ec noTogy La6orator� M M = = DM8-ARM CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 BatchlD: 57378 Sample ID: LCS-57378 SampType: LCS TestCode: 8015_S_DM Units: mq/Kg Prep Date: 8/17/2009 RunNo: 111861 Client ID: LCSS Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 811712009 SegNo: 1764755 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 1086.170 10 1000 0 109 81 128 Sum: D-Terohenvl 99.740 80.00 125 57 144 Sample ID: 106814-007AMS SampType: MS TestCode: 8015_S_DM Units: mg/Kg Prep Date: 8/17/2009 RunNo. 111861 3lient ID: ZZ7777 Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 8/17/2009 SegNo: 1764756 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 953.800 10 1000 0 Sum: p-Terphenyl 89.180 80.00 Sample ID: 106814-007AMSD SampType: MSD TestCode: 8015 S DM Units: mglKg Client ID: ZZZZZZ Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analyte Result PQL SPK value SPK Ref Val DRO 1044.000 10 1000 0 Sum: p-Terphenyl 96.930 80.00 Sample ID: MB-57378 SampType: MBLK TestCode: 8015 S_DM Units: mg/Kg Client ID: PBS Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analyte Result POL SPK value SPK Ref Val DRO NO 10 ORO NO 10 Sum: p-Terphenyl 88.550 80.00 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values T h l 95.4 58 145 ill 57 144 Prep Date: 8/17/2009 Analysis Date: 8117/2009 %REC Lowl-imit HighLimit RPD Ref Val 104 58 145 953.8 121 57 144 Prep Date: 8117/2009 Analysis Date: 8/17/2009 %REC Lowl-imit HighLimit RPD Ref Val ill 57 144 Adranmd rr naa&, j LuOnn+torirs 3275 WalnutArrune, Signal Hill, Get90755 Tch 56Z. 989.4045 Par: 562.989.4040 �9of19 RunNo: 111861 SegNo: 1764757 %RPD RPDLmut Qual 9.03 20 0 0 RunNo: 111861 SegNo: 1764758 %RPD RPDLimit Qual H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatchlD: 57378 ;ample ID: LCS-57378 SampType: LCS TestCode: 8015 S_DSL Units: mg/Kg Prep Date: 8/17/2009 RunNo: 111861 ;lien[ ID: LCSS Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 8/17/2009 SegNo: 1764727 lnalyte Result POL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 1086.170 10 1000 0 109 81 128 Surr. p-Terphenyl 99.740 80.00 125 57 144 ;ample ID: 106814-007AMS SampType: MS TestCode: 8015 S DSL Units: mg/Kg Prep Date: 8/17/2009 RunNo: 111861 ;lient ID. 722277 Batch ID: $7378 TestNo: EPA-8015B(M LUFT Anaysis Date: 8/17/2009 SegNo: 1764728 malyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO 953.800 10 1000 0 95A 58 145 Surr. p-Terphenyl 89.180 80.00 111 57 144 RunNo: 111861 ;ample ID: 106814-007AMSD SampType: MSD TestCode: 8015 S_DSL Units: mgiKg Prep Date: 8/17/2009 Ment ID: 777777 Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 8/17/2009 SegNo: 1764729 malyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] DRO 1044.000 10 1000 0 104 58 145 953.8 9.113 2U Sum p-Terphenyl 96.930 80.00 121 57 144 0 0 Sample ID: MB-57378 SampType: MBLK TestCode: 8015 S_DSL Units: mg/Kg Prep Date: 8/17/2009 RunNo: 111861 Client ID: PBS Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 8/17/2009 SegNo: 1764730 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual DRO ND 10 Sum p-Terphenyl 88.550 80.00 111 57 144 Sample ID: MB-57378 SampType: MBLK TestCode: HC_S ATL Units: mg/Kg Prep Date: 8/17/2009 RunNo: 111861 Client ID: PBS Batch ID: 57378 TestNo: EPA 8015B(M LUFT Analysis Date: 8/17/2009 SegNo: 1764842 Analyte Result POL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual T/R Hydrocarbons: CB -CIO NO 10 Qualifiers: B Analyte detected in the associated MethodBlank E Value above quantitation range H Holding times for preparationor analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Sumogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations atebased on raw values d d r nnred TerAnofo;�•r 7,9AnryfUr/M 3=751f uAnn.(rrnnr, Signa/Hill, 01 90%55 TcL• 562 9$9.404S Far. $62.989.{0{0 CLIENT: Leighton Consulting, Inc- ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatchID: 57378 Sample ID: MB-57378 Client ID: PBS Analyte SampType: MBLK Batch ID: 57378 Result TestCode: HC_S_ATL Units: mg/Kg TestNo: EPA 8015B(M LUFT PQL SPK value SPK Ref Val %uREC Prep Date: 8117/2009 RunNo: 111861 Analysis Date: 8/1712009 SegNo: 1764842 Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual T/R Hydrocarbons: C10-C18 ND 10 T/R Hydrocarbons: C18-C28 NO 10 T/R Hydrocarbons: C28-C36 NO 10 T/R Hydrocarbons: C36-C40 NO 10 T/R Hydrocarbons: C8-C40 Total ND 10 Surr: p-Terphenyl 88.550 80.00 1'll 57 144 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantttation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values .Id,nncedTmhnolagr �= 327513 uubndvetute. Signal Hill, CA 90755 Tel.. 562. 989.404S Fax.- 562..989.4040 I,uhurutories 11 Of 19 Advanced Technology Laboratories Date: 13-Aug-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT NVork Order: 106685 Project: SCE Newport,602497-003 BatchID: 57271 Sample ID: MB-57271 SampType: MBLK TestCode: 8270_S_FUL Units: pg/Kg Prep Date: 8/12/2009 RunNo: 111709 Client ID: PBS Batch ID: 57271 TestNo: EPA 8270C EPA 355OB Analysis Date: 811212009 SegNo: 1761607 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLtmit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene NO 330 1,2-Dichlorobenzene NO 330 1,2-Diphenylhydra7ine NO 330 1,3-Dichlorobenzene NO 330 1,4-Dichlorobenzene NO 330 1,4-Dioxane NO 330 2,4,5-Trichlorophenol NO 330 2,4,6-Trichlorophenol NO 330 2,4-Dichlorophenol NO 1600 2,4-Dimethylphenol NO 330 2,4.Dinitrophenol NO 1600 2,4-Dinitrotoluene ND 330 2,6-Dinitrotoluene NO 330 2-Chloronaphthatene NO 330 2-Chlorophenol NO 330 2-Methyinaphthalene NO 330 2-Methylphenol _ ND 330 2-Nitroanitine NO 1600 2-Nitrophenol NO 330 3,3'-Dichtorobenzidine NO 660 3-Nitroaniline NO 1600 4,6-Dinitro-2-methylphenol NO 1600 4-Bromophenyl-phenylether NO 330 4-Chloro-3-methylphenol NO 660 4-Chloroaniline NO 660 4-Chlorophenyl-phenylether NO 330 3/4-Methylphenol NO 330 4-Methylphenol NO 330 Qualifiers: B Analyte detected m the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arebased on_mw values .1dewneed Tmhrmtagr Labnntnrirs `� 32:'S 11'uinut.bevue, SignulKilf. CA 90755 Tel. 56Z 999.4045 Far- $62.9,99.4040 �� = M M = M M 1"19M M M M M M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatchID: 57271 Sample ID: MB-57271 SampType: MBLK Client ID: PBS Batch ID: 57271 TestCode: 8270_S_FUL Units: pg1Kg TestNo: EPA 8270C EPA 3550B Analyte Result PQL 4-Nilroaniline ND 1600 4-Nitrophenol NO 1600 Acenaphthene ND 330 Acenaphthylene ND 330 Aniline ND 330 Anthracene ND 330 Senzidine (M) ND 1600 Benzo(a)anthmcene NO 330 Benzo(a)pyrene ND 330 Benzo(b)fluoranthene ND 330 Senzo(g,h,i)perylene NO 330 Benzo(k)fluoranthene NO 330 Benzoic acid ND 1600 Benzyl alcohol ND 660 Bis(2-chloroelhoxy)methane NO 330 Bis(2-chloroethyl)elher ND 330 Bis(2-chloroisopropyl)ether NO 330 Bis(2-ethylhexyl)phthelate ND 330 Butylbenzylphthalate NO 330 Carbazole NO 330 Chrysene NO 330 Di-n-butylphthalate ND 330 Di-n-octylphthalate NO 330 Dibenz(a,h)anthracene NO 330 Dibenzofuran ND 330 Diethylphthalate NO 330 Dimethylphthalate ND 330 Fluoranthene ND 330 Fluorene NO 330 Hexachlorobenzene ND 330 SPK value SPK Ref Val Prep Date: 8/12/2009 RunNo: 111709 Analysis Date: 8/1212009 SegNo: 1761607 %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimrt Qua[ Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO surrogate Diluted Out Calculations are based on raw values 11214 Advanced Technology 4abnraforier 3175 lYalnntArcn+re. Signal Hi(f, GI 90755 Tel: 561. 989.4045 !•'a<: 561.989.4040 13 of 19 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 BatchID: 57271 Sample ID: ME-57271 SampType: MBLK TeslCode: 8270_S FUL Units: pg/Kg Prep Date: 8/1212009 RunNo: 111709 Client ID: PBS Balch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 8112/2009 SegNo: 1761607 Analyte Result POL SPK value SPK Ref Val %aREC LowUmit Hight-imtt RPD Ref Val %RPD RPDLimit Oual Hexachlorobutadiene NO 660 Hexachlorocyclopentadiene NO 660 Hexachloroethane NO 330 Indeno(1,2,3•cd)pyrene NO 330 Isophorone NO 330 N-Nitrosodi-n-propylamine NO 330 N-Nilrosodimethylamine NO 330 N-Nitrosodiphenylamine NO 330 Naphthalene ND 330 Nitrobenzene NO 330 Pentachlorophenol NO 1600 Phenanthrene NO 330 Phenol NO 330 Pyrene NO 330 Pyridine NO 1600 Surr. 1,2-Dichlorobenzene-d4 2505.000 Surr: 2,4,6-Tribromophenol 2620.000 Surr. 2-Chlorophenol-d4 2590.333 Surr. 2-Fluorobiphenyl 2573.000 Surr. 2-Fluorophenol 2630.333 Surr. 4-Terphenyl-d14 3021.000 Sort-. Nitrobenzene-d5 3126.333 Sur: Phenol-d5 2790.333 3330 75.2 49 103 3330 78.7 47 129 3330 77.8 54 109 3330 7T.3 59 108 3330 79.0 50 111 3330 90.7 58 135 3330 93.9 64 115 3330 83.8 58 112 Sample ID: LCS-57271 SampType: LCS TeslCode: 8270_S_FUL Units: pg/Kg Prep Date: 8/12/2009 RunNo: 111709 Client ID: LCSS Balch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/1212009 SegNo: 1761608 Analyte Result POL SPK value SPK Ref Val %REC LowUmit Hight-imit RPO Ref Val %RPD RPDLimit Oual 1,2,4-Trichlorobenzene 2911.000 330 3330 0 87.4 61 107 1,4-Dichlorobenzene 2555.667 330 3330 0 76.7 56 100 Qualifiers: B Analytedetected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values 1dranredT"Ithalogr I f>lwmrodes 3?'S p'aLurl Avettne, SignalHil, C.I 90755 Tel.561.9,99.40145 Fae:561.989.41140 _ 1"19 _ M M M M M M M M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 BatchID: 57271 Sample ID: LCS-57271 SampType: LCS TestCode: 8270_S_FUL Units: pg/Kg Prep Date: 811212009 RunNo: 111709 Client ID: LCSS Batch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/1212009 SegNo: 1761608 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual 2,4-Dinitrotoluene 3459.667 330 3330 0 104 72 130 2-Chlorophenol 2594.000 330 3330 0 77.9 64 105 4-Chloro-3-methylphenol 2956.000 660 3330 0 88.8 74 125 4-Nitrophenol 3111.667 1600 3330 0 93.4 77 137 Acenaphthene 2744.000 330 3330 0 82.4 63 117 N-Nitrosodi-n-propylamine 3141.333 330 3330 0 94.3 71 121 Pentachlorophenol 3327.000 1600 3330 0 99.9 69 125 Phenol 2823.667 330 3330 0 84.8 67 ill Pyrene 2669.667 330 3330 0 80.2 60 122 Sum: 1,2-Dichlorobenzene-d4 2587.000 3330 77.7 49 103 Sum: 2,4,6-Tribromophenol 3180.667 3330 95.5 47 129 Sum: 2-Chlorophenol-d4 2738333 3330 82.2 54 109 Sum., 2-Fluorobiphenyl 2723.667 3330 81.8 59 108 Sum: 2-Fluorophenol 2706.667 3330 81.3 50 ill Sum: 4-Terphenyl-dl4 3399.333 3330 102 58 135 Sum. Nitrobenzene-d5 3286.667 3330 98.7 54 115 Sum: Phenol-d5 2948.667 3330 88.5 58 112 Sample ID: 106760-014DMS SampType: MS TestCode. 8270_S_FUL Units: pg/Kg Prep Date: 811212009 RunNo: 111709 Client ID: ZZZZZZ Batch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 811212009 SegNo: 1761609 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imrt RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlombenzene 2855 000 330 3330 0 85.7 60 105 1,4-Dichlorobenzene 2480.667 330 3330 0 74.5 50 99 2,4-Dinitrotoluene 3488.667 330 3330 0 105 70 130 2-Chlorophenol 2629.000 330 3330 0 78.9 58 107 4-Chloro-3-methylphenol 2984.667 660 3330 0 89.6 72 124 4-Nitrophenol 3118.667 1600 3330 0 93.7 69 139 Acenaphthene 2774.667 330 3330 0 83.3 59 118 N-Nttrosodi-n-propylamine 3134.000 330 3330 0 94.1 61 125 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values /, AdwTinred hnolagr 7- 3275 IiulurrrArenue, Signal Hill, CA 90755 Tel.562.989.4045 Pae:561.989.4040 15 of 19 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference CLIENT: Leighton Consulting, Inc, ANALYTICAL QC SUMMARY REPORT Nark Order: 106685 Project: SCE Newport; 602497-003 BatchID: 57271 ample ID: 106760-014DMS SampType: MS TestCode: 8270 S_FUL Units: pg/Kg Prep Date: 8/12/2009 RunNo: 111709 Sent ID: 7222'22 Batch ID: 57271 TestNo: EPA 8270C EPA 3550B Analysis Date: 8/12/2009 SegNo: 1761609 ,nalvte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highlimit RPD Ref Val %RPD RPDLimit Qua[ remauravropnenu, Phenol Pyfene Surr. 1,2-Dichlorobenzene-d4 Sun: 2,4,6-Tribromophenol Sum 2-Chlorophenol-d4 Surr. 2-Fluorobiphenyl Surr. 2-Fiuorophenol Sum. 4-Terphenyl-d14 Surr. Nitrobenzene-d5 ;ample ID: 106760-014DMSD SampType: MSD TeslCode: 8270 S FUL Units: pg/Kg Prep Date: 8/12/2009 RunNo: 111709 Xent ID: 277= Batch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/12/2009 SegNo: 1761610 malvte Result PQL SPK value SPK RelVal %REC Lowl-imit Hight -lint RPD Ref Val %RPD RPDLimit Qua[ I,L,Y-1114IaYrWCI1GG11G 1,4-Dichlorobenzene 2,4-Dinitrotoluene 2-Chlorophenol 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthene N-Nitrosodi-n-propylamine Pentachlorophenot Phenol Pyrene Surr. 1,2-Dichlorobenzene-d4 Surr. 2,4,6 Tribromophenol C,Im 9-f:hlnrnnhann4tld Qualifiers: B Analyte detected in the associated MethodBlank E Value above quantitation range H Holding times for preparation oranalysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values rld,sn I d WrAnor�r Laboforla 3275 Ii uGurf.lrcnn , Signal Hill, Gf 90735 Tel: 56?. 939.JOJ5 Far i629R9.JOJ0 16 of 19 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatchID: 57271 iample ID: 106760-014DMSD SampType: MSD TestCode: 8270_S_FUL Units: pglKg Prep Date: 811212009 RunNo: 111709 ,lient ID: ZZn» Batch ID: 57271 TestNo: EPA 8270C EPA 3550E Analysis Date: 8/1212009 SegNo: 1761610 lnalyte Result PQL SPK value SPK Ref VaI %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Surr: 2-Fluorobiphenyl 2665.000 3330 80.0 59 108 u u Surr: 2-Fluorophenol 2737.667 3330 82.2 50 ill 0 0 Surr: 4-Terphenyl-dl4 3319.333 3330 99.7 58 135 0 0 Surr: Nitrobenzene-d5 3226.667 3330 96.9 54 115 0 0 Surr: Phenol-d5 2930.333 3330 88.0 58 112 0 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values ldr-2 dTerhnolo� nce `"I 3275 Ii'uhnrt Arenne, Signal Hill, CA 90755 Tel. 562. 989.4045 Far: 562.9�89.4040 ♦_ luhurrlorrrs 17 of 19 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Advanced Technology Laboratories Date: 18-A:rg-09 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatchID: 57365 Sample ID: MB-57365 SampType: MBLK TestCode: 8082 S Units: pg/Kg Prep Date: 8/14/2009 RunNo: 111832 Client ID: PBS Batch ID: 57365 TeslNo: EPA 8082 EPA 3550E Analysis Dale: 8/14/2009 SegNo: 1764109 Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Val %RPD RPDLimit Oual Aroclor 1016 ND 16 Aroclor 1221 NO 33 Aroclor 1232 NO 16 Aroclor 1242 NO 16 Aroclor 1248 ND 16 Aroclor 1254 ND 16 Aroclor 1260 NO 16 Aroclor 1262 ND 16 Aroclor 1268 ND 16 Surr: Decachlorobiphenyl 14.643 16.67 87.8 30 124 Surr Tetrachloto-m-xylene 17207 16.67 103 40 118 iample ID: LCS-57365 SampType: LCS TestCode: 8082_S Units: pglKg Prep Date: 8/1412009 RunNo: 111832 'lient ID: LCSS Batch ID: 57365 TeslNo: EPA.8082 EPA 3550E Analysis Dale: 8/14/2009 SegNo: 1764110 knalyte Result POL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor-1016 124.175 16 166.7 0 74.5 56 113 Aroclor 1260 133.330 16 166.7 0 80.0 58 111 Surr. Decachlorobiphenyl 14.003 16.67 84.0 30 124 Sum.. Tetrachloro-m-xylene 15.948 16.67 95.7 40 118 Sample ID: 106685-008AMS SampType: MS TestCode: 8082 S Units: pglKg Prep Date: 811412009 RunNo: 111832 Client ID: B7-7 Batch ID: 57365 TeslNo: EPA 8082 EPA 3550E Analysis Date: 811412009 SegNo: 1764111 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 163.763 16 166.7 0 98.3 Aroclor 1260 164.930 16 166.7 0 99.0 Surr. Decachlorobiphenyl 15.707 16.67 94.2 Qualifiers: 8 Analyte detected in the associated Method Blank E Value,above quantitation range ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO Surrogate Diluted Out Calculations are based on raw values Idmncrd7'mh"fgAr Lu6ursroner 3175 Mdnw Avcuxe, SigunfHill 01 907S5 Tel: S62 089.4045 Fac S62.989.4940 _�� 1• = M M M = M 1W 19M 51 111 39 123 30 124 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside oflimits due to matrix interference M M M M M M M M CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Nexvport, 602497-003 BatchID: 57365 Sample ID: 106685-008AMS SampType: MS TeslCode: 8982 S Units: pglKg Prep Date: 8/1412009 RunNo: 111832 ,lient ID: B7-7 Batch ID: 57365 TestNo: EPA 8082 EPA 3550E Analysis Date: 8/14/2009 SegNo: 1764111 4nalyte Result PQL SPK value SPK Ref Val %REC LowUmit Highl-imit RPD Ref Val %RPD RPDLimit Qual Surr: Tetrachloro-m-xvlene 16.853 16.67 101 4a 116 iample ID: 106685-008AMSD SampType: MSD TeslCode: 8082 S Units: pg/Kg Prep Date: 8/14/2009 RunNo: 111832 ,Bent ID: 87-7 Batch ID: 57365 TestNo: EPA 8082 EPA 3550E Analysis Date: 8/14/2009 SegNo: 1764112 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 165.588 16 166.7 0 99.4 51 ill 163.8 1.11 2u Aroclor 1260 165.392 16 166.7 0 99.2 39 123 164.9 0.280 20 Sur. Decachlorobiphenyl 15.798 16.67 94.8 30 124 0 0 Surf: Tetrachloro-m-xylene 17.182 16.67 103 40 118 0 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits DO surrogate Diluted Out Calculations are based on raw values d dT h / t er . nonce no to 4ahorarories 3275IAalnnr Avenue, SignalHill,CA 90755 Tel.. 562. 989.4045 Far: 562.989.4040 PW 19 Of 19 H Holding times for preparation or analysis exceeded S Spike/Surrogate outside of limits due to matrix interference Page 1 of 1 ' Rachelle Arada From: Meredith Church [mchurch@leightongroup.com) ' Sent: Tuesday, August 11, 2009 6:35 PM To: Rachelle Arada ' Subject: additional -analysis Hi Rachelle, For the Newport Beach Project (submitted on 8/3), we need some additional analysis. In addition, I made a typo on the project number, it should be 602497-003 (not 602597). ' Please Analyze B6-7' for TPH-cc (we don't need TPHg, C10 on up will be fine for all these requests) B7-5' for SVOCs B7-7' for PCBs and TPH-cc ' 13124for PCBs and TPH-cc 13124for PCBs and TPH-cc I will probably be out of the office tomorrow, so if you have any questions, please call me on my cell phone. ' Thanksl 'Meredith Church, PG Project Geologist LEIGHTON ' Solutions You Can Build On 17781 Cowan Irvine, CA 92614 (949) 681-4208 (Direct) ' (949) 293-2519 (Cell) (949) 4774040 (Office) (949) 250-1114 (Fax) 1 1 8/12/2009 '{i ACCCA August 26, 2009 "< Meredith Church ELAP No.:1838 ' Leighton Consulting, Inc. NELAP No.:02107CA 17781 Cowan Street NEVADA.: CA-401 Irvine, CA 92614 CSDLAC No.:10196 TEL: (949) 681-4208 ' FAX: (949) 757-7230 WorkorderNo.: 106685 RE: SCE Newport, 602497-003 ' Attention: Meredith Church II II Enclosed are the results for sample(s) received on August 03, 2009 by Advanced Technology Laboratories . The sample(s)� are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications. This is an addendum report. Please incorporate with documentation previously submitted. Thank you for the opportunity to service the needs of your company. Please feel free to call me at (562)989-4045 if I can be of further assistance to your company. Sincerely, Eddie F. Laboratory The cover letter is an integral part of this analytical report This Laboratory Report cannot be reproduced in part or in its entirety without written pennission from the,client and Advanced Technoloav Laboratories. Advanced Technology 3275 lYalnul Avenue Signal Hill, CA 90755 Tel: 562 989-4045 Fax: 562 939-4040 05\ 0 Laboratories 1 of 6 Advanced TechnoloEv Laboratories Date: 26-Aug-0 CLIENT: Leighton Consulting, Inc. Project: SCE Newport, 602497-003 CASE NARRATIVE Lab Order: 106685 Analytical Comments for EPA 8082 Samples 106685-026A and 106685-027A were analyzed beyond bold time. 14Adwwnced Technolop , Lnbornlorles 327.1WainuMvenue, SignalHlll,CA 90755 Tel: 562.989.4045 2of6 Page 1 of ' Fax: 562.989,4040 ' RESULTS 'ANALYTICAL Advanced Technology Laboratories — _ Print Date: 26-Aug-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B13-2 ' Lab Order: 106685 Collection Date: 8/3/2009 1:12:00 PM Project: SCE Newport,602497-003 Matrix: SOIL Lab ID: 106685-026A Analyses Result PQL Qual Units Dr Date Analyzed PCBS BY GCIECD ' EPA 3550B EPA 8082 RunlD: GCS 090821A QC Batch: 57576 PrepDate: 8/2112009 Analyst: BB Aroclor 1016 ND 16 H pg/Kg 1 8/24/2009 04:44 AM Aroclor 1221 ND 33 H pg/Kg 1 8/24/2009 04:44 AM Aroclor 1232 ND 16 H pg/Kg 1 8/24/2009 04:44 AM Aroclor 1242 ND 16 H pg/Kg 1 8/24/2009 04:44 AM ' Aroclor 1248 NO 16 H pg/Kg 1 8/24/2009 04:44 AM Aroclor 1254 ND 16 H pg/Kg 1 8/2412009 04:44 AM Aroclor 1260 ND 16 H pg/Kg 1 812412009 04:44 AM ' Aroclor 1262 ND 16 H H pg/Kg 1 1 8/24/2009 04:44 AM 8/24/2009 04:44 AM Aroclor 1268 ND 16 pg/Kg Surr: Decachlorobiphenyl 93.8 30.124 H %REC 1 812412009 04:44 AM Surr: Tetrachloro-m-xylene 98.3 40-118 H %REC 1 8124/2009 04:44 AM I Qualifiers: B Analyte detected in the associated Method Blank E Value above quanutation range H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limn S Spike/Surrogate outside of limits due to matrix interference Results arc wct unless otherwise specified DO Surrogate Diluted Out ' /1 Advanced TeeM101091' 3275 Widntd Aveirne, Signalllill, CA 907S5 Tel: 562. 989.4045 Tax: 562.989.4040 O Laboratories 3of6 i' Advanced TechnologyLaboratories ANALYTICAL RESULTS Print Datc: 26-A:rg-09 CLIENT: Leighton Consulting, Inc. Client Sample ID: B13-5 Lab Order: 106685 Collection Date: 8/3/2009 1:16:00 PM Project: SCE Newport,602497-003 Matrix: SOIL Lab ID: 106685.027A Analyses Result PQL Qual Units Dr Date Analyzed PCBS BY GC/ECD EPA 3550B EPA 8082 Run1D: GC5_090821A QC Batch: 57576 PrepDate: 80/2009 Analyst: BB Aroclor 1016 NO 16 H pglKg 1 8/24/2009 05:14 AM Aroclor1221 NO 33 H pg/Kg 1 8/2412009 05:14 AM Aroclor1232 NO 16 H pglKg 1 8/2412009 05:14 AM Aroclor 1242 NO 16 H pg/Kg 1 8/2412009 05:14 AM Aroclor 1248 NO 16 H pg/Kg 1 812412009 05:14 AM Aroclor 1254 NO 16 H pg/Kg 1 8/24/2009 05:14 AM Aroclor 1260 NO 16 H pglKg 1 8124/2009 05:14 AM Aroclor 1262 NO 16 H pg1Kg 1 8/2412009 05:14 AM Aroclor 1268 NO 16 H pg/Kg 1 8/24/2009 05:14 AM Sum Decaehloroblphenyl 93.0 30.124 H %REC 1 8/2412009 05:14 AM Surr. Tetrachloro-m-xylene 93.1 40.118 H %REC 1 8/2412009 08:14 AM Quallacrs: B Analyse delcctdd in the associated Method Blank B Value above quantitation range H Holding limes for preparation or analysis exceeded NO Not Detected at the Reporting Limit S Spike/Surrogale outside or limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out Adranced TecGnologi, Laboratories -12%SlVrr/urrlAvenuc, Signal Hill, CA 9D75Tr: 5 Tel. a562.939.4040 4of6 1 La M M = M M w M =Da4WAzffl0 Advanced ec nology oratories CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport, 602497-003 BatehID: 57576 Sample ID: MB-57576 SampType: MBLK TestCode: 8082 S Units: pg/Kg Prep Date: 8121/2009 RunNo: 112127 Client ID: PBS Batch ID: 57576 TestNo: EPA 8082 EPA 3550E Analysis Date: 812312009 SegNo: 1769952 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmn HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 NO 16 Aroclor 1221 NO 33 Aroclor 1232 NO 16 Aroclor 1242 ND 16 Aroclor 1248 ND 16 Aroclor 1254 NO 16 Aroclor 1260 NO 16 Aroclor 1262 NO 16 Aroclor 1268 NO 16 Sum. Decachlorotaphenyl 14.372 16.67 86.2 30 124 Sum: Tetrachloro-m-xylene 16.308 16.67 97.8 40 118 iample ID: LCS-57576 SampType: LCS TestCode: 8082_S Units: jig/Kg Prep Date: 8121/2009 RunNo: 112127 :lient ID: LCSS Batch ID: 57576 TestNo: EPA 8082 EPA 3550E Analysis Date: 812312009 SegNo: 1769953 lnalyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Ref Val %RPD RPDLimit Qual Aroclor 1016 141.699 16 166.7 0 85.0 55 113 Aroclor 1260 155.838 16 166.7 0 93.5 58 ill Sum: Decachlorobiphenyl 13.808 16.67 82.8 30 124 Sum. Tetmchloro-m-xylene 15.311 1667 91.8 40 118 iample ID: 107030-001AMS SampType: MS TestCode: 8082_S Units: pglKg Prep Date: 8121/2009 RunNo: 112127 :lient ID: 777777 Batch ID: 57576 TestNo: EPA 8082 EPA 3550B Analysis Date: 8/23/2009 SegNo: 1769954 lnalyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Ref Val %RPD RPDLimd Qual Aroclor1016 132.432 Aroclor 1260 149.482 Sum: Decachlorobiphenyl 14.623 16 16 1667 0 79.5 166.7 0 89.7 16.67 87.7 51 ill 39 123 30 124 Qualifiers: B Analylc detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on mw values Adraned Tmhnologr 3275 11'ahud Aveune, Signal Hill, Gl 90755 Tel. 562. 989.4045 lax: 562.989.4040 �= 4obordlarles 5of6 CLIENT: Leighton Consulting, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 106685 Project: SCE Newport,602497-003 DatchID: 57576 Sample ID: 107030-OOIAMS SampType: MS TestCode: 8082 S Units: pglKg Prep Date: 8/21/2009 RunNo: 112127 Client ID: 22Z272 Batch ID: 57576 TesWo: EPA 8082 EPA 3550E Analysis Date: 8123/2009 SegNo: 1769954 Analyte Result PQL SPKvalue SPK Ref Val %aREC LowLimit Hlght-imit RPD Ref Val %RPD RPDLimit Qual Surr. Tetrachloro-m-xylene 15.511 16.67 93.0 40 118 iample ID: 107030-001AMSD SampType: MSD TestCode: 8082 S Units: pglKg Prep Date: 8/21/2009 RunNo: 112127 :IientlD: 777222 Batch ID: 57576 TesWo: EPA 8082 EPA 35506 Analysis Date: 8123/2009 SegNo: 7769955 analyte Result PQL SPK value SPK Ref Val %<REC LowUmit HighUmit RPD Ref Val %oRPD RPDUmit Qual Arodor 1016 133.725 16 166.7 0 80.2 51 ill 132.4 0.972 20 Arodor 1260 150.607 16 166.7 0 90.4 39 123 149.5 0.750 20 Sum Decachlorobiphenyl 14.066 16.67 84.4 30 124 0 0 Sum Tetrachloro-m-xylene 15.550 16.67 93.3 40 118 0 0 Qualifiersr B Analytc detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded NO Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations arc based on raw values Adiaaced rMh"loAr /yAuralorier 32'S n'aLmt frenim SigualJiill, C1 907S5 Tel.• 562. 989.4045 Far: 562.9S9.4040 M� M! � a' M W M M� M M M i M Page 1 of 2 ' Rachelle Arada From: Meredith Church [mchurch@leightongroup.coml ' Sent: Wednesday, August 19, 2009 3:28 PM To: Rachelle Arada ' Subject: RE: Addendum report for SCE Newport, 602497-003 (ATL# 106685add) 1 apologize, I meant 1313-2' and 1313-5'. Thanks. Yes, they are past the 14 day hold time, but please go ahead an ' analyze. Meredith Church, PG Project Geologist LEIGHTON ' Solutions You Can Build On 17781 Cowan Irvine, CA 92614 ' (949) 681-4208 (Direct) (949) 293-2519 (Cell) (949) 477-4040 (Office) (949) 250-1114 (Fax) ' From: Rachelle Arada [malito:Rachelle@atlgiobal.com] Sent: Wednesday, August 19, 2009 8:14 AM To: Meredith Church Subject: RE: Addendum report for SCE Newport, 602497-003 (ATL# 106685add) Hi Meredith, ' I got your request below. I didn't find sample B34in our system, please check. Also, sample B13-5' is beyond hold time for PCB analysis. Do you still want to proceed? Thanks, Rachelle ' - - Original Message----- From: Meredith Church [maiito:mchurch@leightongroup.com] Sent: Tuesday, August 18, 2009 6:39 PM ' To: Rachelle Arada Subject: RE: Addendum report for SCE Newport„ 602497-003 (ATL# 106685add) Hi Rachelle, Can you please run B3-2' and B13-5' for PCBs. Thank you! Meredith Church, PG Project Geologist LEIGHTON Solutions You Can Build On 17781 Cowan ' 8/19/2009 Page 2 of 2 Irvine, CA 92614 (949) 681-4208 (Direct) (949) 293-2519 (Cell) (949) 4774040 (Office) (949)250-1114 (Fax) From: Rachelle Arada [mailto:Rachelle@atiglobal.com] Sent: Tuesday, August 18, 2009 11:31 AM To: Meredith Church Subject: Addendum report for SCE Newport, 602497-003 (ATL# 106685add) H1 Meredith, Enclosed are the results for the above project. Thanks, Rachelle Arada Project Coordinator o, AdvancedTechnology Laboratories new.odyLoyol mtn Fox; 562) 989.404czL237 0 Advanced Technology Laboratories Is a full -service environmental lab providing organic and Inorganic analyses of soil, water, Wastewater; storm water and hazardous waste samples. ATL is accredited by the State of California, NELAP and Stale of Nevada and holds various SSE, DBE and MBEcenlacales and a USDA soil permit. ATL lakes pride in providing our customers With quick turnaround time, excellent customer service and defensible data while offering very competitive ralos. Advancod Technology Labs -Your Parfnerfor Duallly Environmental Tosifng This message is Intended for the use of the Individual or entity to which it Is addressed. This may contain information that is privileged, confidential, and exempt from disclosure under applicable law. If the reader of this message Is not the Intended recipient, or the employee or agent responsible for delivering the message to the Intended recipient, you are hereby notified that any dissemination, distribution or copying of this communication Is strictly prohibited. If you have received this communication in error, please notify us immediately bytolephone and delete the original message. Thank you. I J I� I f '1 Ll I I II� ,I I E 8/19/2009 1 J i 1 1 1 1 � APPENDIX C 1 i i 1 i 1 1 1 I 4 SOIL BORING LOG O PROJECT NUMBER 602497003 BORING/WELL NUMBER B6 PROJECT NAME SCE Newport Beach DATE DRILLED 81312009 LOCATION 1516 W. Balboa Blvd Newport Beach CA CASING TYPEIDIAMETER NIA DRILLING METHOD Direct Push SCREEN TYPEISLOT NIA SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE NIA GROUND ELEVATION NIA fl GROUT TYPE NIA TOP OF CASING ELEV. NIA DEPTH TO WATER NIA ft. LOGGED BY MDW TOTAL DRILL DEPTH 8 ft REMARKS (D U) 3 0 Z > °�' W E a rA U LITHOLOGIC DESCRIPTION IL p � mO o� a W d j W� Q U) Surface - SILTY SAND, light brown, moist, dense, fine grained sand. SM ' @05 -COBBLY SAND, light brown, moist, dense, fine grained sand. SP . 6 B6-2 0.0 • @ 4' - POORLY GRADED SAND, light brown, moist, dense, fine grained sand. 5 6 B6-5 0.0 6 B6-7 0.0 @ T - Groundwater encountered. Soil becomes wet. 10 15 0 2D G z n m m 25 Total Depth= 8' bgs. 0 J Groundwaterwas encountered at T bgs. c� Groundwater sample collected at 1003. m N J m N w 30 SOIL BORING LOG is PROJECT NUMBER 602497003 BORINGIWELL NUMBER B7 PROJECT NAME SCE Newport Beach DATE DRILLED S09009 LOCATION 1516 W. Balboa Blvd Newport Beach CA CASING TYPEIDIAMETER N/A DRILLING METHOD Direct Push SCREEN TYPE/SLOT NIA SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE N/A GROUND ELEVATION NIA it, GROUT TYPE NIA TOP OF CASING ELEV. NIA DEPTH TO WATER NIA ft. LOGGED BY MOW TOTAL DRILL DEPTH 8 ft REMARKS Ui Q. j W o y LITHOLOGIC DESCRIPTION anp co IL SM Surface -COBBLY SILT, light brown, mots!, loose. @2'-COBBLY SAND, brown, molar, dense, fine grained sand. SP 6 87-2 0.0 5 6 87-5 0.0 ' I 6 B7.7 0.0 @7'-Groundwater encountered, soil becomes wet. 10 15 20 i i i 25 I i Total Depth= 8' bgs. i Groundwater was encountered at T bgs. i , Groundwater sample collected at 1055. , � 30 t 1 I I I I L1 I Fri Li SOIL BORING LOG 4/ PROJECT NUMBER 602497003 BORING/WELL NUMBER BS PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 LOCATION 1516 W Balboa Blvd Newport Beach CA CASING TYPE/DIAMETER NIA DRILLING METHOD Direct Push SCREEN TYPEISLOT NIA SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE NIA GROUND ELEVATION NIA ft. GROUT TYPE NIA TOP OF CASING ELEV. NIA DEPTH TO WATER N/A ft LOGGED BY MDW TOTAL DRILL DEPTH 8 ft REMARKS a m rn z a r- w E (6 LITHOLOGIC DESCRIPTION px m0 p r w N We C ate—. D y SM Surface -COBBLY SILT, light brown, moist, loose. ' @1'-COBBLY SAND, brown, moist, dense, fine grained sand. SP 6 BB-2 0.0 @4' -Rock layer encountered. @4.5' -POORLY GRADED SAND, reddish brown, moist, dense, trace sea shells. 5 s Be-s o.o s @5.9'-Groundwater encountered, soil becomes wet. 10 15 3 F 20 0 n 0 25 3 Total Depth= 8' bgs. i Groundwater was encountered at 5.9' bgs. n Groundwater sample collected at 1127. n n n s 30 SOIL BORING LOG PROJECTNUMBER 602497003 BORING/WELLNUMBER B9 PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 LOCATION 1516 W. Balboa Blvd, Newport Beach, CA CASING IYPEIDIAMETER N/A DRILLING METHOD Direct Push SCREEN TYPE/SLOT NIA SAMPLING METHOD Acetate Sleeve FILTER PACKTYPE N/A GROUND ELEVATION N/A ft. GROUTTYPE NIA TOP OF CASING ELEV. N/A DEPTH TO WATER NIA ft LOGGED BY MDW TOTAL DRILL DEPTH 811, _ REMARKS Y p i a m p= �,°ic� a W E ,6a, N LITHOLOGIC DESCRIPTION O C p] W 0 W N Q. SM Surface -COBBLY SILT, light brown, dry, loose, ' @1.5' •COBBLY SAND, brown, moist, dense, fine grained sand. SP 6 B9.2 0.0 5 @45 -SILT layer, brown, moist, hard. 6 B9.6 0.0 @5' -COBBLY SAND, brown, moist, dense, fine grained sand. Q @6' •Groundwater encountered, soil becomes wet. 10 15 2D I i i i 25 i , Total Depth= 8' bgs. , Groundwater was encountered at V bgs. Groundwater sample collected at 1220, l i � 30 I J I N I I I I I —1 I 5 I I ,, I I I I 11 I I� L I I 4 SOIL BORING LOG PROJECT NUMBER 602497003 BORINGMELL NUMBER B10 PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 LOCATION 1516 W. Balboa Blvd Newport Beach CA CASING TYPEIDIAMETER N/A - DRILLING METHOD Direct Push SCREEN TYPE/SLOT N/A SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE N/A GROUND ELEVATION N/A ft GROUT TYPE N/A TOP OF CASING ELEV. NIA DEPTH TO WATER N/A ft LOGGED BY MDW TOTAL DRILL DEPTH 8 ft REMARKS m 3 z �.. > d w r w E of ci LITHOLOGIC DESCRIPTION o co w w—. Q a SM Surface -COBBLY SILT, light brown, moist, loose. ' @1.5' -COBBLY SAND, reddish brown, moist, dense, fine grained sand. SP 6 810.2 0.0 5 @5' -COBBLY SAND, grey brown, less cobbles. Q 6 B10.6 0.0 @6-Groundwater encountered, soil becomes wet. 10 15 " 20 ye 5 LJ n a n 25 3 Total Depth= 8' bgs. z Groundwater was encountered at 6' bgs. p a Groundwater sample collected at 1158. w M m N 30 J 4 SOIL BORING LOG PROJECTNUMBER 602497003 BORING/WELLNUMBER B11 PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 LOCATION 1516 W. Balboa Blvd, Newport Beach, CA CASING TYPE/DIAMETER N/A DRILLING METHOD Direct Push SCREENTYPE/SLOT N/A SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE N/A GROUND ELEVATION NIA fL GROUT TYPE N/A TOP OF CASING ELEV, N/A DEPTH TO WATER N/A fl I LOGGED BY MDW TOTAL DRILL DEPTH 8 ft. REMARKS }o E rb a.coO j �o u a tW C g N LITHOLOGIC DESCRIPTION O4' mV Lu Q. SM Surface-COBBLY SILT, light brown, moist, loose. @1' -POORLY GRADED SAND, light brown, moist, dense, fine grained sand. SP 6 811-2 0.0 @2.5' -POORLY GRADED SAND, reddish brown, moist, dense, fine grained sand. 5 6 B11-5 0.0 @-Groundwater encountered, soil becomes wet. 5' 10 15 20 i i i i I 25 i Total Depth=V bgs. Groundwater Was encountered at 5' bgs. , Groundwater sample collected at 1257. , , r � 30 I I r I I I I♦l SOIL BORING LOG ' PROJECT NUMBER - 602497003 BORINGWELL NUMBER B12 PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 1516 W. Balboa Blvd Newport Beach CA CASING TYPE/DIAMETER N/A 'LOCATION DRILLING METHOD Direct Push SCREEN TYPEISLOT NIA SAMPLING METHOD Acetate Sleeve FILTER PACK TYPE NIA GROUND ELEVATION N/A ft GROUT TYPE NIA TOP OF CASING ELEV. N/A DEPTH TO WATER NIA ft LOGGED BY MDW TOTAL DRILL DEPTH 8 ft. REMARKS tm uj Lu I-- 0 3 z r. > Lu t- w E a of U LITHOLOGIC DESCRIPTION o_ m Surface -COBBLY SAND, light brown, dry, loose, fine grained sand. SP ' 6 B12-2 0.0 @3' -POORLY GRADED SAND, light brown, moist, dense, fine grained sand. . @4' -POORLY GRADED SAND, brown, moist, dense, fine grained sand. 5 6 B12-6 0.0 @6 SILTY SAND, brown, wet, dense, fine grained sand. ' SM — — Groundwater encountered. 10 15 o 20 z z m m 25 °o Total Depth= 8' bgs. u W Groundwaterwas encountered at 6' bgs. m Groundwater sample collected at 1335. U) J m N u 30 ; SOIL BORING LOG PROJECT NUMBER 602497003 BORINGIWELL NUMBER B13 ' PROJECT NAME SCE Newport Beach DATE DRILLED 8/3/2009 LOCATION 1516 W. Balboa Blvd, Newport Beach CA CASING TYPE/DIAMETER NIA DRILLING METHOD Direct Push SCREEN TYPEISLOT N/A SAMPLING METHOD Acetate Sleeve FILTER PACKTYPE N/A GROUND ELEVATION NIA ft. GROUT TYPE N/A TOP OF CASING ELEV. NIA DEPTH TO WATER N/A ft ' LOGGED BY MDW TOTAL DRILL DEPTH 8 tl REMARKS } o 'E a 0 ryj m p j nwJ. �u ,aa, N LITHOLOGIC DESCRIPTION o� m0 w K N SM _ _ Surface-COBBLY SILT, light brown, moist, loose. 6 813.2 0.0 _ @1.5'-COBBLY SAND, brown, moist, dense. SP @4'-COBBLY SAND, reddish brown, metal, trace sea shells. ' 5 6 B13.5 0.0 Sr: @5.5' .Groundwater encountered, soil becomes wet 10 15 20 z z a u 'm m 25 N ° Total Depth= 8' bgs. z o Groundwater was encountered at 5.5' bgs. m Groundwater sample collected at 1315. J m V) � 30